JPS57132059A - Pollution estimating method for flow passage or the like gas chromatography - Google Patents
Pollution estimating method for flow passage or the like gas chromatographyInfo
- Publication number
- JPS57132059A JPS57132059A JP1749581A JP1749581A JPS57132059A JP S57132059 A JPS57132059 A JP S57132059A JP 1749581 A JP1749581 A JP 1749581A JP 1749581 A JP1749581 A JP 1749581A JP S57132059 A JPS57132059 A JP S57132059A
- Authority
- JP
- Japan
- Prior art keywords
- column
- flow passage
- gas
- carrier gas
- pollution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/38—Flow patterns
- G01N30/40—Flow patterns using back flushing
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
Abstract
PURPOSE:To estimate a pollution state and to perform an accurate measurement of gas, by carrying out a back flush of a gas chromatography and removing a pollutant of a flow passage and valve between a gas bomb and a column, and then, measuring a peak eluted collectively. CONSTITUTION:In a measuring apparatus flowing carrier gas in a column 6 in a reverse direction by switching a step 1 of a flow passage shown by a dotted line 4 which is provided with a switching valve 4, to a step 2 of the flow passage shown by a solid line and sending nonmethane hydrocarbons to a gas detector (FID) 9 to measure said hydrocarbons, water is introduced into the carrier gas in a column 6 in an early stage of analysis and steam is passed through the column 6. Next, the carrier gas flows in the column 6 in a reverse direction from the early stage by the flow passage step 2 shown by a dotted line and a peak eluted collectively is measured and a pollutant of the column 6, the flow passage of the carrier gas in the upper stream side of the column and a pressure control valve 2, are measured by the FID9. The pollution is estimated by using this result and the accurate analysis is carried out by correcting the measured value of nonmethane hydrocarbons.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP1749581A JPS57132059A (en) | 1981-02-10 | 1981-02-10 | Pollution estimating method for flow passage or the like gas chromatography |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP1749581A JPS57132059A (en) | 1981-02-10 | 1981-02-10 | Pollution estimating method for flow passage or the like gas chromatography |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS57132059A true JPS57132059A (en) | 1982-08-16 |
JPS6229025B2 JPS6229025B2 (en) | 1987-06-24 |
Family
ID=11945575
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP1749581A Granted JPS57132059A (en) | 1981-02-10 | 1981-02-10 | Pollution estimating method for flow passage or the like gas chromatography |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS57132059A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS61178468U (en) * | 1985-04-25 | 1986-11-07 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5442593U (en) * | 1977-08-31 | 1979-03-22 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5395589A (en) * | 1977-02-02 | 1978-08-21 | Nippon Telegr & Teleph Corp <Ntt> | Semiconductor light amplifying device |
-
1981
- 1981-02-10 JP JP1749581A patent/JPS57132059A/en active Granted
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5442593U (en) * | 1977-08-31 | 1979-03-22 |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS61178468U (en) * | 1985-04-25 | 1986-11-07 |
Also Published As
Publication number | Publication date |
---|---|
JPS6229025B2 (en) | 1987-06-24 |
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