JPS6015541A - Apparatus for measuring particle size distribution of particles - Google Patents

Apparatus for measuring particle size distribution of particles

Info

Publication number
JPS6015541A
JPS6015541A JP58123447A JP12344783A JPS6015541A JP S6015541 A JPS6015541 A JP S6015541A JP 58123447 A JP58123447 A JP 58123447A JP 12344783 A JP12344783 A JP 12344783A JP S6015541 A JPS6015541 A JP S6015541A
Authority
JP
Japan
Prior art keywords
particles
particle size
size distribution
slit
particle
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP58123447A
Other languages
Japanese (ja)
Other versions
JPH0627694B2 (en
Inventor
Takashi Nishikawa
孝 西川
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsubishi Kasei Corp
Original Assignee
Mitsubishi Kasei Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsubishi Kasei Corp filed Critical Mitsubishi Kasei Corp
Priority to JP58123447A priority Critical patent/JPH0627694B2/en
Publication of JPS6015541A publication Critical patent/JPS6015541A/en
Publication of JPH0627694B2 publication Critical patent/JPH0627694B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/10Investigating individual particles
    • G01N15/14Optical investigation techniques, e.g. flow cytometry
    • G01N15/1468Optical investigation techniques, e.g. flow cytometry with spatial resolution of the texture or inner structure of the particle

Landscapes

  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Length Measuring Devices By Optical Means (AREA)

Abstract

PURPOSE:To enable accurate measurement of particle size distribution handily and quickly by irradiating particles dropping from a granulator or the like with a plane strobo light through a slit to take a still image of particles with a TV camera provided vertical to the plane light. CONSTITUTION:When particles 2 are dropped from a granulator, hopper or the like 1, a start signal is sent to a high-speed image processor 7 from a microcomputer 8. Receiving the signal, the processor 7 transmits a signal to a strobo controller 9 to irradiate the particles 2 with a plane strobo light A from a slit strobo light emitter 3. A semicircular image of each particle is taken with a TV camera 4 arranged vertical to the surface A and the image is displayed on a TV monitor via a camera controller 5 while the projection lengths of the particles are calculated, classified and accumulated with the processor 7. The results are transmitted to the computer 8 to compute the particle size distribution, average particle size and the like and the results are outputted to a printer 10 or the like.

Description

【発明の詳細な説明】 本発明は、粒子群の粒度分布や粒径等を測定するもので
、連続しての測定を可能にした装置に関するものである
DETAILED DESCRIPTION OF THE INVENTION The present invention is for measuring the particle size distribution, particle diameter, etc. of a particle group, and relates to an apparatus that enables continuous measurement.

例えば、造粒機によp造粒された粒子や各イ止原制の粒
状物体等は、その粒径や粒度分布等を測定する必要があ
る。これら粒子群の形状、大きさ等の測定手段として、
従来は篩を用いての篩分は等の手段が知られているが、
極めて非能率的なものであった。またストロボ発光装置
とテレビカメラを用いて粒子群の静止画像をめこれによ
って粒子群の形状、大きさ等を測定する方法も知られて
いる。しかしこの静止画像による方法は、多数の粒子群
を撮像する関係から、そのままでは各粒子が重なシ合っ
てしまって粒子個々の大きさ等をめることが困難である
。そのため従来の静止画像による方法では、造粒機やホ
ッパー等より排出される粒子群をそのまま測定せずに、
一度適宜な整列装置を用いて各粒子が成る間隔をもって
整列するようにしてから撮像しなければならない欠点が
あった。
For example, it is necessary to measure the particle size, particle size distribution, etc. of particles granulated by a granulator or granular objects of various Ito-forms. As a means of measuring the shape, size, etc. of these particle groups,
Conventionally, methods such as sieving using a sieve are known,
It was extremely inefficient. Also known is a method of measuring the shape, size, etc. of a particle group using a strobe light emitting device and a television camera to capture a still image of the particle group. However, in this method using still images, since a large number of particle groups are imaged, the particles overlap each other, making it difficult to determine the size of each particle. Therefore, conventional methods using still images do not directly measure the particle group discharged from the granulator or hopper, etc.
There is a drawback that an appropriate alignment device must be used to align the particles at the same intervals before imaging.

本発明は、以上述べたような事情に鑑みなされたもので
あって、造粒機やホッパー等よシ落下する粒子群をスリ
ットを設けたストロボ光発光装置によシ照明し又前記発
光装置により発光しスリットを通った光の面にほぼ直角
な方向に配置し照明された粒子群にピントを合わせであ
るテレビカメラを用いて粒子群を撮像しこの静止画像に
もとづいて形状や粒度分布等−を測定するようにした粒
子群の1111定装置を提供するものである。
The present invention has been made in view of the above-mentioned circumstances, and it illuminates a group of particles falling from a granulator, a hopper, etc. using a strobe light emitting device provided with a slit, and the light emitting device A television camera is used to image the illuminated particles, arranged in a direction almost perpendicular to the plane of the light that emitted and passes through the slit, and then image the particle group using a television camera. Based on this still image, the shape, particle size distribution, etc. The object of the present invention is to provide a particle group 1111 determination device that measures 1111 of particles.

以下1メ]示する実施例にもとづいて本発明の測定装置
べの詳細な内容を説明する。1は造粒機でこれの中の造
粒された漆ヤ子群2がとの造粒機より落下している状態
を示している。3は縦長(上下方向に長い)のスリット
を設けたスリットストロボ光発光装置、4はスリットス
トロボ光発光装置より発光する光の+I4i A (細
長いスリットを通った光はほぼ平面状に進行する)に対
してほぼ直角な位置、に配置されていてこの光の百Aに
ピントを合わせであるテレビカメラ。尚ことで云う[−
はぼ直角」とI:I、直角を中心に画1象の周辺部でも
ピントずれが起らない程度の角度である。5はカメラコ
ントローラー、6はテレビカメラ4により撮像された像
を覗祭するだめのテレビモニター、7は高速イメニジグ
ロセツザー、8はマイクロコンピュータ−19はスリッ
トストロボ光発光装置の発光をコントロールするストロ
ボコントローラー、10ハブリンターである。
The detailed contents of the measuring apparatus of the present invention will be explained below based on the following embodiments. 1 shows a granulator in which the granulated lacquer yarn group 2 is falling from the other granulator. 3 is a slit strobe light emitting device provided with a vertically elongated (long in the vertical direction) slit, and 4 is a +I4i A of the light emitted from the slit strobe light emitting device (the light that passes through the elongated slit travels approximately in a plane). A television camera is placed at a nearly right angle to the camera and focuses on this 100A beam. Furthermore, it is said [-
I:I is an angle that does not cause out-of-focus even at the periphery of the image with the right angle at the center. 5 is a camera controller; 6 is a TV monitor for viewing images taken by the TV camera 4; 7 is a high-speed image sensor; 8 is a microcomputer; Strobe controller, 10 hub linter.

以上のような構成の測定装置において、図示するように
造粒機1にて造粒された粒子群2を落下させる時にマイ
クロコンピュータ−8により開始信号を発信する。この
開始信号を受信して高速イメージプロセツザ−7はスト
ロボコントローラー9に信号を送シこれによってストロ
ボコントローラー9はスリットストロボ光発光装置を発
光させる。このストロボ光により造粒機1より自然落下
中の粒子群2は照明される。これと同時に高速イメージ
プロセッサー7からカメラコントローラー5に信号が送
られカメラコントローラー5によってテレビカメラ4に
よる撮像が行なわれる。
In the measuring apparatus having the above configuration, a start signal is transmitted by the microcomputer 8 when the particle group 2 granulated by the granulator 1 is dropped as shown in the figure. Upon receiving this start signal, the high-speed image processor 7 sends a signal to the strobe controller 9, which causes the slit strobe light emitting device to emit light. The particle group 2 falling naturally from the granulator 1 is illuminated by this strobe light. At the same time, a signal is sent from the high-speed image processor 7 to the camera controller 5, and the camera controller 5 causes the television camera 4 to take an image.

この時の粒子群2の像は例えば第2図に示すようなもの
である。即ち第2図において矢印方向よシストロボ光が
来るので各粒子の在世す半分(図面の斜線部分)が照明
されて明るくなり、これをテレビカメラ4で撮像する。
The image of the particle group 2 at this time is, for example, as shown in FIG. That is, in FIG. 2, the system strobe light comes in the direction of the arrow, so that the half of each particle (the shaded area in the drawing) is illuminated and brightened, and this is imaged by the television camera 4.

撮像された静止画像の信号は、テレビモニター6へ送ら
れこれに映し出されて観察される。この1¥p市画隊の
信号は、同時に高速イメージプロセツザ−7へ送られ、
ここで処理されて各粒子の水平投影長が算出される。算
出された投影長は、n段階に区分された各クラスにその
長さビ応じてクラス分けされる。つll高速イメージプ
ロセッサー7では、各クラスの粒子の数を記憶する。こ
のようにして高速イメージプロセッサー7は、一定の視
野範囲の粒子のデーターをクラス分けして累積し、その
結果をマイクロコンピュータ−8に送る。
The captured still image signal is sent to the television monitor 6 and displayed on it for observation. This signal from the 1¥p City Painting Team is simultaneously sent to the high-speed image processor 7.
Processing is performed here to calculate the horizontal projection length of each particle. The calculated projection lengths are classified into n-level classes according to their lengths. A high speed image processor 7 stores the number of particles in each class. In this manner, the high-speed image processor 7 classifies and accumulates data on particles within a certain field of view, and sends the results to the microcomputer 8.

マイクロコンピュータ−8に送られたデーターは、粒度
分布や平均粒子径等の統計上の数値を演算によってめた
後プリンター10に出力する。
The data sent to the microcomputer 8 is output to the printer 10 after calculating statistical values such as particle size distribution and average particle diameter.

以上述べたように、本発明の測定装置は、ストロボ光発
光装置1/lにより照明してテレビカメラで撮像するの
で落下中の粒子群を静止画像として撮像できる。しかも
発光装置がスリットを備えたスリットストロボ光発光装
置であり、更にテレビカメラをストロボ光の発光方向と
ほぼ直交する位置配置し/こので、テレビカメラの焦点
適合面のみ光が照射さJし、その前後の焦点不適合位置
を落下する粒子群には照明光は照射されない。そのため
焦点ぼけした粒子を誤って訓電することがない。その上
半月状に照射されるので像の水平方向の重なりは分離出
来、したがって高速イメージプロセッサーは垂直方向の
重なシのみ分離すればよいのでその処理が簡単である。
As described above, since the measuring device of the present invention illuminates with the strobe light emitting device 1/l and images with a television camera, it is possible to image falling particles as a still image. In addition, the light emitting device is a slit strobe light emitting device equipped with a slit, and the television camera is placed at a position almost perpendicular to the direction of emission of the strobe light, so that only the focal plane of the television camera is irradiated with light. Illumination light is not irradiated to the particle group falling through out-of-focus positions before and after the particle group. Therefore, there is no possibility of erroneously training an out-of-focus particle. Since the images are irradiated in a half-moon shape, it is possible to separate horizontally overlapping images, and therefore, a high-speed image processor only needs to separate vertically overlapping images, which simplifies processing.

以上のことにより従来の方法のように粒子群を落下させ
る前に整列させる必要もない。
As a result of the above, there is no need to align the particle groups before dropping them, unlike in the conventional method.

尚実施例に瞥いては、造粒機において造粒された固体粒
子群について述べたが、その他の固体粒子群の測定や尿
素造粒の際の液滴粒度分布の測定のように液滴の測定に
対しても適用し得る。また平面状のストロボ光の面は垂
直から水平までの任意の角度に設定し得る。
In addition, in the examples, the solid particle group granulated in the granulator was described, but the measurement of other solid particle groups and the measurement of the droplet particle size distribution during urea granulation, etc. It can also be applied to measurements. Further, the plane of the planar strobe light can be set at any angle from vertical to horizontal.

【図面の簡単な説明】 第1図は本発明の測定装置の構成を示す図、第2図は本
発明装置においてストロボ光にて粒子群を照明した状態
を示す図である。 1・・・・造粒機、2・・・・粒子群、3・・・・スリ
ットストロボ光発光装置、4・・・・テレビカメラ、5
・・・・カメラコントローラー、6・・・・テレヒモニ
ター、7・・・・高速イメージプロセッサー、8・・・
・マイクロコンピュータ−19・・・・ストロボコ” 
ドロー ’y−+ 10・・・・プリン2−8出九!口
人 三菱化成工業株式会社 代理人 向 寛 − 第1図 ■
BRIEF DESCRIPTION OF THE DRAWINGS FIG. 1 is a diagram showing the configuration of a measuring device of the present invention, and FIG. 2 is a diagram showing a state in which a group of particles is illuminated with strobe light in the device of the present invention. 1... Granulator, 2... Particle group, 3... Slit strobe light emitting device, 4... Television camera, 5
...Camera controller, 6...Television monitor, 7...High-speed image processor, 8...
・Microcomputer-19...Stroboko"
Draw 'y-+ 10...pudding 2-8 out 9! Person: Hiroshi Mukai, Agent, Mitsubishi Chemical Industries, Ltd. - Figure 1■

Claims (1)

【特許請求の範囲】[Claims] 落下する粒子群を照明するだめのスリットを有するスト
ロボ光発光装置と、前記スリットを通して進む平面状の
ストロボ光に対しほぼ垂直な方向に配置6されストロボ
光にて照りJされた粒子群位置にピントを合せであるテ
レビカメラとを備えていて、前記ストロボ光発光装置を
発光して照明しテレビカメラにて撮像された粒子群の静
止画像にもとづいてその粒度分布をめるようにした粒子
群の粒度分布の測定装置。
A strobe light emitting device having a slit for illuminating a group of falling particles, and a strobe light emitting device arranged in a direction substantially perpendicular to the planar strobe light traveling through the slit to focus on the position of the particle group illuminated by the strobe light. and a television camera, the strobe light emitting device emits light to illuminate the particle group, and the particle size distribution is determined based on a still image of the particle group captured by the television camera. Particle size distribution measuring device.
JP58123447A 1983-07-08 1983-07-08 Measuring device for particle size distribution of particles Expired - Lifetime JPH0627694B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP58123447A JPH0627694B2 (en) 1983-07-08 1983-07-08 Measuring device for particle size distribution of particles

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP58123447A JPH0627694B2 (en) 1983-07-08 1983-07-08 Measuring device for particle size distribution of particles

Publications (2)

Publication Number Publication Date
JPS6015541A true JPS6015541A (en) 1985-01-26
JPH0627694B2 JPH0627694B2 (en) 1994-04-13

Family

ID=14860830

Family Applications (1)

Application Number Title Priority Date Filing Date
JP58123447A Expired - Lifetime JPH0627694B2 (en) 1983-07-08 1983-07-08 Measuring device for particle size distribution of particles

Country Status (1)

Country Link
JP (1) JPH0627694B2 (en)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS59748U (en) * 1982-06-25 1984-01-06 昭和製袋工業株式会社 bag
JPS62273431A (en) * 1986-05-21 1987-11-27 Takemasa Kamimoto Mean particle diameter measuring instrument for injected fuel
JPH01275490A (en) * 1988-04-26 1989-11-06 Mitsubishi Kasei Corp Production of granulated fertilizer
FR2664983A1 (en) * 1990-07-17 1992-01-24 Centre Tech Ind Papier DEVICE FOR THE CONTINUOUS DETECTION OF CONTRAST IMPURITIES CONTAINED IN A MOVING FLUID MATERIAL.
US5497232A (en) * 1993-10-26 1996-03-05 Fuji Paudal Co., Ltd. Apparatus and method for monitoring granular size and shape during a granulation or coating process
US5707766A (en) * 1994-09-01 1998-01-13 Fuji Electric Co., Ltd. Electrophotographic photosensitive material
CN104777080A (en) * 2015-04-10 2015-07-15 中国石油大学(北京) Online detecting device and method for granules and liquid drops in gas pipelines

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5712458A (en) * 1980-06-25 1982-01-22 Matsushita Electric Ind Co Ltd Disk-type flexible magnetic recorder cartridge

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5712458A (en) * 1980-06-25 1982-01-22 Matsushita Electric Ind Co Ltd Disk-type flexible magnetic recorder cartridge

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS59748U (en) * 1982-06-25 1984-01-06 昭和製袋工業株式会社 bag
JPS62273431A (en) * 1986-05-21 1987-11-27 Takemasa Kamimoto Mean particle diameter measuring instrument for injected fuel
JPH01275490A (en) * 1988-04-26 1989-11-06 Mitsubishi Kasei Corp Production of granulated fertilizer
FR2664983A1 (en) * 1990-07-17 1992-01-24 Centre Tech Ind Papier DEVICE FOR THE CONTINUOUS DETECTION OF CONTRAST IMPURITIES CONTAINED IN A MOVING FLUID MATERIAL.
US5497232A (en) * 1993-10-26 1996-03-05 Fuji Paudal Co., Ltd. Apparatus and method for monitoring granular size and shape during a granulation or coating process
US5707766A (en) * 1994-09-01 1998-01-13 Fuji Electric Co., Ltd. Electrophotographic photosensitive material
CN104777080A (en) * 2015-04-10 2015-07-15 中国石油大学(北京) Online detecting device and method for granules and liquid drops in gas pipelines

Also Published As

Publication number Publication date
JPH0627694B2 (en) 1994-04-13

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