JPS6011438A - Production of ethylene glycol dialkyl ether - Google Patents
Production of ethylene glycol dialkyl etherInfo
- Publication number
- JPS6011438A JPS6011438A JP58118019A JP11801983A JPS6011438A JP S6011438 A JPS6011438 A JP S6011438A JP 58118019 A JP58118019 A JP 58118019A JP 11801983 A JP11801983 A JP 11801983A JP S6011438 A JPS6011438 A JP S6011438A
- Authority
- JP
- Japan
- Prior art keywords
- ethylene glycol
- compound
- palladium
- carbon
- black
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Substances OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 title abstract 3
- -1 ethylene glycol dialkyl ether Chemical class 0.000 title abstract 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 6
- 150000001875 compounds Chemical class 0.000 abstract 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 abstract 2
- 229910052799 carbon Inorganic materials 0.000 abstract 2
- 239000006229 carbon black Substances 0.000 abstract 2
- 239000000969 carrier Substances 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 2
- 229910052739 hydrogen Inorganic materials 0.000 abstract 2
- 239000001257 hydrogen Substances 0.000 abstract 2
- KDLHZDBZIXYQEI-UHFFFAOYSA-N palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 abstract 2
- GPNDARIEYHPYAY-UHFFFAOYSA-N Palladium(II) nitrate Chemical compound [Pd+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O GPNDARIEYHPYAY-UHFFFAOYSA-N 0.000 abstract 1
- 239000006230 acetylene black Substances 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 abstract 1
- 238000006555 catalytic reaction Methods 0.000 abstract 1
- XNWFRZJHXBZDAG-UHFFFAOYSA-N ethylene glycol monomethyl ether Chemical compound COCCO XNWFRZJHXBZDAG-UHFFFAOYSA-N 0.000 abstract 1
- 239000006232 furnace black Substances 0.000 abstract 1
- 229910052763 palladium Inorganic materials 0.000 abstract 1
- 150000002941 palladium compounds Chemical class 0.000 abstract 1
- NXJCBFBQEVOTOW-UHFFFAOYSA-L palladium(2+);dihydroxide Chemical compound O[Pd]O NXJCBFBQEVOTOW-UHFFFAOYSA-L 0.000 abstract 1
- PIBWKRNGBLPSSY-UHFFFAOYSA-L palladium(II) chloride Chemical compound Cl[Pd]Cl PIBWKRNGBLPSSY-UHFFFAOYSA-L 0.000 abstract 1
- 239000002994 raw material Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Abstract
PURPOSE: To provide the titled compound useful as various solvents, etc., easily in high yield, by the catalytic reaction of an ethylene glycol monoalkyl ether with a compound containing carbonyl group in the presence of hydrogen using a palladium catalyst containing carbon black as the carrier.
CONSTITUTION: The objective compound is obtained by reacting an ethylene glycol monoalkyl ether (e.g. ethylene glycol monomethyl ether) with a carbonyl- containing compound (e.g. acetone) in the presence of hydrogen and a catalyst obtained by supporting a palladium compound such as palladium chloride, palladium nitrate, palladium hydroxide, etc. to a carbon black carrier such as furnace black, acetylene black, thermally cracked carbon, channel carbon, etc. The alkyl group of the objective compound can be changed easily by selecting the kind of the raw material.
COPYRIGHT: (C)1985,JPO&Japio
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58118019A JPS6011438A (en) | 1983-06-29 | 1983-06-29 | Production of ethylene glycol dialkyl ether |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP58118019A JPS6011438A (en) | 1983-06-29 | 1983-06-29 | Production of ethylene glycol dialkyl ether |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPS6011438A true JPS6011438A (en) | 1985-01-21 |
Family
ID=14726046
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP58118019A Pending JPS6011438A (en) | 1983-06-29 | 1983-06-29 | Production of ethylene glycol dialkyl ether |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6011438A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH10175899A (en) * | 1996-10-17 | 1998-06-30 | Kao Corp | Production of fluorine-containing ether |
| CN102432437A (en) * | 2011-11-28 | 2012-05-02 | 南京林业大学 | Synthesis method of glycol dialkyl ether |
| WO2017054321A1 (en) * | 2015-09-30 | 2017-04-06 | 中国科学院大连化学物理研究所 | Method for directly preparing glycol dimethyl ether and co-producing ethylene glycol from ethylene glycol monomethyl ether |
-
1983
- 1983-06-29 JP JP58118019A patent/JPS6011438A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH10175899A (en) * | 1996-10-17 | 1998-06-30 | Kao Corp | Production of fluorine-containing ether |
| CN102432437A (en) * | 2011-11-28 | 2012-05-02 | 南京林业大学 | Synthesis method of glycol dialkyl ether |
| WO2017054321A1 (en) * | 2015-09-30 | 2017-04-06 | 中国科学院大连化学物理研究所 | Method for directly preparing glycol dimethyl ether and co-producing ethylene glycol from ethylene glycol monomethyl ether |
| EA036494B1 (en) * | 2015-09-30 | 2020-11-17 | Далянь Инститьют Оф Кемикал Физикс, Чайниз Академи Оф Сайэнс | Method for directly preparing glycol dimethyl ether and co-producing ethylene glycol from ethylene glycol monomethyl ether |
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