JPS59169515A - Suction filter apparatus - Google Patents

Suction filter apparatus

Info

Publication number
JPS59169515A
JPS59169515A JP58043095A JP4309583A JPS59169515A JP S59169515 A JPS59169515 A JP S59169515A JP 58043095 A JP58043095 A JP 58043095A JP 4309583 A JP4309583 A JP 4309583A JP S59169515 A JPS59169515 A JP S59169515A
Authority
JP
Japan
Prior art keywords
filter
filter holder
sample
suction
specimen
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP58043095A
Other languages
Japanese (ja)
Inventor
Masaaki Yamamoto
雅秋 山本
Masao Kohama
政夫 小浜
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Toshiba Corp
Original Assignee
Toshiba Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Toshiba Corp filed Critical Toshiba Corp
Priority to JP58043095A priority Critical patent/JPS59169515A/en
Publication of JPS59169515A publication Critical patent/JPS59169515A/en
Pending legal-status Critical Current

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  • Filtration Of Liquid (AREA)

Abstract

PURPOSE:To provide the titled apparatus easy to handle and capable of certainly performing suction filtering in good efficiency, characterized in that the contact part of the specimen sucking opening part of a vacuum bin and a filter holder is constituted of an elastomer having an upwardly opened shape and high in close adhesiveness. CONSTITUTION:In a suction filter apparatus constituted of a filter holder 2 engaged with a filter fixing tool 2c converted to a liquid receiving part 2f for introducing a specimen 5 by screw parts 2d, 2e and fixing a filter 4 through a washer 2b and a vacuum bin 1 provided with an exhaust opening part 1b, the contact part 1c of the specimen sucking opening part 1a of the above mentioned vacuum bin 1 and the bottom part 2a of the filter body 2 is formed into an upwardly opened shape and at least one of them is formed of an elastomer while both of them are inlaid to each other so as to interpose an O-ring therebetween. By the above mentioned structure, a suction filter apparatus is made easily handleable even in a place to which manual working can not be directly applied.

Description

【発明の詳細な説明】 〔発明の属する技術分野〕・ この発明は吸引濾過装置に関する、 〔従来技術とその問題点〕 試料の濾過を行なう際に、特に微粒子のF多りには通常
孔径の小さい膜フィルタが使用される。しかし膜フィル
タを用いて液体試料の濾過を行なう場合には一般的には
濾過速度を大きくするため減圧−過又は加圧濾過の方法
が用いられる。このうちの減圧濾過はフィルタをフィル
タホルダにより固定し、さらにフィルタホルダを減圧び
ん上に載置して、減圧びん中を排気しながらフィルタ上
に試料を流し、p液を減圧びん中に捕集する方法である
。このとき減圧びんの試料吸引用開口部と、載置された
フィルタホルダの接触部から、減圧びん中に空気が流入
すると、排気による減圧効果が低下し、従りて吸引−過
率も、低下する。このため7′イルタホルダと減圧びん
の試料我社用開口部との密着性を大きくすることが必要
であり、従来、試料吸引用開口部とフィルタホルダとの
接触部にネジ又はフランジを設け、0リング等の封止用
弾性体をはさんでネジ締めや固定器具により固定する方
法、試料吸引用開口部をゴムによ゛って形成し、フィル
タホルダの下部を管状として前記のゴム中に差し込む方
法、及び試料吸引用開口部とフィルタホルダの接触部を
すり合わせガラスによって構成する方法が用いられてき
た。
[Detailed description of the invention] [Technical field to which the invention pertains] - This invention relates to a suction filtration device. [Prior art and its problems] When filtering a sample, the pore diameter is usually A small membrane filter is used. However, when a liquid sample is filtered using a membrane filter, vacuum filtration or pressure filtration is generally used to increase the filtration rate. Among these methods, vacuum filtration involves fixing the filter with a filter holder, placing the filter holder on a vacuum bottle, pouring the sample onto the filter while evacuating the vacuum bottle, and collecting the p liquid in the vacuum bottle. This is the way to do it. At this time, if air flows into the vacuum bottle from the contact area between the sample suction opening of the vacuum bottle and the filter holder placed on it, the depressurization effect due to exhaust will decrease, and the suction-pass rate will also decrease. do. For this reason, it is necessary to increase the adhesion between the 7' filter holder and the sample opening of the vacuum bottle. A method of sandwiching a sealing elastic body such as a ring and fixing it with screws or a fixing device.The sample suction opening is made of rubber, and the lower part of the filter holder is shaped like a tube and inserted into the rubber. A method in which the contact portion between the sample suction opening and the filter holder is made of ground glass has been used.

ところが、操作を直接手作業によって行なうことが困難
な場所、例えば試料が放射能を有するため遮蔽体内に入
れマニピュレータを介して取り扱う場合には、複雑な操
作を行なえないだめ従来の構造では取扱いが困難であっ
たり、破損の恐れがある等の問題があった。
However, in places where it is difficult to perform operations directly by hand, for example, when the sample is radioactive and must be placed inside a shield and handled using a manipulator, it is difficult to handle it using the conventional structure without performing complicated operations. There were problems such as damage or damage.

〔発明の目的〕[Purpose of the invention]

この発明は上述した従来装置の欠点を改良したもので、
直接手作業のできない場所でも容易に取扱い得る吸引濾
過装置を提供することを目的とする。
This invention improves the drawbacks of the conventional device mentioned above.
To provide a suction filtration device that can be easily handled even in places where direct manual operation is not possible.

〔発明の概要〕[Summary of the invention]

本発明は減圧びんの試料吸引用開口部と、フィルタホル
ダとの接触部の少くとも一方を弾性体によって構成し密
着性を高めるとともに、接触部の試料吸引用開口部形状
を上に開いた形状とすることによって、フィルタホルダ
自重または上方から加えた荷重の試料吸引用開口部壁に
かかる分力を増加させた吸引濾過装置である。
In the present invention, at least one of the sample suction opening of the vacuum bottle and the contact portion with the filter holder is made of an elastic material to improve adhesion, and the sample suction opening of the contact portion has a shape that opens upward. This is a suction filtration device in which the component force applied to the sample suction opening wall of the filter holder's own weight or the load applied from above is increased.

〔発明の効果〕〔Effect of the invention〕

本発明によれば、フィルタホルダとの密着効果が大きく
なり、フィルタホルダ荷重が小さい場合でも固定器具を
用いずに効率のよい吸引濾過を行なうことが可能となる
。さらに試料吸引用開口部が上方に開いた構造であるた
めフィルタホルダを載置する際にガイドとなり、所定の
位置に載置することを容易に行ないうる。
According to the present invention, the effect of close contact with the filter holder is increased, and even when the filter holder load is small, efficient suction filtration can be performed without using a fixing device. Further, since the opening for sample suction is opened upward, it serves as a guide when placing the filter holder, and it is possible to easily place the filter holder in a predetermined position.

捷た、フィルタホルダの底面の一部を球面とし、これと
接触する試料吸引用開口部の水平断面形状を円形とすれ
ば、フィルタホルダの載置状態が傾いていても両者の密
着性は確実に保持され一層取扱いが容易となる。
By making part of the bottom of the folded filter holder spherical and making the horizontal cross-sectional shape of the sample suction opening that comes into contact with it circular, the adhesion between the two can be ensured even if the filter holder is placed at an angle. This makes handling easier.

〔発明の実施例〕[Embodiments of the invention]

以下、本発明の実施例を図面に基づいて説明する。 Embodiments of the present invention will be described below based on the drawings.

第1図は本発明による吸引濾過装置の断面図である。減
圧びん1は試料吸引用開口部1aおよび排気用開口部1
bとを有し、試料吸引用開口部1aの上端部直径Aは少
くともフィルタホルダ2の底部直径Bよシも大きい構造
を有する。フィルタホルダ2を載置した状態では、フィ
ルタホルダ2と試料吸引用開口部1aとの接触部1cが
弾性体で構成され、かつ接触部1cにおける試料吸引用
開口部1aの形状が上に開いた形状であることが必要で
ある。−例として試料吸引用開口部1aを円錐状とし、
フィルタホルダ2の底部直径Bと上部直径Cとの中間の
水平断面ぽ径となる試料吸引用開口部1a壁面に0リン
グ3を設置することによって達成される。
FIG. 1 is a sectional view of a suction filtration device according to the present invention. The vacuum bottle 1 has a sample suction opening 1a and an exhaust opening 1.
b, and the upper end diameter A of the sample suction opening 1a is larger than the bottom diameter B of the filter holder 2. When the filter holder 2 is placed, the contact portion 1c between the filter holder 2 and the sample suction opening 1a is made of an elastic body, and the shape of the sample suction opening 1a in the contact portion 1c is open upward. It is necessary that the shape is the same. - As an example, the sample suction opening 1a is conical,
This is achieved by installing the O-ring 3 on the wall surface of the sample suction opening 1a, which has a horizontal cross-sectional diameter midway between the bottom diameter B and the top diameter C of the filter holder 2.

フィルタホルダ2は、フィルタ4を固定し、フィルタ4
を通らずに試料5が漏洩することのない構造であればよ
く、例えばフィルタ支持体2a上にフィルタ4を置きフ
ィルタ圧着用のワッシャ2bを介して液受は用壁面をか
ねたフィルタ固定器具2cによって押さえる構造とする
ことによって達成される。フィルタ固定器具はその外周
部にねじ部2dを有し、フィルタ支持体2aの内周のネ
ジ部2eとの嵌合によって固定することが可能である。
The filter holder 2 fixes the filter 4 and
Any structure is sufficient as long as the sample 5 does not leak through the filter, for example, the filter 4 is placed on the filter support 2a, and the filter fixing device 2c, which also serves as a wall surface, is used to hold the liquid through a washer 2b for pressing the filter. This is achieved by creating a structure that holds the area in place. The filter fixing device has a threaded portion 2d on its outer periphery, and can be fixed by fitting with a threaded portion 2e on the inner periphery of the filter support 2a.

かかる状態でフィルタホルダ2の液受は部2fに試料5
を入れ、排気用開口部1bに図示していない外部の排気
装置をつないで減圧びん1の内部を排気減圧すれば、フ
ィルタホルダ2の自重と減圧びん内外の差圧によって接
触部1Cが封止され、吸引濾過を行なうことが可能とな
る。
In this state, the liquid receiver of the filter holder 2 has the sample 5 in the part 2f.
If the inside of the vacuum bottle 1 is evacuated and depressurized by connecting an external exhaust device (not shown) to the exhaust opening 1b, the contact portion 1C will be sealed by the weight of the filter holder 2 and the differential pressure between the inside and outside of the vacuum bottle. This makes it possible to carry out suction filtration.

〔発明の他の実施例〕[Other embodiments of the invention]

また、第2図に示すようにフィルタホルダ2の底部2a
を球面とし、試料吸引用開口部1aが接触部ICにおい
て円形の水平断面形状をもつ構造とすれば、フィルタホ
ルダ2が傾いて載置されても充分な密着効果が得られ一
層好適である。
In addition, as shown in FIG. 2, the bottom 2a of the filter holder 2
It is more preferable to have a structure in which the sample suction opening 1a has a circular horizontal cross-sectional shape at the contact part IC, since a sufficient adhesion effect can be obtained even if the filter holder 2 is placed at an angle.

なお、吸引びん1、フィルタホルダ2とも、充分な耐圧
性と試料に対する耐性をもつものであれば何で構成して
も良いが、例えば耐薬品性の高いフッ素樹脂により構成
することができる。
Note that the suction bottle 1 and the filter holder 2 may be made of any material as long as it has sufficient pressure resistance and resistance against samples; for example, they may be made of a fluororesin having high chemical resistance.

【図面の簡単な説明】[Brief explanation of drawings]

第1図は吸引r過装置の縦断面図、第2図はフィルタホ
ルダの実施例を示す縦世1面図である。 1・・・減圧びん、la・・・試料吸引用開口部、1b
・・・排気用開口部、lc・・・接触部、2・・・フィ
ルタホルダ、2a・・・底!、2b・・・ワッシャ、2
C・・・フィルタ固定器具、2d・・・ねじ部、2e・
・・ねじ部、2f・・・液受は部、3・・・01ノング
、4・・・フィルタ、5・・・試料。 第  1 図 第2図
FIG. 1 is a longitudinal cross-sectional view of the suction rover device, and FIG. 2 is a vertical front view showing an embodiment of the filter holder. 1... Vacuum bottle, la... Opening for sample suction, 1b
...exhaust opening, lc...contact part, 2...filter holder, 2a...bottom! , 2b... washer, 2
C... Filter fixing device, 2d... Threaded part, 2e.
...Thread part, 2f...Liquid receiver part, 3...01 tongue, 4...filter, 5...sample. Figure 1 Figure 2

Claims (2)

【特許請求の範囲】[Claims] (1)フィルタと、前記フィルタを保持し減圧びん上に
載置されるフィルタホルダと、フィルタを通して試料を
吸引する減圧びんとからなる吸引濾過装置において、前
記減圧びんの試料吸引用開口部上に前記フィルタホルタ
を載置した状態で接触する部分の少くとも一方を弾性体
によって形成し、かつ前記試料吸引用開口部およびフィ
ルタホルダがその接触部において上方に開いた斜面とな
る構造を有することを特徴とした吸引濾過装置。
(1) In a suction filtration device consisting of a filter, a filter holder that holds the filter and is placed on a vacuum bottle, and a vacuum bottle that sucks a sample through the filter, At least one of the parts that come in contact with the filter holder when placed thereon is formed of an elastic body, and the sample suction opening and the filter holder have a structure in which the contact part forms an upwardly open slope. Featured suction filtration device.
(2)フィルタホルダの底部形状を球面としたことを特
徴とする特許請求の範囲第−項記載の吸引濾過装置。
(2) The suction filtration device according to claim 1, wherein the bottom shape of the filter holder is spherical.
JP58043095A 1983-03-17 1983-03-17 Suction filter apparatus Pending JPS59169515A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP58043095A JPS59169515A (en) 1983-03-17 1983-03-17 Suction filter apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP58043095A JPS59169515A (en) 1983-03-17 1983-03-17 Suction filter apparatus

Publications (1)

Publication Number Publication Date
JPS59169515A true JPS59169515A (en) 1984-09-25

Family

ID=12654271

Family Applications (1)

Application Number Title Priority Date Filing Date
JP58043095A Pending JPS59169515A (en) 1983-03-17 1983-03-17 Suction filter apparatus

Country Status (1)

Country Link
JP (1) JPS59169515A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63205110A (en) * 1987-02-21 1988-08-24 Toyo Roshi Kk Automatic filtration sampling device of liquid samples
KR100360172B1 (en) * 2000-08-24 2002-11-11 박헌양 Filtering apparatus

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS63205110A (en) * 1987-02-21 1988-08-24 Toyo Roshi Kk Automatic filtration sampling device of liquid samples
KR100360172B1 (en) * 2000-08-24 2002-11-11 박헌양 Filtering apparatus

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