JPS6167565A - Joining method of ceramics pipe and metallic pipe - Google Patents

Joining method of ceramics pipe and metallic pipe

Info

Publication number
JPS6167565A
JPS6167565A JP18849484A JP18849484A JPS6167565A JP S6167565 A JPS6167565 A JP S6167565A JP 18849484 A JP18849484 A JP 18849484A JP 18849484 A JP18849484 A JP 18849484A JP S6167565 A JPS6167565 A JP S6167565A
Authority
JP
Japan
Prior art keywords
pipe
bellows
ceramics
metal
metallic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP18849484A
Other languages
Japanese (ja)
Inventor
Kazuyuki Tsuchiya
和之 土屋
Masaichi Kouketsu
纐結 政一
Suemi Hirata
平田 末美
Ryoichi Katsuya
勝谷 涼一
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IHI Corp
Original Assignee
IHI Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by IHI Corp filed Critical IHI Corp
Priority to JP18849484A priority Critical patent/JPS6167565A/en
Publication of JPS6167565A publication Critical patent/JPS6167565A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B37/00Joining burned ceramic articles with other burned ceramic articles or other articles by heating
    • C04B37/02Joining burned ceramic articles with other burned ceramic articles or other articles by heating with metallic articles
    • C04B37/023Joining burned ceramic articles with other burned ceramic articles or other articles by heating with metallic articles characterised by the interlayer used
    • C04B37/026Joining burned ceramic articles with other burned ceramic articles or other articles by heating with metallic articles characterised by the interlayer used consisting of metals or metal salts
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16LPIPES; JOINTS OR FITTINGS FOR PIPES; SUPPORTS FOR PIPES, CABLES OR PROTECTIVE TUBING; MEANS FOR THERMAL INSULATION IN GENERAL
    • F16L27/00Adjustable joints, Joints allowing movement
    • F16L27/10Adjustable joints, Joints allowing movement comprising a flexible connection only, e.g. for damping vibrations
    • F16L27/107Adjustable joints, Joints allowing movement comprising a flexible connection only, e.g. for damping vibrations the ends of the pipe being interconnected by a flexible sleeve
    • F16L27/11Adjustable joints, Joints allowing movement comprising a flexible connection only, e.g. for damping vibrations the ends of the pipe being interconnected by a flexible sleeve the sleeve having the form of a bellows with multiple corrugations
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/658Atmosphere during thermal treatment
    • C04B2235/6581Total pressure below 1 atmosphere, e.g. vacuum
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2237/00Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
    • C04B2237/02Aspects relating to interlayers, e.g. used to join ceramic articles with other articles by heating
    • C04B2237/12Metallic interlayers
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2237/00Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
    • C04B2237/30Composition of layers of ceramic laminates or of ceramic or metallic articles to be joined by heating, e.g. Si substrates
    • C04B2237/32Ceramic
    • C04B2237/34Oxidic
    • C04B2237/341Silica or silicates
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2237/00Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
    • C04B2237/30Composition of layers of ceramic laminates or of ceramic or metallic articles to be joined by heating, e.g. Si substrates
    • C04B2237/32Ceramic
    • C04B2237/34Oxidic
    • C04B2237/343Alumina or aluminates
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2237/00Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
    • C04B2237/30Composition of layers of ceramic laminates or of ceramic or metallic articles to be joined by heating, e.g. Si substrates
    • C04B2237/40Metallic
    • C04B2237/405Iron metal group, e.g. Co or Ni
    • C04B2237/406Iron, e.g. steel
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2237/00Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
    • C04B2237/50Processing aspects relating to ceramic laminates or to the joining of ceramic articles with other articles by heating
    • C04B2237/76Forming laminates or joined articles comprising at least one member in the form other than a sheet or disc, e.g. two tubes or a tube and a sheet or disc
    • C04B2237/765Forming laminates or joined articles comprising at least one member in the form other than a sheet or disc, e.g. two tubes or a tube and a sheet or disc at least one member being a tube

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Pressure Welding/Diffusion-Bonding (AREA)
  • Laminated Bodies (AREA)
  • Ceramic Products (AREA)

Abstract

PURPOSE:To prevent ceramics from being damaged, by using a metallic bellows as an intermediate joint. CONSTITUTION:A ceramics pipe 1 consisting of alumina, silica, etc. and a metallic pipe 2 of a stainless steel pipe, etc. are joined by using a metallic bellows 3 as a joint between them. That is to say, the end part of the ceramics pipe 1 is joined to one end 4 of the metallic bellows 3, and the end part of the metallic pipe 2 is joined to the other end 5. The ceramics pipe 1 and the metallic bellows 3 are joined by a vacuum brazing method, etc., and the end part of the ceramics pipe 1 is brought to metallized processing. Also, the metallic pipe 2 and the bellows 3 are joined by TIG welding, etc. According to this method, a distortion force of the joint of the ceramics pipe 1 and the metallic pipe 2 is absorbed by deformation of the bellows 3, and damage of the ceramics can be prevented.

Description

【発明の詳細な説明】 (発明の利用分野) この発明はセラミックス管と金属管とを接合する方法の
改良に係る。
DETAILED DESCRIPTION OF THE INVENTION (Field of Application of the Invention) The present invention relates to an improvement in a method for joining a ceramic tube and a metal tube.

(従来技術と解決すべき問題点) 部分的に耐熱性を必要とする配管等においてセラミック
ス管と金属管とを接合して使用することが行われるよう
になってきている。このような場合従来は第2図に示す
ようにセラミックス管12と金属管14とを直接に真空
中でロー付けすることが行われているが、セラミックス
は脆いので熱、膨豚の差によって生ずる歪力によって接
続部が破損しやすい。これに対して第3図に示すように
傘状の金属薄板11aとセラミックス管I2を接続部1
3において従来通り真空ロー付けで接合し、これと相対
向する傘状の金属薄板11bと金属管14の接合部15
を例えばTIG熔接溶接はプラズマ溶接しておいて傘状
の金属薄Fj、llaと11bをその周縁部16で対接
させ、ここをTIGまたはプラズマ溶接した伸縮管継手
をセラミックス管と金属管との間に設ける方法が提案さ
れているが、薄板のヘリ継手の溶接は技術的に難しく、
特にアルミニウム薄板である場合には気密度の高い溶接
部を得ることは尚一層困難である。
(Prior Art and Problems to be Solved) Ceramic tubes and metal tubes are increasingly being used in conjunction with each other in piping and the like that require partial heat resistance. In such cases, conventionally the ceramic tube 12 and the metal tube 14 have been brazed directly in a vacuum as shown in Figure 2, but since ceramics are brittle, brazing may occur due to differences in heat and expansion. Connections are prone to damage due to strain forces. On the other hand, as shown in FIG.
3, the joint 15 of the umbrella-shaped thin metal plate 11b and the metal tube 14 is joined by vacuum brazing as before, and is opposite to this.
For example, in TIG welding, plasma welding is performed, and the umbrella-shaped metal thin Fj, lla and 11b are brought into contact with each other at their peripheral edges 16, and an expansion pipe joint that is TIG or plasma welded is used to connect a ceramic pipe and a metal pipe. A method has been proposed to provide a helical joint between thin plates, but it is technically difficult to weld helical joints of thin plates.
In particular, in the case of aluminum thin plates, it is even more difficult to obtain a welded part with high airtightness.

さらにセラミックス管に対する熱負荷を避けるためには
この形の伸縮管継手では管外周から外側へ張り出した鍔
部を長くすることが必要であり、管周囲の空間的制限が
厳しい配管に通用することが困難である等の問題点があ
る。
Furthermore, in order to avoid heat load on the ceramic pipe, this type of expansion pipe joint requires a long flange that extends outward from the pipe periphery, making it suitable for piping with severe spatial restrictions around the pipe. There are problems such as difficulty.

この発明は上記の如き問題点を解決して応力による破損
の少ない接合方法を提供することを目的とする。
It is an object of the present invention to solve the above-mentioned problems and provide a joining method that causes less damage due to stress.

(問題点の解決手段) この発明は、セラミックス管と金属管とを接合する方法
において、中間ジヨイントとして金属ベローズを用い、
その一端にセラミックス管を、他端には金属管を接合す
ることを特徴とするセラミックス管と金属管の接合方法
に係る。
(Means for solving problems) The present invention uses a metal bellows as an intermediate joint in a method of joining a ceramic tube and a metal tube,
The present invention relates to a method for joining a ceramic tube and a metal tube, characterized in that a ceramic tube is joined to one end of the ceramic tube and a metal tube is joined to the other end.

次に添付図面第1図を参照して本発明の詳細な説明する
。セラミックス管1と金属管2との中間に金属ベローズ
3をジヨイントとし、金属ベローズの一端4にセラミッ
クス管1の端部を接合し、金属ベローズ3の他端5には
金属管2の端部を接合する。金属ベローズの端部5は板
厚を厚くすると溶接施工が容易になるので便利である。
The present invention will now be described in detail with reference to FIG. 1 of the accompanying drawings. A metal bellows 3 is jointed between the ceramic tube 1 and the metal tube 2, the end of the ceramic tube 1 is joined to one end 4 of the metal bellows, and the end of the metal tube 2 is connected to the other end 5 of the metal bellows 3. Join. It is convenient to make the end portion 5 of the metal bellows thicker because it facilitates welding.

すなわちこのようにすると例えば自動溶接法を採用する
ことにより継手の信頼性を高めることができる。
That is, in this case, the reliability of the joint can be improved by employing, for example, an automatic welding method.

セラミックス管としては電気絶縁、耐食性或いは一様磁
場の確保のため例えばアルミナやシリカ等のセラミック
スが使用され、金属管としてはステンレス鋼管、アルミ
ニウム管、或いは鋼管等が使用される。
As the ceramic tube, a ceramic such as alumina or silica is used to ensure electrical insulation, corrosion resistance, or a uniform magnetic field, and as the metal tube, a stainless steel tube, an aluminum tube, or a steel tube is used.

またジヨイントとして使用する金属ベローズは金泥管と
同じ材料で作ったものが普通であるが、目的用途に応じ
て金属管とへローズとの組合わせにステンレス鋼とコバ
ール、銅と黄銅、或いはチタンとステンレス鋼との組合
わせ等を使用することができる。
Also, the metal bellows used as a joint is usually made of the same material as the gold mud pipe, but depending on the purpose, the combination of the metal pipe and the bellows can be made of stainless steel and Kovar, copper and brass, or titanium. Can be used in combination with stainless steel, etc.

セラミックス管と金属ベローズとの接合は通例の真空ロ
ー材は法によるのが良く、セラミックス管の接合端部に
は通例メタライズ処理を施して接合を容易にしておくと
よい。しかしながらセラミックス管と金属ベローズとの
接合はロー付けに限定されるものではなく、例えば拡散
接合性等接合部の破損が防止できるものであれば適宜そ
の他の方法を用いることができる。
The ceramic tube and the metal bellows are preferably joined by a conventional vacuum brazing method, and the joining end of the ceramic tube is preferably subjected to a customary metallization treatment to facilitate the joining. However, the joining of the ceramic tube and the metal bellows is not limited to brazing, and any other suitable method may be used, such as diffusion bonding, as long as it can prevent damage to the joint.

金属管と金属ベローズの溶接には770等公知の溶接法
を採用することができる。
A known welding method such as 770 can be used to weld the metal pipe and the metal bellows.

金属ベローズは板厚を薄く、山数を多くしてセラミック
ス管までの距離を長くすることが望ましく、溶接熱のセ
ラミックス管への伝導を最少限に抑えるようにする。
It is desirable for the metal bellows to have a thin plate and a large number of ridges to increase the distance to the ceramic tube, so as to minimize the conduction of welding heat to the ceramic tube.

(実施例) 次に実施例について述べる。(Example) Next, an example will be described.

アルミナ(シリカ10%を含む)管とアルミニウム管と
の中間にジヨイントとしてアルミニウム(JISA30
04)製のベローズを用いる場合について述べれば、通
例の通りアルミナ管の接合端部にメタライズ処理を施し
たのち、ロー材としてアルミニウムプレージングシート
を用い、およそl Torrに減圧した雰囲気中で約6
05℃に加熱・  してアルミナ管とアルミニウムベロ
ーズとを接合したのち室温まで冷却した。アルミニウム
ベローズとアルミニウム管とは通例のようにTIG溶接
によって溶接した。
Aluminum (JISA30
Regarding the case of using bellows manufactured by 04), the joint end of the alumina tube is metallized as usual, and then an aluminum plating sheet is used as the soldering material, and the bellows is heated in an atmosphere of reduced pressure to about 1 Torr.
The alumina tube and aluminum bellows were joined together by heating to 0.5°C, and then cooled to room temperature. The aluminum bellows and aluminum tube were conventionally welded by TIG welding.

接合部について真空漏洩試験を行った結果リークは無く
、電子加速器の真空配管に適用して良い結果が得られた
A vacuum leak test was conducted on the joint, and there was no leak, and good results were obtained when applied to the vacuum piping of an electron accelerator.

(効果) 以上述べたように本発明の方法によればセラミックス管
と金属管とを直接ロー付けすることに伴って生ずる熱膨
張率の差により生ずる歪力の発生は無く、セラミックス
管と金属管との接合による歪力は金属ベローズ即ちベロ
ーズ形伸縮管継手の変形によって吸収され、セラミック
スの破損を防止することができる。
(Effects) As described above, according to the method of the present invention, there is no distortion caused by the difference in thermal expansion coefficients that occurs when the ceramic tube and the metal tube are directly brazed, and the ceramic tube and the metal tube are The strain force caused by the connection with the metal bellows is absorbed by the deformation of the metal bellows, that is, the bellows-type expansion joint, and damage to the ceramic can be prevented.

金属管と金属ベローズとの接合には一般の溶接施工が適
用でき、自動溶接によってリーク等の欠陥の発生を防止
することができ、継手の信頼性をたかめることができる
。又金属ベローズの板厚を薄く、かつ山数を充分に多く
とっておけば溶接熱の影Kを防ぐことができる。而も金
属へローズを伸縮管継手としたので接続部の形状がWJ
単で、突出部が無いため狭隘な個所にも配管ができる等
実用上の効果はきわめて大きい。
General welding can be applied to join the metal pipe and metal bellows, and automatic welding can prevent defects such as leaks and increase the reliability of the joint. Also, by making the metal bellows thin and having a sufficiently large number of threads, the shadow K of welding heat can be prevented. Moreover, since the metal rose is used as an expansion pipe joint, the shape of the connection part is WJ.
Since it is simple and has no protruding parts, it has extremely great practical effects, such as allowing piping to be installed in narrow spaces.

【図面の簡単な説明】 第1図は本発明の方法による接合状態を示す一部破砕正
面図、第2図は従来のセラミックス管と金属管のロー付
けによるしか付けの状態を示す断面図、第3図は同しく
従来の中間に金属薄板製の伸縮管継手を介在させて接合
した状態を示す一部破砕正面図である。 1・・・セラミックス管、2・・・金属管、3・・・金
属へローズ、4・・・金属ベローズのセラミックス管接
合端、5・・・金属へローズの金属管接合端出願人代理
人 弁理士 鴨志1)次男 第2図 第3図 第1図
[Brief Description of the Drawings] Fig. 1 is a partially fragmented front view showing a state of joining by the method of the present invention, Fig. 2 is a sectional view showing a state of joining by conventional brazing of a ceramic pipe and a metal pipe, FIG. 3 is a partially exploded front view showing a state in which a conventional expansion pipe joint made of a thin metal plate is interposed between the joints. 1...Ceramics tube, 2...Metal tube, 3...Metal herwels, 4...Ceramics pipe joint end of metal bellows, 5...Metal pipe joint end of metal herwels, applicant's agent Patent Attorney Kamoshi 1) Second son Figure 2 Figure 3 Figure 1

Claims (1)

【特許請求の範囲】[Claims] セラミックス管と金属管を接合する方法において、中間
ジョイントとして金属ベローズを用い、その一端にセラ
ミックス管を、他端には金属管を接合することを特徴と
するセラミックス管と金属管の接合方法。
A method for joining a ceramic tube and a metal tube, the method comprising using a metal bellows as an intermediate joint, and joining a ceramic tube to one end of the bellows and a metal tube to the other end.
JP18849484A 1984-09-08 1984-09-08 Joining method of ceramics pipe and metallic pipe Pending JPS6167565A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP18849484A JPS6167565A (en) 1984-09-08 1984-09-08 Joining method of ceramics pipe and metallic pipe

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP18849484A JPS6167565A (en) 1984-09-08 1984-09-08 Joining method of ceramics pipe and metallic pipe

Publications (1)

Publication Number Publication Date
JPS6167565A true JPS6167565A (en) 1986-04-07

Family

ID=16224709

Family Applications (1)

Application Number Title Priority Date Filing Date
JP18849484A Pending JPS6167565A (en) 1984-09-08 1984-09-08 Joining method of ceramics pipe and metallic pipe

Country Status (1)

Country Link
JP (1) JPS6167565A (en)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0569838A (en) * 1990-12-28 1993-03-23 Danfoss As Controller for complete hydraulic steering system
JPH0663930A (en) * 1992-08-25 1994-03-08 Kubota Corp Heat-resistant composite ceramic pipe and production thereof
US8404398B2 (en) 2008-08-12 2013-03-26 Bloom Energy Corporation Hermetic high temperature dielectric with groove and thermal expansion compensator
US8921001B2 (en) 2012-11-28 2014-12-30 Bloom Energy Corporation Hermetic high temperature dielectric conduit assemblies
US9786043B2 (en) 2014-12-03 2017-10-10 Bloom Energy Corporation Inspection method for the effect of composition on the bond strength of a metallized alumina ceramic
US10050298B2 (en) 2014-06-04 2018-08-14 Bloom Energy Corporation Hermetic high temperature dielectric conduit assemblies
US11916265B2 (en) 2020-02-05 2024-02-27 Bloom Energy Corporation Metal-dielectric conduit assemblies and methods of making thereof

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0569838A (en) * 1990-12-28 1993-03-23 Danfoss As Controller for complete hydraulic steering system
JPH0663930A (en) * 1992-08-25 1994-03-08 Kubota Corp Heat-resistant composite ceramic pipe and production thereof
US8404398B2 (en) 2008-08-12 2013-03-26 Bloom Energy Corporation Hermetic high temperature dielectric with groove and thermal expansion compensator
US8921001B2 (en) 2012-11-28 2014-12-30 Bloom Energy Corporation Hermetic high temperature dielectric conduit assemblies
US10050298B2 (en) 2014-06-04 2018-08-14 Bloom Energy Corporation Hermetic high temperature dielectric conduit assemblies
US9786043B2 (en) 2014-12-03 2017-10-10 Bloom Energy Corporation Inspection method for the effect of composition on the bond strength of a metallized alumina ceramic
US11916265B2 (en) 2020-02-05 2024-02-27 Bloom Energy Corporation Metal-dielectric conduit assemblies and methods of making thereof

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