JPS5446887A - Preparation of acrylic acid or methacrylic acid - Google Patents
Preparation of acrylic acid or methacrylic acidInfo
- Publication number
- JPS5446887A JPS5446887A JP11164177A JP11164177A JPS5446887A JP S5446887 A JPS5446887 A JP S5446887A JP 11164177 A JP11164177 A JP 11164177A JP 11164177 A JP11164177 A JP 11164177A JP S5446887 A JPS5446887 A JP S5446887A
- Authority
- JP
- Japan
- Prior art keywords
- meth
- actinomyces
- acrylamide
- acrylic acid
- enzyme
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Landscapes
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Abstract
PURPOSE: To prepare (meth)acrylic acid in high yield, by contacting an amydaseactive actinomyces or its enzyme with (meth)acrylamide under specific conditions.
CONSTITUTION: Actinomyces which can hydrolyze acrylamide, e.g. Actinomyces 10021 (FERM-P No.3451), or its variant, is inoculated in a nutrient medium, and cultured at pH 6W8 and 25W40°C under aeration and agitation. Produced cells or enzyme existing therein are added (0.5W5% dry basis) to a 5W20% aqueous solution of (meth)acrylamide and made to react at pH 5W9 and 25W40°C. The reaction mixture is centrifuged to separate the microbial cells, and subjected to ion exchange chromatography, solvent extraction, etc. to remove the impurities. (Meth)acrylic acid is recovered from the solution by vaccum concentration or distillation. The separation and purification of the product are easily carried out by this process, since no reagent is used and by-products are little produced in the process.
COPYRIGHT: (C)1979,JPO&Japio
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP11164177A JPS5446887A (en) | 1977-09-19 | 1977-09-19 | Preparation of acrylic acid or methacrylic acid |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP11164177A JPS5446887A (en) | 1977-09-19 | 1977-09-19 | Preparation of acrylic acid or methacrylic acid |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS5446887A true JPS5446887A (en) | 1979-04-13 |
JPS6143037B2 JPS6143037B2 (en) | 1986-09-25 |
Family
ID=14566453
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP11164177A Granted JPS5446887A (en) | 1977-09-19 | 1977-09-19 | Preparation of acrylic acid or methacrylic acid |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPS5446887A (en) |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2610936A1 (en) * | 1987-02-13 | 1988-08-19 | Nalco Chemical Co | PROCESS FOR REDUCING THE ACRYLAMIDE CONTENT OF WATER-IN-OIL EMULSIONS OF ACRYLAMIDE POLYMERS |
FR2610937A1 (en) * | 1987-02-13 | 1988-08-19 | Nalco Chemical Co | PROCESS FOR THE ENZYMATIC TREATMENT OF WATER-IN-OIL EMULSIONS OF ACRYLAMIDE POLYMERS TO REDUCE THE RESIDUAL MONOMER CONTENT |
FR2626288A1 (en) * | 1988-01-27 | 1989-07-28 | Rhone Poulenc Sante | |
FR2626289A1 (en) * | 1988-01-27 | 1989-07-28 | Rhone Poulenc Sante | PROCESS FOR THE PREPARATION OF OPTICALLY ACTIVE ALKANOIC ARYL-2 ACIDS |
CN102822603A (en) * | 2010-02-15 | 2012-12-12 | 松下电器产业株式会社 | Cooking device |
WO2014038216A1 (en) * | 2012-09-10 | 2014-03-13 | 三菱レイヨン株式会社 | Method for producing methacrylic acid and/or ester thereof |
US10851392B2 (en) | 2012-09-10 | 2020-12-01 | Mitsubishi Chemical Corporation | Method for producing methacrylic acid ester |
-
1977
- 1977-09-19 JP JP11164177A patent/JPS5446887A/en active Granted
Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0478641B2 (en) * | 1987-02-13 | 1992-12-11 | Nalco Chemical Co | |
FR2610937A1 (en) * | 1987-02-13 | 1988-08-19 | Nalco Chemical Co | PROCESS FOR THE ENZYMATIC TREATMENT OF WATER-IN-OIL EMULSIONS OF ACRYLAMIDE POLYMERS TO REDUCE THE RESIDUAL MONOMER CONTENT |
JPS63202601A (en) * | 1987-02-13 | 1988-08-22 | ナルコ ケミカル カンパニー | Water in oil type emulsion |
JPS63202606A (en) * | 1987-02-13 | 1988-08-22 | ナルコ ケミカル カンパニー | Reduction of acrylamide content |
FR2610936A1 (en) * | 1987-02-13 | 1988-08-19 | Nalco Chemical Co | PROCESS FOR REDUCING THE ACRYLAMIDE CONTENT OF WATER-IN-OIL EMULSIONS OF ACRYLAMIDE POLYMERS |
FR2626288A1 (en) * | 1988-01-27 | 1989-07-28 | Rhone Poulenc Sante | |
FR2626289A1 (en) * | 1988-01-27 | 1989-07-28 | Rhone Poulenc Sante | PROCESS FOR THE PREPARATION OF OPTICALLY ACTIVE ALKANOIC ARYL-2 ACIDS |
CN102822603A (en) * | 2010-02-15 | 2012-12-12 | 松下电器产业株式会社 | Cooking device |
CN102822603B (en) * | 2010-02-15 | 2015-03-04 | 松下电器产业株式会社 | Heating cooking device |
WO2014038216A1 (en) * | 2012-09-10 | 2014-03-13 | 三菱レイヨン株式会社 | Method for producing methacrylic acid and/or ester thereof |
AU2013314153B2 (en) * | 2012-09-10 | 2016-05-12 | Mitsubishi Chemical Corporation | Method for producing methacrylic acid and/or ester thereof |
US10294500B2 (en) | 2012-09-10 | 2019-05-21 | Mitsubishi Chemical Corporation | Method for producing methacrylic acid and/or ester thereof |
US10851392B2 (en) | 2012-09-10 | 2020-12-01 | Mitsubishi Chemical Corporation | Method for producing methacrylic acid ester |
Also Published As
Publication number | Publication date |
---|---|
JPS6143037B2 (en) | 1986-09-25 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US2658023A (en) | Oxygenation of steroids | |
JPS5446887A (en) | Preparation of acrylic acid or methacrylic acid | |
JPS55144889A (en) | Continuous preparation of acrylamide or methacrylamide by microorganism | |
Nakamura et al. | Synthesis from sulphate and accumulation of S-sulphocysteine by a mutant strain of Aspergillus nidulans | |
JPS5675097A (en) | Thermophilic aspartase and its preparation | |
ATE35826T1 (en) | PROCESSES FOR THE PRODUCTION OF L-ALPHAAMINOS|URES. | |
JPS5894389A (en) | Biochemical preparation of (s)-(-)-alpha-cyano-3-phenoxybenzyl alcohol | |
SU1757473A3 (en) | Method of preparation of amide compound | |
JPH0479894A (en) | Production of d-alanine | |
JPS63251098A (en) | Production of (r)-3-halogeno-1,2-propanediol | |
JPS5459392A (en) | Novel nuclease and its preparation | |
JPS62294096A (en) | Optical resolution of dl-pantolactone | |
US4897357A (en) | (S) α-cyano-3-phenoxy-benzyl acetate | |
SU652214A1 (en) | Method of obtaining propionic acid | |
JPS55135588A (en) | Preparation of heat-resistant catalase | |
JPS5675095A (en) | Preparation of heat-resistant acetic acid kinase | |
JPS5953839B2 (en) | Method for producing (−)-α-hydroxymethylbutyric acid | |
JPS6214788A (en) | Production of methacrylic acid | |
JP2928612B2 (en) | Method for producing optically active amines | |
JP3277930B2 (en) | Method for producing D-malic acid | |
CN112384630A (en) | Anti-viscosity method for catalytic production of phosphatidylserine enzyme and method for producing phosphatidylserine by using same | |
JPH0424992B2 (en) | ||
JPS60210991A (en) | Preparation of hydroquinone | |
JPS5527A (en) | Microbiological preparation of coenzyme q10 | |
JPS5658495A (en) | Preparation of amino acid derivative |