JPS56108791A - Continuous preparation of benzylidenesorbitol compound - Google Patents
Continuous preparation of benzylidenesorbitol compoundInfo
- Publication number
- JPS56108791A JPS56108791A JP1161780A JP1161780A JPS56108791A JP S56108791 A JPS56108791 A JP S56108791A JP 1161780 A JP1161780 A JP 1161780A JP 1161780 A JP1161780 A JP 1161780A JP S56108791 A JPS56108791 A JP S56108791A
- Authority
- JP
- Japan
- Prior art keywords
- reaction
- lower alcohol
- preliminary
- compound
- sorbitol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Abstract
PURPOSE: To prepare the titled compound useful as an additive for various applications, in high yield and selectivity, by reacting a lower alcohol continuously with a preliminary reaction product of sorbitol and benzaldehyde compound in the presence of a catalyst.
CONSTITUTION: The homogeneous liquid obtained by the preliminary reaction of sorbitol (SB), a benzaldehyde compound (BA) and a lower alcohol (ROH) in a preliminary reactor 2, is charged continuously into the reactor 3 together with a hydrocarbon reaction medium S (e.g. cyclohexane, alkyl-substituted cyclohexane, etc.), and reacted to obtain the titled compound. The reaction temperature is pref. about 65W140°C. The vapor generated by heating is condensed with a cooler 6 and separated into the reaction medium, the lower alcohol and water in a decanter 7. The reaction medium is recycled to the reaction system. The lower alcohol acts not only as an initiator of the preliminary reaction but also as a reaction accelerator.
COPYRIGHT: (C)1981,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP55011617A JPS5822156B2 (en) | 1980-02-01 | 1980-02-01 | Continuous production method of 1,3:2,4-dibenzylidene sorbitol or (and) 1,3:2,4:5,6-tribenzylidene sorbitol |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP55011617A JPS5822156B2 (en) | 1980-02-01 | 1980-02-01 | Continuous production method of 1,3:2,4-dibenzylidene sorbitol or (and) 1,3:2,4:5,6-tribenzylidene sorbitol |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS56108791A true JPS56108791A (en) | 1981-08-28 |
JPS5822156B2 JPS5822156B2 (en) | 1983-05-06 |
Family
ID=11782875
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP55011617A Expired JPS5822156B2 (en) | 1980-02-01 | 1980-02-01 | Continuous production method of 1,3:2,4-dibenzylidene sorbitol or (and) 1,3:2,4:5,6-tribenzylidene sorbitol |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5822156B2 (en) |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH01149789A (en) * | 1987-12-07 | 1989-06-12 | New Japan Chem Co Ltd | Batch-type production of acetals |
WO1992003439A1 (en) * | 1990-08-27 | 1992-03-05 | New Japan Chemical Co., Ltd. | Method of producing acetals |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS60242870A (en) * | 1984-05-18 | 1985-12-02 | 中島 恵次 | Ball for baseball |
JPS6194666A (en) * | 1984-10-16 | 1986-05-13 | 横浜ゴム株式会社 | Solid golf ball |
JPS6476881A (en) * | 1987-09-16 | 1989-03-22 | Nagase Kenkoo Kk | Core of ball for baseball |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS4914758A (en) * | 1972-04-11 | 1974-02-08 |
-
1980
- 1980-02-01 JP JP55011617A patent/JPS5822156B2/en not_active Expired
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS4914758A (en) * | 1972-04-11 | 1974-02-08 |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH01149789A (en) * | 1987-12-07 | 1989-06-12 | New Japan Chem Co Ltd | Batch-type production of acetals |
WO1992003439A1 (en) * | 1990-08-27 | 1992-03-05 | New Japan Chemical Co., Ltd. | Method of producing acetals |
Also Published As
Publication number | Publication date |
---|---|
JPS5822156B2 (en) | 1983-05-06 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US4092368A (en) | Vapor phase transesterification | |
JPS5592326A (en) | Simultaneous manufacture of pure methyllterttbutylether and c44hydrocarbon mixture scarecely containing isobutene | |
JPS5734811B2 (en) | ||
JPS56108791A (en) | Continuous preparation of benzylidenesorbitol compound | |
JPS565424A (en) | Preparation of tertiary alcohol | |
US3897478A (en) | Continuous process for the manufacture of alkyl chrysanthemate esters | |
JPS5528928A (en) | Preparation of methoxysilane | |
KR920009757A (en) | Method for preparing methyl tertiary butyl ether from the reaction of methanol and tertiary butyl alcohol | |
JPS57158750A (en) | Preparation of methylene glutaronitrile | |
US2777000A (en) | Process for alkyl ethers of alphahydroxycumene | |
JPS55143919A (en) | Preparation of tertiary alcohol | |
JPS5553228A (en) | Preparation of ethylene glycol mono-tert-butyl ether | |
JPS56110631A (en) | Synthesis of oxygen-containing organic compound | |
JPS5640630A (en) | Production of dimethyl ether | |
JPS5627648A (en) | Preparation of filler for chromatography | |
US3946073A (en) | Process for preparation of urea autocondensation product | |
JPS5430104A (en) | Continuous production of tertiary butyl alcohol | |
JPS55129239A (en) | Purification of methacrylic acid | |
JPS57165341A (en) | Preparation of pivaloyl chloride and benzoyl chloride | |
US2822402A (en) | Preparation of 1, 1-dimethoxycyclo-hexane | |
SU427942A1 (en) | Method of producing 1-trialkylsilyl-2-alkoxyethylenes | |
JPS577428A (en) | Preparation of olefin | |
JPS57142938A (en) | Preparation of pinacolone | |
SU115456A1 (en) | The method of obtaining cellosolve | |
SU490790A1 (en) | The method of obtaining 1,1-dimetillena |