JPS5315313A - Production of oxalic acid diesters - Google Patents

Production of oxalic acid diesters

Info

Publication number
JPS5315313A
JPS5315313A JP8867376A JP8867376A JPS5315313A JP S5315313 A JPS5315313 A JP S5315313A JP 8867376 A JP8867376 A JP 8867376A JP 8867376 A JP8867376 A JP 8867376A JP S5315313 A JPS5315313 A JP S5315313A
Authority
JP
Japan
Prior art keywords
production
oxalic acid
acid diesters
keeping
salts
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP8867376A
Other languages
Japanese (ja)
Other versions
JPS5542058B2 (en
Inventor
Toshiharu Yamazaki
Katsuo Eguchi
Shinichiro Uchiumi
Keigo Nishihira
Masayoshi Yamashita
Hiroshi Itaya
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ube Corp
Original Assignee
Ube Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ube Industries Ltd filed Critical Ube Industries Ltd
Priority to JP8867376A priority Critical patent/JPS5315313A/en
Priority to IN1109/CAL/1977A priority patent/IN145087B/en
Priority to GB30412/77A priority patent/GB1532402A/en
Priority to US05/817,996 priority patent/US4138587A/en
Priority to CA283,465A priority patent/CA1093580A/en
Priority to IT26068/77A priority patent/IT1080789B/en
Priority to BR7704905A priority patent/BR7704905A/en
Priority to DE2733730A priority patent/DE2733730C3/en
Priority to FR7722937A priority patent/FR2359812A1/en
Priority to NLAANVRAGE7708262,A priority patent/NL178684C/en
Publication of JPS5315313A publication Critical patent/JPS5315313A/en
Publication of JPS5542058B2 publication Critical patent/JPS5542058B2/ja
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/34—Esters of acyclic saturated polycarboxylic acids having an esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/36—Oxalic acid esters

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

PURPOSE: To obtain the title compounds effectively by the contact of aliphatic alcohols and carbon monoxide under pressure in the presence of platinum group metals or their salts as a catalyst, and nitric acid and/or nitrogen dioxide, without the need of keeping the reaction system anhydrous.
COPYRIGHT: (C)1978,JPO&Japio
JP8867376A 1976-07-27 1976-07-27 Production of oxalic acid diesters Granted JPS5315313A (en)

Priority Applications (10)

Application Number Priority Date Filing Date Title
JP8867376A JPS5315313A (en) 1976-07-27 1976-07-27 Production of oxalic acid diesters
IN1109/CAL/1977A IN145087B (en) 1976-07-27 1977-07-19
GB30412/77A GB1532402A (en) 1976-07-27 1977-07-20 Process for the preparation of dialkyl oxalates
US05/817,996 US4138587A (en) 1976-07-27 1977-07-22 Process for the preparation of dialkyl oxalates
CA283,465A CA1093580A (en) 1976-07-27 1977-07-25 Process for the preparation of dialkyl oxalates
IT26068/77A IT1080789B (en) 1976-07-27 1977-07-25 PROCEDURE FOR THE PREPARATION OF DIALKYL OXALATES
BR7704905A BR7704905A (en) 1976-07-27 1977-07-26 PROCESS FOR PREPARING DIALKYL OXALATES
DE2733730A DE2733730C3 (en) 1976-07-27 1977-07-26 Process for the preparation of dialkyl oxalates
FR7722937A FR2359812A1 (en) 1976-07-27 1977-07-26 PROCESS FOR PREPARING DEDIALCOYL OXALATES
NLAANVRAGE7708262,A NL178684C (en) 1976-07-27 1977-07-26 PROCESS FOR THE PREPARATION OF DIALKYLOXALATES

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP8867376A JPS5315313A (en) 1976-07-27 1976-07-27 Production of oxalic acid diesters

Publications (2)

Publication Number Publication Date
JPS5315313A true JPS5315313A (en) 1978-02-13
JPS5542058B2 JPS5542058B2 (en) 1980-10-28

Family

ID=13949329

Family Applications (1)

Application Number Title Priority Date Filing Date
JP8867376A Granted JPS5315313A (en) 1976-07-27 1976-07-27 Production of oxalic acid diesters

Country Status (10)

Country Link
US (1) US4138587A (en)
JP (1) JPS5315313A (en)
BR (1) BR7704905A (en)
CA (1) CA1093580A (en)
DE (1) DE2733730C3 (en)
FR (1) FR2359812A1 (en)
GB (1) GB1532402A (en)
IN (1) IN145087B (en)
IT (1) IT1080789B (en)
NL (1) NL178684C (en)

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT1078033B (en) * 1977-04-07 1985-05-08 Snam Progetti PROCESS FOR THE PREPARATION OF ESTERS OF OXALIC ACID
JPS5441813A (en) * 1977-09-07 1979-04-03 Ube Ind Ltd Preparation of oxalic acid diesters
GB2003872B (en) * 1977-09-07 1982-05-19 Ube Industries Process for preparing a diester of oxalic acid
JPS54100312A (en) * 1978-01-25 1979-08-08 Ube Ind Ltd Preparation of oxalic diesters
JPS5481211A (en) * 1977-12-09 1979-06-28 Ube Ind Ltd Production of dicarboxylic diester
USRE31245E (en) * 1978-01-25 1983-05-17 Ube Industries, Ltd. Process for preparing a diester of oxalic acid in the gaseous phase
IT1097268B (en) * 1978-06-23 1985-08-31 Montedison Spa PROCESS FOR THE PREPARATION OF ESTERS OF OXALIC ACID
US4571435A (en) * 1980-06-30 1986-02-18 Tennessee Valley Authority Preparation of nitrogen fertilizers from oxalate esters prepared by the oxidative carbonylation of alcohols over noble metal catalysts utilizing regenerable 2,5-cyclohexadiene-1,4-dione oxidants
JPS6315319Y2 (en) * 1980-12-22 1988-04-28
DE3270056D1 (en) * 1981-01-23 1986-04-30 Union Carbide Corp Vapor state process for the preparation of diesters of oxalic acid
US4629806A (en) * 1981-01-23 1986-12-16 Union Carbide Corporation Vapor state formation of diesters of oxalic acid
US4616093A (en) * 1981-01-23 1986-10-07 Union Carbide Corporation Process for preparing a diester of oxalic acid in the vapor phase
US4410722A (en) * 1981-01-23 1983-10-18 Ube Industries, Ltd. Process for preparing oxalic acid diesters using platinum group metals supported on alumina
JPS57123143A (en) * 1981-01-26 1982-07-31 Ube Ind Ltd Production of glycolic ester
JPS57123141A (en) * 1981-01-26 1982-07-31 Ube Ind Ltd Production of oxalic diester
US4523029A (en) * 1982-06-15 1985-06-11 Chevron Research Company Oxidative carbonylation of alcohols to produce dialkyl oxalates
US4454342A (en) * 1982-07-13 1984-06-12 Atlantic Richfield Company Preparation of dialkyl oxalates using a heterogeneous Pd-V-P catalyst for the oxidative carbonylation of alcohols
US4447638A (en) * 1982-08-02 1984-05-08 Atlantic Richfield Company Preparation of dialkyl oxalates by the oxidative carbonylation of alcohols with a heterogeneous Pd-V-P-Ti containing catalyst system
US4451666A (en) * 1982-08-06 1984-05-29 Atlantic Richfield Company Synthesis of oxalate esters by the oxidative carbonylation of alcohols with a heterogeneous manganese promoted Pd-V-P catalyst
US4447639A (en) * 1982-08-06 1984-05-08 Atlantic Richfield Company Oxidative carbonylation of alcohols to dialkyl oxalates using a heterogeneous iron promoted Pd-V-P catalyst
US4487958A (en) * 1982-09-30 1984-12-11 Union Carbide Corporation Process for preparing a diester of oxalic acid
DE3342291A1 (en) * 1983-11-23 1985-05-30 Röhm GmbH, 6100 Darmstadt METHOD FOR PRODUCING OXAL ACID DIESTERS
CN108003020A (en) * 2017-12-27 2018-05-08 山东汇海医药化工有限公司 A kind of method for preparing diethy-aceto oxalate as solvent with toluene

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3393136A (en) * 1965-09-28 1968-07-16 Union Oil Co Preparation of oxalates
DE2213435A1 (en) * 1972-03-20 1973-10-11 Roehm Gmbh Oxalic acid (ester) prepn - from carbon monoxide and oxygen
US3994960A (en) * 1974-04-05 1976-11-30 Ube Industries, Ltd. Process for preparing dialkyl oxalates
JPS536369B2 (en) * 1974-11-22 1978-03-07
JPS51157311U (en) * 1975-06-06 1976-12-15

Also Published As

Publication number Publication date
BR7704905A (en) 1978-04-11
FR2359812A1 (en) 1978-02-24
CA1093580A (en) 1981-01-13
JPS5542058B2 (en) 1980-10-28
NL178684C (en) 1986-05-01
DE2733730B2 (en) 1981-05-07
FR2359812B1 (en) 1983-03-18
NL7708262A (en) 1978-01-31
IT1080789B (en) 1985-05-16
DE2733730A1 (en) 1978-02-02
GB1532402A (en) 1978-11-15
DE2733730C3 (en) 1982-04-08
IN145087B (en) 1978-08-19
NL178684B (en) 1985-12-02
US4138587A (en) 1979-02-06

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