JPH11345545A - Gas recovery device and gas recovery method - Google Patents

Gas recovery device and gas recovery method

Info

Publication number
JPH11345545A
JPH11345545A JP10150916A JP15091698A JPH11345545A JP H11345545 A JPH11345545 A JP H11345545A JP 10150916 A JP10150916 A JP 10150916A JP 15091698 A JP15091698 A JP 15091698A JP H11345545 A JPH11345545 A JP H11345545A
Authority
JP
Japan
Prior art keywords
gas
container
vacuum pump
gas recovery
separation device
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP10150916A
Other languages
Japanese (ja)
Other versions
JP3728927B2 (en
Inventor
Tokio Yamagiwa
時生 山極
Kenji Tsuchiya
賢治 土屋
Kunio Hirasawa
邦夫 平澤
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hitachi Ltd
Original Assignee
Hitachi Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hitachi Ltd filed Critical Hitachi Ltd
Priority to JP15091698A priority Critical patent/JP3728927B2/en
Publication of JPH11345545A publication Critical patent/JPH11345545A/en
Application granted granted Critical
Publication of JP3728927B2 publication Critical patent/JP3728927B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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  • Separation Using Semi-Permeable Membranes (AREA)
  • Gas-Insulated Switchgears (AREA)
  • Driving Mechanisms And Operating Circuits Of Arc-Extinguishing High-Tension Switches (AREA)

Abstract

PROBLEM TO BE SOLVED: To recover an SF6 gas separately into a small container by installing a storage container between a vacuum pump and a separation device, also installing a cross valve between the separation device and an SF6 gas recovery container, and circulating a mixed gas in the storage container from the separation device through the cross valve and the vacuum pump back to the storage container by switching over the cross valve. SOLUTION: When a stop valve 13 is opened from a condition that the stop valves 13, 14 and a cross valve 15 are closed, a mixed gas in a gas insulation switching device 1 is recovered into a storage container 5 by a vacuum pump 9 and thereafter transferred to a separation device 3 after its pressure is reduced by a pressure reducing valve 16. Then. when the stop valve 13 is closed and the cross valve 15 is so switched over as to pass the gas in the direction (shown in square), the mixed gas with an SF6 gas in a chamber 2a of the separation device 3 is recirculated into the separation device 3 through the storage container 5 and the pressure reducing valve 16 by the vacuum pump 9 and is separated again. By repeating this process, the purity of the SF6 gas is increased. Then, when the cross valve 15 is so switched over as to pass the gas in the direction of, the SF6 gas is transferred to an SF6 gas recovery container 6 to be stored.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明はガス絶縁開閉装置の
ガス回収装置に係わり、特にSF6 ガスと他のガスとの
混合ガスを回収するのに好適なガス絶縁開閉装置用のガ
ス回収装置に関する。
The present invention relates to relates to gas recovery device relates to, in particular gas recovery apparatus for suitable gas insulated switchgear to recover a mixed gas of SF 6 gas and other gases in the gas insulated switchgear .

【0002】[0002]

【従来の技術】SF6 ガスと他のガスとの混合ガスを用
いたガス絶縁開閉装置用の従来の回収装置は、特開昭63
−26497 号公報に記載のように混合ガスを分離すること
なく回収容器に液化して回収している。
2. Description of the Related Art A conventional recovery device for a gas insulated switchgear using a mixed gas of SF 6 gas and another gas is disclosed in
As described in -26497, the mixed gas is liquefied and collected in a collection container without being separated.

【0003】[0003]

【発明が解決しようとする課題】特開昭63−26497 号公
報に記載の装置は、混合ガスの成分を分離することなく
すべてのガス成分を回収しているため、大容量の回収容
器が必要となる。一方、回収容器の容積を小さくする場
合、液化して回収するためには、SF6 ガス以外のガス
は一般的に液化温度が低く、この液化温度の低いガスを
冷却するためには大規模な冷却装置が必要となるという
問題があった。
The apparatus described in JP-A-63-26497 recovers all gas components without separating the components of the mixed gas, so that a large-capacity recovery container is required. Becomes On the other hand, when the volume of the recovery container is reduced, gases other than SF 6 gas generally have a low liquefaction temperature in order to liquefy and recover, and a large-scale gas is required to cool the gas having a low liquefaction temperature. There was a problem that a cooling device was required.

【0004】本発明の第1の目的は、小型の容器に分離
回収できるSF6 ガスとの混合ガスを用いたガス絶縁開
閉装置のガス回収装置を提供することにある。
A first object of the present invention is to provide a gas recovery device of a gas insulated switchgear using a mixed gas with SF 6 gas which can be separated and recovered in a small container.

【0005】本発明の第2の目的は、混合ガスを液化し
ないでSF6 ガスを回収できるガス絶縁開閉装置のガス
回収装置を提供することにある。
A second object of the present invention is to provide a gas recovery device of a gas insulated switchgear which can recover SF 6 gas without liquefying a mixed gas.

【0006】[0006]

【課題を解決するための手段】上記目的を達成するため
に、本発明のガス絶縁開閉装置用のガス回収装置は、混
合ガスが封入されたガス絶縁開閉装置と、該ガス絶縁開
閉装置に真空ポンプを介して接続された分離装置と、該
分離装置内に設けられた気体分離膜で仕切られ前記真空
ポンプに連通する一方の室に接続されたSF6 ガス回収
容器とを備えたことを特徴とする。
In order to achieve the above object, a gas recovery apparatus for a gas insulated switchgear according to the present invention comprises: a gas insulated switchgear in which a mixed gas is sealed; A separation device connected via a pump, and an SF 6 gas recovery container connected to one chamber separated by a gas separation membrane provided in the separation device and connected to the vacuum pump. And

【0007】又、前記真空ポンプと前記分離装置間に貯
溜容器が具備され、前記分離装置とSF6 ガス回収容器
間に三方弁が設けられるものであって、前記三方弁を切
換えて前記貯溜容器内の混合ガスを前記分離装置,三方
弁,真空ポンプ,貯溜容器の順に循環させるものであ
る。又、前記気体分離膜が、ポリイミド膜,炭素膜,ゼ
オライト膜のいずれかで構成されているものである。
又、前記貯溜容器と分離装置間に減圧弁を設けたもので
ある。又、前記SF6 ガス回収容器が重量計に載置され
るものであって、該SF6 ガス回収容器および混合ガス
ボンベがガス混合容器,ポンプを介してガス絶縁開閉装
置に接続されているものである。
Further, a storage container is provided between the vacuum pump and the separation device, and a three-way valve is provided between the separation device and the SF 6 gas recovery container, and the storage container is switched by switching the three-way valve. The mixed gas is circulated in the order of the separation device, the three-way valve, the vacuum pump, and the storage container. Further, the gas separation membrane is formed of any one of a polyimide membrane, a carbon membrane, and a zeolite membrane.
Further, a pressure reducing valve is provided between the storage container and the separation device. Further, the SF 6 gas recovery container is mounted on a weighing scale, and the SF 6 gas recovery container and the mixed gas cylinder are connected to a gas insulated switchgear via a gas mixing container and a pump. is there.

【0008】本発明のガス回収方法は、混合ガスが封入
されたガス絶縁開閉装置から真空ポンプにより気体分離
膜を具備した分離装置に混合ガスを流し、気体分離膜に
よりSF6 ガス以外のガスを分離し、純度が高められた
SF6 ガスをSF6 ガス回収容器に回収することを特徴
とする。
[0008] In the gas recovery method of the present invention, the mixed gas is passed from the gas insulated switchgear in which the mixed gas is sealed to a separation device having a gas separation membrane by a vacuum pump, and a gas other than SF 6 gas is removed by the gas separation membrane. The method is characterized in that the SF 6 gas having been separated and having a higher purity is recovered in a SF 6 gas recovery container.

【0009】[0009]

【発明の実施の形態】以下、本発明の一実施例を図1に
より説明する。図1は本実施例のガス絶縁開閉装置及び
ガス回収装置の構成を示す図である。
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS One embodiment of the present invention will be described below with reference to FIG. FIG. 1 is a diagram showing a configuration of a gas insulated switchgear and a gas recovery device of the present embodiment.

【0010】SF6 ガスとその他のガス、例えば窒素ガ
ス、空気との混合ガスが封入されたガス絶縁開閉装置1
には、ガス配管4が接続されており、止弁13を介して
真空ポンプ9に接続されている。真空ポンプ9は貯蔵容
器5に接続されており、この貯蔵容器5では真空ポンプ
9によって回収された混合ガスを一時貯蔵している。貯
蔵容器5は減圧弁16を介して混合ガスの分離装置3
(濾過装置3ともいう)に接続されている。この分離装
置3内には、気体分離膜2が設けられており、気体分離
膜2で仕切られた一方の室2aに混合ガスが流れるよう
になっている。室2aは三方弁15に接続されている。
気体分離膜2で仕切られた他方の室2bは、ポンプ10
に接続されポンプ10の他端は大気開放になっている。
そのため、ポンプ10により気体分離膜2で分離された
気体を外気に放出するようになっている。
A gas-insulated switchgear 1 in which a mixed gas of SF 6 gas and other gases, for example, nitrogen gas and air is filled.
Is connected to a gas pipe 4, and is connected to a vacuum pump 9 via a stop valve 13. The vacuum pump 9 is connected to the storage container 5, and the storage container 5 temporarily stores the mixed gas recovered by the vacuum pump 9. The storage vessel 5 is connected to the mixed gas separation device 3 through a pressure reducing valve 16.
(Also referred to as a filtration device 3). A gas separation membrane 2 is provided in the separation device 3, and a mixed gas flows into one chamber 2 a partitioned by the gas separation membrane 2. The chamber 2a is connected to the three-way valve 15.
The other chamber 2b partitioned by the gas separation membrane 2 has a pump 10
And the other end of the pump 10 is open to the atmosphere.
Therefore, the gas separated by the gas separation membrane 2 by the pump 10 is discharged to the outside air.

【0011】三方弁15の一方側は止弁13と真空ポン
プ9とを接続する配管の途中に接続されており、三方弁
15の他方の側は、ポンプ11を介してSF6 ガス回収
容器6に接続されている。SF6 ガス回収容器6は重量
計17に載置されており、SF6 ガス回収容器6の重さ
を計量するようになっている。SF6 ガス回収容器6
は、ガス混合容器8に接続されており、このガス混合容
器8にはSF6 ガス以外のガスの混合ガスボンベ7と接
続されている。ガス混合容器8の出口側は、ポンプ1
2,止弁14を介してガス絶縁開閉装置1に接続されて
いる。
One side of the three-way valve 15 is connected in the middle of a pipe connecting the stop valve 13 and the vacuum pump 9, and the other side of the three-way valve 15 is connected via the pump 11 to the SF 6 gas recovery container 6. It is connected to the. The SF 6 gas recovery container 6 is placed on a weighing scale 17, and weighs the SF 6 gas recovery container 6. SF 6 gas recovery container 6
It is connected to a gas mixing vessel 8, and is connected to the mixed gas cylinder 7 of gases other than SF 6 gas in the gas mixing vessel 8. The outlet side of the gas mixing container 8 is
2. It is connected to the gas insulated switchgear 1 via the stop valve 14.

【0012】このように構成されたガス絶縁開閉装置の
ガス回収装置のガス回収について説明する。最初、止弁
13,14,三方弁15は閉じた状態にある。この状態
で止弁13を開くと真空ポンプ9により、ガス絶縁開閉
装置1内の混合ガスが貯蔵容器5に回収される。貯蔵容
器5に回収された混合ガスは、減圧弁16により減圧さ
れて分離装置3に送られる。分離装置3内の気体分離膜
2は、分子径の大きなSF6 ガスは透過させないが、混
合ガスに含まれる窒素,酸素のような分子径の小さなガ
スは透過させるものを用いている。気体分離膜2として
は、ポリイミド膜,炭素膜,ゼオライト膜のいずれかが
適用される。従って、この気体分離膜2では、SF6
スは、室2a内に残留し、SF6 ガス以外のガスは、気
体分離膜2を透過して室2b内に移動する。室2b内に
移動したSF6 以外のガスは、ポンプ10により排気さ
れ大気中に放出される。
The gas recovery of the gas recovery device of the gas insulated switchgear thus configured will be described. First, the stop valves 13, 14, and the three-way valve 15 are in a closed state. When the stop valve 13 is opened in this state, the mixed gas in the gas insulated switchgear 1 is collected in the storage container 5 by the vacuum pump 9. The mixed gas collected in the storage container 5 is depressurized by the pressure reducing valve 16 and sent to the separation device 3. The gas separation membrane 2 in the separation device 3 does not allow passage of SF 6 gas having a large molecular diameter but allows passage of gas having a small molecular diameter such as nitrogen and oxygen contained in a mixed gas. As the gas separation membrane 2, any of a polyimide membrane, a carbon membrane, and a zeolite membrane is applied. Therefore, in the gas separation membrane 2, the SF 6 gas remains in the chamber 2a, and gases other than the SF 6 gas pass through the gas separation membrane 2 and move into the chamber 2b. The gas other than SF 6 that has moved into the chamber 2b is exhausted by the pump 10 and released into the atmosphere.

【0013】次に止弁13を閉じて三方弁15を図1中
に矢印ロで示す方向に流れるように切換える。この状態
では、分離装置3内の室2a内のSF6 ガスとの混合ガ
スは、真空ポンプ9により貯蔵容器5,減圧弁16を介
して分離装置3内に再び循環され、再度分離が行われ
る。この過程を繰り返すことにより、気体分離膜2を透
過されず室2a内に残留したSF6 ガス以外のガスが室
2b内に移動して濾過され、SF6 ガスの純度が高ま
る。この純度は、図示しない検出器により検出され、こ
の純度が予め設定された純度に達したら、三方弁15を
図1中の矢印イで示す方向に流れるように切換える。こ
の状態で、ポンプ11によりSF6 ガスをSF6 ガス回
収容器6に送られて貯溜される。SF6 ガス回収容器6
に蓄えられたSF6 ガスの重量は、重量計17により計
量される。
Next, the stop valve 13 is closed and the three-way valve 15 is switched so as to flow in the direction shown by the arrow B in FIG. In this state, the mixed gas with the SF 6 gas in the chamber 2a in the separation device 3 is circulated again into the separation device 3 by the vacuum pump 9 via the storage container 5 and the pressure reducing valve 16, and the separation is performed again. . By repeating this process, gases other than the SF 6 gas remaining in the chamber 2a without passing through the gas separation membrane 2 move into the chamber 2b and are filtered, thereby increasing the purity of the SF 6 gas. The purity is detected by a detector (not shown), and when the purity reaches a preset purity, the three-way valve 15 is switched so as to flow in a direction indicated by an arrow A in FIG. In this state, the SF 6 gas is sent to the SF 6 gas recovery container 6 by the pump 11 and stored therein. SF 6 gas recovery container 6
Weight of SF 6 gas stored in is weighed by the weight meter 17.

【0014】このようにして回収されたSF6 ガスを混
合ガスとしてガス絶縁開閉装置1に充填する場合は、次
のようにして行う。止弁13を閉状態,止弁14を開状
態,三方弁15を矢印ロの方向に切換える。SF6ガス
回収容器6に蓄えられたSF6ガスをガス混合容器8に
導くとともに、混合ガスボンベ7に蓄えられたSF6
外のガスをガス混合容器8に導く。ここで、混合ガスボ
ンベ7には、SF6 ガス以外のガスを混合したもの、あ
るいはSF6 ガス以外の単独のガスが封入されている。
ガス混合容器8内では、SF6 ガスとSF6 以外のガス
とが混合され、ポンプ12により止弁14を介してガス
絶縁開閉装置1に充填される。SF6 ガスに混合するS
6 以外のガスの量は、重量計17で計量したSF6
スの重量の変化量をもとに、予め設定された混合比とな
るように調整される。
When the gas insulated switchgear 1 is filled with the SF 6 gas thus recovered as a mixed gas, the following procedure is performed. The stop valve 13 is closed, the stop valve 14 is opened, and the three-way valve 15 is switched in the direction of arrow B. The SF 6 gas stored in the SF 6 gas recovery container 6 guides the gas mixing vessel 8, guides the SF 6 gas other than that stored in the mixed gas cylinder 7 to the gas mixing container 8. Here, the mixing gas cylinder 7, as a mixture of gases other than SF 6 gas or SF 6 except gas alone gas is enclosed.
In the gas mixing container 8, SF 6 gas and a gas other than SF 6 are mixed and filled in the gas insulated switchgear 1 by the pump 12 via the stop valve 14. S mixed with SF 6 gas
The amount of the gas other than F 6 is adjusted based on the change in the weight of SF 6 gas measured by the weigh scale 17 so as to have a preset mixing ratio.

【0015】本実施例では、以上述べたように、気体分
離膜を利用した分離装置でSF6 ガスとSF6 ガス以外
のガスを分離しているので、混合ガスを液化する必要が
なく、大規模な冷却装置を設置する必要がない。又、貯
蔵容器に貯蔵された混合ガスを循環させて分離させてい
るので、SF6 ガスの純度を高くすることができ、再利
用が可能である。又、気体分離膜で分離されたSF6
ス以外のガスは大気放出できるので、SF6 ガス回収容
器を小型にできる。又、重量計でSF6 ガス回収容器に
回収されたSF6 ガスの重量を計量しているので、混合
ガスの混合比を設定でき、ガス絶縁開閉装置に予め設定
された混合比の混合ガスを充填できる。
[0015] In this embodiment, as mentioned above, since the separation of the SF 6 gas and SF 6 gas other than the gas in the separation device using a gas separation membrane, it is not necessary to liquefy the mixed gas, large There is no need to install a large-scale cooling device. Further, since the mixed gas stored in the storage container is circulated and separated, the purity of the SF 6 gas can be increased, and the gas can be reused. Further, since gases other than the SF 6 gas separated by the gas separation membrane can be released to the atmosphere, the SF 6 gas recovery container can be downsized. In addition, since the weighed weight of the SF 6 gas recovered in SF 6 gas recovery container weighing scale, it can set the mixture ratio of the mixed gas, a mixed gas of a predetermined mixing ratio in the gas insulated switchgear Can be filled.

【0016】[0016]

【発明の効果】以上説明したように、本発明によれば、
混合ガスを液化させる必要がなく、SF6 ガスを小型の
容器に分離回収できるガス絶縁開閉装置用のガス回収装
置を提供できる。
As described above, according to the present invention,
There is no need to liquefy the mixed gas, and it is possible to provide a gas recovery device for a gas insulated switchgear that can separate and recover SF 6 gas in a small container.

【図面の簡単な説明】[Brief description of the drawings]

【図1】本発明の一実施例であるガス絶縁開閉装置及び
ガス回収装置の構成を示す図である。
FIG. 1 is a diagram showing a configuration of a gas insulated switchgear and a gas recovery device according to one embodiment of the present invention.

【符号の説明】[Explanation of symbols]

1…ガス絶縁開閉装置、2…気体分離膜、3…分離装
置、4…ガス配管、5…貯蔵容器、6…SF6 ガス回収
容器、7…混合ガスボンベ、8…ガス混合容器、9…真
空ポンプ、10,11,12…ポンプ、13,14…止
弁、15…三方弁、16…減圧弁、17…重量計。
1 ... Gas-insulated switchgear, 2 ... a gas separation membrane, 3 ... separator, 4 ... gas pipe, 5 ... storage container, 6 ... SF 6 gas collecting container, 7 ... mixed gas cylinder, 8 ... gas mixing vessel, 9 ... vacuum Pumps, 10, 11, 12: pumps, 13, 14, stop valves, 15: three-way valves, 16: pressure reducing valves, 17: weight scales.

Claims (6)

【特許請求の範囲】[Claims] 【請求項1】混合ガスが封入されたガス絶縁開閉装置
と、該ガス絶縁開閉装置に真空ポンプを介して接続され
た分離装置と、該分離装置内に設けられた気体分離膜で
仕切られ前記真空ポンプに連通する一方の室に接続され
たSF6 ガス回収容器とを備えたことを特徴とするガス
回収装置。
1. A gas-insulated switchgear filled with a mixed gas, a separator connected to the gas-insulated switchgear via a vacuum pump, and a gas separation membrane provided in the separator. A gas recovery device comprising: a SF 6 gas recovery container connected to one chamber communicating with a vacuum pump.
【請求項2】前記真空ポンプと前記分離装置間に貯溜容
器が具備され、前記分離装置とSF6ガス回収容器間に三
方弁が設けられるものであって、前記三方弁を切換えて
前記貯溜容器内の混合ガスを前記分離装置,三方弁,真
空ポンプ,貯溜容器の順に循環させる請求項1に記載の
ガス回収装置。
2. A storage container is provided between the vacuum pump and the separation device, and a three-way valve is provided between the separation device and the SF 6 gas recovery container. The storage container is switched by switching the three-way valve. The gas recovery device according to claim 1, wherein the mixed gas in the gas is circulated in the order of the separation device, the three-way valve, the vacuum pump, and the storage container.
【請求項3】前記気体分離膜が、ポリイミド膜,炭素
膜,ゼオライト膜のいずれかで構成されている請求項1
又は2に記載のガス回収装置。
3. The gas separation membrane according to claim 1, wherein the gas separation membrane is made of any one of a polyimide membrane, a carbon membrane, and a zeolite membrane.
Or the gas recovery device according to 2.
【請求項4】前記貯溜容器と分離装置間に減圧弁を設け
た請求項2に記載のガス回収装置。
4. The gas recovery device according to claim 2, wherein a pressure reducing valve is provided between the storage container and the separation device.
【請求項5】前記SF6 ガス回収容器が重量計に載置さ
れるものであって、該SF6 ガス回収容器および混合ガ
スボンベがガス混合容器、ポンプを介してガス絶縁開閉
装置に接続されている請求項1から4のいずれかに記載
のガス回収装置。
5. The SF 6 gas recovery container is mounted on a weighing scale, wherein the SF 6 gas recovery container and the mixed gas cylinder are connected to a gas insulated switchgear via a gas mixing container and a pump. The gas recovery device according to any one of claims 1 to 4.
【請求項6】混合ガスが封入されたガス絶縁開閉装置か
ら真空ポンプにより気体分離膜を具備した分離装置に混
合ガスを流し、気体分離膜によりSF6 ガス以外のガス
を分離し、純度が高められたSF6 ガスをSF6 ガス回
収容器に回収することを特徴とするガス回収方法。
6. A mixed gas is flowed from a gas-insulated switchgear in which the mixed gas is sealed to a separator equipped with a gas separation membrane by a vacuum pump, and gases other than SF 6 gas are separated by the gas separation membrane to increase purity. gas recovery method comprising recovering SF 6 gas which is in SF 6 gas recovery container.
JP15091698A 1998-06-01 1998-06-01 Gas recovery device and gas recovery method Expired - Fee Related JP3728927B2 (en)

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Publication number Priority date Publication date Assignee Title
US6921428B2 (en) 2001-01-25 2005-07-26 Ube Industries, Ltd. Device and method for separating and collecting halide gas
JP2003190744A (en) * 2001-12-26 2003-07-08 Ube Ind Ltd Apparatus for separating and recovering halogen compound gas and separation and recovering method using the same
CN103322408A (en) * 2013-05-28 2013-09-25 国家电网公司 System for pumping and inflating SF6 for gas insulated switchgear
CN103495443A (en) * 2013-09-29 2014-01-08 广州供电局有限公司 Centralized control recycling device and method for waste gas in laboratory
KR20160009895A (en) * 2014-07-17 2016-01-27 한국과학기술연구원 Apparatus and method for recovery of retentate
KR20160009894A (en) * 2014-07-17 2016-01-27 한국과학기술연구원 Apparatus and method for recovery of retentate

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