JPS5812219B2 - Manufacturing method for fired lightweight building materials - Google Patents

Manufacturing method for fired lightweight building materials

Info

Publication number
JPS5812219B2
JPS5812219B2 JP55009975A JP997580A JPS5812219B2 JP S5812219 B2 JPS5812219 B2 JP S5812219B2 JP 55009975 A JP55009975 A JP 55009975A JP 997580 A JP997580 A JP 997580A JP S5812219 B2 JPS5812219 B2 JP S5812219B2
Authority
JP
Japan
Prior art keywords
manufacturing
building materials
lightweight building
temperature
fired
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP55009975A
Other languages
Japanese (ja)
Other versions
JPS56109858A (en
Inventor
黒川利一
川村資三
徳永良邦
鈴木章平
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Steel Corp
National Institute of Advanced Industrial Science and Technology AIST
Original Assignee
Agency of Industrial Science and Technology
Nippon Steel Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Agency of Industrial Science and Technology, Nippon Steel Corp filed Critical Agency of Industrial Science and Technology
Priority to JP55009975A priority Critical patent/JPS5812219B2/en
Publication of JPS56109858A publication Critical patent/JPS56109858A/en
Publication of JPS5812219B2 publication Critical patent/JPS5812219B2/en
Expired legal-status Critical Current

Links

Landscapes

  • Curing Cements, Concrete, And Artificial Stone (AREA)
  • Porous Artificial Stone Or Porous Ceramic Products (AREA)
  • Producing Shaped Articles From Materials (AREA)

Description

【発明の詳細な説明】 本発明は高炉水砕ヌラグを有効利用した耐水、耐候性に
富み、かつ軽量にして断熱効果の大きい建築用材特に軽
量質のボート、パネルなどの製造方法の改良に関するも
のである。
DETAILED DESCRIPTION OF THE INVENTION The present invention relates to an improvement in the manufacturing method of construction materials, particularly lightweight boats and panels, which are highly water-resistant, weather-resistant, lightweight, and have a large heat-insulating effect, by effectively utilizing granulated blast furnace nullag. It is.

近年、新しい工法によるプレハブ住宅の開発は目覚しい
ものがあり、これに伴い軽量で耐水、耐候性、断熱性に
すぐれ、かつ、意匠的価値の高い屋根瓦および外装材が
要求されるようになったが、そのような性質を有する材
料は未だ開発されていない。
In recent years, the development of prefabricated houses using new construction methods has been remarkable, and as a result, there has been a demand for roof tiles and exterior materials that are lightweight, have excellent water resistance, weather resistance, and heat insulation, and have high design value. However, a material with such properties has not yet been developed.

例えば、ケイ酸カルシウムの水熱合成材料あるいはセツ
コウ系建材は無機質の新建材として近年需用の伸びは著
るしいが、それぞれ耐火性、耐水性の面で弱点を有し、
したがってまた釉薬を施こすことができないなどの欠点
がある。
For example, the demand for hydrothermally synthesized calcium silicate materials or setzukou-based building materials has increased significantly in recent years as new inorganic building materials, but each has weaknesses in terms of fire resistance and water resistance.
Therefore, there are also drawbacks such as the inability to apply glaze.

これらの欠点を改良し、高炉水砕ヌラグの有効利用を計
る目的で高炉水砕ヌラグにケイ酸に富む廃砂などの未利
用資源を配合し、Si02.CaOを夫々60〜90重
量係、4〜25重量係含む混合物に調整し、さらに必要
に応じバインダー(水ガラヌ)或は適当な発泡助剤を加
えたものを冷間(常温)で予備成型した後、900〜1
200℃の温度で加熱し、この加熱物を800〜110
0℃の温度に保持し乍ら圧縮成形し、さらにこの圧縮成
形物を700〜600℃の温度で施釉し、ついで800
℃〜1000℃前後で釉焼して釉瓦を製造する方法があ
る。
In order to improve these drawbacks and effectively utilize the granulated blast furnace nlug, unused resources such as waste sand rich in silicic acid are blended with the granulated blast furnace nlug, and Si02. Mixtures containing CaO of 60 to 90% by weight and 4 to 25% by weight were prepared, and if necessary, a binder (water guaranu) or a suitable foaming aid was added, and the mixtures were preformed in the cold (room temperature). After, 900-1
Heating at a temperature of 200℃, the heated material is heated to a temperature of 800 to 110℃.
Compression molding is performed while maintaining the temperature at 0°C, and the compression molded product is further glazed at a temperature of 700 to 600°C, and then glazed at 800°C.
There is a method of manufacturing glazed roof tiles by glazing at a temperature of about 1000°C to 1000°C.

(特開昭54−65716)この方法は在来のケイ酸カ
ルシウムの水熱合成材料或はセツコウ系建材の弱点を補
ない、かつ釉薬処理を可能とする方法ではあるが高炉水
砕ヌラグ、ケイ酸含有物などの原料粉末を一旦冷間にお
いて予備成形するという点で工程がはん雑となっている
(Japanese Unexamined Patent Publication No. 54-65716) Although this method compensates for the weaknesses of conventional calcium silicate hydrothermally synthesized materials or settsuko-based building materials, and enables glazing treatment, it is The process is complicated in that raw material powder such as acid-containing material is once preformed in the cold.

しかも800〜1100℃の圧縮成形において成形型毎
に一個一個処理するバッチタイプ方式をとるため生産性
があがらないという欠点がある。
Moreover, in compression molding at 800 to 1100 DEG C., a batch type method is used in which each mold is processed one by one, which has the drawback of not increasing productivity.

特に例えば耐火ボートのようなフラットな均一形状のも
のを製造する場合には、余り好ましい作業工程とは云え
ない。
This is not a very desirable process, especially when manufacturing flat, uniformly shaped items such as fireproof boats.

本発明はこのような不利な欠点を解消するためになされ
たもので、従来の前記製造工程を改良し、しかも冷間に
おける予備成形を省略することによって工程の簡略化を
計り、同時に生産性の向上を意図した製造方法を提供せ
んとするものである。
The present invention has been made in order to eliminate these disadvantages, and it improves the conventional manufacturing process, simplifies the process by omitting cold preforming, and at the same time improves productivity. The purpose is to provide a manufacturing method that is intended to improve the quality of the product.

すなわちその要旨は高炉水砕ヌラグにケイ酸含有物及び
発泡助剤を配合した粉末原料を型に充填し、加熱炉にお
いて900〜1200℃に加熱焼成して発泡させた後、
800〜1100℃の雰囲気温度において発泡物上面を
連続的に成形するものである。
In other words, the gist is that a powder raw material made by blending silicic acid-containing substances and foaming aids with granulated blast furnace nlug is filled into a mold, heated and fired at 900 to 1200°C in a heating furnace to foam, and then
The upper surface of the foam is continuously molded at an ambient temperature of 800 to 1100°C.

本発明は高炉水砕ヌラグ、ケイ酸含有物、その他の発泡
助剤からなる配合物を予めボールミル等で粉砕し、この
原料粉末を予め一旦予備成形することなく直に焼成用の
型に充填するものである。
The present invention involves crushing a compound consisting of granulated blast furnace nlag, a silicic acid-containing material, and other foaming aids in advance using a ball mill, etc., and directly filling this raw material powder into a baking mold without preforming it in advance. It is something.

この焼成用の焼成用の形状は、加熱炉中に延在して一定
の長さに有し、加熱炉中を連続して移動出来るものであ
る。
This firing shape extends into the heating furnace, has a certain length, and can be moved continuously through the heating furnace.

勿論加熱炉の延長長さに連続した長さの焼成用の型であ
ってもよい。
Of course, the mold for firing may have a length that is continuous with the extended length of the heating furnace.

焼成用Q型の材質としては炭化ケイ素質、コーデイユラ
イト等のセラミック、又はsus310等の耐熱鋼製で
あることが必要である。
The material of the Q-shape for firing must be silicon carbide, ceramic such as cordeurite, or heat-resistant steel such as SUS310.

このようにして焼成型内に充填した乾燥粉末原料は加熱
炉に順次装入され加熱焼成をうけ900〜1200℃の
温度で軟化融着して一体化され更に発泡し膨張する。
The dry powder raw materials filled into the baking mold in this manner are sequentially charged into a heating furnace and heated and fired, softened and fused at a temperature of 900 to 1200° C. to be unified, and further foamed and expanded.

そこでの発泡した焼成物の上面をロールによるロール掛
けし膨張部分を押しつぶし、又一部をフローさせながら
均一表面に成形する。
The upper surface of the foamed baked product is rolled with a roll to crush the expanded portion and to form a uniform surface while allowing a portion to flow.

本発明者らの実験によればロール圧下力を0.2〜3k
g/cm2にとることによって極めてち密な表面が得ら
れることが分った。
According to experiments by the present inventors, the roll rolling force is 0.2 to 3k.
It was found that a very dense surface could be obtained by adjusting the amount to 1 g/cm2.

即ち圧下力が強すぎると発泡成形物の気泡の多くが圧縮
変形して歪を内在したり、あるいは気泡が破壊されやす
い。
That is, if the rolling force is too strong, many of the cells in the foamed molded product will be compressively deformed, causing distortion or being likely to be destroyed.

一方圧下力か弱すぎると目的とする形状が得られ難い。On the other hand, if the rolling force is too weak, it will be difficult to obtain the desired shape.

かくして連続的にロール圧下を受けた発泡焼成物はその
後熱間施釉釉焼を行うか、又はそのまま冷却して次工程
の処理をうけることになる。
The foamed fired product thus continuously subjected to roll reduction is then subjected to hot glazing or glaze firing, or is directly cooled and subjected to the next process.

以上のとおり本発明は熱間工程だけで、圧延成形してい
るので、従来の例えば粘土釉瓦、パネル製造に比較し工
程が簡略化されるという効果があり、生産性も極めてよ
い。
As described above, since the present invention performs rolling forming using only a hot process, it has the effect of simplifying the process compared to the conventional manufacturing of clay glazed tiles and panels, and has extremely high productivity.

以下本発明の実施例を述べる。Examples of the present invention will be described below.

実施例 高炉水砕ヌラグ27係、微砂粉砕物55乞ガ2ラヌ廃棄
物17.8%、sico.2%の配合物をポールミルで
よく混合した後、脱水乾燥し、炭化ケイ素質製の焼成型
(1200Lx300wx35mmH)にこの粉末を充
填する。
Example Blast furnace granulated nurag 27 parts, fine sand pulverized material 55 grains 2 ranu waste 17.8%, sico. After thoroughly mixing the 2% blend in a pole mill, it is dehydrated and dried, and the powder is filled into a silicon carbide baking mold (1200L x 300w x 35mmH).

この型を図に示す加熱炉に導入し50℃温度ある加熱帯
2に順次搬入して昇温させ、1150℃温度に20分間
保持した。
This mold was introduced into the heating furnace shown in the figure, and sequentially carried into the heating zone 2 having a temperature of 50° C. to raise the temperature, and maintained at a temperature of 1150° C. for 20 minutes.

次にこの型を850℃に保温した成型室3に移しロール
4により焼成物上面を連続的に0. 5 k9/cm2
の圧下力でロール掛けした。
Next, this mold was transferred to a molding chamber 3 kept at a temperature of 850°C, and the upper surface of the fired product was continuously rolled to a temperature of 0. 5 k9/cm2
It was rolled with a rolling force of .

このようにして得た材料の性能は以下の通りであった。The performance of the material thus obtained was as follows.

カサ比重 1.3 曲げ強度 270kg/cm
2吸水率 0.3係 熱伝導率 0.25kcal/
mhrc吸音率12〜30係〔125〜4000Hz〕
この性能は内外装壁材、防音壁として十分満足するもの
であった。
Bulk specific gravity 1.3 Bending strength 270kg/cm
2 Water absorption coefficient 0.3 Thermal conductivity 0.25kcal/
mhrc sound absorption coefficient 12-30 [125-4000Hz]
This performance was fully satisfactory as an interior/exterior wall material and a soundproof wall.

【図面の簡単な説明】[Brief explanation of drawings]

図は本発明方法を実施する具体的装置の一例を示す。 1……加熱炉、2……加熱帯、3……ロール成型室、4
……ロール。
The figure shows an example of a specific apparatus for carrying out the method of the present invention. 1... Heating furnace, 2... Heating zone, 3... Roll forming chamber, 4
……roll.

Claims (1)

【特許請求の範囲】[Claims] 1 高炉水砕ヌラグにケイ酸含有物及び発泡助剤を配合
した粉末原料を型に充填し、加熱炉において900°〜
1200℃に加熱焼成して発泡させた後、800°〜1
100℃の雰囲気温度において,発泡物上面を連続的に
成形することを特徴とする,焼成軽量建材の製造方法。
1 Fill a mold with powdered raw material prepared by blending silicic acid-containing material and foaming aid with granulated blast furnace nlug, and heat in a heating furnace at 900°~
After heating and firing at 1200℃ and foaming, 800℃~1
1. A method for manufacturing a fired lightweight building material, characterized by continuously molding the upper surface of a foam at an ambient temperature of 100°C.
JP55009975A 1980-02-01 1980-02-01 Manufacturing method for fired lightweight building materials Expired JPS5812219B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP55009975A JPS5812219B2 (en) 1980-02-01 1980-02-01 Manufacturing method for fired lightweight building materials

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP55009975A JPS5812219B2 (en) 1980-02-01 1980-02-01 Manufacturing method for fired lightweight building materials

Publications (2)

Publication Number Publication Date
JPS56109858A JPS56109858A (en) 1981-08-31
JPS5812219B2 true JPS5812219B2 (en) 1983-03-07

Family

ID=11734908

Family Applications (1)

Application Number Title Priority Date Filing Date
JP55009975A Expired JPS5812219B2 (en) 1980-02-01 1980-02-01 Manufacturing method for fired lightweight building materials

Country Status (1)

Country Link
JP (1) JPS5812219B2 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20180130518A (en) 2016-03-29 2018-12-07 토요잉크Sc홀딩스주식회사 Laminate and manufacturing method thereof

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5465716A (en) * 1977-11-05 1979-05-26 Kogyo Gijutsuin Method and apparatus for making enameld roof tile

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5465716A (en) * 1977-11-05 1979-05-26 Kogyo Gijutsuin Method and apparatus for making enameld roof tile

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20180130518A (en) 2016-03-29 2018-12-07 토요잉크Sc홀딩스주식회사 Laminate and manufacturing method thereof

Also Published As

Publication number Publication date
JPS56109858A (en) 1981-08-31

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