JPS5780557A - Manufacture of filling agent for liquid-phase chromatography - Google Patents

Manufacture of filling agent for liquid-phase chromatography

Info

Publication number
JPS5780557A
JPS5780557A JP55157059A JP15705980A JPS5780557A JP S5780557 A JPS5780557 A JP S5780557A JP 55157059 A JP55157059 A JP 55157059A JP 15705980 A JP15705980 A JP 15705980A JP S5780557 A JPS5780557 A JP S5780557A
Authority
JP
Japan
Prior art keywords
compound
porous polymer
polyvinyl
beads
filling agent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP55157059A
Other languages
Japanese (ja)
Other versions
JPS6361618B2 (en
Inventor
Isao Kaiho
Ryuji Takahashi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Resonac Holdings Corp
Original Assignee
Showa Denko KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Showa Denko KK filed Critical Showa Denko KK
Priority to JP55157059A priority Critical patent/JPS5780557A/en
Publication of JPS5780557A publication Critical patent/JPS5780557A/en
Publication of JPS6361618B2 publication Critical patent/JPS6361618B2/ja
Granted legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02—Column chromatography
    • G01N30/50—Conditioning of the sorbent material or stationary liquid

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Graft Or Block Polymers (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Polymerisation Methods In General (AREA)

Abstract

PURPOSE:To obtain a filling agent excellent in strength and separating ability with less shrinking and swelling, by a solvent by forming a microporous gel consisting of a monovinyl compound and a polyvinyl compound in an on the surface of pore of beads of a certain huge reticulate porous polymer. CONSTITUTION:Beads (specific surface area; 2-100m<2>/g, pore size; 100-1,000Angstrom , particle diameter; 5-50mu) of a huge reticulate porous polymer is obtained by condensing a monovinyo aromatic compound and (meta-)acrylonitrile under the presence of a polyvinyl aromatic compound. These beads are impregnated with a mixture solution of (A) a monovinyl compound (ex. styrene), (B) a polyvinyl compound (ex. divinyl benzene), (C) a precipitant (ex. benzene) and (D) a polymerization initiator (ex. lauroyl peroxide), and this is polymerized by suspension. A combined polymer (a porous polymer consisting of a monovinyl compound and a polyvinyl compound) of ca. 10-50wt% is adhered to the above mentioned huge reticular porous polymer, and a filling agent is obtained.
JP55157059A 1980-11-10 1980-11-10 Manufacture of filling agent for liquid-phase chromatography Granted JPS5780557A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP55157059A JPS5780557A (en) 1980-11-10 1980-11-10 Manufacture of filling agent for liquid-phase chromatography

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP55157059A JPS5780557A (en) 1980-11-10 1980-11-10 Manufacture of filling agent for liquid-phase chromatography

Publications (2)

Publication Number Publication Date
JPS5780557A true JPS5780557A (en) 1982-05-20
JPS6361618B2 JPS6361618B2 (en) 1988-11-29

Family

ID=15641304

Family Applications (1)

Application Number Title Priority Date Filing Date
JP55157059A Granted JPS5780557A (en) 1980-11-10 1980-11-10 Manufacture of filling agent for liquid-phase chromatography

Country Status (1)

Country Link
JP (1) JPS5780557A (en)

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS59202210A (en) * 1983-04-28 1984-11-16 Idemitsu Kosan Co Ltd Production of vinyl compound polymer particle
JPS61225254A (en) * 1985-03-30 1986-10-07 Nitto Electric Ind Co Ltd Fine particle having uniform particle size and production thereof
JPS62127336A (en) * 1985-11-28 1987-06-09 Japan Synthetic Rubber Co Ltd Polymer particle having internal hole and its production
JPS63182564A (en) * 1987-01-24 1988-07-27 Hitachi Ltd Separation column
JPS6463858A (en) * 1987-04-24 1989-03-09 Unilever Nv Substrate and manufacture thereof
JP2006348279A (en) * 2005-05-18 2006-12-28 Rohm & Haas Co Method for producing macroporous acrylic resin
JP2007100035A (en) * 2005-10-07 2007-04-19 Jsr Corp Organic polymer particles and their production method
JP2009221426A (en) * 2008-03-18 2009-10-01 Japan Organo Co Ltd Monolith-shaped organic porous body, manufacturing method, monolith-shaped organic porous ion exchanger
JP2011045812A (en) * 2009-08-26 2011-03-10 Tosoh Corp Particulate anion exchange resin, method of manufacturing the resin and method of producing dichlorobutene using the resin
JP2013053300A (en) * 2011-08-31 2013-03-21 Dow Global Technologies Llc Improved shell-functionalized ion exchange resin

Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS59202210A (en) * 1983-04-28 1984-11-16 Idemitsu Kosan Co Ltd Production of vinyl compound polymer particle
JPS6367805B2 (en) * 1983-04-28 1988-12-27 Idemitsu Kosan Co
JPS61225254A (en) * 1985-03-30 1986-10-07 Nitto Electric Ind Co Ltd Fine particle having uniform particle size and production thereof
JPH0572923B2 (en) * 1985-03-30 1993-10-13 Nitto Denko Corp
JPH0468324B2 (en) * 1985-11-28 1992-11-02 Japan Synthetic Rubber Co Ltd
JPS62127336A (en) * 1985-11-28 1987-06-09 Japan Synthetic Rubber Co Ltd Polymer particle having internal hole and its production
JPS63182564A (en) * 1987-01-24 1988-07-27 Hitachi Ltd Separation column
JPS6463858A (en) * 1987-04-24 1989-03-09 Unilever Nv Substrate and manufacture thereof
JP2006348279A (en) * 2005-05-18 2006-12-28 Rohm & Haas Co Method for producing macroporous acrylic resin
JP2007100035A (en) * 2005-10-07 2007-04-19 Jsr Corp Organic polymer particles and their production method
JP2009221426A (en) * 2008-03-18 2009-10-01 Japan Organo Co Ltd Monolith-shaped organic porous body, manufacturing method, monolith-shaped organic porous ion exchanger
JP2011045812A (en) * 2009-08-26 2011-03-10 Tosoh Corp Particulate anion exchange resin, method of manufacturing the resin and method of producing dichlorobutene using the resin
JP2013053300A (en) * 2011-08-31 2013-03-21 Dow Global Technologies Llc Improved shell-functionalized ion exchange resin

Also Published As

Publication number Publication date
JPS6361618B2 (en) 1988-11-29

Similar Documents

Publication Publication Date Title
US4140653A (en) Solid support for liquid chromatography
EP0626976B1 (en) Preparation of surface-functional polymer particles
US4045353A (en) High-energy radiation induced polymerization on a chromatographic solid support
US4250052A (en) Catalyst structure and a process for its preparation
KR860003044A (en) Composite porous material, preparation method thereof, and method for separating metal element
JPS5780557A (en) Manufacture of filling agent for liquid-phase chromatography
NZ214793A (en) A process for making void-containing polymers
KR950703023A (en) POROUS COPOLYMERS HAVING A CELLULAR POLYMERIC STRUCTURE SUITABLE FOR PREPARING ION-EXCHANGE RESINS AND ADSORBENTS Suitable for Preparing Ion-Exchange Resins and Adsorbents
KR840005161A (en) Method for producing rubber reinforced polymer of monovinylidene aromatic compound
DE3375402D1 (en) Macroporous hydrophilic enzyme carrier
GB1271766A (en) Process for the purification of gases and vapours
AU2561692A (en) Selective affinity material, preparation thereof by molecular imprinting, and use of the same
GB1260208A (en) Swellable polymers
CA2096224A1 (en) Macroporous Polymeric Particles as Biocompatible Supports
JPS6426617A (en) Production of crosslinked polymer particle
Hosoya et al. Uniform-size hydrophobic polymer-based separation media selectively modified with a hydrophilic external polymeric layer
EP1242490A1 (en) Single stage seed polymerisation for the production of large polymer particles with a narrow size distribution
GB849122A (en) Improvements relating to ion-exchange resins and their manufacture
GB1335585A (en) Process for preparing a cross-linked porous copolymer
GB2091581A (en) Macroporous polymer adsorbents
JPH037068B2 (en)
DK435081A (en) PEARL POLYMERIZATE AND ITS USE FOR ENZYMIM MOBILIZATION
JPS5339978A (en) Preparation of microcapsule having wall of semipermeable membrane
ES8609408A1 (en) Ion exchange resins.
KR0141989B1 (en) Process for preparation of synthesized absorbent