JPS5598352A - Quantitative analysis method of carbon in metal by electrochemical method - Google Patents
Quantitative analysis method of carbon in metal by electrochemical methodInfo
- Publication number
- JPS5598352A JPS5598352A JP572679A JP572679A JPS5598352A JP S5598352 A JPS5598352 A JP S5598352A JP 572679 A JP572679 A JP 572679A JP 572679 A JP572679 A JP 572679A JP S5598352 A JPS5598352 A JP S5598352A
- Authority
- JP
- Japan
- Prior art keywords
- oxygen
- sample
- pipe
- carbon
- concentration cell
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Measuring Oxygen Concentration In Cells (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
- Investigating And Analyzing Materials By Characteristic Methods (AREA)
Abstract
PURPOSE: To analyze with good reproducibility by a simple device easy in hadling by heating metal sample in oxygen to make carbon in the sample CO2, introduce the mixed gas current of CO2 and O2 to an oxygen concentration cell and integrating by time the voltage thereof.
CONSTITUTION: A ceramic burning boat containing a metal sample 1 of a predetermined amount is charged into a portion of a heating furnace 3 of a ceramic burning pipe 4 and oxygen gas from an oxygen feed pipe 5 is fed. The sample 1 is heated to burn carbon in the sample, the produced CO2 is mixed into the oxygen gas current and this mixed gas current is fed to the oxygen concentration cell from the sample gas feed pipe 14 through an exhaust pipe 6. In the oxygen concentration cell, the temperature of the electrolytic pipe 11 is maintained at a fixed one by the heating furnace 16 and voltage generated by the difference between the partial pressure of oxygen of the sample gas outside the electrolytic pipe 11 and an internal reference oxygen partial pressure is integrated by time to obtain the content of carbon.
COPYRIGHT: (C)1980,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP572679A JPS5598352A (en) | 1979-01-19 | 1979-01-19 | Quantitative analysis method of carbon in metal by electrochemical method |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP572679A JPS5598352A (en) | 1979-01-19 | 1979-01-19 | Quantitative analysis method of carbon in metal by electrochemical method |
Publications (1)
Publication Number | Publication Date |
---|---|
JPS5598352A true JPS5598352A (en) | 1980-07-26 |
Family
ID=11619119
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP572679A Pending JPS5598352A (en) | 1979-01-19 | 1979-01-19 | Quantitative analysis method of carbon in metal by electrochemical method |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5598352A (en) |
-
1979
- 1979-01-19 JP JP572679A patent/JPS5598352A/en active Pending
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