JPH1128076A - Production of refreshing drink containing natural calcium - Google Patents

Abstract

PROBLEM TO BE SOLVED: To produce a refreshing drink capable of containing natural calcium in a large amount by mixing a natural calcium-dissolved raw solution obtained by dissolving non-calcined egg shell in a lactic acid with granulated sugar, lactic acid, a perfume and pure water and subsequently sterilizing the mixture. SOLUTION: This method for producing the refreshing drink comprises mixing a natural calcium-dissolved raw solution obtained by dissolving non-calcined egg shell in lactic acid with granulated sugar, lactic acid, a perfume and pure water, and subsequently sterilizing the mixture. The natural calcium-dissolved solution is obtained by mixing 100 g of a 50% lactic acid solution with 400 g of 50 deg.C pure water, gradually adding 30 g of about 400-1000 mesh finely ground non-calcined egg shell to the obtained solution with stirring, aging the non-calcined egg shell mixture solution at 50 deg.C for 30-50 min with stirring, further aging the mixture for 3-4 hr, and subsequently naturally or forcibly separating the left egg shell.

Description

DETAILED DESCRIPTION OF THE INVENTION

[0001]

BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for producing a natural calcium-containing soft drink containing a large amount of natural calcium.

[0002]

2. Description of the Related Art One of the necessary health factors is calcium, which is an important component of bone,
Muscle excitability, blood coagulation, cell membrane function, enzyme activation,
It has many important functions such as hormone secretion. And children and pregnant women in the process of forming bone must get enough calcium. For that reason, processed milk, yogurt, cheese, eggs, tofu,
Food such as drinks and foods to which small fish, spinach, and calcium were added was appropriately taken.

[0003]

However, it is difficult to take such foods every day from the menu point of view, and it is not suitable for meat etc. or according to the taste of the person, and it is difficult to use processed milk and yogurt. It is common to rely on drinks. This drink was also very inconvenient in terms of calcium intake, such as having a preference or being physically unsuitable.

[0004]

An object of the present invention is to provide a method for producing a natural calcium-containing soft drink which eliminates such inconveniences, absorbs calcium sufficiently, and is easy to drink. A natural calcium dissolving solution obtained by dissolving unbaked eggshell with lactic acid is mixed with granulose, lactic acid (or organic acids that do not recrystallize), fragrance, pure water, etc. according to the prescription,
It has been sterilized. As a natural calcium solution stock solution, 100 g of a 50% lactic acid solution and 400 g of 50 ° C. pure water are mixed to form a lactic acid solution. Then, 30 g of unfired eggshell finely divided into about 400 to 1000 mesh is added to the mixture while gradually stirring, and a reaction of Ca carbonate and lactic acid as a mixture of unfired eggshell occurs, and a reaction gas (carbon dioxide gas) occurs for 30 to 50 minutes.
As a result, an antifoaming agent (such as silicon) is added at about 0.3% as necessary.

[0005] Then, the mixture of the unfired eggshell mixture is gently stirred and aged for 30 to 50 minutes while maintaining 50 ° C for 3 hours to
Aging is performed while maintaining the liquid temperature for 4 hours. The remaining eggshell is subjected to natural separation (natural precipitation) or forced separation (screw decanter or spacra filter treatment) to obtain a natural calcium solution stock solution. Adjust the pH with lactic acid (or organic acids that do not recrystallize with Ca) at the time of preparing
As a supplemental drinking water type (water PH is 6.5-
6.8 is normal), and PH4 or more is desirable. As a sterilization condition, a treatment having an F value of 4 or more (sterilization at 120 ° C. for 10 minutes) is performed.
Next, using a Ca extract as described above as a treatment for a shorts drink system providing a sour taste as a Ca supplement beverage of PH4 or less, adjusting PH3 to PH4 with lactic acid (or organic acids which do not recrystallize with Ca) and filling at 92 ° C. After packing, sterilization is performed at 75 ° C. for 15 minutes.

[0006]

An embodiment of the prescription will be described below. First, Table 1 shows the contents of the natural calcium solution stock solution.

[0007]

[Table 1]

[0008] As shown in Table 1, the mixture of unfired eggshell mixture was 30 to 5
Stirring and aging are performed gently while maintaining 50 ° C. for 0 minutes, and aging is performed while maintaining the liquid temperature for 3 to 4 hours. The remaining eggshell is subjected to natural separation (natural precipitation) or forced separation (screw decanter or spacra filter treatment) to obtain a natural calcium solution stock solution. PH is adjusted to 4 or more as a Ca-supplemented beverage water type by adjusting the pH with lactic acid (or an organic acid that does not recrystallize with Ca) at the time of the content finish blending (the pH of water is generally 6.5 to 6.8), and preferably 4 or more. As a sterilization condition, a treatment having an F value of 4 or more (sterilization at 120 ° C. for 10 minutes) is performed. Next, using a Ca extract as described above as a treatment for a shorts drink system providing a sour taste as a Ca supplement beverage of PH4 or less, adjusting PH3 to PH4 with lactic acid (or organic acids which do not recrystallize with Ca) and filling at 92 ° C. 75 ° C after packing
Sterilize for 15 minutes. Table 2 shows the case of using this natural calcium solution to formulate.

[0009]

[Table 2]

Retort sterilization is performed at 120 ° C. × 10 minutes for PH4 or more, and pasteur sterilization at 75 ° C. for 15 minutes after packing at 92 ° C. for PH4 or less. In this case, a calcium analysis value of 300 mg or more in 350 g of the product was confirmed.

[0011]

As described above, the present invention uses a natural calcium-dissolved stock solution obtained by dissolving unbaked eggshell with lactic acid, thereby making it possible to use conventional Ca raw materials (animal bone meal, shaved meal, coral, etc.).
This invention is excellent in industrial use because it is superior in cost, has a good solubility in water, has a low odor and bitterness, and has a large amount of dissolved calcium.

──────────────────────────────────────────────────続 き Continued on the front page (51) Int.Cl. ⁶ Identification code FI A61K 35/54 AED A61K 35/54 AED

Claims (4)

[Claims] 1. A natural calcium-containing soft drink produced by mixing a natural calcium-dissolved stock solution obtained by dissolving an unbaked eggshell with lactic acid and granulose, lactic acid, flavor, and pure water according to a prescription and sterilizing the mixture. Method. 2. The natural calcium solution stock solution includes 50
100 g of a 100% lactic acid solution and 400 g of pure water at 50 ° C. are mixed to obtain a lactic acid solution, and 30 g of unfired eggshell finely divided into about 400 to 1000 mesh is added thereto while stirring gradually to obtain a mixed liquid of unfired eggshell. Unbaked eggshell mixture 30 ~
The mixture was allowed to react by stirring aging for 50 minutes at 50 ° C., and after aging for 3 to 4 hours, the eggshell was subjected to natural separation (natural precipitation) or forced separation (screw decanter treatment). The method for producing a natural calcium-containing soft drink according to claim 1. 3. The method for producing a natural calcium-containing soft drink according to claim 1, wherein the retort sterilization is carried out so that the product PH is 4 or more and the F value is 4 or more. 4. The method for producing a natural calcium-containing soft drink according to claim 1, wherein pasteurizer sterilization is performed at 75 ° C. for 15 minutes after packing at a filling temperature of 92 ° C. for products PH4 or less.