JPH11223619A - Hydrogen flame ionization detector - Google Patents
Hydrogen flame ionization detectorInfo
- Publication number
- JPH11223619A JPH11223619A JP10041069A JP4106998A JPH11223619A JP H11223619 A JPH11223619 A JP H11223619A JP 10041069 A JP10041069 A JP 10041069A JP 4106998 A JP4106998 A JP 4106998A JP H11223619 A JPH11223619 A JP H11223619A
- Authority
- JP
- Japan
- Prior art keywords
- chimney
- exhaust port
- combustion chamber
- hydrogen flame
- drain water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Abstract
Description
【0001】[0001]
【発明の属する技術分野】本発明は、例えば自動車から
の排気ガス中に含まれる全炭化水素濃度等を測定するた
めに用いられる水素炎イオン化検出器に関する。BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a flame ionization detector used for measuring, for example, the concentration of all hydrocarbons contained in exhaust gas from automobiles.
【0002】[0002]
【従来の技術】水素炎イオン化検出器は有機化合物に感
度があり、含有炭素数にほぼ比例する信号が得られ比較
的安定性に優れているため、ガスクロマトグラフの検出
器や炭化水素等の連続ガス分析装置の検出器等として広
く用いられている。2. Description of the Related Art A flame ionization detector is sensitive to organic compounds, provides a signal substantially proportional to the number of carbon atoms contained therein, and has relatively excellent stability. It is widely used as a detector of a gas analyzer.
【0003】このような水素炎イオン化検出器では、従
来、例えば図2に示されるように、水素炎aを発生させ
るノズルbを有する燃焼室cを内部に形成したチムニー
dは垂直上向きに設けられ、その頂部に排気口eが開設
されており、その側壁部に設けたリードfによってイオ
ン電流が検出されるようになっている。In such a hydrogen flame ionization detector, conventionally, as shown in FIG. 2, for example, a chimney d having a combustion chamber c having a nozzle b for generating a hydrogen flame a is provided vertically upward. An exhaust port e is opened at the top, and an ion current is detected by a lead f provided on the side wall.
【0004】[0004]
【発明が解決しようとする課題】しかし、上述した従来
の水素炎イオン化検出器では、水素が燃焼した時に生成
される水蒸気が、水素炎消火後、排気口eのまわりに凝
縮して水滴となって下部に落下し、ノズルbに付着する
等により、次回に水素炎を発生させた時に、その水滴に
よって検出感度に影響が及ぶこともあり、燃焼室c内で
の絶縁不良が生じることもあった。However, in the above-described conventional flame ionization detector, water vapor generated when hydrogen is burned is condensed around the exhaust port e after the flame is extinguished to form water droplets. The next time a hydrogen flame is generated due to falling to the lower part and adhering to the nozzle b, the detection sensitivity may be affected by the water droplets next time, and the insulation failure in the combustion chamber c may occur. Was.
【0005】また、チムニーdの頂部に開設した排気口
eから温調用の風等が燃焼室c内に吹き込まれることが
あり、これにより、水素炎aにゆらぎが生じ検出信号の
ベースラインの不安定を生じる等の影響を受けることも
あった。又、水蒸気の発生に伴う絶縁不良や水素炎のゆ
らぎも高感度計では無視できない場合があった。[0005] In addition, a temperature control wind or the like may be blown into the combustion chamber c from an exhaust port e opened at the top of the chimney d, thereby causing fluctuations in the hydrogen flame a and causing a non-standard line of the detection signal. In some cases, the stability was affected. In addition, insufficiency of insulation and fluctuation of hydrogen flame due to generation of water vapor sometimes cannot be ignored by a high-sensitivity meter.
【0006】本発明はこのような実情に鑑みてなされ、
水滴や外乱による影響を少なくした水素炎イオン化検出
器を提供することを目的としている。The present invention has been made in view of such circumstances,
It is an object of the present invention to provide a flame ionization detector with reduced influence of water droplets and disturbance.
【0007】[0007]
【課題を解決するための手段】本発明は上述の課題を解
決するための手段を以下のように構成している。すなわ
ち、請求項1に記載の発明では、内部に燃焼室が形成さ
れたチムニーの排気口を下向きに開設し、その排気口か
らドレン水を排出させるように構成してなることを特徴
としている。According to the present invention, means for solving the above-mentioned problems are constituted as follows. That is, the first aspect of the present invention is characterized in that the exhaust port of the chimney in which the combustion chamber is formed is opened downward, and drain water is discharged from the exhaust port.
【0008】チムニーの排気口を下向きに開設したこと
により、その排気口からドレン水を外部に排出させるこ
とができ、水素炎消火後にドレン水が燃焼室の内部に溜
まるのが防止される。Since the exhaust port of the chimney is opened downward, drain water can be discharged from the exhaust port to the outside, and the drain water is prevented from accumulating in the combustion chamber after extinguishing the hydrogen flame.
【0009】請求項2に記載の発明では、請求項1に記
載の発明における前記チムニーを横向きに配置してなる
ことを特徴としている。According to a second aspect of the present invention, the chimney according to the first aspect of the invention is arranged laterally.
【0010】特に、チムニーを横向きに配置することに
より、下向きに開設した排気口からドレン水を外部に排
出させやすくなる。In particular, by arranging the chimney horizontally, drain water can be easily discharged to the outside from an exhaust port opened downward.
【0011】請求項3に記載の発明では、請求項1また
は請求項2に記載の発明における前記チムニーの頂部を
閉塞してなることを特徴としている。According to a third aspect of the present invention, the top of the chimney in the first or second aspect of the invention is closed.
【0012】チムニーの頂部を閉塞することにより、温
調風の吹き込み等による外乱の影響を受けにくくするこ
とができる。By closing the top of the chimney, it is possible to make it less susceptible to disturbances caused by blowing in a temperature control wind.
【0013】[0013]
【発明の実施の形態】以下に本発明の水素炎イオン化検
出器の実施形態を図面を参照しつつ詳細に説明する。図
1は水素炎イオン化検出器の斜視図で、符号1は横向き
円筒状に形成されたチムニーで、その頂部2は閉塞され
ており、その内部に形成される燃焼室3にノズル4が設
けられ、そのノズル4の先端で発生する水素炎5がイオ
ン化してチムニー1の側壁に設けたリード6によってイ
オン電流として検出されるようになっており、その側壁
の下部には、下向きの排気口7が開設されている。DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS An embodiment of a flame ionization detector according to the present invention will be described below in detail with reference to the drawings. FIG. 1 is a perspective view of a flame ionization detector. Reference numeral 1 denotes a chimney formed in a laterally cylindrical shape, the top 2 of which is closed, and a nozzle 4 is provided in a combustion chamber 3 formed therein. The hydrogen flame 5 generated at the tip of the nozzle 4 is ionized and detected as an ion current by a lead 6 provided on the side wall of the chimney 1. A downward exhaust port 7 is provided at a lower portion of the side wall. Has been established.
【0014】上述のような構成により、まず、排気口7
を下向きに開設したことにより、その排気口7からドレ
ン水を外部に排出させることができる。従って、水素炎
消火後にドレン水が燃焼室3の内部に溜まるのが防止さ
れ、水滴による検出感度の低下や燃焼室3内での絶縁不
良等の発生が防がれる。特に、リード6の部分をチムニ
ー上部に設けるとその効果はより増大する。With the above configuration, first, the exhaust port 7
, The drain water can be discharged from the exhaust port 7 to the outside. Therefore, drain water is prevented from accumulating in the combustion chamber 3 after the extinguishing of the hydrogen flame, and a drop in detection sensitivity due to water droplets and occurrence of insulation failure in the combustion chamber 3 are prevented. In particular, when the lead 6 is provided above the chimney, the effect is further increased.
【0015】また、チムニー1を横向けにしてその頂部
2を閉塞していることによって、室内の温調風の吹き込
み等による外乱の影響を受けにくくすることができ、バ
ックグランドの影響を低減し、ベースラインの安定化を
図ることができる。Further, since the chimney 1 is turned sideways and its top 2 is closed, the chimney 1 is less susceptible to disturbances such as the blowing of temperature-controlled air in the room, and the influence of the background is reduced. Thus, the baseline can be stabilized.
【0016】[0016]
【発明の効果】以上説明したように、本発明の水素炎イ
オン化検出器によれば、チムニーの排気口を下向きに開
設したので、水素炎消火後に燃焼室内にドレン水が溜ま
るのが防止され、水滴等による検出感度の低下、フラツ
キや燃焼室内での絶縁不良の発生が防止される。As described above, according to the hydrogen flame ionization detector of the present invention, since the exhaust port of the chimney is opened downward, the accumulation of drain water in the combustion chamber after extinguishing the hydrogen flame is prevented. A drop in detection sensitivity due to water droplets and the like, and occurrence of flicker and insulation failure in the combustion chamber are prevented.
【0017】また、チムニーを横向きに配置することに
より、下向きに開設した排気口からドレン水を外部に排
出させやすくなる。Further, by disposing the chimney horizontally, it becomes easier to drain the drain water from the exhaust port opened downward.
【0018】そして、チムニーの頂部を閉塞することに
より、温調風の吹き込み等による外乱の影響を受けにく
くすることができる。By closing the top of the chimney, it is possible to make it less susceptible to disturbances caused by blowing in a temperature-controlled wind or the like.
【図1】本発明の水素炎イオン化検出器の一実施形態を
示す斜視図である。FIG. 1 is a perspective view showing one embodiment of a hydrogen flame ionization detector of the present invention.
【図2】従来の水素炎イオン化検出器の一例を示す斜視
図である。FIG. 2 is a perspective view showing an example of a conventional flame ionization detector.
1…チムニー、2…頂部、3…燃焼室、7…排気口。 1. Chimney, 2 top, 3 combustion chamber, 7 exhaust port.
Claims (3)
気口を下向きに開設し、その排気口からドレン水を排出
させるように構成してなることを特徴とする水素炎イオ
ン化検出器。1. A flame flame ionization detector characterized in that an exhaust port of a chimney in which a combustion chamber is formed is opened downward, and drain water is discharged from the exhaust port.
とを特徴とする請求項1に記載の水素炎イオン化検出
器。2. The flame ionization detector according to claim 1, wherein the chimney is arranged horizontally.
を特徴とする請求項1または請求項2に記載の水素炎イ
オン化検出器。3. The flame ionization detector according to claim 1, wherein a top portion of the chimney is closed.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP04106998A JP3523483B2 (en) | 1998-02-07 | 1998-02-07 | Flame ionization detector |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP04106998A JP3523483B2 (en) | 1998-02-07 | 1998-02-07 | Flame ionization detector |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH11223619A true JPH11223619A (en) | 1999-08-17 |
JP3523483B2 JP3523483B2 (en) | 2004-04-26 |
Family
ID=12598167
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP04106998A Expired - Fee Related JP3523483B2 (en) | 1998-02-07 | 1998-02-07 | Flame ionization detector |
Country Status (1)
Country | Link |
---|---|
JP (1) | JP3523483B2 (en) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2007218873A (en) * | 2006-02-20 | 2007-08-30 | Shimadzu Corp | Instrument for measuring volatile organic compound |
CN102004120A (en) * | 2010-09-08 | 2011-04-06 | 中国兵器工业第二一三研究所 | Test instrument of flame sensitivity of loading material for initiating explosive device |
CN103512948A (en) * | 2012-06-14 | 2014-01-15 | 株式会社堀场制作所 | Hydrogen flame ionization type exhaust gas analyzer |
CN104181264A (en) * | 2014-08-19 | 2014-12-03 | 北京大学 | Low-pressure hydrogen flame ionization detector |
CN105891395A (en) * | 2015-01-14 | 2016-08-24 | 山东鲁南瑞虹化工仪器有限公司 | Hydrogen flame ionization detector |
-
1998
- 1998-02-07 JP JP04106998A patent/JP3523483B2/en not_active Expired - Fee Related
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2007218873A (en) * | 2006-02-20 | 2007-08-30 | Shimadzu Corp | Instrument for measuring volatile organic compound |
CN102004120A (en) * | 2010-09-08 | 2011-04-06 | 中国兵器工业第二一三研究所 | Test instrument of flame sensitivity of loading material for initiating explosive device |
CN103512948A (en) * | 2012-06-14 | 2014-01-15 | 株式会社堀场制作所 | Hydrogen flame ionization type exhaust gas analyzer |
CN104181264A (en) * | 2014-08-19 | 2014-12-03 | 北京大学 | Low-pressure hydrogen flame ionization detector |
CN104181264B (en) * | 2014-08-19 | 2015-12-30 | 北京大学 | A kind of pressure hydrogen flame ionization detector |
CN105891395A (en) * | 2015-01-14 | 2016-08-24 | 山东鲁南瑞虹化工仪器有限公司 | Hydrogen flame ionization detector |
Also Published As
Publication number | Publication date |
---|---|
JP3523483B2 (en) | 2004-04-26 |
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