JPS5513243A - Preparation of hydroxymethylfurfural - Google Patents

Preparation of hydroxymethylfurfural

Info

Publication number
JPS5513243A
JPS5513243A JP8635178A JP8635178A JPS5513243A JP S5513243 A JPS5513243 A JP S5513243A JP 8635178 A JP8635178 A JP 8635178A JP 8635178 A JP8635178 A JP 8635178A JP S5513243 A JPS5513243 A JP S5513243A
Authority
JP
Japan
Prior art keywords
hexoses
dehydrated
hydroxymethylfurfural
preparation
ketohexoses
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP8635178A
Other languages
Japanese (ja)
Inventor
Yoshio Nakamura
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Noguchi Institute
Original Assignee
Noguchi Institute
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Noguchi Institute filed Critical Noguchi Institute
Priority to JP8635178A priority Critical patent/JPS5513243A/en
Publication of JPS5513243A publication Critical patent/JPS5513243A/en
Pending legal-status Critical Current

Links

Classifications

    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts

Abstract

PURPOSE: To obtain the title compound useful as a starting material for perfumes, medicines, and high polymers economically, by heating hexoses prepared through hydrolysis of cellulose and starch, in the presence of a specific catalyst easily separable and reusable after the reaction.
CONSTITUTION: Hexoses or di- or polysaccharides containing hexoses are dehydrated or hydrolyzed and dehydrated in the presence of a heat-resistant inorganic solid catalyst, e.g. zirconium phosphate, in a polar solvent, e.g. DMSO, at 80W200°C, preferably 120W170°C, to give hydroxymethylfurfural. Ketohexoses, e.g. D-fructose or L-sorbose, may be preferred as the hexoses, and inulin, fructan, or isomerized sugar of glucose may be used as the raw material.
COPYRIGHT: (C)1980,JPO&Japio
JP8635178A 1978-07-14 1978-07-14 Preparation of hydroxymethylfurfural Pending JPS5513243A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP8635178A JPS5513243A (en) 1978-07-14 1978-07-14 Preparation of hydroxymethylfurfural

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP8635178A JPS5513243A (en) 1978-07-14 1978-07-14 Preparation of hydroxymethylfurfural

Publications (1)

Publication Number Publication Date
JPS5513243A true JPS5513243A (en) 1980-01-30

Family

ID=13884448

Family Applications (1)

Application Number Title Priority Date Filing Date
JP8635178A Pending JPS5513243A (en) 1978-07-14 1978-07-14 Preparation of hydroxymethylfurfural

Country Status (1)

Country Link
JP (1) JPS5513243A (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4394255A (en) * 1982-07-07 1983-07-19 Phillips Petroleum Company Isomerization process
JP2007196174A (en) * 2006-01-28 2007-08-09 Osaka Industrial Promotion Organization Heterogeneous zirconium phosphate catalyst, dehydration process, 5-hydroxymethylfurfural production method, cellulose decomposition process, and regeneration method of heterogeneous zirconium phosphate catalyst
KR101428912B1 (en) * 2013-02-04 2014-08-08 충북대학교 산학협력단 Conversion Method of Fructose to 5-HMF(5-hydroxymethylfurfural) in DMSO(dimethylsulfoxide) solvent
CN104923315A (en) * 2015-05-29 2015-09-23 盐城工学院 Solid acid catalyst TiP/ATP and preparation method and application thereof
US9770705B2 (en) 2010-06-11 2017-09-26 Rennovia Inc. Oxidation catalysts
CN108610311A (en) * 2018-05-30 2018-10-02 盐城工学院 A kind of method that the low-temperature catalyzed glucose of boehmite prepares 5 hydroxymethyl furfural

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4394255A (en) * 1982-07-07 1983-07-19 Phillips Petroleum Company Isomerization process
JP2007196174A (en) * 2006-01-28 2007-08-09 Osaka Industrial Promotion Organization Heterogeneous zirconium phosphate catalyst, dehydration process, 5-hydroxymethylfurfural production method, cellulose decomposition process, and regeneration method of heterogeneous zirconium phosphate catalyst
US9770705B2 (en) 2010-06-11 2017-09-26 Rennovia Inc. Oxidation catalysts
US9808790B2 (en) 2010-06-11 2017-11-07 Rennovia Inc. Processes for the manufacturing of oxidation catalysts
US10807074B2 (en) 2010-06-11 2020-10-20 Archer-Daniels-Midland Company Oxidation catalysts
US11596927B2 (en) 2010-06-11 2023-03-07 Archer-Daniels-Midland Company Oxidation catalysts
KR101428912B1 (en) * 2013-02-04 2014-08-08 충북대학교 산학협력단 Conversion Method of Fructose to 5-HMF(5-hydroxymethylfurfural) in DMSO(dimethylsulfoxide) solvent
CN104923315A (en) * 2015-05-29 2015-09-23 盐城工学院 Solid acid catalyst TiP/ATP and preparation method and application thereof
CN108610311A (en) * 2018-05-30 2018-10-02 盐城工学院 A kind of method that the low-temperature catalyzed glucose of boehmite prepares 5 hydroxymethyl furfural
CN108610311B (en) * 2018-05-30 2021-12-10 盐城工学院 Method for preparing 5-hydroxymethylfurfural by using boehmite to catalyze glucose at low temperature

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