JPS5461123A - Preparation of tetramethylthiuram monosulfide - Google Patents
Preparation of tetramethylthiuram monosulfideInfo
- Publication number
- JPS5461123A JPS5461123A JP12580177A JP12580177A JPS5461123A JP S5461123 A JPS5461123 A JP S5461123A JP 12580177 A JP12580177 A JP 12580177A JP 12580177 A JP12580177 A JP 12580177A JP S5461123 A JPS5461123 A JP S5461123A
- Authority
- JP
- Japan
- Prior art keywords
- hcn
- reacting
- waste water
- tetramethylthiuram
- tetramethylthiuram disulfide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PURPOSE: To prepare the title compound in high yield and purity, using low-cost raw materials, by reacting tetramethylthiuram disulfide with HCN and NH3 as desulfurizing agents, in an aqueous medium, at 20W70°C.
CONSTITUTION: Tetramethylthiuram monosulfide II is prepared by reacting tetramethylthiuram disulfide I with stoichiometric amounts of HCN and NH3 at 20W 70°C, pref. 30W60°C.
EFFECT: Precise control of pH value of the reaction system is unnecessary. Little side reactions. Easy purification. Use of stoichiometric amount of HCN reduces the problems inherent to separation, processing, waste water treatment etc. There is no metal component in the waste water, and the incineration and disposal can also be simplified.
USE: Vulcanization accelerator for rubber chemicals
COPYRIGHT: (C)1979,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP12580177A JPS5461123A (en) | 1977-10-21 | 1977-10-21 | Preparation of tetramethylthiuram monosulfide |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP12580177A JPS5461123A (en) | 1977-10-21 | 1977-10-21 | Preparation of tetramethylthiuram monosulfide |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5461123A true JPS5461123A (en) | 1979-05-17 |
JPS5711903B2 JPS5711903B2 (en) | 1982-03-08 |
Family
ID=14919227
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP12580177A Granted JPS5461123A (en) | 1977-10-21 | 1977-10-21 | Preparation of tetramethylthiuram monosulfide |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5461123A (en) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS58139002U (en) * | 1982-03-15 | 1983-09-19 | 宮丸 幸雄 | Cultivating Rotor's Cultivating Sword |
-
1977
- 1977-10-21 JP JP12580177A patent/JPS5461123A/en active Granted
Also Published As
Publication number | Publication date |
---|---|
JPS5711903B2 (en) | 1982-03-08 |
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