JPS5843262A - Atomizing method for liquid to uniform size and device for embodiment thereof - Google Patents
Atomizing method for liquid to uniform size and device for embodiment thereofInfo
- Publication number
- JPS5843262A JPS5843262A JP14109381A JP14109381A JPS5843262A JP S5843262 A JPS5843262 A JP S5843262A JP 14109381 A JP14109381 A JP 14109381A JP 14109381 A JP14109381 A JP 14109381A JP S5843262 A JPS5843262 A JP S5843262A
- Authority
- JP
- Japan
- Prior art keywords
- liquid
- groups
- uniform
- large number
- micro
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000007788 liquid Substances 0.000 title claims abstract description 37
- 238000000034 method Methods 0.000 title claims abstract description 17
- 238000010894 electron beam technology Methods 0.000 claims abstract description 3
- 239000002245 particle Substances 0.000 claims description 7
- 239000007787 solid Substances 0.000 claims description 4
- 238000001694 spray drying Methods 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 2
- 238000003672 processing method Methods 0.000 claims 2
- 229910001220 stainless steel Inorganic materials 0.000 abstract description 4
- 239000010935 stainless steel Substances 0.000 abstract description 4
- 238000003466 welding Methods 0.000 abstract description 2
- 230000010355 oscillation Effects 0.000 abstract 2
- 238000004080 punching Methods 0.000 abstract 1
- 238000005516 engineering process Methods 0.000 description 8
- 238000000889 atomisation Methods 0.000 description 5
- 239000012530 fluid Substances 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 238000009688 liquid atomisation Methods 0.000 description 1
- 238000003754 machining Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000005459 micromachining Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05B—SPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
- B05B17/00—Apparatus for spraying or atomising liquids or other fluent materials, not covered by the preceding groups
- B05B17/04—Apparatus for spraying or atomising liquids or other fluent materials, not covered by the preceding groups operating with special methods
- B05B17/06—Apparatus for spraying or atomising liquids or other fluent materials, not covered by the preceding groups operating with special methods using ultrasonic or other kinds of vibrations
- B05B17/0607—Apparatus for spraying or atomising liquids or other fluent materials, not covered by the preceding groups operating with special methods using ultrasonic or other kinds of vibrations generated by electrical means, e.g. piezoelectric transducers
- B05B17/0615—Apparatus for spraying or atomising liquids or other fluent materials, not covered by the preceding groups operating with special methods using ultrasonic or other kinds of vibrations generated by electrical means, e.g. piezoelectric transducers spray being produced at the free surface of the liquid or other fluent material in a container and subjected to the vibrations
Landscapes
- Special Spraying Apparatus (AREA)
- Glanulating (AREA)
Abstract
Description
【発明の詳細な説明】
本発明は、レーザ加工技術、電子ビーム加工技術を利用
して、構造体に均一径微小孔群をせん孔し、該せん孔群
に加圧した液体を供給し、該せん孔群よシ、均一微小径
の液柱群を発生させ、との液柱群に超音波高周波振動を
印加し、均一径の微小液滴群を発生させる方法及び装置
。さらに、該微粒化方法をガス雰囲気中及び液体中にお
いて使用し、また、溶媒を含む溶液を噴霧乾燥させるこ
とによる均一径固体粒子群の発生に関するものである。DETAILED DESCRIPTION OF THE INVENTION The present invention utilizes laser processing technology and electron beam processing technology to drill a group of uniform diameter micro holes in a structure, and supplies a pressurized liquid to the drilled holes. A method and apparatus for generating a group of liquid columns with a uniform minute diameter, applying ultrasonic high-frequency vibration to the group of liquid columns, and generating a group of minute droplets with a uniform diameter. It further relates to the use of the atomization method in a gas atmosphere and in a liquid, and to the generation of uniformly sized solid particles by spray drying a solution containing a solvent.
さて、液体の微粒化方法を工業的ニーズの観点から検討
するならば、均−従機粒子群の多量製造は、噴霧装置の
気化効率、液体燃料バーナーの燃焼効率の向上及びそれ
に伴う装置の小型化、あるいは、異種液体中における均
一径微粒化、噴霧乾燥による均一固体粒子群の発生等の
製品の均質化及び装置の小型化等その工業的意義は多大
である。Now, if we consider liquid atomization methods from the viewpoint of industrial needs, the production of large quantities of homogeneous particles will improve the vaporization efficiency of spray equipment, the combustion efficiency of liquid fuel burners, and the associated miniaturization of equipment. It has great industrial significance, such as homogenization of products such as oxidation, atomization of uniform diameters in different liquids, generation of uniform solid particle groups by spray drying, and miniaturization of equipment.
ところで従来からの微粒化方法には、気体、液体流を利
用した二流体ノズル等種々実施されている。超音波高周
波振動を印加させる方法もその一つである。さて均−従
機小成滴群の多量発生の観点から、微粒化法を検討する
と、二流体ノズルの場合は多量発生が可能であるが、液
滴径が比較的太きく、シかも粒子径分布を有し、均一径
の液滴が得られない欠点がある。一方超音波高周波振動
印加方法は二流体法に比較して微小径粒子群が得られる
こと、印加振動を調節することにより、微粒化特性の制
御が簡単であること等の利点があるが、多量発生が困難
であるため、工業的寿多量発生には不適当で利用されな
かった。By the way, various conventional atomization methods have been implemented, such as a two-fluid nozzle using gas or liquid flow. One of the methods is to apply ultrasonic high-frequency vibrations. Now, considering the atomization method from the viewpoint of generating a large amount of small droplets evenly, it is possible to generate a large amount with a two-fluid nozzle, but the droplet size is relatively large, and the particle size may be small. There is a drawback that droplets with a uniform diameter cannot be obtained. On the other hand, the method of applying ultrasonic high-frequency vibrations has advantages over the two-fluid method, such as being able to obtain particles with minute diameters and easily controlling the atomization characteristics by adjusting the applied vibrations. Because it is difficult to generate, it is not suitable for industrial production in large quantities and has not been used.
しかし橙がら、近年レーザ加工技術、電子ビー・雫′:
、。However, in recent years, laser processing technology, electronic bee droplets:
,.
ム加工技術等の精密加工技術が進歩し、数百μmから数
μm程度の微小孔の穴あけ加工が可能となった。またレ
ーザ技術等を利用した位置制御も可能となったことによ
り、微小面積に多数個の微小孔群をぜん孔することがで
きる。Advances in precision machining technology, such as micro-machining technology, have made it possible to drill micro holes ranging from several hundred micrometers to several micrometers. Furthermore, position control using laser technology or the like has become possible, making it possible to form a large number of microhole groups in a microscopic area.
本発明は近年開発された前記のような高度々技術を利用
することにより、多数の均一径微小孔を自動的にせん孔
し、多数の均一径微小の液流柱を発生させ、この液流柱
群に対して高周波振動を印加させることにより多量の均
−従機小成滴群を発生させる方法である。The present invention utilizes the above-mentioned advanced technology developed in recent years to automatically drill a large number of uniform diameter micropores, generate a large number of uniform diameter microscopic liquid flow columns, and generate a large number of uniform diameter microscopic liquid flow columns. This is a method of generating a large amount of homogeneous small droplet groups by applying high frequency vibration to the group.
以下添付図面に従い具体例を示す。Specific examples will be shown below according to the attached drawings.
図1において1はステンレス、セラミック等の薄円板に
レーザ加工技術により微小孔を多数せん孔したものであ
る。この薄板1を液の流出口2に01Jング3又は溶接
により気密に設置する。液送入口aより少し加圧した液
を送入すると、高周波振動を印加しない場合は、薄板1
の微小孔より多数の微小径液柱となって流出する。これ
らの液柱群に対して、平打方向すあるいは垂直方向Cに
装′ζ
置4へ高周波振動容を印加すると、多量の均一径の微小
液滴群12が発生する。In FIG. 1, reference numeral 1 indicates a thin circular plate made of stainless steel, ceramic, etc., in which a large number of microscopic holes are drilled by laser processing technology. This thin plate 1 is airtightly installed at the liquid outlet 2 by 01J ring 3 or by welding. When a slightly pressurized liquid is sent from the liquid inlet a, if high frequency vibration is not applied, thin plate 1
The liquid flows out from the micropores in the form of numerous microscopic liquid columns. When a high frequency vibration volume is applied to the apparatus 4 in the flat direction or in the vertical direction C to these liquid columns, a large number of minute droplets 12 of uniform diameter are generated.
図2は、図1と同様本発明による一例であシ、図1の装
置に比較して多量の均−微小液滴群12を発生させるこ
とができるもので日商状薄板5に微小孔をせん孔したも
のでより多くの穴をせん孔できる。振動方向は軸方占適
当である。FIG. 2 shows an example of the present invention similar to FIG. 1, and is capable of generating a large number of uniform micro droplets 12 compared to the device shown in FIG. You can drill more holes with the drilled one. The direction of vibration is appropriately axial.
高周波印加装置は発振器6からの信号を増巾器7により
増巾した後、磁歪、電歪素子8に印加して、電気信号を
機械振動に変化させて、液柱群に振動を加える。一方液
体はポンプ等11によシ加圧された後、フィルター10
を経て、発生部に供給される。
。The high frequency application device amplifies the signal from the oscillator 6 using the amplifier 7, and then applies it to the magnetostrictive/electrostrictive element 8, converting the electrical signal into mechanical vibration and applying vibration to the liquid column group. On the other hand, the liquid is pressurized by a pump etc. 11, and then the filter 10
After that, it is supplied to the generating section.
.
実施例について更に説明する。厚さ0.2 mm及び0
.1mmのステンレス薄円板に約30μmの均一径の穴
をピンチ0.2mmの条件で、YAGレーザを使用して
、多数の穴をせん孔した。このステンレス製薄円板を図
1の装置に取付けた後、図3の装置を接続した。液体は
約0.5〜2気圧のゲージ圧力の範囲で、1μmのフィ
ルターを通して図1の装置に供給した。印加した超音波
は201<Hz〜70kHzで実施した。発生した均−
液滴群の大きさは約60μmであった。また発生する均
−液滴群の大きさは、アルコール等の揮発性の液体を混
合することによシ約10μmから60μm″11で変化
させることができた。さらに食塩、糖等の固体を溶媒に
溶かして噴霧後、乾燥させると均一径の固体粒子群を発
生させることができた。Examples will be further described. Thickness 0.2 mm and 0
.. A large number of holes with a uniform diameter of about 30 μm were punched in a 1 mm stainless steel thin disk using a YAG laser with a pinch of 0.2 mm. After this stainless steel thin disk was attached to the device shown in FIG. 1, the device shown in FIG. 3 was connected. Liquids were fed into the apparatus of FIG. 1 through a 1 μm filter at a gauge pressure ranging from about 0.5 to 2 atmospheres. The applied ultrasound was performed at 201<Hz to 70kHz. The generated average
The size of the droplet group was approximately 60 μm. Furthermore, the size of the homogeneous droplets generated could be changed from approximately 10 μm to 60 μm''11 by mixing volatile liquids such as alcohol. By dissolving it in a solution, spraying it, and drying it, it was possible to generate solid particles of uniform diameter.
図1、図2は微小孔をせん孔した均一液滴発生装置の主
要部分である。図3は高周波振動を印加させるだめの電
気装置及び液体供給装置である。FIGS. 1 and 2 show the main parts of a uniform droplet generator in which micropores are drilled. FIG. 3 shows an electric device and a liquid supply device for applying high frequency vibration.
Claims (5)
シ多数個の均一微小孔を、容器状構造体にせん孔し、該
微小せん孔群よシ液体を流出させ、均−a微小液柱群を
発生させると同時に、該容器状構造体の全体あるいは該
せん孔部分に高周波振動を印加させることによシ、多量
の均−従機小液滴群を発生させることを特徴とする液体
の微粒化方法0(1) A large number of uniform microholes are drilled into a container-like structure using a laser beam processing method, an electron beam processing method, etc., and the liquid is flowed out through the microholes to form a uniform micro-liquid column group. A method for atomizing liquid, characterized in that a large number of uniform small droplets are generated by simultaneously applying high-frequency vibration to the entire container-like structure or to the perforated portion. 0
の方法を使用する液体の微粒化の方法。(2) A method for atomizing a liquid using the method set forth in claim 1 in a gas atmosphere.
を使用する液体の微粒化の方法。(3) A method for atomizing a liquid in a different liquid using the method according to claim 1.
使用して噴霧乾燥させることによる、均一径固体粒子群
の発生方法。(4) A method for generating uniform-diameter solid particles by spray-drying a solution containing a solvent using the method set forth in claim 1.
。(5) An apparatus for carrying out the method set forth in claim 1.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP14109381A JPS5843262A (en) | 1981-09-09 | 1981-09-09 | Atomizing method for liquid to uniform size and device for embodiment thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP14109381A JPS5843262A (en) | 1981-09-09 | 1981-09-09 | Atomizing method for liquid to uniform size and device for embodiment thereof |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS5843262A true JPS5843262A (en) | 1983-03-12 |
Family
ID=15284026
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP14109381A Pending JPS5843262A (en) | 1981-09-09 | 1981-09-09 | Atomizing method for liquid to uniform size and device for embodiment thereof |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5843262A (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6142361A (en) * | 1984-08-07 | 1986-02-28 | P S Kankyo Giken Kk | Atomizing apparatus |
US7001981B2 (en) | 2003-04-25 | 2006-02-21 | Sun Chemical Corporation | Acrylated natural resins |
JP2009131849A (en) * | 2009-03-09 | 2009-06-18 | Optnics Precision Co Ltd | Method for manufacturing spherical hyperfine particle |
-
1981
- 1981-09-09 JP JP14109381A patent/JPS5843262A/en active Pending
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS6142361A (en) * | 1984-08-07 | 1986-02-28 | P S Kankyo Giken Kk | Atomizing apparatus |
US7001981B2 (en) | 2003-04-25 | 2006-02-21 | Sun Chemical Corporation | Acrylated natural resins |
US7411035B2 (en) | 2003-04-25 | 2008-08-12 | Sun Chemical Corporation | Acrylated natural resins |
US7411036B2 (en) | 2003-04-25 | 2008-08-12 | Sun Chemical Corporation | Acrylated natural resins |
JP2009131849A (en) * | 2009-03-09 | 2009-06-18 | Optnics Precision Co Ltd | Method for manufacturing spherical hyperfine particle |
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