JPS5665006A - Manufacture of polyvinylpyrrolidoneeiodine - Google Patents

Manufacture of polyvinylpyrrolidoneeiodine

Info

Publication number
JPS5665006A
JPS5665006A JP14452580A JP14452580A JPS5665006A JP S5665006 A JPS5665006 A JP S5665006A JP 14452580 A JP14452580 A JP 14452580A JP 14452580 A JP14452580 A JP 14452580A JP S5665006 A JPS5665006 A JP S5665006A
Authority
JP
Japan
Prior art keywords
iodine
acid
polyvinylpyrrolidoneeiodine
manufacture
pvp
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP14452580A
Other languages
Japanese (ja)
Other versions
JPS6360762B2 (en
Inventor
Dentsuingaa Warutaa
Harutoman Hainritsuhi
Shiyuuarutsu Uorufugangu
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of JPS5665006A publication Critical patent/JPS5665006A/en
Publication of JPS6360762B2 publication Critical patent/JPS6360762B2/ja
Granted legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/12—Iodine, e.g. iodophors; Compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F8/00—Chemical modification by after-treatment
    • C08F8/18—Introducing halogen atoms or halogen-containing groups
    • C08F8/20—Halogenation
    • C08F8/22—Halogenation by reaction with free halogens

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Engineering & Computer Science (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Agronomy & Crop Science (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Plant Pathology (AREA)
  • Medicinal Chemistry (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Medicinal Preparation (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

A process for the preparation of PVP-iodine having an iodine:iodide ratio of about 2:1 and a partition coefficient of 180-250, by reacting PVP with elementary iodine in the presence of formic acid, oxalic acid or an ammonium salt or amide of carbonic acid, formic acid or oxalic acid, in aqueous solution.
JP14452580A 1979-10-18 1980-10-17 Manufacture of polyvinylpyrrolidoneeiodine Granted JPS5665006A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19792942179 DE2942179A1 (en) 1979-10-18 1979-10-18 METHOD FOR PRODUCING PVP IOD

Publications (2)

Publication Number Publication Date
JPS5665006A true JPS5665006A (en) 1981-06-02
JPS6360762B2 JPS6360762B2 (en) 1988-11-25

Family

ID=6083796

Family Applications (1)

Application Number Title Priority Date Filing Date
JP14452580A Granted JPS5665006A (en) 1979-10-18 1980-10-17 Manufacture of polyvinylpyrrolidoneeiodine

Country Status (6)

Country Link
US (1) US4402937A (en)
EP (1) EP0027613B1 (en)
JP (1) JPS5665006A (en)
AT (1) ATE2107T1 (en)
CA (1) CA1158798A (en)
DE (2) DE2942179A1 (en)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4704102A (en) * 1982-09-30 1987-11-03 Geneco Inc. Method of eliminating intra abdominal infections
US4704436A (en) * 1986-05-02 1987-11-03 Barabas Eugene S Water soluble complex of a poly(vinylpyrrolidone) copolymer and α-methyl-(2-methylpropyl)benzene acetic acid
US5066497A (en) * 1988-07-28 1991-11-19 Albert L. Jacobs, Jr. Antimicrobial veterinary compositions and methods
US4935248A (en) * 1988-07-28 1990-06-19 Albert L. Jacobs Antimicrobial veterinary compositions and methods
WO1990014834A1 (en) * 1989-06-05 1990-12-13 Gaf Chemicals Corporation Pvp-hi-i2 complexes having a partition coefficient above 300, and process for making same
GB9006346D0 (en) * 1990-03-21 1990-05-16 Euro Celtique Sa Pharmaceutical composition
DE19944464A1 (en) * 1999-09-16 2001-03-22 Basf Ag Process for the preparation of polyvinylpyrrolidone iodine in aqueous solution
US20080172032A1 (en) * 2007-01-11 2008-07-17 James Pitzer Gills Method for preventing tissue damage associated with irrigation of tissue with an antimicrobial solution
CN101838359B (en) * 2010-05-21 2012-06-27 上海宇昂生物科技有限公司 Non-ionic N-vinyl butyrate lactam iodine, high-stability non-ionic N-vinyl butyrate lactam iodine and relevant overspeed preparation method
AU2012258633A1 (en) 2011-05-24 2013-11-28 Agienic, Inc. Compositions and methods for antimicrobial metal nanoparticles
DE102014010694A1 (en) 2014-07-09 2016-01-28 Beuth Hochschule Für Technik Berlin Iodine-containing pharmaceutical composition with antimicrobial properties and process for the preparation
CN107428864A (en) * 2015-03-25 2017-12-01 日本瑞翁株式会社 Polymer, moulding material and resin-formed body
CA3031822C (en) * 2016-07-28 2021-01-05 eXion labs Inc. Polymer-based antimicrobial compositions and methods of use thereof
BR112022017042A2 (en) * 2020-02-26 2022-11-08 Carefusion Corp SYSTEMS AND METHODS FOR STERILIZING IODOPHOR COMPOSITIONS

Family Cites Families (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2739922A (en) * 1952-03-13 1956-03-27 Herman A Shelanski Mixtures of polymeric n-vinyl pyrrolidone and halogens
US2826532A (en) * 1952-04-15 1958-03-11 Gen Aniline & Film Corp Process of stabilizing polyvinyl pyrrolidone-iodine compositions
BE615889A (en) * 1952-04-15 1900-01-01
US2900305A (en) * 1952-04-15 1959-08-18 Gen Aniline & Film Corp Preparation of iodine polyvinylpyrrolidone adducts
US2914516A (en) * 1956-05-07 1959-11-24 Gen Aniline & Film Corp Purification of polyvinylpyrrolidone
US3028300A (en) * 1960-09-13 1962-04-03 West Laboratories Inc Germicidal compositions and methods for preparing the same
US3898326A (en) * 1973-05-14 1975-08-05 West Laboratories Inc Polyvinylpyrrolidone-iodide compositions and polyvinylpyrrolidone-iodide-iodine complexes prepared therefrom
YU193875A (en) * 1974-08-16 1982-02-28 Basf Ag Process for producing polyvinyl pyrrolidone-iodine
DE2514127C3 (en) * 1975-03-29 1981-05-14 Basf Ag, 6700 Ludwigshafen Process for the preparation of polymers of N-vinylpyrrolidone-2
US4094967A (en) * 1976-10-22 1978-06-13 Allor Foundation Iodine-polyvinylpyrrolidone solid product and method of preparation
US4128633A (en) * 1977-04-27 1978-12-05 Gaf Corporation Process for preparing PVP-iodine complex
DE2818767C2 (en) * 1978-04-28 1980-03-20 Basf Ag, 6700 Ludwigshafen Process for the production of polyvinylpyrrolidone-iodine
US4271149A (en) * 1979-09-21 1981-06-02 West Agro-Chemical, Inc. Germicidal iodine compositions with enhanced iodine stability
DE2941387A1 (en) * 1979-10-12 1981-05-07 Basf Ag, 6700 Ludwigshafen METHOD FOR PRODUCING POLYVINYLPYRROLIDONE IODINE

Also Published As

Publication number Publication date
ATE2107T1 (en) 1983-01-15
US4402937A (en) 1983-09-06
EP0027613A1 (en) 1981-04-29
EP0027613B1 (en) 1982-12-29
CA1158798A (en) 1983-12-13
DE2942179A1 (en) 1981-05-07
JPS6360762B2 (en) 1988-11-25
DE3061514D1 (en) 1983-02-03

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