JPS5938294A - Water/glycol-base hydraulic oil - Google Patents
Water/glycol-base hydraulic oilInfo
- Publication number
- JPS5938294A JPS5938294A JP14972282A JP14972282A JPS5938294A JP S5938294 A JPS5938294 A JP S5938294A JP 14972282 A JP14972282 A JP 14972282A JP 14972282 A JP14972282 A JP 14972282A JP S5938294 A JPS5938294 A JP S5938294A
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- Prior art keywords
- hydraulic oil
- glycol
- water
- present
- value
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Abstract
Description
【発明の詳細な説明】
本発明は、水−グリコ−ル型作動油、特に廃液処理性の
高い水−グリコール型作動油に関するものである。従来
の水−グリコール型作動油はその長所ぐある水どの親和
性が極めて良いことから、廃液を処理する場合に、水に
無限大に拡散し、廃液処理が極めて困Ｈな実情にある。DETAILED DESCRIPTION OF THE INVENTION The present invention relates to a water-glycol type hydraulic oil, particularly a water-glycol type hydraulic oil with high waste liquid treatment properties. Conventional water-glycol type hydraulic fluids have the advantage of having extremely good affinity for water, and therefore, when treating waste fluids, they diffuse infinitely into the water, making waste fluid treatment extremely difficult.
本発明は、掛る問題点に鑑み、作動油自体のＣＯＤ分σ
月３０Ｄ１ｎの向」−を「１的とする。′？Ｊなわら、
従来の作動油のＣＯ［）値が４５万Ｐ Ｉ−’ Ｍへ・
１２０万ｌ） Ｆ） Ｍであっ１＝ものを４０７７ＰＰ
Ｍ以千とづる。また、伯の目的は活性汚泥処理等の生物
処理性の良１）Ｔな作動油を得ることを目的と゛りる。In view of this problem, the present invention provides a COD component σ of the hydraulic fluid itself.
The direction of the moon 30D1n is considered to be 1.'?J.
The CO[) value of conventional hydraulic fluid has decreased to 450,000 P I-'M.
1.2 million liters) F) M 1 = 4077 PP
M is a thousand words. In addition, the objective is to obtain a hydraulic fluid with good 1) T properties for biological treatment such as activated sludge treatment.
具体的には生物処理でＣＯＤ値の７０％以上を除去づる
。Specifically, biological treatment removes more than 70% of the COD value.
本発明の廃液処理性の１ぐれた水−グリコール型作動油
は、エヂレングリニ】−ル、プロピレングリコ１−ルま
たはそれらの混合物１０〜５０％、Ａレイン酸１−・２
０％、ポリオキシアルキレン誘導体１５％以下、防錆剤
、酸化防」１剤、金属イオン封鎖剤等の添加剤１０．０
％以下、残部水、どＪ、りなることを特徴とづるもので
ある。The water-glycol type hydraulic oil having excellent waste liquid treatment properties of the present invention includes 10 to 50% of ethylene glycol, propylene glycol, or a mixture thereof, A-leic acid 1-2.
0%, polyoxyalkylene derivative 15% or less, rust preventive agent, oxidation preventive agent, metal ion sequestering agent and other additives 10.0
% or less, the remaining water, and the remaining water.
本発明の水−グリ：」−ル型作動油Ｃは、作動油自体の
ＣＯＤ ｌａが４０万ＰＰＭ以下Ｃあり、生物処理によ
るＣＯＤ除去率は、７０％ｊメトである。。The water-grid type hydraulic oil C of the present invention has a COD la of 400,000 PPM or less, and a COD removal rate of 70% by biological treatment. .
ここでＣＯＯ値とは化学的酸素消費量を、またＢＯＤ値
とは生物化学的酸素消費量をいう。Here, the COO value refers to chemical oxygen consumption, and the BOD value refers to biochemical oxygen consumption.
本発明の水−グリ」−ル型作動油では、第１に流動点降
Ｆ剤あるいは粘度調整剤として使用されているグリ−」
−ル類をエチレングリコール、プロピレングリコールあ
るいはそれらの混合物に限定し、その組成割合を１０〜
５０％としている。発明者等は、グリニ１−ル類の活性
汚泥による処理性を検討した結果、１ニヂレングリコー
ル及びプロピレングリコールが他のジコーヂレングリ］
−ル、ジプロピレングリコール等に比較し、非常に良好
であることを見いだし、グリコール類をエチレングリニ
Ｉ−ルどプロピレングリコールに限定したものである。In the water-grill type hydraulic oil of the present invention, firstly, the water-grill type hydraulic oil is used as a pour point depressing agent or a viscosity modifier.
-Limit the alcohol to ethylene glycol, propylene glycol, or a mixture thereof, and set the composition ratio to 10 to 10.
It is set at 50%. As a result of examining the processability of glycols with activated sludge, the inventors found that 1-nidylene glycol and propylene glycol were superior to other dicodylene glycols.
The glycols were found to be very good compared to ethylene glycol, dipropylene glycol, etc., and the glycols were limited to ethylene glycol and propylene glycol.
又、これらグリコール類の配合量を従来のしのに比較し
て低くし、１０〜５０％とした。Furthermore, the amount of these glycols added was lower than that of conventional products, ranging from 10 to 50%.
なＪ３、グリニ１−ル類のより好ましい配合量は３５゜
０へ・５０．０％である。A more preferable blending amount of J3 and Greenyl is 35.0 to 50.0%.
第２に、油性向上剤どして使用されている脂肪酸をＡレ
イン酸に限定し、その配合量を１〜２０％としたことで
ある。１はＩｌｈ酸は活性汚泥等により比較的容易に分
解される。しかし、Ａ１ツイン酸の分解′ａ度は他の脂
肪酸より良く又、Ａレイン酸を使用ザることによりグリ
−」−ル類のｉＩ！ｌ’Ｉ！ｌ ’ｆ、ｒ泥にＪ、る分
解速度も速まることを＋ｉ９認し−（いる。Ｊ、り好ま
しいＡレイン酸ｄ配合割合は、１・〜１０％である。Second, the fatty acid used as an oiliness improver is limited to A-leic acid, and its blending amount is 1 to 20%. 1, Ilh acid is relatively easily decomposed by activated sludge and the like. However, the degree of decomposition of A1 acid is better than that of other fatty acids, and by using A1 acid, the degree of decomposition of glycols is improved. l'I! It has been recognized that the decomposition rate of J in mud is also accelerated. J, A preferred blending ratio of A-leic acid is 1-10%.
第３の特色は、増粘剤であるポリオキシアルキレン誘導
体の配合用を１５％１ス下に限ったこと（゛ある。ポリ
オキシアルキレン誘導体は、微生物による処理が極めて
困難で、配合用は少ない程廃水処理には好ましい。ポリ
オキシアルキレン誘導体としては、ポリアルキレンポリ
オールが用いられる。その配合用を少量とするため、で
しＣ少ｆｆｉ ”ｒも充分な粘度の作動油を与えるため
、分子間は大きい方が好ましく、平均分子量で１０．０
００〜２００．０００程度のものがよい。The third feature is that the amount of polyoxyalkylene derivatives used as thickeners in the formulation is limited to 15% or less. Polyalkylene polyol is used as the polyoxyalkylene derivative.In order to use a small amount of the compound, the intermolecular is preferably larger, with an average molecular weight of 10.0
A value of about 00 to 200,000 is preferable.
その他、防錆剤、酸化防止剤、金属イオン封鎖剤等の添
加剤は、１０．０％以■としている。そしＣ残部を水と
で構成している。Other additives such as rust preventives, antioxidants, and sequestering agents are kept at 10.0% or more. The remainder of C is made up of water.
防錆剤及び酸化防止剤につい−（も廃液処理の而からは
可能な限り少ないのが望ましく、本発明の作動油Ｃ（よ
１．０−・５．Ｑ％程度がにり好ましい。Regarding rust preventives and antioxidants, it is desirable to have as little as possible from the perspective of waste liquid treatment, and it is preferable that the amount of the hydraulic oil C of the present invention is about 1.0-5.Q%.
防錆剤としてはモルホリン、安息香酸、シクロヘキシル
アミン、トリエタノールアミン等が、酸化防止剤として
は、ベンゾ１〜リアゾール、メルカプトヘンシイミダゾ
ール、メルカプトベンゾチアゾール等が金属イオン封鎖
剤としては、［Ｄ−１−Δ、Ｄ Ｔ Ｐ Ａ 、グル１
２Ｍツートリウム等のキレ−（〜止剤が、１日調整剤と
してｔよ苛性カリ、苛性′ソーダ等が従来と同様に使用
される。Rust inhibitors include morpholine, benzoic acid, cyclohexylamine, triethanolamine, etc. Antioxidants include benzo-1-lyazole, mercaptohencyimidazole, mercaptobenzothiazole, etc. Sequestering agents include [D-1 −Δ, D T P A , Glu 1
A deterrent agent such as 2M tutorium is used, and caustic potash, caustic soda, etc. are used as day-adjusting agents in the same manner as in the past.
本発明の水−グリコール型作動油は、作動油としての粘
度、粘度指数、Ｐ Ｈ、泡だち度、腐蝕性、錆止め性等
については、従来の水グリコール型作動油どはば同等の
性能を示す。そして、廃液処理性を７ｊＳ１ＣＯＤ値は
、７ＩＯノｊＰＰＭ以−トであり、従来の水−グリコー
ル型作動油に比較して、２０〜５０％ＣＯＤ値が小さい
。又、生物処理ｉこよるＣｏｔ）除去率が８０％程度に
なり、従来一般の作動油のＣＯＤ除去率が３０〜４０％
程度であることから考え、生物処理によるＣＯＤ除去率
が６０％程度向上している。The water-glycol type hydraulic oil of the present invention has performance equivalent to that of conventional water-glycol type hydraulic oil in terms of viscosity, viscosity index, PH, foaminess, corrosion resistance, rust prevention properties, etc. shows. The waste liquid treatment property has a 7jS1 COD value of 7IO notes or more, which is 20 to 50% smaller than that of conventional water-glycol type hydraulic fluids. In addition, the COD removal rate due to biological treatment is about 80%, and the COD removal rate of conventional general hydraulic oil is 30 to 40%.
Considering this, the COD removal rate by biological treatment is improved by about 60%.
本発明の水−グリコール型作動油を使用りるど、一般の
活性汚泥処理装首に通７：（の凝集、処理装置を追加づ
るだけで、１−分にＣＯＤ値の低減が可能である。従っ
て、規制の厳しいＴ場にａ３いても、１−分に廃液処理
が可能どなる。又、エチレングリニー１−ル、プ（−１
ピレングリ二１−ル、Ａレイン酸を）重用し、モルホリ
ン、ベンゾｌ−リアゾールの吊を必要最小限にし／ｊた
めに、ｍ性が軽減され、安全衛生面が向上している。By using the water-glycol type hydraulic oil of the present invention, it is possible to reduce the COD value in 1 minute by simply adding a coagulation and treatment device to a general activated sludge treatment head. Therefore, even if you are in a T field with strict regulations, it is possible to treat waste liquid in 1 minute.
By making heavy use of pyrene glycol and A-leic acid and minimizing the amount of morpholine and benzo-l-lyazole, the chemical properties are reduced and safety and hygiene are improved.
以下、実施例にＪ、り説明ηる。The following is a detailed explanation of the examples.
第１表のＡ、Ｂに示プ゛、２種類の本発明の水−グリコ
−ル型作動油を調整した。尚、参考までに、従来の水−
グリ」−ル型作動油Ｃ１（〕、〔ｑ）３種類についての
組成を合けて第１表（Ｊ承り。ここｒは、水の配合量を
４０％に統一した、。Two types of water-glycol type hydraulic fluids of the present invention were prepared as shown in A and B of Table 1. For reference, conventional water
The compositions of the three types of grille type hydraulic oils C1 (], [q) are combined in Table 1 (according to J. Here, the water content is unified to 40%.
本１’ｌ明のＡの作動油にａ３いては、プロピレングリ
ココールを／１．０％、ポリオキシアルキレン誘導体を
１２，５％としている。又、脂肪酸としてはＡレイン酸
５％を用いている。本発明品の１３の作動第１表
油においては、Ｉヂレングリコール２０％、プロピレン
グリニ］−ル２０％とし、グリ」−ル類を４０％どして
いる。従来の作動油Ｃ及びＤについては、グリコールと
して、ジエチレングリ」−ル及びジプロピレングリコー
ルが用いられている。又、従来の作動油であるＤはグリ
コールとしで、エチレングリコールおよびプロピレング
リコ１−ルが使用され−Ｃいるがその総Ｈ）は３０％Ｃ
ある。本発明の作動油に４３いては、ポリオ−１ジノノ
ルキレン誘導体が１２．５％であるのに対し、従来のも
の１，１２７％’１５％及び２２％Ｃある。又、本発明
の作動油においては、モルホリン、安息香酸等の防錆剤
が１％であるのに対し、従来品では２．／Ｉ−・２゜６
％添加されている。又、ベンゾ１〜リアソールは本発明
の作動油においては０．２％であるが、従来の作動油に
Ｊ３いでは０．３〜０．／Ｉ％添加されている。Ｆ Ｄ
ＴΔイの他の添加剤に′）いＣ６木発明の場合は、０
．１％従来のしのは０．２％程度添加されている。A3 of the hydraulic oil A in this book contains 1.0% propylene glycocol and 12.5% polyoxyalkylene derivative. In addition, 5% A-leic acid was used as the fatty acid. In the No. 1 working oil of the product of the present invention, 20% I-dylene glycol, 20% propylene glycol, and 40% glycol. For conventional hydraulic fluids C and D, diethylene glycol and dipropylene glycol are used as glycols. In addition, D, which is a conventional hydraulic oil, is a glycol, and ethylene glycol and propylene glycol are used.The total H) is 30%C.
be. In the hydraulic oil of the present invention, the polyo-1 dinonorkylene derivative has a C content of 12.5%, whereas the conventional oil has a C content of 1,127%, 15% and 22%. In addition, in the hydraulic oil of the present invention, the amount of rust preventive agents such as morpholine and benzoic acid is 1%, whereas in the conventional product it is 2. /I-・2゜6
% added. Furthermore, the amount of benzo 1 to rear sole is 0.2% in the hydraulic fluid of the present invention, but it is 0.3 to 0.0% in the conventional hydraulic fluid J3. /I% is added. FD
In the case of C6 wood invention with other additives of TΔi, 0
．． About 0.2% of Shino is added compared to 1% of conventional Shino.
次にこれらの作動油についての性状を第２表に示づ。第
２表にＪ３いては、比重、色、粘度、粘度指数、予備ア
ルカリ劇、水分、（〕１１１１１Ｊ、泡だち度、銅板＋
１ｉ！蝕性、錆止め性、ＢＯＤ値、ＣＯ［〕値を測定し
た。尚、［３ＯＤ値は生物化学的酸素消費量を示し、活
性汚′ｄピ等の生物処理により、処理できる割合を示づ
ものでＢＯＤ値が高い稈生物処理性が容易であることを
示している。尚、備考にそれぞ第２表
れの項目についての試験方法を記載する。Next, the properties of these hydraulic fluids are shown in Table 2. Table 2 shows J3's specific gravity, color, viscosity, viscosity index, preliminary alkali content, water content, (11111J, degree of foaming, copper plate +
1i! The corrosion resistance, rust prevention property, BOD value, and CO[] value were measured. In addition, [3OD value indicates the biochemical oxygen consumption amount and indicates the rate at which it can be treated by biological treatment such as activated pollutants, and culms with a high BOD value indicate that biological treatment is easy. There is. In addition, the test method for each item in the second table is described in the notes.
第２表にり明らかなように、本発明の作動油で６５るΔ
及びＢは従来の作動油で′ある０、１〕、［ど比較し、
作動油としての一般項［」Ｃある比（口、色、粘度、粘
度指数、予備アルカリ度、水分、Ｐｌ−１、泡たち度、
銅板腐蝕性、錆止め性ははどんと同一である。それに対
しく−１［３０１）値は、従来のものが３５万８壬、２
乃１千、３９力乏３壬であるの（Ｊ対して、本発明の伯
動油では５６ ｒＪ’ ６丁、５Ｆ）万７壬と５０カ以
上となり非常に高い値を示している。−：＋’ｊ、ＣＯ
Ｄ値は、従来のものが５９ノ）、７２万、４６万どいず
れも／ＩＯ万Ｊ５ス」−て・あるの【ご対し、本発明の
ものは３ε３７ｊ、３９カと／Ｉ Ｏ７Ｊ以下どなって
いる。このように、本発明の作動油（ＪＣＯＤ値が／Ｉ
Ｏ万以下と少なく、かつ生物処理性を示ｉＪ’ ［’３
ＯＤ値カ５０ 万以上となり、Ｃ０１） Ｉｉｉ’ｆ
ト１３０Ｄ値が逆転し、廃液処Ｊ１！性が向上してい
る。尚、廃液処理層の検討どしては０．５％の作動油を
含む廃液を供試液どし、活性汚泥に投入し、Ｍ ｌ−Ｓ
Ｓ（Ｍｉｘｅｄ Ｌｉｑｕｏｒ ５ｕｓｐｃｎｄｅ
ｔｌ ５ｏｌｉｃｌ）を２７００１１１１ｍに調整して
、活性汚泥処Ｊ１１１試験をｆｉつた。なお図に活性汚
泥処理試験時の００１）曲線を示Ｊ０第１図にり本発明
の作動油であるΔ、１３は処理部間４８時間後にほぼ５
０％が分解され、さらにその後においても、徐々に分解
が進み、経過時間１２０時間後には、約７５％が分解さ
れているのが分る。従来品のＥのものも比較的活ｆ１汚
泥ににる分解がづぐれているが、１２０時間後において
も、約５５％程度の分解率になってｄ３す、本発明のへ
、Ｂに比べ生物処理性は良くない。尚、従来のＣ，［）
の作動油については、活性汚泥にＪζりほどんど分解せ
ず処理が困難である。As is clear from Table 2, the hydraulic oil of the present invention has a Δ of 65
and B are conventional hydraulic oils'0, 1], [compared with
General terms for hydraulic oil [C] Certain ratios (mouth, color, viscosity, viscosity index, reserve alkalinity, moisture, Pl-1, degree of foaming,
Copper plate corrosion resistance and rust prevention properties are the same as Hadon. On the other hand, the -1 [301) value of the conventional one is 358,000 yen and 2
It is 1,000, 39, 3 jin (compared to J, 56 rJ' 6, 5F for the Hakudo oil of the present invention), which is over 50, 7,000, which is a very high value. -:+'j, CO
The D value of the conventional one is 59, 720,000, and 460,000, all of which are /IO,000,000 J5. It has become. In this way, the hydraulic oil of the present invention (JCOD value /I
iJ'['3
OD value is over 500,000, C01) Iiii'f
The 130D value is reversed, and the waste liquid treatment J1! sex is improving. In addition, when examining the waste liquid treatment layer, the waste liquid containing 0.5% hydraulic oil was drained as a test liquid, and then poured into activated sludge.
S(Mixed Liquor 5uspcnde
The activated sludge treatment J111 test was completed by adjusting the tl 5 olicl) to 27001111 m. In addition, the figure shows the 001) curve during the activated sludge treatment test.As shown in J0 figure 1, the hydraulic oil of the present invention, Δ, 13, has a value of approximately 5 after 48 hours between the treatment sections.
It can be seen that 0% was decomposed, and even after that, the decomposition progressed gradually, and after 120 hours, about 75% had been decomposed. The conventional product E also has relatively good decomposition into active f1 sludge, but even after 120 hours, the decomposition rate is about 55%, which is d3 compared to the present invention. Biological treatment properties are not good. In addition, the conventional C, [)
Hydraulic oil hardly decomposes into activated sludge and is difficult to treat.
図は実施例でなされた本発明の２種類の作動油と従来の
作動油についての活性汚泥処理試験における時間どＣＯ
Ｄの関係を示す線図である。符号Δ、Ｂは本発明の作動
油をＣ１１〕、［三は従来の作動油をそれぞれ承り。
経３１ｈ時）関 （Ｈｒ）The figure shows CO over time in an activated sludge treatment test for two types of hydraulic oil of the present invention and a conventional hydraulic oil.
It is a diagram showing the relationship between D. Symbols Δ and B represent the hydraulic fluid of the present invention; C11] and [3] represent the conventional hydraulic fluid, respectively. 31 hours) Seki (Hr)
Claims (1)
はそれらの混合物１０〜５０％、Δレイン酸１〜２０％
、 ポリオキシアルキレン誘導体１５％以下、防錆剤、酸化
防止剤、金属イオン封鎖剤等の添加剤１０．０％以下、 残部水、 とよりなる廃液処理ｆ１のずぐれた水−グリ」−ル型作
動油。 （２）添加剤を構成覆る防錆剤、および酸化防止剤は０
．１〜５．０％である特許請求の範囲第１項記載の作動
油。[Claims] <1>■ Dilene glycol, propylene glycol or a mixture thereof 10-50%, Δleic acid 1-20%
, 15% or less of polyoxyalkylene derivatives, 10.0% or less of additives such as rust preventives, antioxidants, sequestering agents, etc., and the remainder water. mold hydraulic oil. (2) Rust inhibitors and antioxidants that make up the additives are 0
．． The hydraulic oil according to claim 1, which has a content of 1 to 5.0%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP14972282A JPS5938294A (en) | 1982-08-27 | 1982-08-27 | Water/glycol-base hydraulic oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP14972282A JPS5938294A (en) | 1982-08-27 | 1982-08-27 | Water/glycol-base hydraulic oil |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS5938294A true JPS5938294A (en) | 1984-03-02 |
| JPS6121598B2 JPS6121598B2 (en) | 1986-05-28 |
Family
ID=15481381
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP14972282A Granted JPS5938294A (en) | 1982-08-27 | 1982-08-27 | Water/glycol-base hydraulic oil |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS5938294A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006265345A (en) * | 2005-03-23 | 2006-10-05 | Sanyo Chem Ind Ltd | Lubricating oil for ship propulsor bearing |
| JP2007039570A (en) * | 2005-08-03 | 2007-02-15 | Cosmo Sekiyu Lubricants Kk | Water-containing lubricating oil composition and property stabilizer used in the same |
| JP2007039569A (en) * | 2005-08-03 | 2007-02-15 | Cosmo Sekiyu Lubricants Kk | Water-containing lubricating oil composition and property stabilizer used in the same |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS54129256A (en) * | 1978-03-28 | 1979-10-06 | Sanyo Chemical Ind Ltd | Waterrglycol affiliated incombustible working fluid |
-
1982
- 1982-08-27 JP JP14972282A patent/JPS5938294A/en active Granted
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS54129256A (en) * | 1978-03-28 | 1979-10-06 | Sanyo Chemical Ind Ltd | Waterrglycol affiliated incombustible working fluid |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006265345A (en) * | 2005-03-23 | 2006-10-05 | Sanyo Chem Ind Ltd | Lubricating oil for ship propulsor bearing |
| JP2007039570A (en) * | 2005-08-03 | 2007-02-15 | Cosmo Sekiyu Lubricants Kk | Water-containing lubricating oil composition and property stabilizer used in the same |
| JP2007039569A (en) * | 2005-08-03 | 2007-02-15 | Cosmo Sekiyu Lubricants Kk | Water-containing lubricating oil composition and property stabilizer used in the same |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS6121598B2 (en) | 1986-05-28 |
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