JPS5564593A - Preparation of phosphoric monoester - Google Patents

Preparation of phosphoric monoester

Info

Publication number
JPS5564593A
JPS5564593A JP13661278A JP13661278A JPS5564593A JP S5564593 A JPS5564593 A JP S5564593A JP 13661278 A JP13661278 A JP 13661278A JP 13661278 A JP13661278 A JP 13661278A JP S5564593 A JPS5564593 A JP S5564593A
Authority
JP
Japan
Prior art keywords
alkylene oxide
adduct
alcohol
30mol
azeotropic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP13661278A
Other languages
Japanese (ja)
Other versions
JPS5838435B2 (en
Inventor
Akio Manba
Tomihiro Kurosaki
Norio Nishikawa
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kao Corp
Original Assignee
Kao Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kao Corp filed Critical Kao Corp
Priority to JP13661278A priority Critical patent/JPS5838435B2/en
Publication of JPS5564593A publication Critical patent/JPS5564593A/en
Publication of JPS5838435B2 publication Critical patent/JPS5838435B2/en
Expired legal-status Critical Current

Links

Abstract

PURPOSE: To obtain the title compound useful as detergents, textile finishes, and medicines, in high yield, by esterifying orthophosphoric acid with an alcohol or its alkylene oxide adduct with azeotropic or vacuum dehydration.
CONSTITUTION: One mole of an 8W20C straight or branched chain (un)saturated aliphatic alcohol, e.g. lauryl alcohol, or its adduct with an alkylene oxide (≤30mol), or a 1W20C alkylphenol adduct with an alkylene oxide (≤30mol) is esterified with 0.5W2.9mol of orthophosphoric acid in the presence or absence of an organic solvent, e.g. xylene, at 100W150°C, preferably 120W140°C, with azeotropic or vacuum dehydration to give the compound of the formula (R is organic hydroxy compound residue).
EFFECT: Safely used as creams or lipsticks directly applied to the skin due to almost no arsenic.
COPYRIGHT: (C)1980,JPO&Japio
JP13661278A 1978-11-06 1978-11-06 Method for producing phosphoric acid monoester Expired JPS5838435B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP13661278A JPS5838435B2 (en) 1978-11-06 1978-11-06 Method for producing phosphoric acid monoester

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP13661278A JPS5838435B2 (en) 1978-11-06 1978-11-06 Method for producing phosphoric acid monoester

Publications (2)

Publication Number Publication Date
JPS5564593A true JPS5564593A (en) 1980-05-15
JPS5838435B2 JPS5838435B2 (en) 1983-08-23

Family

ID=15179363

Family Applications (1)

Application Number Title Priority Date Filing Date
JP13661278A Expired JPS5838435B2 (en) 1978-11-06 1978-11-06 Method for producing phosphoric acid monoester

Country Status (1)

Country Link
JP (1) JPS5838435B2 (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1991004978A1 (en) * 1989-10-06 1991-04-18 Daikin Industries, Ltd. Process for preparing monofluoroalkyl ester of phosphoric acid
JP2010031009A (en) * 2008-07-25 2010-02-12 Air Products & Chemicals Inc Method for removing trace of arsenic impurity from triethyl phosphate (tepo)
CN101838286A (en) * 2010-04-29 2010-09-22 苏州元素集化学工业有限公司 Method and equipment for preparing fatty alcohol (ether) phosphate
CN103012469A (en) * 2012-12-29 2013-04-03 山东科技大学 Method for preparing high-carbon alkyl phosphate for cosmetics
JP2019518750A (en) * 2016-06-27 2019-07-04 ディーエスエム アイピー アセッツ ビー．ブイ．Ｄｓｍ Ｉｐ Ａｓｓｅｔｓ Ｂ．Ｖ． Topical composition
JP2019518749A (en) * 2016-06-27 2019-07-04 ディーエスエム アイピー アセッツ ビー．ブイ．Ｄｓｍ Ｉｐ Ａｓｓｅｔｓ Ｂ．Ｖ． Composition comprising micro pigment

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1991004978A1 (en) * 1989-10-06 1991-04-18 Daikin Industries, Ltd. Process for preparing monofluoroalkyl ester of phosphoric acid
JP2010031009A (en) * 2008-07-25 2010-02-12 Air Products & Chemicals Inc Method for removing trace of arsenic impurity from triethyl phosphate (tepo)
CN101838286A (en) * 2010-04-29 2010-09-22 苏州元素集化学工业有限公司 Method and equipment for preparing fatty alcohol (ether) phosphate
CN103012469A (en) * 2012-12-29 2013-04-03 山东科技大学 Method for preparing high-carbon alkyl phosphate for cosmetics
JP2019518750A (en) * 2016-06-27 2019-07-04 ディーエスエム アイピー アセッツ ビー．ブイ．Ｄｓｍ Ｉｐ Ａｓｓｅｔｓ Ｂ．Ｖ． Topical composition
JP2019518749A (en) * 2016-06-27 2019-07-04 ディーエスエム アイピー アセッツ ビー．ブイ．Ｄｓｍ Ｉｐ Ａｓｓｅｔｓ Ｂ．Ｖ． Composition comprising micro pigment

Also Published As

Publication number Publication date
JPS5838435B2 (en) 1983-08-23

Similar Documents

Publication Publication Date Title
DE3778866D1 (en) FUEL OR LUBRICANT COMPOSITION CONTAINING POLYBUTYL OR POLYISOBUTYL DERIVATIVES.
MX159485A (en) A PROCEDURE FOR PREPARING A 2,3-DIALCOXYPROPYL GLYCERYLIC ETHER
JPS5564593A (en) Preparation of phosphoric monoester
JPS54119494A (en) Preparation of cephalosporin compound
JPS5576810A (en) Liquid hair tonic composition
JPS52806A (en) Preparation of ester
JPS5427523A (en) Preparation of hydroxy fatty acid ester
JPS5432456A (en) Preparation of jasmonic acid analogue
JPS5645405A (en) Emulsified stick cosmetic
JPS5424818A (en) Preparation of high purity maleic acid monoalcohol ester
JPS5522700A (en) Preparation of sugar ester
JPS54132502A (en) Preparation of esters
JPS5656223A (en) Starch sugar ester
JPS5334719A (en) Preparation of substituted or unsubstituted alpha-oxysuccinic acid esters
JPS53105467A (en) Preparation of phenyletheralcohol derivative acrylates or methacylates
JPS5259135A (en) Process for preparation of succinylsuccinic acid diester
JPS5493A (en) Preparation of oligomer having low skin irritating property
JPS54107885A (en) Antistatic agent
JPS55147232A (en) Branched higher secondary alcohol
GB1501786A (en) Process for the preparation of the o,o-dimethyl-o-(2,2-dichlorovinyl)ester and the o,o-diethyl-o-(2,2-dichlorovinyl)ester of thionophosphoric acid
JPS55133303A (en) Perfume controller
JPS5620594A (en) Preparation of mixed diester of phosphoric acid
JPS549214A (en) Preparation of carboxylic acid ester of secondary or tertiary alcohol
JPS54109910A (en) Preparation of unsaturated ester
JPS54145796A (en) Preparation of fatty acid ester of polyalkylene glycol