JPS61149319A - Preparation of thermosetting resin castings - Google Patents

Preparation of thermosetting resin castings

Info

Publication number
JPS61149319A
JPS61149319A JP27173484A JP27173484A JPS61149319A JP S61149319 A JPS61149319 A JP S61149319A JP 27173484 A JP27173484 A JP 27173484A JP 27173484 A JP27173484 A JP 27173484A JP S61149319 A JPS61149319 A JP S61149319A
Authority
JP
Japan
Prior art keywords
mold
thermosetting resin
resin
setting
heating oven
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP27173484A
Other languages
Japanese (ja)
Inventor
Hideo Onuma
大沼 秀夫
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Toshiba Corp
Original Assignee
Toshiba Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Toshiba Corp filed Critical Toshiba Corp
Priority to JP27173484A priority Critical patent/JPS61149319A/en
Publication of JPS61149319A publication Critical patent/JPS61149319A/en
Pending legal-status Critical Current

Links

Landscapes

  • Casting Or Compression Moulding Of Plastics Or The Like (AREA)

Abstract

PURPOSE:To prevent fillers in resin from sedimenting and to disperse them uniformly by vibrating them with an ultrasonic vibrator in the primary setting process. CONSTITUTION:Fillers are prepared, defoamed under a vacuum state, stirred and then settled. A mold 4 is mounted on the ultrasonic vibrator plate 3 of a heating oven 2. Thermosetting resin is cast calmly and promptly along the inner wall surface of the mold 4. The heating oven 2 is shut and the mold 4 is vibrated by the ultrasonic vibrator plate 3. The inner temperature of the heating oven 2 is elevated up to the primary setting temperature of the thermosetting resin and kept for a fixed time before the primary setting has been completed. The structure of the mold 4 and the thicknesses of each section are designed so that the resin comes in contact with the lower mold, the primary setting begins from the surface, goes to the middle section of the thickness, further, to the upper section and finally the total setting ends with setting of the upper casting hole. The fluid filler is not settled but suspended by ultrasonic vibration, dispersed equally, and finally set. Therefore, the castings are short of partial segregation and dispersion in physical and mechanical properties.

Description

【発明の詳細な説明】 〔発明の技術分野〕 本発明は金属酸化物または金属酸化物等の充填剤C;配
合した熱硬化性樹脂注型品の製造方法に関するものであ
る。
DETAILED DESCRIPTION OF THE INVENTION [Technical Field of the Invention] The present invention relates to a method for producing a thermosetting resin cast product containing filler C such as a metal oxide or a metal oxide.

〔発明の技術的背景とその問題点〕[Technical background of the invention and its problems]

従来の熱硬化性注型樹脂注型品は熱硬化性樹脂(=各種
の充填剤を配付し、真空状態に数いて撹拌して混合した
鎌成形用金屋に注型し、連続加熱式電気炉に数いて一次
硬化処理を施こし、−次硬化完了後注型用金型を分解し
て熱硬化性注型樹脂夷品を取出し、二次硬化処理を施こ
している。かかる製造方法によれば一次硬化途中鴫二数
いて熱硬化性注型樹脂より、比重の重い各種の充#14
剤が沈降し分散が不均一(−なる欠点が1、谷部の物理
的性質および機械的性質にも差異が生じ、ひいては。
Conventional thermosetting resin casting products are made by distributing thermosetting resin (= various fillers, casting in a vacuum state, stirring and mixing, casting into a sickle molding metal molding machine, and then heating in a continuous heating electric furnace. After the first curing process is completed, the casting mold is disassembled to take out the thermosetting resin product, and the second curing process is performed. During the primary curing process, various types of filler #14, which have a heavier specific gravity than thermosetting resin, are used.
One drawback is that the agent settles and the dispersion becomes uneven (-), and differences occur in the physical and mechanical properties of the valleys.

充填剤の含有量の多い部位と少ない部位との境界#(=
於いて一次硬化時);収縮率の差異(:起因する微細亀
裂発生の要因となるなどの欠点がある。
Boundary # (=
There are drawbacks such as differences in shrinkage rate (during primary curing) and micro-cracking.

〔発明の目的〕[Purpose of the invention]

本発明は上述の点に罐み、従来技術の欠点を除き熱硬化
性注型樹脂内の充填剤の沈降を防止して均一シニ分散さ
せ物理的性質および機械的性質の部分的なバラツキをな
くして、周囲の急激な温度変化が生ずる環境条件下にお
いても亀裂等の発生がなく眠気絶縁性能を維持して、長
期間のイ慕頼性を有する熱硬化性樹脂注型品の製造方法
を提供することを目的とする。
The present invention satisfies the above points, eliminates the drawbacks of the prior art, prevents the filler from settling in the thermosetting casting resin, uniformly disperses it, and eliminates local variations in physical and mechanical properties. To provide a method for manufacturing a thermosetting resin cast product that maintains its drowsy insulation performance without cracking even under environmental conditions where rapid changes in ambient temperature occur, and has long-term reliability. The purpose is to

〔発明の概要〕[Summary of the invention]

かかる目的を達成するために本発明によれば、熱硬化性
注型樹脂の一次硬化過程ζ二数て、超音波発振装置)二
より前記注型中の樹脂に振動を与え、これによシ注壓樹
脂中(=充填されている充填剤の沈降を防止して、樹脂
中鴫二充填剤を均一に分布させるようにしている。
In order to achieve such an object, according to the present invention, during the primary curing process of the thermosetting resin, vibration is applied to the resin in the casting mold by an ultrasonic oscillator (2), and the casting resin is vibrated by this. Pouring into the resin (= Preventing the sedimentation of the filled filler and ensuring uniform distribution of the filler in the resin.

〔発明の実施例〕[Embodiments of the invention]

次に本発明の一実施例について説明する。 Next, one embodiment of the present invention will be described.

図は本発明の一実施例を示す概略構成図である。The figure is a schematic configuration diagram showing one embodiment of the present invention.

加熱炉2内(=、充填剤を混合した熱硬化性庄屋樹脂を
注入した江型用金減4を、超音波振動発振装置1の超音
波振動子板3上に載置して収納しである。
Inside the heating furnace 2 (=, the E-shaped mold 4 injected with thermosetting Shoya resin mixed with filler is placed on the ultrasonic vibrator plate 3 of the ultrasonic vibration oscillator 1 and stored. be.

熱硬化性注型樹脂に、機械的性質を高めることを目的と
した例えば酸化アルミニウムまたは炭化硅素など、その
他の充填剤を配合した後、真空状態下(=於いて、真空
脱泡し乍ら充分(:攪拌した後十分に礁静させて1図(
=示す如く加熱炉2の内部1:配置された超音波振動子
板3の上区二金屋4を載置する。気泡の巻込み等を防止
するために金盤4の内壁面(=沿って熱硬化性注型樹脂
を、静かに。
After adding other fillers to the thermosetting casting resin, such as aluminum oxide or silicon carbide, to improve its mechanical properties, the thermosetting resin is thoroughly degassed under vacuum conditions. (Figure 1: After stirring, let the reef settle down sufficiently.)
= Inside the heating furnace 2 as shown 1: Place the upper part of the ultrasonic transducer plate 3 on which the upper part 4 is placed. Gently apply thermosetting resin along the inner wall surface of the metal plate 4 to prevent air bubbles from being trapped.

且迅速C:注型する。しかるのちに加熱炉2を密閉状態
にして超音波発振装置11を作動させて、超音波振動子
板3を駆−させることC二熱硬化性注型樹脂を庄屋され
た金型4に超音波振動が与えられる。
And quick C: Casting. Thereafter, the heating furnace 2 is sealed and the ultrasonic oscillator 11 is activated to drive the ultrasonic transducer plate 3. vibration is given.

この状態で加熱炉2の内部温度を熱硬化性注型樹脂の一
次硬化温度迄上昇させ′C1金m、4の内部の熱硬化性
庄屋樹脂の一次硬化が完了するまで一定時間m述の一次
硬化温度で保持する。尚熱硬化性注型樹脂製の注型品が
大形の場合で置型4えの注型途中に於いて充填剤の沈I
4現象が兄生し得る場合(=は、前述の製造方法に限定
されるものではなく金型4えの熱硬化性庄屋樹脂の注型
開始以前から超音波振動発振装置1を作動させて超音波
振動子板3を駆動させて金!!、4T二超音波振動を与
え乍ら、注型を行なうようにすればよい。
In this state, the internal temperature of the heating furnace 2 is raised to the primary curing temperature of the thermosetting resin. Hold at curing temperature. In addition, if the cast product made of thermosetting resin is large, the filler may be precipitated during the casting process.
4 phenomena can occur together (= is not limited to the above-mentioned manufacturing method, but the ultrasonic vibration oscillator 1 is activated before the start of casting the thermosetting Shoya resin in the mold 4). Casting may be performed while driving the sonic vibrator plate 3 to apply ultrasonic vibrations of gold and 4T.

金型4の構造および金型各部の肉厚は金型内部に注をさ
れた熱硬化性庄屋樹脂は、金型下部の金at=接触して
表面から一次硬化が開始し1肉厚中央部に硬化が進行し
上部に向って進展しfIIt終的嘔二は金型上部に設け
られた注型口が硬化して、全体の硬化が完了する様4−
金屋の構造および金星各部肉厚が設計されている。従っ
て、超音波振動を与えられることによυ流動状態i:b
る熱硬化性注型樹脂内の配合された充填剤は常に沈咋す
ることなく熱硬化性注型樹脂内に浮遊した状態で均一(
=分散させた状態を最終値化児了崎点まで維持する事が
可能でめる。このため充填剤が全体(=均一(;分散し
、局部的な偏析がなく物理的性質および機械的性質のバ
ラツキがなく、磁気flIA縁性能の後れた、長期信頼
性の有る、各種の充填剤を含有する熱硬化性注型樹脂#
!注型品を製造する事が可i目である。
The structure of the mold 4 and the wall thickness of each part of the mold are as follows: The thermosetting Shoya resin poured into the inside of the mold contacts the metal at the bottom of the mold and primary hardening starts from the surface, and the thickness of the thermosetting Shoya resin starts from the surface. The curing progresses toward the top, and finally, the casting hole provided at the top of the mold hardens, and the entire hardening is completed.4-
The structure of the gold shop and the wall thickness of each part of Venus are designed. Therefore, by applying ultrasonic vibration, υ flow state i:b
The filler blended into the thermosetting resin is always suspended uniformly in the thermosetting resin without settling.
= It is possible to maintain the dispersed state until the final value is reached. Therefore, the filler is uniform throughout (=dispersed, there is no local segregation, there is no variation in physical and mechanical properties, and the magnetic flIA edge performance is inferior to that of other types of fillings, which have long-term reliability.) Thermosetting casting resin containing agent#
! It is possible to manufacture cast products.

〔発明の効果〕〔Effect of the invention〕

以上説明したように本発明(=よれば、充填剤を、熱硬
化性注型樹脂の内部に全体に均−艦=分散させた状態で
一次硬化させることがでさ、従ってこの過程を経て製造
された注型品は4!l!l埋的及び機械的性質のバラツ
キのない注型品とすることができる。
As explained above, according to the present invention, it is possible to primary cure the filler in a state in which the filler is uniformly dispersed throughout the inside of the thermosetting casting resin. The cast product obtained by this method can be a cast product with no variation in 4!l!l buried and mechanical properties.

【図面の簡単な説明】[Brief explanation of the drawing]

図は本発明(:よる注型品の製造方法の一実施例を示す
概略構成図である。
The figure is a schematic diagram showing an embodiment of the method for manufacturing a cast product according to the present invention.

Claims (1)

【特許請求の範囲】[Claims] 熱硬化性注型樹脂に酸化アルミニウムまたは炭化硅素等
の充填剤を配合して熱硬化性注型樹脂注型品を製造する
ものに於いて、前記熱硬化性注型樹脂を金型に注型後の
一次硬化の過程に於いて超音波発振装置等により金型に
振動を与えて充填剤を均一に分布させるようにして一次
硬化を行なうようにした熱硬化性樹脂注型品の製造方法
When manufacturing a thermosetting resin cast product by blending a filler such as aluminum oxide or silicon carbide with a thermosetting resin, the thermosetting resin is cast into a mold. A method for manufacturing a thermosetting resin cast product, in which primary curing is performed by applying vibration to the mold using an ultrasonic oscillator or the like to uniformly distribute the filler during the subsequent primary curing process.
JP27173484A 1984-12-25 1984-12-25 Preparation of thermosetting resin castings Pending JPS61149319A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP27173484A JPS61149319A (en) 1984-12-25 1984-12-25 Preparation of thermosetting resin castings

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP27173484A JPS61149319A (en) 1984-12-25 1984-12-25 Preparation of thermosetting resin castings

Publications (1)

Publication Number Publication Date
JPS61149319A true JPS61149319A (en) 1986-07-08

Family

ID=17504087

Family Applications (1)

Application Number Title Priority Date Filing Date
JP27173484A Pending JPS61149319A (en) 1984-12-25 1984-12-25 Preparation of thermosetting resin castings

Country Status (1)

Country Link
JP (1) JPS61149319A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5093050A (en) * 1989-11-17 1992-03-03 Laboratorium Fur Experimentelle Chirurgie Method for producing oriented, discontinuous fiber reinforced composite materials
JPH0641630U (en) * 1992-11-11 1994-06-03 タイガー魔法瓶株式会社 Insulated lunch box
KR100507955B1 (en) * 1999-11-25 2005-08-17 한국하이테크공업(주) Method of diffusing filling material to resin
CN103847051A (en) * 2012-12-04 2014-06-11 吴秉筠 Mold

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5093050A (en) * 1989-11-17 1992-03-03 Laboratorium Fur Experimentelle Chirurgie Method for producing oriented, discontinuous fiber reinforced composite materials
JPH0641630U (en) * 1992-11-11 1994-06-03 タイガー魔法瓶株式会社 Insulated lunch box
KR100507955B1 (en) * 1999-11-25 2005-08-17 한국하이테크공업(주) Method of diffusing filling material to resin
CN103847051A (en) * 2012-12-04 2014-06-11 吴秉筠 Mold

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