JPH1190218A - Irregular packing for vapor-liquid contact - Google Patents

Irregular packing for vapor-liquid contact

Info

Publication number
JPH1190218A
JPH1190218A JP9251572A JP25157297A JPH1190218A JP H1190218 A JPH1190218 A JP H1190218A JP 9251572 A JP9251572 A JP 9251572A JP 25157297 A JP25157297 A JP 25157297A JP H1190218 A JPH1190218 A JP H1190218A
Authority
JP
Japan
Prior art keywords
gas
plate
packing
liquid contact
filling
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP9251572A
Other languages
Japanese (ja)
Inventor
Reiji Ikawa
玲二 伊川
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TOKYO TOKUSHU KANAAMI KK
Original Assignee
TOKYO TOKUSHU KANAAMI KK
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by TOKYO TOKUSHU KANAAMI KK filed Critical TOKYO TOKUSHU KANAAMI KK
Priority to JP9251572A priority Critical patent/JPH1190218A/en
Publication of JPH1190218A publication Critical patent/JPH1190218A/en
Pending legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/30Loose or shaped packing elements, e.g. Raschig rings or Berl saddles, for pouring into the apparatus for mass or heat transfer
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/30Details relating to random packing elements
    • B01J2219/302Basic shape of the elements
    • B01J2219/30223Cylinder
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/30Details relating to random packing elements
    • B01J2219/302Basic shape of the elements
    • B01J2219/30257Wire
    • B01J2219/30265Spiral

Landscapes

  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Gas Separation By Absorption (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

PROBLEM TO BE SOLVED: To economically form an irregular filler packing of a shape which allow an intentional arrangement of a condition in some extent and to improve productivity. SOLUTION: A coil-shaped packing main body 2 is formed by winding clockwisely or counterclockwisely a belt-like sheet member 1 with a definite width. A definite facing gap 3 is formed in the axial direction of the coil-shaped packing from both side edges of the sheet-like member 1 forming this packing main body 2. This facing gap 3 is made the same or smaller than the width of the sheet-like member 1. In addition, the length of the filler main body 2 in the axial direction is formed larger than the outer diameter. In addition, clockwisely wound packing main bodies 2 and counterclockwisely wound packing main bodies 2 are mixed by a ratio being close to the same and are packed into a vapor-liq. contacting device. In addition, it is possible to have pref. packed condition and excellent vapor-liq. contacting performance even when the irregular fillers are randomly packed in the vapor-liq. contacting device.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【産業上の利用分野】本発明は、蒸留設備、吸収設備、
冷水設備、水処理設備などの気液接触装置内に不規則に
充填し、気体と液体とを接触させて物質移動、熱移動、
化学反応を単独または何れかを組み合わせた処理、ある
いは全ての処理を同時に行わせるための気液接触用不規
則充填物に係るものである。
The present invention relates to a distillation facility, an absorption facility,
Irregular filling in gas-liquid contacting equipment such as chilled water equipment, water treatment equipment, etc.
The present invention relates to an irregular packing for gas-liquid contact for performing a chemical reaction singly or in any combination thereof, or performing all the processes simultaneously.

【0002】[0002]

【従来の技術】従来、蒸留設備、吸収設備、冷水設備、
水処理設備などの気液接触装置内に気液接触用の充填物
を充填し、気体と液体とを接触させて物質移動、熱移
動、化学反応などを単独または何れかを組み合わせた処
理、あるいは全ての処理を同時に行わせる方法があっ
た。この気液接触用充填物には、気液接触装置内の空間
で各々の充填物の方向や相互の位置関係を考慮せずに、
無秩序に挿入して充填する不規則充填物と、気液接触装
置内部で規則的な配置となるよう、気液接触装置への充
填以前に予め整然とした充填物の集合体として製造する
規則充填物とが存在する。
2. Description of the Related Art Conventionally, distillation equipment, absorption equipment, chilled water equipment,
Filling a gas-liquid contacting material in a gas-liquid contacting device such as a water treatment facility, and contacting a gas and a liquid to perform mass transfer, heat transfer, chemical reaction, etc., alone or in combination, or There was a method in which all processes were performed simultaneously. In this space for gas-liquid contact, without considering the direction and mutual positional relationship of each space in the space inside the gas-liquid contact device,
Ordered packing that is produced as an aggregate of random packing that is randomly inserted and filled, and that is pre-ordered before filling into the gas-liquid contact device so that it is regularly arranged inside the gas-liquid contact device. And exists.

【0003】そして、不規則充填物には、ラシヒリング
やポールリングなどに代表される多くの種類が存在し
て、古くから蒸留塔などの気液接触装置内部での気体と
液体との接触面積を提供する手段として広く利用されて
きた。また、気液接触装置内部での気体と液体の双方の
流動状態は、個々の充填物の向きや充填物相互の位置関
係によって大きく影響される。そして、気液接触装置全
体としての気液接触性能は、充填物の空隙率や表面積、
充填物と気液との接触面積、流通速度、圧力損失率な
ど、様々な要因が気液の流動状態に総合的に作用して決
定されるものである。
[0003] There are many types of irregular packing such as Raschig rings and Paul rings, and the contact area between a gas and a liquid inside a gas-liquid contacting device such as a distillation column has long been known. It has been widely used as a means of providing. In addition, the flow state of both gas and liquid inside the gas-liquid contact device is greatly affected by the direction of individual packings and the positional relationship between the packings. The gas-liquid contact performance of the entire gas-liquid contact device is determined by the porosity and surface area of the filler,
Various factors, such as the contact area between the filler and the gas-liquid, the flow rate, and the pressure loss rate, are determined by comprehensively acting on the flow state of the gas-liquid.

【0004】[0004]

【発明が解決しようとする課題】しかしながら、不規則
充填物は、装置内に不規則で無秩序に充填されるため、
充填物相互の位置関係が場所によって異なる事により、
空隙率も場所によって異なるものとなる。このように、
不規則充填物では、充填物の全てを装置内に理想的に配
置させる事は原理的に困難である。そして、このような
不均一な充填状態では、気液の流動に偏りが生じ、気液
接触装置内で理想的な流動状態を期待する事が困難であ
った。そのため、従来の不規則充填物を用いた装置で
は、高い気液接触性能を実現するには限度があった。
However, since the random packing is irregularly and randomly filled in the apparatus,
Due to the fact that the positional relationship between the packings differs depending on the location,
The porosity also varies depending on the location. in this way,
With random packing, it is in principle difficult to ideally place all of the packing in the apparatus. In such a non-uniform filling state, the gas-liquid flow is biased, and it is difficult to expect an ideal flow state in the gas-liquid contact device. For this reason, there is a limit in realizing high gas-liquid contact performance in a conventional apparatus using random packing.

【0005】そこで、近年このような無秩序な配置の充
填状態に起因する気液接触性能の低下を防ぐため、充填
物の全てが均一な充填状態となるように構成した規則充
填物が普及している。この規則充填物は、装置内部で理
想的な配置となるよう所定体積の充填物を予め構造的に
一体化させたブロック単位に製造されて、これらの複数
のブロックが整然とした集合体として装置内部に充填さ
れるものとなる。
In order to prevent the gas-liquid contact performance from being reduced due to the disordered arrangement of the packing state in recent years, a structured packing in which all of the packings are in a uniform filling state has been widely used. I have. This ordered packing is manufactured in a block unit in which a predetermined volume of packing is structurally integrated in advance so as to have an ideal arrangement inside the apparatus, and these blocks are arranged in an orderly assembly inside the apparatus. Will be filled.

【0006】上記の如き規則充填物は、多くの工程を経
て製造されるとともに、使用する装置個々の形状に合わ
せて加工するため、製造方法が複雑となる。そのため、
規則充填物の製造設備が大規模となり、大量生産の場合
に於いては経済性を発揮するが、塔径が小さい気液接触
装置向けなどの少量生産の場合に於いては、製造費が割
高なものとなる。
[0006] The ordered packing as described above is manufactured through many steps, and is processed according to the shape of each device to be used, so that the manufacturing method becomes complicated. for that reason,
Large-scale production equipment for structured packing is economical in large-scale production, but production costs are high in small-volume production for gas-liquid contactors with small tower diameters. It becomes something.

【0007】一方、不規則充填物は、ブロック化などを
行わず、一個一個が独立しているため、規模の大小に関
わらず比較的容易に製造できる。また、規則充填物は、
気液接触装置内部で理想的な充填状態が実現できるた
め、高い気液接触性能を期待できるが、その反面、製造
法に起因する不経済性、個々の使用条件での不適性さな
ど、様々な問題点がある。そのため、規則充填物が、必
ずしも全てに於いて不規則充填物よりも優れている訳で
はない。
[0007] On the other hand, the random packing is independent of each other without being blocked, so that it can be manufactured relatively easily regardless of the size of the scale. In addition, ordered packing is
Since the ideal filling state can be realized inside the gas-liquid contact device, high gas-liquid contact performance can be expected, but on the other hand, various factors such as uneconomical due to the manufacturing method, unsuitability under individual use conditions, etc. Problems. As a result, ordered packings are not necessarily all superior to random packings.

【0008】また、他の従来例として、特開平8−11
0118号公報記載の如き充填物が存在する。この充填
物は、ステンレス細線を圧延して板状部材を形成し、こ
の板状部材をカール加工した後に、一定方向にコイル状
に複数回巻廻した後、この帯状のコイル状板状部材を互
いに絡ませる事により、ステンレススポンジの如き塊状
の充填物本体を形成するものである。これを気液接触装
置に充填することにより、規則充填物の如き均一な充填
状態を実現する事ができるとともに、低価格に製品を得
る事ができる。
Another conventional example is disclosed in Japanese Patent Application Laid-Open No. 8-11 / 1996.
There is a filler as described in 0118. This filler is formed by rolling a stainless steel thin wire to form a plate-like member, curling the plate-like member, winding it in a coil in a predetermined direction a plurality of times, and then removing the band-like coil-like plate-like member. By being entangled with each other, a lump-shaped filler body such as a stainless sponge is formed. By filling this into a gas-liquid contact device, a uniform filling state such as structured packing can be realized, and a product can be obtained at low cost.

【0009】しかし、この充填物では、ステンレス細線
を圧延したり、カール加工を施す等の作業があり、手間
や技術を要して、生産性に欠けるものであった。また、
帯状のコイル状板状部材が、互いに絡みあいながら、コ
イルの内部に入り込んでいるので、空隙率が減少した
り、偏流を生じ易い不均一な充填状態となる。そのた
め、良好な気液の流通や接触が行えなくなり、圧力降下
や気液接触効率の低下を生じるものとなる。
[0009] However, with this filling, there are operations such as rolling a stainless fine wire and performing a curling process, which requires labor and technology, and lacks productivity. Also,
Since the band-shaped coil-shaped plate-like members are entangled with each other and enter the inside of the coil, the porosity is reduced and an uneven filling state is liable to occur. Therefore, good gas-liquid distribution and contact cannot be performed, resulting in a pressure drop and a decrease in gas-liquid contact efficiency.

【0010】従って、不規則充填物のように比較的容易
に製造でき、しかも規則充填物の充填特性をある程度兼
ね備えた充填物が実現できれば望ましいものである。す
なわち、生産量に関わらず常に容易に製造でき、しかも
気液接触装置内部での充填状態をある程度秩序立てて充
填可能として、充填状態の無秩序さに起因する性能の劣
化を最小限にできれば、価格及び性能の両面が均衡し
て、優れた充填物となり得る。
Therefore, it would be desirable to be able to produce a packing that is relatively easy to manufacture, such as an irregular packing, and that has some of the packing characteristics of the structured packing. In other words, if it can be easily manufactured at all times regardless of the production volume and the filling state inside the gas-liquid contact device can be filled to some degree in order, and the deterioration of performance due to disorder in the filling state can be minimized, And both performance and performance can be balanced to provide an excellent packing.

【0011】本発明は上述の如き課題を解決しようとす
るものであって、不規則充填物を無秩序に充填しても、
気液接触装置内部で、ある程度充填状態を意図的に配置
可能な形状で、経済的に形成する事を可能とするもので
ある。そのため、円筒形の不規則充填物を、直径に対し
て円筒の形成長さの比率を相対的に大きく形成する事に
より、重心を高位置に移動して倒れ易く形成する。その
結果、不規則充填物の多くを円筒軸が水平または傾斜し
た状態で配置させる事ができ、無秩序な充填状態をある
程度緩和する事が可能となるものである。しかも、この
ような配置状態に於いても十分な開放空間が確保されて
おり、不規則充填物を通過する気体の流通面積の減少が
ない。このため、圧力損失が少なくて、処理能力を低下
させる事のないような不規則充填物を得る事を可能とす
るものである。
[0011] The present invention is to solve the above-mentioned problems, and even if the irregular packing is randomly filled,
It is possible to economically form the inside of the gas-liquid contacting device in a shape capable of intentionally arranging the filling state to some extent. Therefore, by forming the cylindrical irregular packing material such that the ratio of the formation length of the cylinder to the diameter is relatively large, the center of gravity is moved to a high position to easily fall. As a result, most of the irregular packing can be arranged in a state where the cylindrical axis is horizontal or inclined, and the disordered filling state can be alleviated to some extent. In addition, a sufficient open space is ensured even in such an arrangement state, and there is no decrease in the flow area of the gas passing through the irregular packing. For this reason, it is possible to obtain an irregular packing which has a small pressure loss and does not lower the processing capacity.

【0012】また、従来は多数の不連続で複雑な工程で
構成していた不規則充填物の製造工程を、単純で工程数
の少ない方法で行い、生産速度の向上を目指すものであ
る。そして、上述の如き不規則充填物を得る事により、
気液接触装置内に無秩序に充填しても、好ましい充填状
態と優れた気液接触性能を実現しようとするものであ
る。
Another object of the present invention is to improve the production speed by performing a process for producing an irregular packing, which has conventionally been constituted by a large number of discontinuous and complicated processes, by a simple and small number of processes. And by obtaining the irregular packing as described above,
Even if the gas-liquid contacting device is randomly charged, it is intended to achieve a preferable filling state and excellent gas-liquid contact performance.

【0013】[0013]

【課題を解決するための手段】本発明は、上述の如き課
題を解決するため、一定幅を有する帯状の板状部材を複
数回右巻または左巻に巻廻してコイル状の充填物本体を
形成し、この充填物本体を形成する板状部材の両側縁
が、コイル状の軸方向に於いて一定の対向間隔を形成
し、この対向間隔を、板状部材の幅と同一または板状部
材の幅よりも小さく形成するとともに、充填物本体の軸
方向の長さを、外径よりも大きく形成したもので、この
右巻の充填物本体と左巻の充填物本体とを混合して気液
接触装置に充填して成るものである。
SUMMARY OF THE INVENTION In order to solve the above-mentioned problems, the present invention provides a coil-shaped filling body by winding a band-shaped plate member having a fixed width into a right-handed or left-handed plural times. The two side edges of the plate-like member forming the filling body form a constant opposing interval in the axial direction of the coil, and the opposing interval is the same as the width of the plate-shaped member or the plate-shaped member. The width of the packing body is smaller than the width of the packing body, and the length of the packing body in the axial direction is larger than the outer diameter of the packing body. It is formed by filling a liquid contact device.

【0014】また、板状部材は、金属材、プラスチック
材またはセラミック材の何れかにより形成しても良い。
Further, the plate member may be formed of any one of a metal material, a plastic material and a ceramic material.

【0015】また、板状部材は、広幅板状の金属材、ま
たは広幅板状のプラスチック材を複数にスリットして形
成しても良い。
The plate-like member may be formed by slitting a wide plate-like metal material or a wide plate-like plastic material into a plurality of slits.

【0016】また、板状部材は、平滑な平板状に形成し
ても良い。
Further, the plate member may be formed in a smooth flat plate shape.

【0017】また、板状部材は、網材により形成しても
良い。
The plate member may be formed of a net material.

【0018】また、板状部材は、表面に、凹凸、長穴、
小孔、溝の何れか一つまたは複数種を組み合わせて表面
加工を施したものであっても良い。
Further, the plate-shaped member has unevenness, a long hole,
Surface treatment may be performed by combining one or a plurality of small holes and grooves.

【0019】また、充填物本体は、外径に対する軸方向
の長さ比を、1.2〜3.0としても良い。
Further, the filling body may have an axial length ratio to the outer diameter of 1.2 to 3.0.

【0020】また、充填物本体は、板状部材を右巻に形
成したものと、板状部材を左巻に形成したものとを、
1.0:0.8〜1.0:1.2の割合で混合しても良
い。
[0020] The filler body includes a plate-shaped member formed into a right-handed form and a plate-shaped member formed into a left-handed form.
They may be mixed at a ratio of 1.0: 0.8 to 1.0: 1.2.

【0021】また、充填物本体は、板状部材を右巻に形
成したものと、板状部材を左巻に形成したものとを、一
定の比率で混合して充填するものであっても良い。
The filling body may be one in which a plate-shaped member formed into a right-handed form and a plate-shaped member formed into a left-handed form are mixed at a fixed ratio and filled. .

【0022】また、充填物本体は、板状部材の先端をコ
イルの内径内に折曲したものであっても良い。
Further, the filling body may be one in which the tip of a plate-like member is bent into the inside diameter of the coil.

【0023】[0023]

【作用】本発明は、上述の如く構成したものであるか
ら、この不規則充填物を蒸留設備、吸収設備、冷水設
備、水処理設備、その他の気液接触装置内に充填する
と、充填物本体は、軸方向の長さを外径よりも大きく形
成しているので、重心が高くなり横倒しとなり易いか
ら、無秩序に充填しても、気液接触装置内部で充填物本
体の軸が水平方向または傾斜方向に配置される割合が多
くなり、充填物本体の軸が垂直方向に配置される割合を
少なくする事ができ、ある程度秩序的に不規則充填物を
充填可能となる。そして、充填物本体は、外径に対する
軸方向の長さ比を、1.2〜3.0とする事により、上
述の如く充填物本体の軸が水平方向または傾斜方向に配
置され易くなるとともに、適度な充填密度で気液接触装
置内に配置されるものとなる。
Since the present invention is constructed as described above, when the irregular packing is filled in a distillation facility, an absorption facility, a chilled water facility, a water treatment facility, or another gas-liquid contacting device, the filling body is Since the length in the axial direction is larger than the outer diameter, the center of gravity is high and it is easy to fall down. The proportion arranged in the inclined direction increases, and the proportion of the axis of the filling body arranged in the vertical direction can be reduced, so that the irregular filling can be filled to some extent. And by setting the length ratio of the axial direction with respect to an outer diameter to 1.2-3.0, the axis | shaft of a filler main body becomes easy to arrange | position the axis | shaft of a filler main body in a horizontal direction or an inclined direction as mentioned above. , With a suitable packing density in the gas-liquid contact device.

【0024】ちなみに、充填物本体の軸が垂直方向に配
置される割合が多いと、気体の多くが、充填物本体の円
筒内部の空間に留まる事なく簡単に通過してしまう。ま
た、液体の大部分も、充填物本体の円筒内部に留まるこ
となく、円筒内を直ちに落下してしまい、充填物本体の
表面に十分に液体が付着しないものとなる。その結果、
充填物本体の表面に付着する液体と気体との接触頻度が
減少して、気液間での物質移動が十分に行われず、気液
接触能力が低下する。また、気液接触装置内で充填物本
体が互いに積み重なる事により発生する荷重で、コイル
状の充填物本体は軸方向に圧縮されて収縮し、充填容積
が局部的に減少するため不均一となり、充填状態を悪く
するものとなる。
By the way, if the proportion of the axis of the filling body in the vertical direction is large, most of the gas easily passes without remaining in the space inside the cylinder of the filling body. In addition, most of the liquid does not stay inside the cylinder of the filling body, but immediately falls in the cylinder, and the liquid does not sufficiently adhere to the surface of the filling body. as a result,
The frequency of contact between the liquid and the gas adhering to the surface of the packing body is reduced, so that mass transfer between the gas and liquid is not sufficiently performed, and the gas-liquid contact ability is reduced. In addition, due to the load generated by stacking of the packing bodies in the gas-liquid contact device, the coil-shaped packing body is compressed and shrunk in the axial direction, and the filling volume is locally reduced, and thus becomes non-uniform. This will make the filling state worse.

【0025】しかし、先述の如く、本発明の不規則充填
物は、充填物本体の軸が水平方向または傾斜方向に配置
される割合が多いから、良好な充填状態を実現できる。
また、充填による荷重は、円筒軸に対してほぼ垂直方向
に掛かるので、コイル状の充填物本体が圧縮されにく
く、充填容積の減少も抑えるものとなる。そして、気体
は充填物本体の板状部材の両側縁で形成される対向間隔
を通過して充填物本体の内部に流入する。この対向間隔
を通過して流入する際に、気体の分裂が起こり、その後
円筒内で再び合一化する。すなわち、対向間隔を介して
気体の頻繁な離合集散が起こる事により、気体の乱流が
発生し、液体との接触機会が増加するとともに、攪拌作
用の働きをして気液の接触状態を良好なものして気液間
の物質移動を促進するものとなる。また、この気体の離
合集散により、気体が気液接触装置内を一気に通過する
事がなく、充填物本体内部での滞留時間が長くなる事
も、気液の接触頻度を向上させるものとなる。
However, as described above, the random packing of the present invention can achieve a good filling state because the axis of the packing main body is arranged in a horizontal direction or an inclined direction in many cases.
Further, since the load due to the filling is applied in a direction substantially perpendicular to the cylindrical axis, the coil-shaped filling body is hardly compressed, and the reduction of the filling volume is suppressed. Then, the gas flows into the inside of the filling body through the opposing gaps formed on both side edges of the plate-shaped member of the filling body. As it flows past this opposing distance, the gas splits and then coalesces again in the cylinder. In other words, frequent convergence of the gas through the opposing interval causes turbulence of the gas, increasing the chances of contact with the liquid and acting as a stirring function to improve the gas-liquid contact state. This promotes mass transfer between gas and liquid. In addition, due to the separation and collection of the gas, the gas does not pass through the gas-liquid contact device at a stretch, and the residence time inside the filling body is prolonged. This also improves the frequency of gas-liquid contact.

【0026】また、従来のラシヒリングやポールリング
は、外周面の開放部分が限定されるため、円筒軸を水平
または傾斜して配置すると、気体が流通可能な空隙が殆
ど形成されず、気体の圧力損失が増大し、処理能力が低
下する事がある。本発明の充填物本体も、気体は板状部
材の表面に突き当たる事により、流動抵抗が増加し、圧
力損失が増加する懸念がある。しかし、充填物本体に
は、対向間隔を形成しているので、処理に支障を来す程
の圧力損失は発生せず、気液接触の処理能力に優れた不
規則充填物を得る事が可能となる。
In the conventional Raschig ring or pole ring, since the open portion of the outer peripheral surface is limited, if the cylindrical shaft is arranged horizontally or inclined, a gap through which gas can flow is hardly formed, and the gas pressure is reduced. Losses may increase and throughput may decrease. In the packing body of the present invention as well, there is a concern that the gas may impinge on the surface of the plate member, thereby increasing the flow resistance and increasing the pressure loss. However, since the packing body has an opposing space, there is no pressure loss that would hinder the processing, and it is possible to obtain irregular packing with excellent gas-liquid contact processing ability. Becomes

【0027】一方、液体も気液接触装置内を一気に流れ
落ちるのではなく、板状部材に突き当たった後、板状部
材の表面を分散しながら対向間隔を通過して、一定時間
を経て滴下するものとなる。そのため、板状部材の水平
面や傾斜面に於ける濡れ面積を増加させて、気液の有効
接触面積を増加させるものとなる。また、対向間隔での
分散効果により、気液接触装置内に於いて、液体は一点
に集中して流動したり、一気に落下する事がなく、板状
部材表面を均一に一定時間を経過して流動するものとな
る。そして、良好に液体の付着した充填物本体を、乱流
状態の気体が通過する事により、効率的に気液の接触が
起こり、物質移動が促進されるものとなる。
On the other hand, the liquid does not flow down all at once in the gas-liquid contacting device, but hits the plate-like member and then drops over a certain time after passing through the facing space while dispersing the surface of the plate-like member. Becomes Therefore, the wet area on the horizontal surface or the inclined surface of the plate-like member is increased, and the effective contact area between gas and liquid is increased. In addition, due to the dispersion effect at the opposing interval, the liquid does not flow at a single point in the gas-liquid contact device and does not drop at a stroke, and the surface of the plate-like member is uniformly moved for a certain period of time. It will flow. When the gas in the turbulent state passes through the packing body to which the liquid is well attached, gas-liquid contact occurs efficiently, and mass transfer is promoted.

【0028】また、充填物本体の板状部材の両側縁で形
成される対向間隔を、板状部材の幅よりも大きく形成す
ると、充填物本体の単位面積当たりの表面積が減少し
て、気液接触機能が低下したり、充填物本体の耐荷重強
度が低下し、充填状態を悪化させるものとなる。更に、
充填物本体は、コイル状に形成しているので、充填時の
振動や気液の通過による衝撃などで、一方の充填物本体
の対向間隔内に、他方の充填物本体の板状部材が入り込
んで、充填物本体が互いに絡み合って一体化してしまう
事もある。そして、多数の充填物本体が次々と結合して
団塊状となり、充填容積を減少させたり、不均一な充填
となったりする事が考えられる。
Further, if the opposing interval formed on both side edges of the plate-like member of the filling body is formed to be larger than the width of the plate-like member, the surface area per unit area of the filling body decreases, and gas-liquid The contact function is reduced, the load-bearing strength of the filling body is reduced, and the filling state is deteriorated. Furthermore,
Since the filling body is formed in a coil shape, the plate-like member of the other filling body enters into the facing space of one filling body due to vibration at the time of filling or impact due to passage of gas-liquid. In some cases, the filler bodies are entangled with each other and integrated. Then, it is conceivable that a large number of filler bodies are successively combined to form a nodular shape, thereby reducing the filling volume or causing uneven filling.

【0029】しかし、本発明の充填物本体は、対向間隔
を、板状部材の幅と同一または板状部材の幅より小さく
形成しているので、一方の充填物本体の対向間隔に他方
の充填物本体の板状部材が入り込みにくいものとなり、
絡み合いから生じる充填容積の減少を防いで良好な充填
状態を実現する事が可能となる。ただし、対向間隔が狭
すぎると、外周面の開放部分が限定され気液の流動抵抗
が高くなり、圧力降下を引き起こして、気液の接触能力
が低下する虞れがあるので、好ましくは対向間隔を、板
状部材の幅の3分の1以上で同幅以下とするのが良い。
However, in the packing body of the present invention, the opposing interval is formed to be equal to or smaller than the width of the plate-shaped member. It becomes difficult for the plate-shaped member of the object body to enter,
It is possible to realize a good filling state while preventing a decrease in the filling volume caused by entanglement. However, if the facing distance is too narrow, the open portion of the outer peripheral surface is limited and the gas-liquid flow resistance increases, causing a pressure drop, which may reduce the gas-liquid contact ability. Is preferably not less than one third and not more than the width of the plate-shaped member.

【0030】また、上述の如き対向間隔で充填物本体を
形成した場合でも、右巻の充填物本体のみ、あるいは左
巻の充填物本体のみを気液接触装置に充填すると、振動
などで回転するうちに、一方の充填物本体が隣接する他
方の充填物本体の内部に入り込んで絡み合い、気液接触
装置全体の充填容積を減少させるものとなる。しかし、
本発明では、充填物本体は、板状部材を右巻に形成した
ものと、板状部材を左巻に形成したものとを、一定の比
率で混合して気液接触装置に充填しているので、互いに
反対方向に巻廻した充填物同志が接触する確率が高くな
り、巻廻し方向が交差するので互いに絡まりにくいもの
となる。そして、充填容積が減少する事のない良好な充
填状態を実現可能となる。また、この右巻と左巻の充填
物本体の混合割合は、1.0:0.8〜1.0:1.2
で行うのが好ましく、1.0:1.0に近くなる程、同
方向に巻廻した充填物本体同志が隣接する確率が低くな
り、更に絡まりにくいものとなる。
Even when the packing bodies are formed at the opposed intervals as described above, if only the right-handed packing body or only the left-handed packing body is filled in the gas-liquid contact device, it rotates by vibration or the like. At this time, one of the filling bodies enters into the adjacent one of the other filling bodies and becomes entangled with each other, thereby reducing the filling volume of the entire gas-liquid contact device. But,
In the present invention, the filling body is formed by mixing a plate-shaped member formed into a right-handed form and a plate-shaped member formed into a left-handed form at a fixed ratio and filling the mixture into a gas-liquid contact device. Therefore, the probability that the packing materials wound in opposite directions contact each other is increased, and the winding directions intersect with each other, so that the packing materials are hardly entangled with each other. Then, it is possible to realize a good filling state without reducing the filling volume. The mixing ratio of the right-handed and left-handed filling bodies is 1.0: 0.8 to 1.0: 1.2.
The closer to 1.0: 1.0, the lower the probability of adjacent packing bodies wound in the same direction being adjacent to each other, and the more difficult it is for them to be entangled.

【0031】また、充填物本体が絡み合うのは、一方の
板状部材の先端の内側に、他方の板状部材の先端が侵入
し、振動などの刺激が加わる事により徐々に絡んでいく
可能性があるので、板状部材の先端をコイルの内径内に
折曲すれば、隣り合った充填物本体の各々の先端が互い
に接触することがないので、互いの絡み合いを防止する
効果がより向上するものとなる。
Further, the filler body may become entangled with the tip of one plate-like member, and the tip of the other plate-like member may penetrate into the body, and may gradually become entangled by stimulation such as vibration. Therefore, if the tip of the plate-shaped member is bent within the inner diameter of the coil, the tips of the adjacent filler bodies do not come into contact with each other, and the effect of preventing entanglement with each other is further improved. It will be.

【0032】また、板状部材は、金属材、プラスチック
材またはセラミック材で形成すれば、切り取ったり、コ
イル状に成形する作業を容易に行う事が可能であり、耐
荷重性に優れた充填物本体を、廉価に形成する事ができ
る。
If the plate-like member is formed of a metal material, a plastic material or a ceramic material, it is possible to easily cut or form it into a coil shape, and to provide a filling material excellent in load resistance. The main body can be formed inexpensively.

【0033】また、板状部材は、平滑な平板状に形成す
れば、加工作業が単純で製造コストが廉価なものとな
る。また、板状部材は、網材により形成すれば、気液が
網目を通過する事により、気液の分散効果が高くなる。
更に、網材はそれ自体に濡れ効果があるため、液体の板
状部材への滞留量が増加し、気液接触性能を向上させる
事が可能となる。
Further, if the plate-like member is formed into a smooth flat plate, the working operation is simple and the production cost is low. Further, if the plate-like member is formed of a mesh material, the gas-liquid dispersion effect is enhanced by the gas-liquid passing through the mesh.
Further, since the net material itself has a wetting effect, the amount of liquid staying in the plate-like member increases, and the gas-liquid contact performance can be improved.

【0034】また、板状部材は、表面に、凹凸、長穴、
小孔、溝の何れか一つまたは複数種を組み合わせて表面
加工を施せば、平板状に形成したり、網材を使用して形
成するよりも手間はかかるが、気液の分散能力を向上さ
せたり、板状部材の表面積を拡大する事が可能となる。
そして、板状部材の表面への液体の濡れ効果による有効
接触面積の増大を計り、効率的な気液接触を可能とす
る。
The plate-like member has a surface with irregularities, slots,
If surface treatment is performed by combining one or more of small holes and grooves, it takes more time than forming a flat plate or using a net material, but improves the gas-liquid dispersion capacity. Or increase the surface area of the plate-shaped member.
The effective contact area is increased by the liquid wetting effect on the surface of the plate-shaped member, and efficient gas-liquid contact is enabled.

【0035】[0035]

【実施例】以下、本発明の一実施例を図面に於て説明す
れば、(1)は板状部材で、厚さ0.2mmの広幅のステ
ンレス板材を、幅3.0mmにスリット加工して形成し
ている。そして、この板状部材(1)を、外径が15.0
mmとなるように4回右巻に巻廻して、図1に示す如
く、軸方向の長さを27.0mmとするコイル状の充填
物本体(2)を形成している。従って、外径よりも軸方向
の長さが長尺となり、外径に対する軸方向の長さ比は、
1.8倍となる。また、充填物本体(2)は、コイル状に
巻廻した板状部材(1)の両側縁により、図2に示す如
く、軸方向に一定の対向間隔(3)を形成しているが、こ
の対向間隔(3)を、板状部材(1)と同幅の3.0mmと
している。
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS An embodiment of the present invention will be described below with reference to the drawings. (1) is a plate-like member which is formed by slitting a wide stainless steel plate having a thickness of 0.2 mm to a width of 3.0 mm. It is formed. Then, this plate-shaped member (1) is made to have an outer diameter of 15.0.
As shown in FIG. 1, a coil-shaped filling main body (2) having a length of 27.0 mm in the axial direction is formed as shown in FIG. Therefore, the axial length becomes longer than the outer diameter, and the axial length ratio to the outer diameter is:
1.8 times. Further, as shown in FIG. 2, the filling body (2) forms a constant opposing interval (3) in the axial direction by both side edges of the plate-like member (1) wound in a coil shape. The facing interval (3) is set to 3.0 mm which is the same width as the plate-like member (1).

【0036】このように、ステンレス板材をスリット加
工して板状部材(1)を形成する第1工程と、この板状部
材(1)をコイル状に巻廻す第2工程と、コイル状の板状
部材(1)を一定の長さで次々と切断する第3工程とによ
り、不規則充填物(4)の製造工程を構成している。第1
工程のスリット加工による板状部材(1)の形成は、連続
して作業が可能であり、大量のものを一度にかつ簡単に
形成できる。また、第2工程と第3工程は、板状部材
(1)をコイル状に巻廻しながら、同時にこのコイル状の
板状部材(1)を所定の長さに次々と切断すれば、作業を
一体化させ、連続的に充填物本体(2)を製造する事がで
きる。その結果、不規則充填物(4)の製造を一連の作業
で簡単に行う事ができ、生産効率が向上するものとな
る。しかも、各々の作業工程は何れも単純で高価な設備
も不要であるので、コスト削減効果が大きいものとな
る。
As described above, the first step of forming the plate member (1) by slitting the stainless plate material, the second step of winding the plate member (1) in a coil shape, The third step of cutting the shaped member (1) one after another at a constant length constitutes a step of producing the irregularly packed material (4). First
The formation of the plate-like member (1) by the slit processing in the process can be performed continuously, and a large number of the members can be formed at once and easily. Further, the second step and the third step include a plate-shaped member.
While winding (1) in a coil shape and simultaneously cutting the coil-shaped plate-shaped member (1) one after another to a predetermined length, the work is integrated and the filling body (2) is continuously formed. Can be manufactured. As a result, the production of the irregular packing (4) can be easily performed in a series of operations, and the production efficiency is improved. In addition, since each work process is simple and does not require expensive equipment, the cost reduction effect is large.

【0037】また、充填物本体(2)の、他の異なる製造
方法として、一個分の充填物本体(2)に要する長さに相
当するステンレス板材を用意する。そして、第1工程で
このステンレス板材を幅方向に細くスリット加工して、
一個分の板状部材(1)を得る。その後、第2工程でこの
板状部材(1)をコイル状に巻廻して充填物本体(2)を得
る。この方法だと、コイル状の板状部材(1)を充填物本
体(2)ごとに一個一個切り離す作業を省略して、製造方
法を簡略化する事ができる。
As another different method of manufacturing the packing body (2), a stainless steel plate material corresponding to the length required for one packing body (2) is prepared. Then, in the first step, this stainless steel plate is slit into a narrow width direction,
One plate-like member (1) is obtained. Thereafter, in a second step, the plate-like member (1) is wound in a coil shape to obtain a filling body (2). According to this method, the operation of separating the coil-shaped plate-like members (1) one by one for each filling body (2) can be omitted, and the manufacturing method can be simplified.

【0038】また、上記の如き右巻の充填物本体(2a)
と同様の素材、寸法及び製造工程で、左巻に板状部材
(1)を巻廻して、図3に示す如く、左巻の充填物本体
(2b)を形成する。
The right-handed filling body (2a) as described above
With the same material, dimensions and manufacturing process as in
(1) is wound, and as shown in FIG.
(2b) is formed.

【0039】そして、上述の如く形成した不規則充填物
(4)を、気液接触装置(図示せず)に適宜に充填する。こ
の充填は、右巻の充填物本体(2a)と左巻の充填物本体
(2b)とを1.0:1.0の割合で均一に混合する事に
より行っている。ちなみに、充填物本体(2)の軸が、垂
直方向に配置されると、充填の荷重により、コイル状の
充填物本体(2)は長さ方向に収縮してしまい、気液接触
装置全体の充填容積を減少させてしまうが、本発明の充
填物本体(2)は、軸方向の長さを外径よりも大きく形成
しているので、重心が高くなり、横倒しとなって気液接
触装置内部では、図4に示す如く、充填物本体(2)の軸
が水平方向あるいは傾斜方向に配置されるものとなる。
そして、充填物本体(2)は、円筒の幅方向の耐荷重性に
優れているから、充填による荷重で充填物本体(2)が潰
れる事がなく、荷重によって充填状態が変化する事はな
いものとなる。
Then, the irregular packing formed as described above
(4) is appropriately filled in a gas-liquid contact device (not shown). This filling is performed by a right-handed packing body (2a) and a left-handed packing body.
(2b) is uniformly mixed at a ratio of 1.0: 1.0. By the way, if the axis of the filling body (2) is arranged in the vertical direction, the filling load causes the coil-shaped filling body (2) to shrink in the length direction, and the entire gas-liquid contact device becomes Although the filling volume is reduced, the filling body (2) of the present invention is formed so that the length in the axial direction is larger than the outer diameter, so that the center of gravity is increased, and the gas-liquid contact device is turned over. Inside, as shown in FIG. 4, the axis of the filling body (2) is arranged in a horizontal direction or an inclined direction.
And since the filling main body (2) is excellent in load resistance in the width direction of the cylinder, the filling main body (2) does not collapse due to the load due to filling, and the filling state does not change due to the load. It will be.

【0040】また、充填物本体(2)は、板状部材(1)の
対向間隔(3)を、板状部材(1)の幅と同一または小さく
形成しているので、充填時の振動などの刺激を受けて
も、この対向間隔(3)に、隣接する他の充填物本体(2)
の板状部材(1)が侵入して、互いに入れ込むような不具
合を解消する事ができる。更に、右巻の充填物本体(2
a)と左巻の充填物本体(2b)とを1.0:1.0の割
合で混合しているので、コイル巻廻し方向が異なるもの
同志が隣接する可能性が高い。すると、巻廻し方向が相
対するので、この隣接する充填物本体(2)が互いに入れ
込むのを、より効果的に防ぎ、多数が団塊状となる事の
ない良好な充填状態を実現するものとなる。
Further, in the filling body (2), the opposing interval (3) of the plate-like member (1) is formed to be the same as or smaller than the width of the plate-like member (1). Even if it receives the stimulus of this, in this opposed space (3), the other filling body (2)
The inconvenience that the plate-shaped members (1) intrude and enter each other can be solved. In addition, the right-hand packing body (2
Since a) and the left-handed filling body (2b) are mixed at a ratio of 1.0: 1.0, there is a high possibility that two coils having different coil winding directions are adjacent to each other. Then, since the winding directions are opposite to each other, it is possible to more effectively prevent the adjacent filling bodies (2) from entering each other, and to realize a good filling state in which a large number does not become a lump. Become.

【0041】そして、上述の如く不規則充填物(4)を充
填した気液接触装置に於いて、気液接触を行うと、気体
は、コイル状の板状部材(1)に突き当たる事により、流
動抵抗が生じるが、対向間隔(3)による流通路を設けて
いるので、圧力損失を引き起こす事なく、この対向間隔
(3)を通過して攪拌されながら、充填物本体(2)の内部
に流動する。また、この対向間隔(3)が広すぎると、充
填物本体(2)内部を気体が流動抵抗を受ける事なく迅速
に通過してしまい、気液接触能力が低下する虞れがあ
る。
When the gas-liquid contact is performed in the gas-liquid contact device filled with the irregular packing (4) as described above, the gas hits the coil-shaped plate-like member (1). Although flow resistance is generated, since the flow path is provided by the opposed distance (3), the opposed distance can be reduced without causing a pressure loss.
While passing through (3) and being stirred, it flows into the inside of the filling body (2). On the other hand, if the facing distance (3) is too wide, the gas will quickly pass through the inside of the filling body (2) without receiving the flow resistance, and the gas-liquid contact capability may be reduced.

【0042】また、対向間隔(3)が狭すぎると、流動抵
抗が高くなり、気体の圧力損失が著しいものとなり、や
はり気液接触能力が低下する。しかし、本実施例では、
対向間隔(3)を板状部材(1)と同一幅に形成して充填物
本体(2)の表面積の半分程度とする事により、気体は適
度な流動抵抗を受けながら、充填物本体(2)内部を通過
するので、充填物本体(2)内部で十分に攪拌されて、液
体との接触機会を増大させ、しかも気体の圧力損失も良
好に抑える効果を得るものとなる。
On the other hand, if the facing distance (3) is too narrow, the flow resistance increases, the pressure loss of the gas becomes remarkable, and the gas-liquid contacting ability also decreases. However, in this embodiment,
By forming the facing gap (3) to be the same width as the plate-like member (1) and about half the surface area of the packing body (2), the gas receives moderate flow resistance, and ) Since the gas passes through the inside of the packing body (2), the inside of the packing body (2) is sufficiently agitated, so that the chance of contact with the liquid is increased and the pressure loss of the gas is effectively suppressed.

【0043】また、コイル状の対向間隔(3)により、気
体は分裂して充填物本体(2)内部に流入し、この内部で
再び一体化した後、再び対向間隔(3)から分散されて流
出する。この気体の頻繁な離合集散により、気体の乱流
が生じる。そして、この乱流が攪拌作用の働きをして、
気液の接触による物質移動、熱移動、化学反応を効率的
に促進するものとなる。
Further, the gas is divided by the coil-shaped opposing interval (3), flows into the inside of the filling body (2), and is integrated again therein, and then dispersed again from the opposing interval (3). leak. This frequent separation and dispersion of the gas causes turbulence of the gas. And this turbulence acts as a stirring action,
It effectively promotes mass transfer, heat transfer, and chemical reaction by gas-liquid contact.

【0044】また、液体は、板状部材(1)の表面を流動
したり、流通間隔(3)で流通経路を分散されながら、充
填物本体(2)内に流入する。そのため、液体は一気に流
れ落ちるのではなく、一定時間を経過しながら気液接触
装置内を流動するものとなり、気体との接触頻度が多く
なる。更に、充填物本体(2)は軸が水平または傾斜して
配置されているので、板状部材(1)の表面に液体が付着
し易くなるし、この表面に長く滞留して、気液接触に有
効な濡れ表面積を増加させるものとなる。
The liquid flows into the packing body (2) while flowing on the surface of the plate-like member (1) or while being dispersed in the circulation path at the circulation interval (3). Therefore, the liquid does not flow down at once, but flows through the gas-liquid contact device while a certain period of time passes, and the frequency of contact with the gas increases. Further, since the filling body (2) is arranged with its axis being horizontal or inclined, the liquid easily adheres to the surface of the plate-like member (1), stays on this surface for a long time, and comes into contact with gas-liquid. This increases the effective wetting surface area.

【0045】また、上記第1実施例の充填物本体(2)
は、対向間隔(3)を板状部材(1)と同一幅に形成した
り、巻廻し方向が異なるものを混在させて気液接触装置
に充填する事により、充填物本体(2)が互いに絡み合う
のを良好に防止している。しかし、同一方向に巻廻した
充填物本体(2)同志が隣接することも絶無とは言えず、
この場合は一方の板状部材(1)の先端が他方の板状部材
(1)の先端の内側に入り込み、この状態で振動などの刺
激が加わる事により、これらの充填物本体(2)が互いに
絡み合って一体化し、充填状態を悪くする可能性があ
る。
Further, the filling body (2) of the first embodiment is described.
By filling the gas-liquid contacting device with the facing space (3) having the same width as the plate-like member (1) or by mixing materials having different winding directions, the packing bodies (2) are Good prevention of entanglement. However, it cannot be said that the packing bodies (2) wound together in the same direction are adjacent to each other.
In this case, the tip of one plate-like member (1) is connected to the other plate-like member.
By entering the inside of the tip of (1) and applying a stimulus such as vibration in this state, there is a possibility that these filling bodies (2) are entangled and integrated with each other to deteriorate the filling state.

【0046】そのため、他の異なる第2実施例では、図
5に示す如く、板状部材(1)の両方の先端をコイルの内
径内に折曲して充填物本体(2)を形成している。する
と、充填物本体(2)の円筒同志が互いに接触しても、各
々の板状部材(1)の先端同志が接触する事がないので、
絡み合いを防止する効果が更に向上するものとなる。
尚、本実施例では、コイルの内径を15mmとしている
ので、この内径内に先端を配置可能とするために、板状
部材(1)を先端から10mmの長さで内側に折曲してい
る。
Therefore, in another different second embodiment, as shown in FIG. 5, both ends of the plate-like member (1) are bent into the inner diameter of the coil to form the filling body (2). I have. Then, even if the cylinders of the filler body (2) come into contact with each other, the tips of the plate-like members (1) do not come into contact with each other.
The effect of preventing entanglement is further improved.
In this embodiment, since the inner diameter of the coil is 15 mm, the plate-like member (1) is bent inward at a length of 10 mm from the front end so that the front end can be arranged within this inner diameter. .

【0047】また、上記各実施例では、板状部材(1)を
ステンレス板材で形成しているが、用途や性能、気液の
成分に対する耐食性、予算に応じて、板状部材(1)を炭
素鋼、銅、アルミニウム、チタン、その他の金属部材、
プラスチック、セラミックなどで形成しても良い。
In each of the above embodiments, the plate-like member (1) is formed of a stainless steel plate. However, the plate-like member (1) may be formed in accordance with the application, performance, corrosion resistance to gas-liquid components, and budget. Carbon steel, copper, aluminum, titanium, other metal members,
It may be formed of plastic, ceramic, or the like.

【0048】また、板状部材(1)は、広幅板状の金属材
や、広幅板状のプラスチック材をスリット加工して形成
しているが、この材料は、平滑な平板状のものを使用し
ても良いし、幅広板状の網材を使用しても良い。平板状
の材料であれば、経済性に優れるとともに製造作業が単
純で容易なものとなる。また、板状部材(1)に網材を使
用すれば、板状部材(1)の表面に、この網材による無数
の孔が形成されるので、液体の表面張力による良好な濡
れ効果が生じ、気液の接触が可能な表面積が増加するこ
とで、気液接触能力に優れた不規則充填物(3)を得る事
ができる。
The plate-like member (1) is formed by slitting a wide plate-like metal material or a wide plate-like plastic material. Alternatively, a wide plate-like net material may be used. A plate-shaped material is excellent in economical efficiency, and the manufacturing operation is simple and easy. If a net material is used for the plate-like member (1), numerous holes are formed by the net material on the surface of the plate-like member (1), so that a good wetting effect due to the surface tension of the liquid occurs. In addition, since the surface area where gas-liquid contact is possible is increased, it is possible to obtain an irregular packing (3) having excellent gas-liquid contact ability.

【0049】また、板状部材(1)は、表面に、凹凸、長
穴、小孔、溝の何れか一つまたは複数種を組み合わせて
表面加工を施して形成しても、板状部材(1)の気液接触
に有効な表面積が増加することで、良好な気液接触を可
能とする。
The plate-like member (1) may be formed by subjecting the surface to surface processing by combining one or more of irregularities, long holes, small holes, and grooves. Good gas-liquid contact is enabled by increasing the effective surface area for the gas-liquid contact of 1).

【0050】また、充填物本体(2)の外径に対する軸方
向の長さ比は、1.2〜3.0倍とするのが望ましい。
長さ比が1.2倍よりも小さいと、充填物本体(2)の重
心が低くなるので、軸が水平または傾斜して配置される
割合が低下し、気液接触能力を悪くする。また、長さ比
が3.0倍よりも大きいと、気液接触装置内での充填状
態の粗密の度合いが顕著となり、充填状態が悪化するも
のとなる。
The ratio of the length in the axial direction to the outer diameter of the filling body (2) is desirably 1.2 to 3.0 times.
If the length ratio is smaller than 1.2 times, the center of gravity of the packing body (2) becomes lower, so that the ratio of the horizontal or inclined arrangement of the shaft is reduced, and the gas-liquid contact ability is deteriorated. On the other hand, if the length ratio is larger than 3.0 times, the degree of density in the filling state in the gas-liquid contact device becomes remarkable, and the filling state deteriorates.

【0051】そして、本発明のコイル状の不規則充填物
及び従来より存在するポールリングを使用して、全環流
蒸留実験による圧力損失の比較を実施し、その結果を図
6に表した。尚、表中に示すCo_15は、本発明のコイル
状の不規則充填物で、厚さ0.1mm、幅3.0mmの
ステンレス部材を用いて直径15mmで形成している。
また、PR_15は、ステンレス部材のポールリングで、円
筒の直径を15mmで形成している。
Using the coiled random packing of the present invention and a conventional pole ring, a comparison of pressure loss was conducted in a total reflux distillation experiment, and the results are shown in FIG. Note that Co_15 shown in the table is a coil-shaped irregular packing of the present invention, and is formed with a diameter of 15 mm using a stainless member having a thickness of 0.1 mm and a width of 3.0 mm.
PR_15 is a pole ring made of a stainless steel member and has a cylindrical diameter of 15 mm.

【0052】実験の結果より、Co_15とPR_15では、本発
明のCo_15の方が直径が同一にもかかわらず、圧力損失
が少なかった。従って、本発明の不規則充填物が圧力損
失の少ない優れた製品である事がわかる。
From the results of the experiment, it was found that Co_15 of the present invention had a smaller pressure loss, despite having the same diameter, between Co_15 and PR_15. Therefore, it can be seen that the irregular packing of the present invention is an excellent product with low pressure loss.

【0053】また、図6の実験で使用した2種類の不規
則充填物に於いて、各々の1理論段数あたりの充填高さ
を表すH.E.T.Pの比較を実施し、その結果を図7に表し
た。
In addition, in the two kinds of irregular packings used in the experiment of FIG. 6, a comparison of HETP showing the filling height per one theoretical plate was carried out, and the results are shown in FIG. .

【0054】実験の結果より、Co_15とPR_15では、本発
明のCo_15の方がH.E.T.Pが非常に小さかった。従って、
本発明の不規則充填物は、1理論段数あたりの充填高さ
が低く優れた気液接触能力を発揮するものであり、性能
面からみた経済性も優れた製品である事がわかる。
From the experimental results, it was found that the Co_15 of the present invention had a much smaller HETP than that of Co_15 and PR_15. Therefore,
The irregularly packed material of the present invention has a low filling height per theoretical plate and exhibits excellent gas-liquid contacting ability, and it is understood that the product is excellent in economical efficiency from the viewpoint of performance.

【0055】[0055]

【発明の効果】本発明は上述の如く構成したものである
から、不規則充填物を気液接触装置に無秩序に充填して
も、その大多数は、コイル状の充填物本体の軸が水平ま
たは傾斜して配置され、ほぼ全てを規則的に配置する事
が可能となる。その結果、充填物本体のコイル状の板状
部材の両側縁で形成される、コイル状の対向間隔を通過
して、気液が充填物本体内部を通過する。この対向間隔
を通過時に、気体は分裂や合一を繰り返すので、気体の
乱流が発生し、液体との接触能力を向上させる。また、
液体も分散して流動し、板状部材の表面に付着し易くな
り、濡れ効果が向上する。このような頻繁な離合集散を
繰り返す気体と、板状部材に分散する液体とが良好に接
触し、気液間の物質移動、熱移動、化学反応の著しい促
進が可能となる。
Since the present invention is constructed as described above, even if the irregular packing is randomly filled in the gas-liquid contacting device, the majority of the axis of the coil-shaped packing body is horizontal. Alternatively, they can be arranged at an angle, and almost all can be arranged regularly. As a result, the gas-liquid passes through the inside of the filling body, passing through the coil-shaped opposing interval formed by both side edges of the coil-shaped plate-shaped member of the filling body. When the gas passes through the opposing interval, the gas repeatedly splits and coalesces, so that turbulence of the gas is generated, and the contact ability with the liquid is improved. Also,
The liquid also disperses and flows, and easily adheres to the surface of the plate member, and the wetting effect is improved. The gas which repeats such frequent separation / dispersion and the liquid dispersed in the plate-shaped member are in good contact with each other, so that mass transfer, heat transfer and chemical reaction between gas and liquid can be remarkably promoted.

【0056】また、水平または傾斜して配置される事に
より、充填物本体が荷重で押しつぶされることがない。
また、右巻と左巻の充填物本体を同一に近い比率で混合
したり、充填物本体の板状部材の対向間隔を、板状部材
の幅と同一または狭小に形成しているので、充填物本体
同志が互いに絡み合ったりせず、均一で良好な充填状態
を実現できる。そのため、気体の圧力損失を抑えるとと
もに気液の偏流を防ぎ、気液接触能力を向上させるもの
となる。
Further, by being arranged horizontally or inclined, the filling body is not crushed by the load.
In addition, the right-handed and left-handed filling bodies are mixed at almost the same ratio, and the facing distance between the plate-like members of the filling body is formed to be equal to or smaller than the width of the plate-like member. The object bodies do not become entangled with each other, and a uniform and good filling state can be realized. Therefore, the gas pressure loss is suppressed, the gas-liquid drift is prevented, and the gas-liquid contact capability is improved.

【0057】また、板状部材を巻廻すだけで容易に充填
物本体を形成可能となる。そして、径の大小に束縛され
ず、径小なものでも径大なものでも自由に形成できると
ともに、気液接触装置のサイズに合わせる必要もなく、
簡易な製造工程で廉価に不規則充填物を形成する事が可
能となる。
Further, it is possible to easily form the filler body simply by winding the plate-shaped member. And, without being restricted by the size of the diameter, it can be formed freely even with a small diameter or a large diameter, and there is no need to match the size of the gas-liquid contact device,
It is possible to form an irregular packing at low cost by a simple manufacturing process.

【図面の簡単な説明】[Brief description of the drawings]

【図1】本発明の第1実施例の右巻に巻廻した充填物本
体の斜視図。
FIG. 1 is a perspective view of a right-hand wound packing body according to a first embodiment of the present invention.

【図2】図1のA−A線断面図。FIG. 2 is a sectional view taken along line AA of FIG.

【図3】左巻に巻廻した充填物本体の斜視図。FIG. 3 is a perspective view of a filling body wound left-handed.

【図4】右巻及び左巻の充填物本体を充填した状態の斜
視図。
FIG. 4 is a perspective view of a state where right and left-handed filling bodies are filled.

【図5】第2実施例の充填物本体の斜視図。FIG. 5 is a perspective view of a filling body according to a second embodiment.

【図6】F−factorと圧力損失の関係を表すグラ
フ。
FIG. 6 is a graph showing a relationship between F-factor and pressure loss.

【図7】F−factorとH.E.T.Pの関係を表
すグラフ。
FIG. 7: F-factor and H. E. FIG. T. 7 is a graph showing the relationship of P.

【符号の説明】[Explanation of symbols]

1 板状部材 2 充填物本体 3 対向間隔 4 不規則充填物 DESCRIPTION OF SYMBOLS 1 Plate-shaped member 2 Filling body 3 Opposite spacing 4 Irregular filling

Claims (9)

【特許請求の範囲】[Claims] 【請求項1】 一定幅を有する帯状の板状部材を複数回
右巻または左巻に巻廻してコイル状の充填物本体を形成
し、この充填物本体を形成する板状部材の両側縁が、コ
イル状の軸方向に於いて一定の対向間隔を形成し、この
対向間隔を、板状部材の幅と同一または板状部材の幅よ
りも小さく形成するとともに、充填物本体の軸方向の長
さを、外径よりも大きく形成したもので、この右巻の充
填物本体と左巻の充填物本体とを混合して気液接触装置
に充填する事を特徴とする気液接触用不規則充填物。
1. A coil-shaped filler body is formed by winding a band-shaped plate member having a constant width into a right-handed or left-handed winding a plurality of times. In the axial direction of the coil, a constant opposing interval is formed, and the opposing interval is formed to be the same as or smaller than the width of the plate member, and the length of the filling body in the axial direction is reduced. The irregular shape for gas-liquid contact, characterized in that the right-handed filling body and the left-handed filling body are mixed and filled into a gas-liquid contact device. Filling.
【請求項2】 板状部材は、金属材、プラスチック材ま
たはセラミック材の何れかにより形成した事を特徴とす
る請求項1の気液接触用不規則充填物。
2. The irregular packing for gas-liquid contact according to claim 1, wherein the plate member is formed of any one of a metal material, a plastic material and a ceramic material.
【請求項3】 板状部材は、広幅板状の金属材、または
広幅板状のプラスチック材を複数にスリットして形成し
た事を特徴とする請求項1の気液接触用不規則充填物。
3. The irregular packing for gas-liquid contact according to claim 1, wherein the plate-like member is formed by slitting a wide plate-like metal material or a wide plate-like plastic material into a plurality of slits.
【請求項4】 板状部材は、平滑な平板状に形成した事
を特徴とする請求項1の気液接触用不規則充填物。
4. The irregular packing for gas-liquid contact according to claim 1, wherein the plate-like member is formed in a smooth flat plate shape.
【請求項5】 板状部材は、網材により形成した事を特
徴とする請求項1の気液接触用不規則充填物。
5. The irregular packing for gas-liquid contact according to claim 1, wherein the plate-like member is formed of a net material.
【請求項6】 板状部材は、表面に、凹凸、長穴、小
孔、溝の何れか一つまたは複数種を組み合わせて表面加
工を施したものである事を特徴とする請求項1の気液接
触用不規則充填物。
6. The plate-like member according to claim 1, wherein the surface is subjected to surface processing by combining one or more of irregularities, long holes, small holes, and grooves on the surface. Random packing for gas-liquid contact.
【請求項7】 充填物本体は、外径に対する軸方向の長
さ比を、1.2〜3.0とした事を特徴とする請求項1
の気液接触用不規則充填物。
7. The packing body according to claim 1, wherein an axial length ratio to an outer diameter is set to 1.2 to 3.0.
Random packing for gas-liquid contact.
【請求項8】 充填物本体は、板状部材を右巻に形成し
たものと、板状部材を左巻に形成したものとを、1.
0:0.8〜1.0:1.2の割合で混合するものであ
る事を特徴とする請求項1の気液接触用不規則充填物。
8. The filling body includes a plate-shaped member formed into a right-handed form and a plate-shaped member formed into a left-handed form.
2. The irregular packing for gas-liquid contact according to claim 1, wherein the mixture is mixed at a ratio of 0: 0.8 to 1.0: 1.2.
【請求項9】 充填物本体は、板状部材の先端をコイル
の内径内に折曲したものである事を特徴とする請求項1
の気液接触用不規則充填物。
9. The packing body according to claim 1, wherein the tip of the plate-shaped member is bent into the inner diameter of the coil.
Random packing for gas-liquid contact.
JP9251572A 1997-09-17 1997-09-17 Irregular packing for vapor-liquid contact Pending JPH1190218A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP9251572A JPH1190218A (en) 1997-09-17 1997-09-17 Irregular packing for vapor-liquid contact

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP9251572A JPH1190218A (en) 1997-09-17 1997-09-17 Irregular packing for vapor-liquid contact

Publications (1)

Publication Number Publication Date
JPH1190218A true JPH1190218A (en) 1999-04-06

Family

ID=17224818

Family Applications (1)

Application Number Title Priority Date Filing Date
JP9251572A Pending JPH1190218A (en) 1997-09-17 1997-09-17 Irregular packing for vapor-liquid contact

Country Status (1)

Country Link
JP (1) JPH1190218A (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100391588C (en) * 2006-04-04 2008-06-04 湘潭大学 Tapered spiral filling
JP2010129461A (en) * 2008-11-28 2010-06-10 Nissan Motor Co Ltd Polymer electrolyte fuel cell
CN102010070A (en) * 2010-10-19 2011-04-13 大连善水德水务工程有限责任公司 Spiral floated water treatment packing (SFWP), preparation method of SFWP and application of SFWP in water treatment
JP2011125841A (en) * 2009-11-17 2011-06-30 Kiriyama Seisakusho:Kk Packing material for distillation
JP2014155895A (en) * 2013-02-15 2014-08-28 Kiriyama Seisakusho:Kk Packing material for distillation
JP2016107181A (en) * 2014-12-03 2016-06-20 有限会社桐山製作所 Distillation tower filled with filler

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100391588C (en) * 2006-04-04 2008-06-04 湘潭大学 Tapered spiral filling
JP2010129461A (en) * 2008-11-28 2010-06-10 Nissan Motor Co Ltd Polymer electrolyte fuel cell
JP2011125841A (en) * 2009-11-17 2011-06-30 Kiriyama Seisakusho:Kk Packing material for distillation
CN102010070A (en) * 2010-10-19 2011-04-13 大连善水德水务工程有限责任公司 Spiral floated water treatment packing (SFWP), preparation method of SFWP and application of SFWP in water treatment
JP2014155895A (en) * 2013-02-15 2014-08-28 Kiriyama Seisakusho:Kk Packing material for distillation
JP2016107181A (en) * 2014-12-03 2016-06-20 有限会社桐山製作所 Distillation tower filled with filler

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