JPS61145825A - Cleaning end detection for plasma chemical vapor deposition apparatus - Google Patents

Cleaning end detection for plasma chemical vapor deposition apparatus

Info

Publication number
JPS61145825A
JPS61145825A JP26908884A JP26908884A JPS61145825A JP S61145825 A JPS61145825 A JP S61145825A JP 26908884 A JP26908884 A JP 26908884A JP 26908884 A JP26908884 A JP 26908884A JP S61145825 A JPS61145825 A JP S61145825A
Authority
JP
Japan
Prior art keywords
end point
deposition chamber
power
discharge
thin film
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP26908884A
Other languages
Japanese (ja)
Other versions
JPH0642457B2 (en
Inventor
Ikunori Kobayashi
郁典 小林
Sadakichi Hotta
堀田 定▲吉▼
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Panasonic Holdings Corp
Original Assignee
Matsushita Electric Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Matsushita Electric Industrial Co Ltd filed Critical Matsushita Electric Industrial Co Ltd
Priority to JP26908884A priority Critical patent/JPH0642457B2/en
Publication of JPS61145825A publication Critical patent/JPS61145825A/en
Publication of JPH0642457B2 publication Critical patent/JPH0642457B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/52Controlling or regulating the coating process
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C16/00Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
    • C23C16/44Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the method of coating
    • C23C16/4401Means for minimising impurities, e.g. dust, moisture or residual gas, in the reaction chamber
    • C23C16/4405Cleaning of reactor or parts inside the reactor by using reactive gases
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/32Gas-filled discharge tubes
    • H01J37/32431Constructional details of the reactor
    • H01J37/32798Further details of plasma apparatus not provided for in groups H01J37/3244 - H01J37/32788; special provisions for cleaning or maintenance of the apparatus
    • H01J37/32853Hygiene
    • H01J37/32862In situ cleaning of vessels and/or internal parts
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01JELECTRIC DISCHARGE TUBES OR DISCHARGE LAMPS
    • H01J37/00Discharge tubes with provision for introducing objects or material to be exposed to the discharge, e.g. for the purpose of examination or processing thereof
    • H01J37/32Gas-filled discharge tubes
    • H01J37/32917Plasma diagnostics
    • H01J37/32935Monitoring and controlling tubes by information coming from the object and/or discharge
    • H01J37/32963End-point detection

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Plasma & Fusion (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Analytical Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Epidemiology (AREA)
  • Public Health (AREA)
  • Testing Or Measuring Of Semiconductors Or The Like (AREA)
  • Drying Of Semiconductors (AREA)

Abstract

PURPOSE:To detect the cleaning end point within a deposition chamber by obtaining an output from a wattmeter which measures a reflection power for discharge input power or from a voltmeter which measures a DC bias voltage of discharge electrode and outputting a signal when a voltage reaches the selectively preset value. CONSTITUTION:After starting glow discharge by into reducing etching into the deposition chamber to which deposited film is adhered, inductance and capacitance of matching circuit 3 are adjusted so that the power indicated by a reflection power meter 4 is minimized. Thereafter, when a thin film adhered to the deposition chamber is removed, a reflection power is increased and the cleaning end point can be monitored by detecting that a reflection power reaches a preset value with an end point detector 5. When a thin film adhered to the deposition chamber, change of DC bias voltage of discharge power can be measured with a bias voltmeter 8, it is detected by the end point detector 5 that the DC bias voltage has reached a preset value and thereby the cleaning end point can be monitored.

Description

【発明の詳細な説明】 産業上の利用分野 本発明はプラズマ放電を用いて半導体薄膜あるいは絶縁
体薄膜を堆積するプラズマ化学気相堆積装置の堆積室内
に付着した薄膜をエツチングガスおよびプラズマ放電を
用いて除去する工程の際にその除去工程終点をモニをす
る方法に関するものである。
DETAILED DESCRIPTION OF THE INVENTION Field of Industrial Application The present invention uses etching gas and plasma discharge to remove a thin film deposited within the deposition chamber of a plasma chemical vapor deposition apparatus that deposits a semiconductor thin film or an insulating thin film using plasma discharge. The present invention relates to a method for monitoring the end point of the removal process during the removal process.

従来の技術 従来、プラズマ化学気相堆積装置の堆積室内のクリーニ
ング終点全モートする技術としては、例えば菅野卓雄編
著「半導体プラズマプロセス技術」(昭56.7.10
)、産業図書、Plllに示されているように、質量分
析法、発光分光法等ドライエツチング技術に適用されて
いるモニタ一方式が応用されていた。
Conventional technology Conventionally, as a technique for cleaning all end points in the deposition chamber of a plasma chemical vapor deposition apparatus, for example, "Semiconductor Plasma Process Technology" edited by Takuo Kanno (July 10, 1982)
), Sangyo Tosho, Plll, a monitor system applied to dry etching techniques such as mass spectrometry and emission spectroscopy was applied.

発明が解決しようとする問題点 このような従来のモニタ一方式では、プラズマ化学気相
堆積装置に薄膜堆積時には直接必要としない終点検出装
置等を設置しなければならない上に、絶えずその検出装
置のメンテナンスを必要とした。
Problems to be Solved by the Invention With such a conventional one-monitor system, it is necessary to install an end point detection device, etc., which is not directly required during thin film deposition, in the plasma chemical vapor deposition apparatus, and the detection device is constantly being monitored. Maintenance required.

本発明はかかる問題点に鑑みなされたもので、本来プラ
ズマ化学気相堆積装置に設置されている反射電力計、D
Cバイアス電圧計を使用して、容易に堆積室内のクリー
ニング終点を検出する方法を提供することを目的として
いる。
The present invention was made in view of such problems, and is based on a reflection power meter originally installed in a plasma chemical vapor deposition apparatus.
It is an object of the present invention to provide a method for easily detecting the end point of cleaning in a deposition chamber using a C bias voltmeter.

問題点を解決するための手段 本発明は上記問題を解決するため、放電投入電力に対す
る反射電力を測定する電力計あるいは放電電極のDCバ
イアス電圧を測定する電圧計よりその出力を得て、任意
の設定値に到達した時に信号を出力できるものである。
Means for Solving the Problems In order to solve the above problems, the present invention obtains the output from a wattmeter that measures the reflected power with respect to the discharge input power or a voltmeter that measures the DC bias voltage of the discharge electrode, and It can output a signal when a set value is reached.

作用 本発明は上記した構成により、堆積薄膜が付着した堆積
室内にエツチングガスを導入しグロー放電を開始した後
に整合回路のインダクタンス、キャパシタンスを固定す
ることにより、堆積室に付着した薄膜が除去された時放
電投入電力に対する反射電力の上昇が検出され、任意の
設定値に到達した時出力される信号によりクリーニング
終点をモニターできる。
According to the above-described structure, the present invention introduces etching gas into the deposition chamber to which the deposited thin film has adhered, starts glow discharge, and then fixes the inductance and capacitance of the matching circuit, thereby removing the thin film adhered to the deposition chamber. The end point of cleaning can be monitored by a signal output when an increase in reflected power with respect to power applied during discharge is detected and reaches an arbitrary set value.

実施例 第1図は本発明のクリーニング終点をモニターする回路
の一実施例を示すブロック図である。第1図において、
1は堆積室、2は放電電極であって、高周波電源7によ
り放電電力を投入する。この時投入電力は投入電力計6
により測定し、反射電力計4に示される電力が最小にな
るように整合回路3のインダクタンスおよびキャパシタ
ンスを調整する。その後堆積室に付着した薄膜が除去さ
れた時反射電力が増加し、設定値にその反射電力が到達
したことを終点検出器6により検知してクリーニングの
終点をモニターすることができる。
Embodiment FIG. 1 is a block diagram showing an embodiment of a circuit for monitoring the cleaning end point of the present invention. In Figure 1,
1 is a deposition chamber and 2 is a discharge electrode, to which discharge power is applied by a high frequency power source 7. At this time, the input power is input power meter 6
The inductance and capacitance of the matching circuit 3 are adjusted so that the power shown on the reflected power meter 4 is minimized. Thereafter, when the thin film adhering to the deposition chamber is removed, the reflected power increases, and the end point detector 6 detects that the reflected power has reached a set value, thereby making it possible to monitor the end point of cleaning.

第2図に本発明の一実施例においてアモルファスシリコ
ンが付着した堆積室をCF、+10%02のエツチング
ガスを用いて放電投入電力を400Wとした場合のクリ
ーニング時間に対する反射電力の変化とクリーニング終
点を示す。図に示すように、クリーニング時間eの時点
より反射電力が徐々に上昇し、反射電力が40Wに達し
た時クリーニングが終了していることがわかる。従って
第1図の終点検出器5の設定値140Wに設定しておく
ことにより、クリーニング終点を容易にモニターできる
Figure 2 shows the change in reflected power and cleaning end point with respect to the cleaning time when the deposition chamber to which amorphous silicon was deposited was etched with CF, +10%02 etching gas, and the discharge input power was 400 W in one embodiment of the present invention. show. As shown in the figure, the reflected power gradually increases from the cleaning time e, and when the reflected power reaches 40 W, it can be seen that the cleaning has been completed. Therefore, by setting the end point detector 5 of FIG. 1 to a set value of 140 W, the cleaning end point can be easily monitored.

第3図は本発明の他の実施例におけるクリーニング終点
をモニターする回路のブロック図である。
FIG. 3 is a block diagram of a circuit for monitoring the cleaning end point in another embodiment of the present invention.

本実施例は、堆積室に付着した薄膜が除去された時、放
電電力のDCバイアス電圧の変化をDCバイアス電圧計
8により測定し、そのDCバイアス電圧が設定値に到達
したことを終点検出器6により感知してクリーニング終
点をモニターする。
In this embodiment, when the thin film attached to the deposition chamber is removed, the change in the DC bias voltage of the discharge power is measured by the DC bias voltmeter 8, and the end point detector detects that the DC bias voltage has reached the set value. 6 to monitor the cleaning end point.

第4図にアモルファスシリコンが付着した堆積室をay
、+1o%へのエツチングガスを用いて放電投入電力1
400Wとした場合のクリーニング時間に対するDCバ
イアス電圧の変化とクリーニング終点を示す。図に示す
ように、クリーニング時間6よりDCバイアス電圧が減
少しはじめ、−42vに達した時クリーニングが終了し
ていることがわかる。従って、第3図の終点検出器6の
設定値f−42Vに設定しておくことにより、クリーニ
ング終点を容易にモニターできる。
Figure 4 shows the deposition chamber with amorphous silicon attached.
, discharge input power 1 using etching gas to +1o%
The change in DC bias voltage and the cleaning end point with respect to the cleaning time when the power is 400W are shown. As shown in the figure, the DC bias voltage begins to decrease from cleaning time 6, and when it reaches -42V, it can be seen that the cleaning has been completed. Therefore, by setting the end point detector 6 of FIG. 3 to the set value f-42V, the cleaning end point can be easily monitored.

発明の効果 以上述べてきたように、本発明は、本来プラズマCVD
装置に必須である。放電反射電力計またはDCバイアス
電圧計を用いて、きわめて簡易な構成で容易にクリーニ
ング終点をモニタできる効果を有する。
Effects of the Invention As mentioned above, the present invention is originally based on plasma CVD.
Required for the device. Using a discharge reflection wattmeter or a DC bias voltmeter, the cleaning end point can be easily monitored with a very simple configuration.

【図面の簡単な説明】[Brief explanation of drawings]

第1図は本発明の一実施例におけるクリーニング終点モ
ニター回路のブロック図、第2図はクリーニング時間に
対する反射電力の変化を示す図、第3図は本発明の他の
実施例におけるクリーニング終点モニター回路のブロッ
ク図、第4図はクリーニング時間に対するDCバイアス
電圧の変化を示す図である。 1・・・・・・堆積室、2・・・・・・放電電極、3・
・・・・・整合回路、4・・・・・・反射電力計、5・
・・・・・終点検出器、6・・・・・・投入電力計、7
・・・・・・高周波電源、8・・・・・・DCバイアス
電圧計。 代理人の氏名 弁理士 中 尾 敏 男 ほか1名第1
図 第2図 クリ−;ンヂ蒔聞(秒先学it) 第3図 第4図
FIG. 1 is a block diagram of a cleaning end point monitor circuit in one embodiment of the present invention, FIG. 2 is a diagram showing changes in reflected power with respect to cleaning time, and FIG. 3 is a cleaning end point monitor circuit in another embodiment of the present invention. FIG. 4 is a block diagram showing changes in DC bias voltage with respect to cleaning time. 1...Deposition chamber, 2...Discharge electrode, 3.
...Matching circuit, 4...Reflected power meter, 5.
... End point detector, 6 ... Power supply meter, 7
...High frequency power supply, 8...DC bias voltmeter. Name of agent: Patent attorney Toshio Nakao and 1 other person No. 1
Figure 2 Cree;

Claims (1)

【特許請求の範囲】[Claims] プラズマ化学気相堆積装置の堆積室内に付着した半導体
薄膜あるいは絶縁体薄膜をエッチングガス及びグロー放
電等のプラズマ放電を用いて前記薄膜を除去する工程の
際に、放電投入電力に対する反射電力またはプラズマ電
極に発生するバイアス電圧を計測することにより、前記
堆積室内の薄膜除去工程の終点をモニターすることを特
徴とするプラズマ化学気相堆積装置のクリーニング終点
検出方法。
During the process of removing a semiconductor thin film or an insulating thin film deposited in the deposition chamber of a plasma chemical vapor deposition apparatus using an etching gas and plasma discharge such as glow discharge, the reflected power or plasma electrode with respect to the discharge input power is removed. A cleaning end point detection method for a plasma chemical vapor deposition apparatus, characterized in that the end point of a thin film removal process in the deposition chamber is monitored by measuring a bias voltage generated in the deposition chamber.
JP26908884A 1984-12-19 1984-12-19 Cleaning chemical endpoint detection method for plasma chemical vapor deposition apparatus Expired - Fee Related JPH0642457B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP26908884A JPH0642457B2 (en) 1984-12-19 1984-12-19 Cleaning chemical endpoint detection method for plasma chemical vapor deposition apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP26908884A JPH0642457B2 (en) 1984-12-19 1984-12-19 Cleaning chemical endpoint detection method for plasma chemical vapor deposition apparatus

Publications (2)

Publication Number Publication Date
JPS61145825A true JPS61145825A (en) 1986-07-03
JPH0642457B2 JPH0642457B2 (en) 1994-06-01

Family

ID=17467498

Family Applications (1)

Application Number Title Priority Date Filing Date
JP26908884A Expired - Fee Related JPH0642457B2 (en) 1984-12-19 1984-12-19 Cleaning chemical endpoint detection method for plasma chemical vapor deposition apparatus

Country Status (1)

Country Link
JP (1) JPH0642457B2 (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61256637A (en) * 1985-05-06 1986-11-14 インターナショナル・ビジネス・マシーンズ・コーポレーション Monitoring of plasma etching process
WO2001077406A2 (en) * 2000-04-07 2001-10-18 Philips Semiconductors, Inc. A method of determining the end point of a plasma cleaning operation
US7534469B2 (en) 2005-03-31 2009-05-19 Asm Japan K.K. Semiconductor-processing apparatus provided with self-cleaning device
WO2018193584A1 (en) * 2017-04-20 2018-10-25 堺ディスプレイプロダクト株式会社 Cvd device and cleaning method therefor
WO2022234831A1 (en) * 2021-05-06 2022-11-10 東京エレクトロン株式会社 Plasma treatment device and endpoint detection method

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61256637A (en) * 1985-05-06 1986-11-14 インターナショナル・ビジネス・マシーンズ・コーポレーション Monitoring of plasma etching process
JPH0528895B2 (en) * 1985-05-06 1993-04-27 Intaanashonaru Bijinesu Mashiinzu Corp
WO2001077406A2 (en) * 2000-04-07 2001-10-18 Philips Semiconductors, Inc. A method of determining the end point of a plasma cleaning operation
WO2001077406A3 (en) * 2000-04-07 2002-01-24 Philips Semiconductors Inc A method of determining the end point of a plasma cleaning operation
US6543459B1 (en) 2000-04-07 2003-04-08 Koninklijke Philips Electronics N.V. Method of determining an end point for a remote microwave plasma cleaning system
US7534469B2 (en) 2005-03-31 2009-05-19 Asm Japan K.K. Semiconductor-processing apparatus provided with self-cleaning device
WO2018193584A1 (en) * 2017-04-20 2018-10-25 堺ディスプレイプロダクト株式会社 Cvd device and cleaning method therefor
WO2022234831A1 (en) * 2021-05-06 2022-11-10 東京エレクトロン株式会社 Plasma treatment device and endpoint detection method

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