JPS5641204A - Preparation of saponified ethylene-vinyl acetate copolymer - Google Patents
Preparation of saponified ethylene-vinyl acetate copolymerInfo
- Publication number
- JPS5641204A JPS5641204A JP11817879A JP11817879A JPS5641204A JP S5641204 A JPS5641204 A JP S5641204A JP 11817879 A JP11817879 A JP 11817879A JP 11817879 A JP11817879 A JP 11817879A JP S5641204 A JPS5641204 A JP S5641204A
- Authority
- JP
- Japan
- Prior art keywords
- vinyl acetate
- acetate copolymer
- saponified ethylene
- saponification
- ethylene
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Compositions Of Macromolecular Compounds (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Abstract
PURPOSE: To prepare a saponified ethylene-vinyl acetate copolymer with excellent heat resistance and moldability, by the addition of calcium acetate and a specified organic acid to a saponified ethylene-vinyl acetate copolymer, after the removal of saponification by-products.
CONSTITUTION: A saponified ethylene-vinyl acetate copolymer of ethylene contant 20W80mol% and of saponification degree ≥85%, is washed with an ion-exchange water of pH≤5 acidified with acetic acid, to remove saponification by-products. Then 0.001W0.1wt% of calcium acetate and/or magnesium acetate, and 0.001W 0.3wt% of an organic acid of boiling pt. ≥140°C under normal pressure and of PKa of 3.5W5.5, such as adipic acid or propionic acid, are added to the saponified ethylene-vinyl acetate copolymer.
EFFECT: It is possible to obtain a film free from fish eye, roughness or discoloration.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP11817879A JPS5641204A (en) | 1979-09-13 | 1979-09-13 | Preparation of saponified ethylene-vinyl acetate copolymer |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP11817879A JPS5641204A (en) | 1979-09-13 | 1979-09-13 | Preparation of saponified ethylene-vinyl acetate copolymer |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5641204A true JPS5641204A (en) | 1981-04-17 |
JPS6210523B2 JPS6210523B2 (en) | 1987-03-06 |
Family
ID=14730059
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP11817879A Granted JPS5641204A (en) | 1979-09-13 | 1979-09-13 | Preparation of saponified ethylene-vinyl acetate copolymer |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5641204A (en) |
Cited By (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2556357A1 (en) * | 1983-12-09 | 1985-06-14 | Nippon Synthetic Chem Ind | METHOD FOR FORMING A FILM OF AN ETHYLENE-HYDROLYSED VINYL ACETATE COPOLYMER |
JPS6268840A (en) * | 1985-09-20 | 1987-03-28 | Toyo Seikan Kaisha Ltd | Resin composition and container made of said composition |
JPS62288649A (en) * | 1986-04-15 | 1987-12-15 | イー・アイ・デユポン・ドウ・ヌムール・アンド・カンパニー | Polyacetal stabilizing composition |
JPS6464843A (en) * | 1987-09-07 | 1989-03-10 | Kuraray Co | Laminate |
JPS6466262A (en) * | 1987-09-07 | 1989-03-13 | Kuraray Co | Ethylene-vinyl alcohol copolymer composition |
JPS6469653A (en) * | 1987-09-08 | 1989-03-15 | Kuraray Co | Ethylene/vinyl alcohol copolymer composition |
FR2621320A1 (en) * | 1987-10-02 | 1989-04-07 | Nippon Synthetic Chem Ind | VINYL HYDROLYSIS ETHYLENE-ACETATE COPOLYMER |
EP0863163A1 (en) * | 1997-03-03 | 1998-09-09 | Rohm And Haas Company | Polymer emulsions and polymer powders therefrom |
WO1999005213A1 (en) * | 1997-07-25 | 1999-02-04 | Nippon Gohsei Kagaku Kogyo Kabushiki Kaisha | Resin composition, process for preparing the same, and laminate containing layer of said resin composition |
JPH11293079A (en) * | 1998-04-08 | 1999-10-26 | Nippon Synthetic Chem Ind Co Ltd:The | Preparation of resin composition |
JP2000026689A (en) * | 1998-07-07 | 2000-01-25 | Nippon Synthetic Chem Ind Co Ltd:The | Resin composition and its manufacture and use |
EP1067152A1 (en) * | 1999-07-07 | 2001-01-10 | Kuraray Co., Ltd. | Resin composition comprising ethylene-vinyl alcohol copolymer with good interlayer adhesiveness |
EP1090953A1 (en) * | 1999-09-29 | 2001-04-11 | Kuraray Co., Ltd. | Resin composition of good long-run workability comprising ethylene-vinyl alcohol copolymer |
US6232382B1 (en) | 1997-10-02 | 2001-05-15 | Nippon Gohsei Kagaku Kogyo Kabushiki Kaisha | Saponified ethylene-vinyl acetate copolymer resin composition and laminate having a layer of said resin composition |
US6238606B1 (en) | 1997-09-08 | 2001-05-29 | Nippon Gohsei Kagaku Kogyo | Process for preparing pellets of saponified ethylene/vinyl acetate copolymer |
EP1108744A2 (en) * | 1999-12-16 | 2001-06-20 | Kuraray Co., Ltd. | Ethylene-vinyl alcohol copolymer resin composition of improved long-run workability, and its shaped articles |
WO2002053639A1 (en) * | 2000-12-28 | 2002-07-11 | Kuraray Co., Ltd. | Ethylene/vinyl alcohol copolymer resin composition |
EP2196312A2 (en) | 1998-10-07 | 2010-06-16 | Kuraray Co., Ltd. | Multilayer structure and process for producing the same |
WO2022078458A1 (en) * | 2020-10-15 | 2022-04-21 | 中国石油化工股份有限公司 | Ethylene-vinyl alcohol copolymer composition and preparation method therefor |
-
1979
- 1979-09-13 JP JP11817879A patent/JPS5641204A/en active Granted
Cited By (26)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2556357A1 (en) * | 1983-12-09 | 1985-06-14 | Nippon Synthetic Chem Ind | METHOD FOR FORMING A FILM OF AN ETHYLENE-HYDROLYSED VINYL ACETATE COPOLYMER |
JPS6268840A (en) * | 1985-09-20 | 1987-03-28 | Toyo Seikan Kaisha Ltd | Resin composition and container made of said composition |
JPH0717810B2 (en) * | 1986-04-15 | 1995-03-01 | イ−・アイ・デユポン・デ・ニモアス・アンド・カンパニ− | Stabilized composition of polyacetal |
JPS62288649A (en) * | 1986-04-15 | 1987-12-15 | イー・アイ・デユポン・ドウ・ヌムール・アンド・カンパニー | Polyacetal stabilizing composition |
JPS6464843A (en) * | 1987-09-07 | 1989-03-10 | Kuraray Co | Laminate |
EP0308703A2 (en) * | 1987-09-07 | 1989-03-29 | Kuraray Co., Ltd. | Ethylene-vinyl alcolhol co-polymer composition and multilayered structure utilizing the same |
US5360670A (en) * | 1987-09-07 | 1994-11-01 | Kuraray Co., Ltd. | Multilayered structure containing an ethylene-vinyl alcohol layer |
JPS6466262A (en) * | 1987-09-07 | 1989-03-13 | Kuraray Co | Ethylene-vinyl alcohol copolymer composition |
JPS6469653A (en) * | 1987-09-08 | 1989-03-15 | Kuraray Co | Ethylene/vinyl alcohol copolymer composition |
FR2621320A1 (en) * | 1987-10-02 | 1989-04-07 | Nippon Synthetic Chem Ind | VINYL HYDROLYSIS ETHYLENE-ACETATE COPOLYMER |
EP0863163A1 (en) * | 1997-03-03 | 1998-09-09 | Rohm And Haas Company | Polymer emulsions and polymer powders therefrom |
WO1999005213A1 (en) * | 1997-07-25 | 1999-02-04 | Nippon Gohsei Kagaku Kogyo Kabushiki Kaisha | Resin composition, process for preparing the same, and laminate containing layer of said resin composition |
US6174949B1 (en) | 1997-07-25 | 2001-01-16 | Nippon Gohsei Kagaku Kogyo Kabushiki Kaisha | Resin composition, process for preparing the same, and laminate containing layer of said resin composition |
US6238606B1 (en) | 1997-09-08 | 2001-05-29 | Nippon Gohsei Kagaku Kogyo | Process for preparing pellets of saponified ethylene/vinyl acetate copolymer |
US6232382B1 (en) | 1997-10-02 | 2001-05-15 | Nippon Gohsei Kagaku Kogyo Kabushiki Kaisha | Saponified ethylene-vinyl acetate copolymer resin composition and laminate having a layer of said resin composition |
JPH11293079A (en) * | 1998-04-08 | 1999-10-26 | Nippon Synthetic Chem Ind Co Ltd:The | Preparation of resin composition |
JP2000026689A (en) * | 1998-07-07 | 2000-01-25 | Nippon Synthetic Chem Ind Co Ltd:The | Resin composition and its manufacture and use |
EP2196312A2 (en) | 1998-10-07 | 2010-06-16 | Kuraray Co., Ltd. | Multilayer structure and process for producing the same |
EP1067152A1 (en) * | 1999-07-07 | 2001-01-10 | Kuraray Co., Ltd. | Resin composition comprising ethylene-vinyl alcohol copolymer with good interlayer adhesiveness |
EP1090953A1 (en) * | 1999-09-29 | 2001-04-11 | Kuraray Co., Ltd. | Resin composition of good long-run workability comprising ethylene-vinyl alcohol copolymer |
US9346940B2 (en) | 1999-09-29 | 2016-05-24 | Kuraray Co., Ltd. | Resin composition of good long-run workability comprising ethylene-vinyl alcohol copolymer |
EP1108744A2 (en) * | 1999-12-16 | 2001-06-20 | Kuraray Co., Ltd. | Ethylene-vinyl alcohol copolymer resin composition of improved long-run workability, and its shaped articles |
US6964990B2 (en) | 1999-12-16 | 2005-11-15 | Kuraray Co., Ltd. | Ethylene-vinyl alcohol copolymer resin composition of improved long-run workability, and its shaped articles |
EP1108744B1 (en) * | 1999-12-16 | 2006-10-11 | Kuraray Co., Ltd. | Ethylene-vinyl alcohol copolymer resin composition of improved long-run workability, and its shaped articles |
WO2002053639A1 (en) * | 2000-12-28 | 2002-07-11 | Kuraray Co., Ltd. | Ethylene/vinyl alcohol copolymer resin composition |
WO2022078458A1 (en) * | 2020-10-15 | 2022-04-21 | 中国石油化工股份有限公司 | Ethylene-vinyl alcohol copolymer composition and preparation method therefor |
Also Published As
Publication number | Publication date |
---|---|
JPS6210523B2 (en) | 1987-03-06 |
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