JPS5770842A - Preparation of 1,12-dodecanediamine - Google Patents

Preparation of 1,12-dodecanediamine

Info

Publication number
JPS5770842A
JPS5770842A JP55146335A JP14633580A JPS5770842A JP S5770842 A JPS5770842 A JP S5770842A JP 55146335 A JP55146335 A JP 55146335A JP 14633580 A JP14633580 A JP 14633580A JP S5770842 A JPS5770842 A JP S5770842A
Authority
JP
Japan
Prior art keywords
dodecanedinitrile
hydrogenating
hydrogen
catalytic activity
dodecanediamine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP55146335A
Other languages
Japanese (ja)
Inventor
Shinichi Furusaki
Hisao Yamashina
Koji Ishichi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ube Corp
Original Assignee
Ube Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ube Industries Ltd filed Critical Ube Industries Ltd
Priority to JP55146335A priority Critical patent/JPS5770842A/en
Publication of JPS5770842A publication Critical patent/JPS5770842A/en
Pending legal-status Critical Current

Links

Classifications

    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/52Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Landscapes

  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

PURPOSE: To prepare the titled compound useful as a raw material of polyamides, by hydrogenating dodecanedinitrile using a granular catalyst having long-lasting catalytic activity, resistant to pulverization, and containing an active component composed essentially of element iron.
CONSTITUTION: 1,12-Dodecanediamine is prepared by hydrogenating dodecanedinitrile. The hydrogenation is carried out at a relatively low temperature (but high enough to keep the sufficiently high catalytic activity), e.g. at 80W150°C, in liquid phase, under pressure (pref. 150W300kg/cm2G), in the presence of ammonia and hydrogen, and a granular catalyst having a diameter of 5W20mm and obtained by calcining or melting a mixture of iron oxide and 1W10wt%, based on the iron oxide, of aluminum oxide at≥1,400°C, cooling, crushing, and reducing in hydrogen.
EFFECT: The use of the catalyst enables the continuous operation for a long period.
COPYRIGHT: (C)1982,JPO&Japio
JP55146335A 1980-10-21 1980-10-21 Preparation of 1,12-dodecanediamine Pending JPS5770842A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP55146335A JPS5770842A (en) 1980-10-21 1980-10-21 Preparation of 1,12-dodecanediamine

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP55146335A JPS5770842A (en) 1980-10-21 1980-10-21 Preparation of 1,12-dodecanediamine

Publications (1)

Publication Number Publication Date
JPS5770842A true JPS5770842A (en) 1982-05-01

Family

ID=15405355

Family Applications (1)

Application Number Title Priority Date Filing Date
JP55146335A Pending JPS5770842A (en) 1980-10-21 1980-10-21 Preparation of 1,12-dodecanediamine

Country Status (1)

Country Link
JP (1) JPS5770842A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2021015242A1 (en) 2019-07-22 2021-01-28 旭化成株式会社 Genetically modified microorganism and method for producing diamine compound

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS516907A (en) * 1974-07-09 1976-01-20 Ube Industries

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS516907A (en) * 1974-07-09 1976-01-20 Ube Industries

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2021015242A1 (en) 2019-07-22 2021-01-28 旭化成株式会社 Genetically modified microorganism and method for producing diamine compound
KR20220032084A (en) 2019-07-22 2022-03-15 아사히 가세이 가부시키가이샤 Genetically Recombinant Microorganisms and Methods for Manufacturing Diamine Compounds

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