JPS61573A - Sputtering apparatus - Google Patents

Sputtering apparatus

Info

Publication number
JPS61573A
JPS61573A JP11988484A JP11988484A JPS61573A JP S61573 A JPS61573 A JP S61573A JP 11988484 A JP11988484 A JP 11988484A JP 11988484 A JP11988484 A JP 11988484A JP S61573 A JPS61573 A JP S61573A
Authority
JP
Japan
Prior art keywords
exhaust
sputtering
pressure
gas
chamber
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP11988484A
Other languages
Japanese (ja)
Inventor
Takahiro Yamamoto
隆洋 山本
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TDK Corp
Original Assignee
TDK Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by TDK Corp filed Critical TDK Corp
Priority to JP11988484A priority Critical patent/JPS61573A/en
Publication of JPS61573A publication Critical patent/JPS61573A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C14/00Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
    • C23C14/22Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
    • C23C14/34Sputtering

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Physical Vapour Deposition (AREA)
  • Physical Deposition Of Substances That Are Components Of Semiconductor Devices (AREA)

Abstract

PURPOSE:To make the regulation of gas pressure of an ionized gas ease and to perform excellent filming by providing the first exhaust path having a turbo- pump and the second exhaust path having a cryopump to a sputtering chamber. CONSTITUTION:An exhaust duct 7 is fitted to a sputtering chamber 1 provided with a target 2, a base plate holder 3 and an introduction port 4 for sputtering gas such as argon via a gate valve 6. An exhaust duct 7 is provided with a turbopump 10 having an exhaust line 15 and a cryopump 14 having an exhaust line 16. The exhaust lines 15, 16 are connected with a rotary pump 17. The exhaust of whole period of the chamber 1 is performed by means of the exhaust system contg. the turbopump 10 plus the rotary pump and the pressure of the inside of the chamber 1 is regulated to prescribed pressure by the regulation of a variable valve 12 in the exhaust system contg. the cryopump 14 and the rotary pump. The pressure of the inside of the chamber 1 can be easily regulated to the prescribed pressure and the characteristics of a film and film quality due to the sputtering can be uniformly maintained always.

Description

【発明の詳細な説明】 本発明はスパッタ装置に関し、特にその排気系の改良に
関する。
DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a sputtering apparatus, and particularly to improvements in its exhaust system.

〔従来技術とその問題点〕[Prior art and its problems]

スパッタ決は、スパッタチャンバーにイオン化用のガス
を導入してこれをイオン化し、成膜すべき物質より成る
ターゲットにこのイオン化ガスを衝撃して成膜物質の分
子または原子をスパッタし、これを基板面へ付着させる
ことから成る成膜方法である。導入ガス圧は成膜物質、
導入ガスの種類等に応じて調整する必要がある。
Sputtering involves introducing an ionizing gas into a sputtering chamber, ionizing it, bombarding a target made of the material to be deposited with the ionized gas, sputtering molecules or atoms of the material, and sputtering the molecules or atoms of the material onto the substrate. This is a film formation method that consists of depositing the film on the surface. The introduced gas pressure is the film forming material,
It is necessary to adjust according to the type of introduced gas, etc.

従来のスパッタ装置は、排気系の能力を固定しているた
め、スパッタ導入ガスの流量又は圧力を変えてスパッタ
時の調圧を行なっていた。しかし、この方法では中間流
領域(10”” 〜10−’Torr)ノスパツタガス
圧ではガスの流れの方向が乱れて膜質を良好にすること
ができなかった。又、別な方法として可変オリアイスを
排気系に挿入して排気能力を調整する方法があるが、こ
の方法も基本的には能力の変動範囲が限定されるため、
導入ガスの圧力または流量を変えざるを得す、同様な問
題を生じた。スパッタは通常10−!〜10 ”−’ 
Torrの範囲のガス圧で実行されるが、この範囲内で
所望のガス圧への調圧を行なうと、従来法では上記のよ
うに流れのパターンが変ってしまい、またガスのよどみ
個所などが発生して膜の特性や均一性に問題を生じたの
である。
In conventional sputtering apparatuses, the capacity of the exhaust system is fixed, so the pressure during sputtering is adjusted by changing the flow rate or pressure of the sputtering gas. However, in this method, the direction of gas flow is disturbed in the intermediate flow region (10'' to 10-'Torr) at the nosputter gas pressure, making it impossible to improve the film quality. Another method is to insert a variable orifice into the exhaust system to adjust the exhaust capacity, but this method also basically limits the range of variation in capacity.
A similar problem occurred where the pressure or flow rate of the introduced gas had to be changed. Spatter is usually 10-! ~10"-'
The process is performed at a gas pressure in the Torr range, but if the pressure is adjusted to the desired gas pressure within this range, in the conventional method, the flow pattern changes as described above, and gas stagnation points occur. This caused problems with the properties and uniformity of the film.

〔発明の目的〕[Purpose of the invention]

本発明は、イオン化ガス形成用のガス圧が一様に調整で
き、すぐれた成膜を行なうことができるスパッタ装置を
提供することを目的とする。
An object of the present invention is to provide a sputtering apparatus that can uniformly adjust the gas pressure for forming ionized gas and can perform excellent film formation.

〔発明の構成と効果の概要〕[Summary of structure and effects of the invention]

本発明は、イオン化ガス形成用のガス導入口を有するス
パッタチャンバーの排気系をターボポンプを有する第1
排気路と、クライオポンプを有する第2排気路とを並列
に形成し各々に可変オリフィスを付は一定流量の導入ガ
スと残留ガスの比を変えずにスパッタガス圧を調整でき
ることを特徴とするスパッタ装置である。
The present invention provides a first exhaust system having a turbo pump for a sputtering chamber having a gas inlet for forming ionized gas.
A sputtering device characterized in that an exhaust path and a second exhaust path having a cryopump are formed in parallel and each is provided with a variable orifice so that the sputtering gas pressure can be adjusted without changing the ratio between the constant flow rate of introduced gas and the residual gas. It is a device.

4      本発明によると、中間流領域に対しても
十分な排気能力が得られ、これら両排気路をスパッタ操
作中に併用することによりクライオポンプの寿命導入し
ながらスパッタ時の圧力を排気系の制御により調整する
ことができる。従って、導入ガスの圧力や流量の変動が
原因となるガスの流動方向の変化やよどみの発生が無く
その圧力を調整できるので、生成されるスパッタ膜の膜
質及び膜分布の均一性を向上させることができる。
4 According to the present invention, sufficient exhaust capacity is obtained even for the intermediate flow region, and by using both of these exhaust channels during sputtering operation, the pressure during sputtering can be controlled by the exhaust system while extending the life of the cryopump. It can be adjusted by Therefore, the pressure can be adjusted without changing the gas flow direction or causing stagnation caused by fluctuations in the pressure or flow rate of the introduced gas, improving the quality and uniformity of the film distribution of the sputtered film produced. I can do it.

〔実施例の構成〕[Configuration of Example]

第1図は本発明の実施例によるスパッタ装置を示す。ス
パッタ装置は2極または多極のDCまたはRFスパッタ
装置等任意のものでありうる。気密スパッタチャンバー
1は所定の型式のもので2はターゲット、3は基板ホル
ダーであり、チャンバー1にはアルゴンガス等所定のス
パッタガス(イオン化ガス形成用のガス)導入口4が設
けてあり、ガスは弁5を経て図示しないガス源に接続さ
れている。
FIG. 1 shows a sputtering apparatus according to an embodiment of the invention. The sputtering device can be any type of device, such as a bipolar or multipolar DC or RF sputtering device. The airtight sputtering chamber 1 is of a predetermined type, with reference numeral 2 a target and 3 a substrate holder. is connected to a gas source (not shown) via a valve 5.

スパッタチャンバー1の排気口にはゲートバルブ6を介
して排気ダクト1が接続されており、また必要に応じて
ダクト7内にはコールドトラップ(液化Nt等)8が配
置されている。コールドトラップ8は主に逆流防止用で
あり、またある程度の排気能を有する。排気ダクト7の
排気側は2つに分肢しており、一方はゲートパルプ9と
可変オリフィス11を介してターボポンプ10に、他方
は可変オリフィス12及びゲートバルブ15を介してク
ライオポンプ14に接続されている。ターボポンプ10
はライン15を介して口〒タリボンプ17に接続され、
またクライオポンプ14はライン16を介してロータリ
ポンプ17に接続されている。
An exhaust duct 1 is connected to the exhaust port of the sputter chamber 1 via a gate valve 6, and a cold trap (liquefied Nt or the like) 8 is disposed within the duct 7 as required. The cold trap 8 is mainly used to prevent backflow, and also has a certain degree of exhaust ability. The exhaust side of the exhaust duct 7 is divided into two parts, one of which is connected to a turbo pump 10 via a gate pulp 9 and a variable orifice 11, and the other to a cryopump 14 via a variable orifice 12 and a gate valve 15. has been done. turbo pump 10
is connected via line 15 to the output terminal pump 17,
Further, the cryopump 14 is connected to a rotary pump 17 via a line 16.

ターボポンプ10、ライン15及びロータリポンプ17
を含む排気系はチャンバー1の全期間の排気を受持つ。
Turbo pump 10, line 15 and rotary pump 17
The exhaust system including the exhaust system is in charge of exhausting the chamber 1 during the entire period.

クライオポンプ14を含む排%、1は高真空の達成とス
パッタガス導入による中間流領域でのスパッタ動作中に
使用される。ターボポンプ及びクライオポンプの容量の
1例を述べれば、チャンバー1の容積が800cm”な
らばそれぞれ5toz/分、2600t/秒などの能力
を有するものを用いうる。
The cryopump 14 is used during sputtering operations in the intermediate flow region by achieving high vacuum and introducing sputtering gas. To give an example of the capacity of a turbo pump and a cryopump, if the volume of the chamber 1 is 800 cm'', pumps having capacities of 5 toz/min and 2600 t/sec, respectively, can be used.

〔動作と作用効果〕[Operations and effects]

スパッタチャンバー1を十分に排気した後、弁5を開い
て一定流量のアルゴンガスを導入する。
After the sputter chamber 1 is sufficiently evacuated, the valve 5 is opened to introduce a constant flow of argon gas.

排気系は2系統が共に用いられる。ターボポンプ10を
含む系椰は中間流領域におけるチャンバー1の圧力を大
体所定の値に定める。クライオポンプ14を含む系統は
可変パルプ12を調整することによりチャンバー1内の
圧力を調整して所定のスパッタ圧力を確立する。ターボ
ポンプ10の前にある可変オリフィス11を調整してさ
らに精細な調圧を行なう。
Two exhaust systems are used together. The system including the turbo pump 10 sets the pressure in the chamber 1 in the intermediate flow region to approximately a predetermined value. A system including the cryopump 14 adjusts the pressure within the chamber 1 by adjusting the variable pulp 12 to establish a predetermined sputtering pressure. The variable orifice 11 in front of the turbo pump 10 is adjusted to achieve more precise pressure regulation.

本発明による著しい作用効果は、導入ガスの流量や導入
圧力を変える必要がなく、単に排気系、特にクライオポ
ンプ14を調整することによりチャンバー1内の所定圧
力が達成できることにある。
A significant effect of the present invention is that a predetermined pressure within the chamber 1 can be achieved simply by adjusting the exhaust system, particularly the cryopump 14, without changing the flow rate or pressure of the introduced gas.

導入ガスの流量は一定であるから排気能力を変えること
によりスパッタガスの流速と圧力が変化するものであり
、これによりスパッタガスの流動パターンは実質的に変
化せず、スパッタにより形成される膜の特性及び膜質は
均一になる。また、りライオポンプは高真空側で初めて
作動されるから、その排気能力は長時間にわたって保持
することができる。さらに、本発明によると、ガス圧力
を調整できる範囲が従来よりも広範囲となりスパッタ条
件制御が容易になる。
Since the flow rate of the introduced gas is constant, changing the exhaust capacity will change the flow rate and pressure of the sputtering gas.As a result, the flow pattern of the sputtering gas will not substantially change, and the flow rate of the film formed by sputtering will change. The properties and film quality become uniform. In addition, since the Lyopump is first operated on the high vacuum side, its evacuation ability can be maintained for a long period of time. Furthermore, according to the present invention, the range in which the gas pressure can be adjusted is wider than in the past, making it easier to control sputtering conditions.

これに対して、可変オリアイスとターボポンプ、又は可
変オリアイスとクライオポンプを有する排気系を備えた
スパッタ装置を用いる場合には、一定流量の導入ガスに
対して可変オリフィスを変化させて排気能力を変えるた
め、残留ガス分圧に対する導入ガス分圧の比率が変化し
、無視できなくなり、膜組成に変化を生じる。このよう
な変化をさけるために入力ガス量を変化させると今度は
チャンバー内での流動パターンが変化してやはり膜質が
変化する。本発明の装置ではこのような問題がなく、基
本排気系すなわちターボポンプ系での排気能力を変化さ
せずにクライオポンプ側の可変オリフィスを変化させる
のみモ圧力の調整ができ4     るので、十分排気
能力にゆとりがあり、可変オリフィスによる能力変化に
対して残留ガス分圧と導入ガス分圧の比率も可変オリア
イス分しか変化しないので十分無視できる程度である。
On the other hand, when using a sputtering system equipped with an exhaust system that includes a variable orifice and a turbo pump, or a variable orifice and a cryopump, the exhaust capacity is changed by changing the variable orifice for a constant flow rate of introduced gas. Therefore, the ratio of the introduced gas partial pressure to the residual gas partial pressure changes and cannot be ignored, causing a change in the film composition. If the amount of input gas is changed to avoid such changes, the flow pattern within the chamber will change and the film quality will also change. The device of the present invention does not have this problem, and the pressure can be adjusted only by changing the variable orifice on the cryopump side without changing the pumping capacity of the basic pumping system, that is, the turbo pump system, so that sufficient pumping can be achieved. There is plenty of capacity, and the ratio of the residual gas partial pressure to the introduced gas partial pressure changes only by the variable orifice amount, so that it can be ignored.

例えば、水の分圧を測定したところ、従来の排気系と本
発明の排気系ではそれぞれ第2図及び第3図の結果が得
られ、大きな差異が生じた。
For example, when the partial pressure of water was measured, the results shown in FIGS. 2 and 3 were obtained for the conventional exhaust system and the exhaust system of the present invention, respectively, indicating a large difference.

【図面の簡単な説明】[Brief explanation of drawings]

第1図は本発明のスパッタ装置を示す図、第2図は従来
のスパッタ装置の排気特性を示すグラフ及び第3図は本
発明のスパッタ装置の排気特性を示すグラフである。 1ニスバツタチヤンバー 2:ターゲット 3:基板ホルダ 4:ガス導入口 6.9.16;ゲートバルブ 7:排気ダクト 10:ターボポンプ 11:可変オリフィス 12:可動バルブ 14:クライオポンプ 17:ロータリポンプ \−し−〆
FIG. 1 is a diagram showing the sputtering apparatus of the present invention, FIG. 2 is a graph showing the exhaust characteristics of the conventional sputtering apparatus, and FIG. 3 is a graph showing the exhaust characteristics of the sputtering apparatus of the present invention. 1 Varnish Bubble Chamber 2: Target 3: Substrate holder 4: Gas inlet 6.9.16; Gate valve 7: Exhaust duct 10: Turbo pump 11: Variable orifice 12: Movable valve 14: Cryopump 17: Rotary pump\ −shi−〆

Claims (1)

【特許請求の範囲】 1、一定流量のイオン化ガス形成用のガス導入口を有す
るスパッタチャンバーと、該チャンバーを排気する排気
系とを有するスパッタ装置において、前記排気系はター
ボポンプを有する第1排気路と、クライオポンプを有す
る第2排気路を並列に有することを特徴とするスパッタ
装置。 2、イオン化ガスの流路を変えずその個数を変化させて
ガス圧を調整できるようにした前記第1項記載のスパッ
タ装置 3、イオン化ガスの圧力と残留(放出)ガスの比を一定
のまま圧力を変える排気系を有する第1項記載のスパッ
タ装置。
[Scope of Claims] 1. A sputtering apparatus having a sputtering chamber having a gas inlet for forming ionized gas at a constant flow rate, and an exhaust system for evacuating the chamber, wherein the exhaust system includes a first exhaust having a turbo pump. What is claimed is: 1. A sputtering apparatus comprising a second exhaust path having a cryopump and a second exhaust path having a cryopump in parallel. 2. The sputtering apparatus 3 according to the above item 1, in which the gas pressure can be adjusted by changing the number of ionized gases without changing the flow path of the ionized gas, the ratio of the ionized gas pressure to the residual (released) gas being kept constant. 2. The sputtering apparatus according to claim 1, having an exhaust system that changes the pressure.
JP11988484A 1984-06-13 1984-06-13 Sputtering apparatus Pending JPS61573A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP11988484A JPS61573A (en) 1984-06-13 1984-06-13 Sputtering apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP11988484A JPS61573A (en) 1984-06-13 1984-06-13 Sputtering apparatus

Publications (1)

Publication Number Publication Date
JPS61573A true JPS61573A (en) 1986-01-06

Family

ID=14772616

Family Applications (1)

Application Number Title Priority Date Filing Date
JP11988484A Pending JPS61573A (en) 1984-06-13 1984-06-13 Sputtering apparatus

Country Status (1)

Country Link
JP (1) JPS61573A (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7281854B2 (en) 2002-10-24 2007-10-16 Taiho Kogyo Co., Ltd. Oil-feeding device for an engine crankshaft
US8714824B2 (en) 2012-02-23 2014-05-06 Daido Metal Company Ltd. Bearing apparatus for crankshaft of internal combustion engine
US8876391B2 (en) 2011-12-16 2014-11-04 Daido Metal Company Ltd. Main bearing for crankshaft of internal combustion engine
US8905639B2 (en) 2012-01-17 2014-12-09 Daido Metal Company Ltd. Main bearing for crankshaft of internal combustion engine
CN110027975A (en) * 2018-01-12 2019-07-19 奥的斯电梯公司 Door operation controller
CN111455332A (en) * 2019-09-03 2020-07-28 北京北方华创微电子装备有限公司 Sputtering chamber

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7281854B2 (en) 2002-10-24 2007-10-16 Taiho Kogyo Co., Ltd. Oil-feeding device for an engine crankshaft
US8876391B2 (en) 2011-12-16 2014-11-04 Daido Metal Company Ltd. Main bearing for crankshaft of internal combustion engine
US8905639B2 (en) 2012-01-17 2014-12-09 Daido Metal Company Ltd. Main bearing for crankshaft of internal combustion engine
US8714824B2 (en) 2012-02-23 2014-05-06 Daido Metal Company Ltd. Bearing apparatus for crankshaft of internal combustion engine
CN110027975A (en) * 2018-01-12 2019-07-19 奥的斯电梯公司 Door operation controller
CN111455332A (en) * 2019-09-03 2020-07-28 北京北方华创微电子装备有限公司 Sputtering chamber

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