JPH1049868A - Cleaning method for substrate for magnetic disk - Google Patents

Cleaning method for substrate for magnetic disk

Info

Publication number
JPH1049868A
JPH1049868A JP8207069A JP20706996A JPH1049868A JP H1049868 A JPH1049868 A JP H1049868A JP 8207069 A JP8207069 A JP 8207069A JP 20706996 A JP20706996 A JP 20706996A JP H1049868 A JPH1049868 A JP H1049868A
Authority
JP
Japan
Prior art keywords
cleaning
substrate
scrub
magnetic disk
rinsing water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP8207069A
Other languages
Japanese (ja)
Inventor
Yukihiro Nishimura
幸浩 西村
Toru Kuroe
徹 黒江
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsubishi Chemical Corp
Original Assignee
Mitsubishi Chemical Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsubishi Chemical Corp filed Critical Mitsubishi Chemical Corp
Priority to JP8207069A priority Critical patent/JPH1049868A/en
Publication of JPH1049868A publication Critical patent/JPH1049868A/en
Pending legal-status Critical Current

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  • Cleaning In General (AREA)
  • Cleaning By Liquid Or Steam (AREA)
  • Manufacturing Of Magnetic Record Carriers (AREA)

Abstract

PROBLEM TO BE SOLVED: To obtain a cleaning method in which the amount of stuck foreign bodies is reduced sharply and which enhances a cleaning effect by pressing a scrubber at a specific speed of rotation to a substrate for a magnetic disk, which is turning, and cleaning the substrate for a specific time with a shower of a specific quantity of rinsing water. SOLUTION: The scrubber 2 which is turning, is pressed to the substrate 1 for a magnetic disk, which is turning, rinsing water is showered form a nozzle 4, and the substrate is cleaned. At this time, the scrubber 2 is set at a speed of rotation of 1400 to 4600rpm, and a quantity of rinsing water is set at 2 liters/ min or more. In addition, the cleaning time by showering the rinsing water is set at 10 to 30sec. Thereby, the number of stuck foreign bodies after a cleaning operation by a urethane-based scrubber can be reduced to 1/2 to 1/3. In addition, the speed of rotation of a scrubber is set at 1500 ±100rpm, while being 750rpm so far, the quantity of rinsing water is set at 2 liters/min or more, while being 1.7 liter/min. so far, and the cleaning time by showering the rinsing water is set at 10 to 30sec. Thereby, the amount of stuck foreign bodies is reduced sharply, and a cleaning effect can be enhanced.

Description

【発明の詳細な説明】DETAILED DESCRIPTION OF THE INVENTION

【0001】[0001]

【発明の属する技術分野】本発明は磁気ディスク用基板
の洗浄方法に係り、特に、テキスチャー加工後の磁気デ
ィスク用基板のスクラブ洗浄を効率的に行う方法に関す
る。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for cleaning a magnetic disk substrate, and more particularly to a method for efficiently performing scrub cleaning of a magnetic disk substrate after texture processing.

【0002】[0002]

【従来の技術】コンピュータ等の外部記憶装置として用
いられる磁気ディスクとしては、一般に、アルミニウム
合金基板にアルマイト処理やNi−Pメッキ等の非磁性
メッキ処理を施した後に、Cr等の下地層を形成し、次
いでCo系合金の磁性層を形成し、更に炭素質の保護層
を形成されたものが使用されている。
2. Description of the Related Art Generally, a magnetic disk used as an external storage device of a computer or the like is formed by subjecting an aluminum alloy substrate to a non-magnetic plating treatment such as alumite treatment or Ni-P plating and then forming an underlayer such as Cr. Then, a magnetic layer of a Co-based alloy is formed, and a carbonaceous protective layer is further formed.

【0003】近年、このような磁気ディスクについては
高密度化が図られ、それに伴ない、磁気ディスクと磁気
ヘッドとの間隔、即ち浮上量は益々小さくなり、最近で
は0.15μm以下が要求されている。このように磁気
ヘッドの浮上量が著しく小さいため、磁気ディスク面に
突起があるとヘッドクラッシュを招き、ディスク表面を
傷つけることがある。また、ヘッドクラッシュに至らな
いような微小な突起でも情報の読み書きの際の種々のエ
ラーの原因となり易い。このため、磁気ディスクの製造
においては、基板へのゴミ等の異物(パーティクル)付
着による表面欠陥を低減するために基板の洗浄処理が重
要となっている。
In recent years, the density of such magnetic disks has been increased, and as a result, the distance between the magnetic disk and the magnetic head, that is, the flying height, has become smaller and smaller. I have. As described above, since the flying height of the magnetic head is extremely small, if there is a projection on the magnetic disk surface, a head crash may be caused, and the disk surface may be damaged. Further, even a minute protrusion that does not lead to a head crash tends to cause various errors when reading and writing information. For this reason, in the manufacture of magnetic disks, cleaning of the substrate is important in order to reduce surface defects due to adhesion of foreign substances (particles) such as dust to the substrate.

【0004】一方、磁気ディスクは大容量化、高密度化
と並行して小型化も進められており、スピンドル回転用
のモーター等も益々小さくなっている。このため、モー
ターのトルクが不足し、磁気ヘッドが磁気ディスク面に
固着したまま浮上しないという現象が生じ易い。この磁
気ヘッドの固着を、磁気ヘッドと磁気ディスク表面との
接触を小さくすることにより防止する手段として、磁気
ディスクの基板表面に微細な溝を形成する、テクスチャ
ー加工と称する表面加工を施す処理が行われている。
On the other hand, the size of magnetic disks has been reduced in parallel with the increase in capacity and density, and motors for rotating spindles and the like have become smaller. For this reason, a phenomenon in which the torque of the motor is insufficient and the magnetic head does not fly while being fixed to the magnetic disk surface is likely to occur. As means for preventing the sticking of the magnetic head by reducing the contact between the magnetic head and the surface of the magnetic disk, a process of forming a fine groove on the substrate surface of the magnetic disk and performing surface processing called texture processing is performed. Have been done.

【0005】従って、従来、磁気ディスクの製造に当っ
ては、前述のメッキ処理を施した基板は、テクスチャー
加工後、テキスチャー加工時に基板表面に付着した有機
物や微小なゴミを除去するために、スクラブ洗浄及び超
音波洗浄等の洗浄が行われ、次いで乾燥後、下地層、磁
性層及び保護層の成膜工程に供される。
[0005] Therefore, conventionally, in the production of a magnetic disk, a substrate subjected to the above-mentioned plating treatment is subjected to scrubbing to remove organic substances and fine dust adhering to the substrate surface during texturing after texturing. Washing such as washing and ultrasonic washing is performed, and then, after drying, the film is subjected to a step of forming an underlayer, a magnetic layer, and a protective layer.

【0006】具体的には、図2に示す如く、テキスチャ
ー加工後、スクラブ洗浄(前スクラブ洗浄)を行い、そ
の後、基板を洗浄水中にて超音波洗浄し、再度スクラブ
洗浄(後スクラブ洗浄)を行った後、超音波を照射する
メガシャワー後、スピンドライ乾燥が行われる。
Specifically, as shown in FIG. 2, after texture processing, scrub cleaning (pre-scrub cleaning) is performed, then the substrate is ultrasonically cleaned in cleaning water, and scrub cleaning (post-scrub cleaning) is performed again. After performing, after mega shower which irradiates an ultrasonic wave, spin dry is performed.

【0007】スクラブ洗浄は、図1に示すように、基板
1の両側に配置したロール状のスクラブ2に配管3から
洗浄水を供給しつつスクラブ2を回転させ、これを回転
する基板1に押し付けて基板1の両表面を擦り洗浄した
後、ノズル4からリンス水を基板1に向けてシャワーす
ることで実施されている。
In the scrub cleaning, as shown in FIG. 1, the scrub 2 is rotated while supplying cleaning water from a pipe 3 to a roll-shaped scrub 2 disposed on both sides of the substrate 1, and the scrub 2 is pressed against the rotating substrate 1. After rubbing and cleaning both surfaces of the substrate 1, rinsing water is showered from the nozzle 4 toward the substrate 1.

【0008】従来、スクラブ2としてはウレタンスポン
ジが用いられ、一般に、次のような条件で洗浄が行われ
ている。
Conventionally, a urethane sponge has been used as the scrub 2, and cleaning is generally performed under the following conditions.

【0009】基板回転数:80rpm スクラブ回転数:750rpm スクラブの基板への押圧力:100g/cm2 洗浄水量:0.75リットル/min(基板の1表面当
り) スクラブによる擦り洗浄時間:4sec リンス水量:1.75リットル/min(基板の1表面
当り) リンス水シャワー時間:2sec
The number of rotations of the substrate: 80 rpm The number of rotations of the scrub: 750 rpm The pressing force of the scrub on the substrate: 100 g / cm 2 The amount of cleaning water: 0.75 liter / min (per one surface of the substrate) The time of scrubbing by scrubbing: The amount of rinsing water: 4 sec 1.75 l / min (per surface of substrate) Rinse water shower time: 2 sec

【0010】[0010]

【発明が解決しようとする課題】前述の如く、磁気ディ
スクの高密度化に伴い、基板表面の欠陥を低減するため
に、基板表面のゴミ等の異物は極力少なくすることが必
要とされる。
As described above, as the density of a magnetic disk increases, it is necessary to reduce foreign matter such as dust on the substrate surface as much as possible in order to reduce defects on the substrate surface.

【0011】しかしながら、従来、テキスチャー加工
後、図2に示すような一連の洗浄、乾燥工程を経て得ら
れる基板は、1表面当りゴミ等の異物が10〜20個付
着しており、十分に清浄であるとは言えない。
However, conventionally, a substrate obtained through a series of washing and drying steps as shown in FIG. 2 after the texturing process has 10 to 20 foreign substances such as dust per one surface, and is sufficiently clean. It cannot be said that.

【0012】本発明は上記従来の問題点を解決し、テキ
スチャー加工後の基板のスクラブ洗浄で基板表面を高度
に清浄化することができる磁気ディスク用基板の洗浄方
法を提供することを目的とする。
SUMMARY OF THE INVENTION It is an object of the present invention to solve the above-mentioned conventional problems and to provide a method of cleaning a substrate for a magnetic disk which can highly clean the substrate surface by scrub cleaning of the substrate after the texture processing. .

【0013】[0013]

【課題を解決するための手段】本発明の磁気ディスク用
基板の洗浄方法は、磁気ディスク用基板に回転するスク
ラブを押し付けて洗浄し、リンス水をシャワーする磁気
ディスク用基板の洗浄方法において、ポリビニルアセタ
ール系樹脂よりなるスクラブを用いて、スクラブ回転数
1400〜1600rpm,リンス水量2リットル/m
in以上、リンス水シャワー時間10〜30secで洗
浄することを特徴とする。
According to a method of cleaning a magnetic disk substrate of the present invention, a method of cleaning a magnetic disk substrate by pressing a rotating scrub against a magnetic disk substrate and showering rinse water is provided. Using a scrub made of an acetal resin, a scrub rotation speed of 1400 to 1600 rpm, and a rinse water amount of 2 liter / m
The cleaning is characterized by washing with a rinse water shower time of 10 to 30 seconds or more.

【0014】なお、本発明において、リンス水量は基板
の1表面当りの水量を示す。
In the present invention, the amount of rinsing water indicates the amount of water per one surface of the substrate.

【0015】本発明によれば、従来のウレタン製スクラ
ブをポリビニルアセタール系樹脂製スクラブに代えるこ
とで、洗浄後の異物付着個数を約1/2〜1/3に低減
できる。また、スクラブ回転数を従来の750rpmか
ら1500±100rpmとすること、リンス水量を従
来の1.7リットル/minから2リットル/min以
上とすること、及びリンス水シャワー時間を従来の2s
ecから10〜30secとすることにより、各々、洗
浄後の異物付着個数を大幅に低減することができ、本発
明では、これらのスクラブ洗浄条件の最適化により、著
しく良好な洗浄効果を得ることができる。
According to the present invention, the number of foreign substances adhered after cleaning can be reduced to about 1/2 to 1/3 by replacing the conventional urethane scrub with a polyvinyl acetal resin scrub. Further, the scrub rotation speed is set to 1500 ± 100 rpm from the conventional 750 rpm, the amount of rinsing water is set to 2 liter / min or more from the conventional 1.7 liter / min, and the rinsing water shower time is set to 2 s of the conventional
By setting the time from ec to 10 to 30 seconds, the number of adhered foreign substances after the cleaning can be greatly reduced. In the present invention, by optimizing the scrub cleaning conditions, a remarkably good cleaning effect can be obtained. it can.

【0016】[0016]

【発明の実施の形態】以下に本発明の実施の形態を説明
する。
Embodiments of the present invention will be described below.

【0017】本発明においては、スクラブ洗浄用スクラ
ブとして、ポリビニルアセタール系樹脂(ポリビニルホ
ルマールを含む広義のポリビニルアセタール樹脂)製ス
クラブを用い、スクラブ回転数1400〜1600rp
mで洗浄を行う。このスクラブ回転数が1400rpm
未満でも1600rpmを超えても洗浄後の異物残存量
が多くなる。
In the present invention, a scrub made of polyvinyl acetal resin (polyvinyl acetal resin in a broad sense including polyvinyl formal) is used as a scrub for scrub cleaning, and the scrub rotation speed is 1400 to 1600 rpm.
Wash with m. This scrub rotation speed is 1400 rpm
If it is less than 1600 rpm or more than 1600 rpm, the amount of foreign matter remaining after cleaning increases.

【0018】本発明において、リンス水量は2リットル
/min以上とする。このリンス水量が2リットル/m
in未満では、十分な洗浄効果が得られない。リンス水
量は過度に多くても洗浄効果の向上効果に大差はなく、
徒に使用水量が増え好ましくない。一般に、リンス水量
は2〜3リットル/minとするのが好ましい。
In the present invention, the amount of rinsing water is 2 liter / min or more. This rinse water volume is 2 liters / m
If it is less than "in", a sufficient cleaning effect cannot be obtained. Even if the amount of rinse water is excessively large, there is no significant difference in the effect of improving the cleaning effect,
However, the amount of water used is undesirably increased. Generally, it is preferable that the amount of rinsing water is 2-3 liters / min.

【0019】また、リンス水シャワー時間は10〜30
秒とする。このリンス水シャワー時間が10秒未満では
十分な洗浄効果が得られない。リンス水シャワー時間が
30秒を超えてもリンス工程時間が徒に長くなり、ま
た、リンス水量が大量になり、洗浄効率が悪くなる。こ
のため、リンス水シャワー時間は10〜30秒とする。
The rinsing water shower time is 10-30.
Seconds. If the rinsing water shower time is less than 10 seconds, a sufficient cleaning effect cannot be obtained. Even if the rinsing water shower time exceeds 30 seconds, the rinsing step time is unnecessarily long, and the amount of rinsing water is large, resulting in poor cleaning efficiency. For this reason, the rinse water shower time is set to 10 to 30 seconds.

【0020】本発明において、スクラブ材質、スクラブ
回転数、リンス水量及びリンス水シャワー時間を上記の
ものとすること以外は、通常のスクラブ洗浄条件を採用
することができ、その他のスクラブ洗浄条件は、例えば
次のような値を採用するのが好ましい。
In the present invention, ordinary scrub cleaning conditions can be adopted except that the scrub material, the scrub rotation speed, the amount of rinse water and the rinse water shower time are as described above. For example, it is preferable to adopt the following values.

【0021】基板回転数:60〜100rpm スクラブの基板への押圧力:100〜200g/cm2 洗浄水量:0.75〜1.5リットル/min スクラブによる擦り洗浄時間:4〜10sec また、本発明において、スクラブ洗浄以外の洗浄及び乾
燥条件についても特に制限はなく常法に従って実施する
ことができる。
Number of rotations of the substrate: 60 to 100 rpm Pressing force of the scrub on the substrate: 100 to 200 g / cm 2 Cleaning water amount: 0.75 to 1.5 L / min Scrub cleaning time by scrub: 4 to 10 sec In the above, washing and drying conditions other than the scrub washing are not particularly limited, and can be carried out according to a conventional method.

【0022】なお、スクラブ洗浄は、一般に、図2に示
す如く、超音波洗浄の前と後に実施される。本発明に係
る特定のスクラブ材質、スクラブ回転数、リンス水量及
びリンス水シャワー時間を採用するスクラブ洗浄は、前
スクラブ洗浄及び後スクラブ洗浄のうちの両方であって
もいずれか一方であっても良いが、少なくとも、微小な
ゴミの除去に特に有効と考えられる後スクラブ洗浄につ
いて、本発明に係るスクラブ洗浄条件を採用するのが好
適である。
The scrub cleaning is generally performed before and after the ultrasonic cleaning as shown in FIG. Scrub cleaning employing the specific scrub material, scrub rotation speed, rinse water amount and rinse water shower time according to the present invention may be both or either one of pre-scrub cleaning and post-scrub cleaning. However, it is preferable to adopt the scrub cleaning conditions according to the present invention at least for post-scrub cleaning which is considered to be particularly effective for removing minute dust.

【0023】[0023]

【実施例】以下に実施例及び比較例を挙げて本発明をよ
り具体的に説明する。
The present invention will be described more specifically below with reference to examples and comparative examples.

【0024】実施例1 図2に示す如く、テキスチャー加工後の磁気ディスク用
基板を、下記条件で前スクラブ洗浄、超音波洗浄、後ス
クラブ洗浄及びメガシャワーした後、スピンドライし、
得られた基板の1表面当りの異物付着個数(サンプル1
0個の平均値)を調べ、結果を表1に示した。
Example 1 As shown in FIG. 2, the magnetic disk substrate after the texture processing was subjected to pre-scrub cleaning, ultrasonic cleaning, post-scrub cleaning and mega shower under the following conditions, and then spin-dried.
The number of foreign substances adhering to one surface of the obtained substrate (sample 1
(Average value of 0) was examined, and the results are shown in Table 1.

【0025】前スクラブ洗浄 スクラブ材質:ウレタン 基板回転数:80rpm スクラブ回転数:750rpm スクラブの基板への押圧力:150g/cm2 洗浄水量:0.75リットル/min スクラブによる擦り洗浄時間:4sec リンス水量:1.5リットル/min リンス水シャワー時間:6sec超音波洗浄 洗浄時間:150sec後スクラブ洗浄 スクラブ材質:ポリビニルアセタール系樹脂(鐘紡社製
「ベルクリン」) 基板回転数:80rpm スクラブ回転数:1500rpm スクラブの基板への押圧力:150g/cm2 洗浄水量:0.75リットル/min スクラブによる擦り洗浄時間:4sec リンス水量:2リットル/min リンス水シャワー時間:10secメガシャワー シャワー時間:8secスピンドライ 乾燥時間:8sec 実施例2,3、比較例1〜8 後スクラブ洗浄の洗浄条件を表1に示すものとしたこと
以外は実施例1と同様にしてテキスチャー加工後の磁気
ディスク用基板の洗浄及び乾燥を行い、得られた基板の
1表面当りの異物付着個数を調べ、結果を表1に示し
た。
Pre-scrub cleaning Scrub material: urethane substrate rotation speed: 80 rpm scrub rotation speed: 750 rpm pressing force of scrub on substrate: 150 g / cm 2 cleaning water amount: 0.75 liter / min scrub cleaning time by scrub: 4 seconds rinse water amount : 1.5 liter / min Rinse water shower time: 6 sec Ultrasonic cleaning time: Scrub cleaning after 150 sec Scrub material: Polyvinyl acetal resin ("Berlin" manufactured by Kanebo Co.) Substrate rotation speed: 80 rpm Scrub rotation speed: 1500 rpm Pressing force on substrate: 150 g / cm 2 Cleaning water amount: 0.75 L / min Scrub cleaning time with scrub: 4 sec Rinse water amount: 2 L / min Rinse water shower time: 10 sec Mega shower shower time: 8 sec Spin dry Drying time: 8 sec Examples 2 and 3 and Comparative Examples 1 to 8 Cleaning of the magnetic disk substrate after texture processing and the same procedure as in Example 1 except that the cleaning conditions for the post-scrub cleaning were as shown in Table 1. After drying, the number of adhered foreign substances on one surface of the obtained substrate was examined. The results are shown in Table 1.

【0026】[0026]

【表1】 [Table 1]

【0027】表1より明らかなように、本発明のスクラ
ブ洗浄条件を採用することにより、著しく良好な洗浄結
果を得ることができる。
As is clear from Table 1, remarkably good cleaning results can be obtained by employing the scrub cleaning conditions of the present invention.

【0028】[0028]

【発明の効果】以上詳述した通り、本発明の磁気ディス
ク用基板の洗浄方法によれば、テキスチャー加工により
基板表面に付着したゴミ等の異物を効率的に洗浄除去す
ることができ、異物付着量の著しく少ない磁気ディスク
用基板を得ることができる。
As described in detail above, according to the method for cleaning a magnetic disk substrate of the present invention, foreign substances such as dust adhered to the substrate surface by texture processing can be efficiently removed by cleaning. A very small amount of magnetic disk substrate can be obtained.

【0029】従って、本発明に従ってスクラブ洗浄した
基板を用いることにより、欠陥のない高品質の磁気ディ
スクを歩留り良く製造することが可能となる。
Therefore, the use of the scrub-cleaned substrate according to the present invention makes it possible to manufacture high-quality magnetic disks free of defects with a high yield.

【図面の簡単な説明】[Brief description of the drawings]

【図1】スクラブ洗浄の実施方法を示す斜視図である。FIG. 1 is a perspective view showing a method of performing scrub cleaning.

【図2】テキスチャー加工後の洗浄、乾燥工程を示す工
程図である。
FIG. 2 is a process diagram showing a washing and drying process after texture processing.

【符号の説明】[Explanation of symbols]

1 基板 2 スクラブ 3 配管 4 ノズル 1 substrate 2 scrub 3 piping 4 nozzle

Claims (1)

【特許請求の範囲】[Claims] 【請求項1】 磁気ディスク用基板に回転するスクラブ
を押し付けて洗浄し、リンス水をシャワーする磁気ディ
スク用基板の洗浄方法において、 ポリビニルアセタール系樹脂よりなるスクラブを用い
て、スクラブ回転数1400〜1600rpm,リンス
水量2リットル/min以上、リンス水シャワー時間1
0〜30secで洗浄することを特徴とする磁気ディス
ク用基板の洗浄方法。
1. A method for cleaning a magnetic disk substrate, in which a rotating scrub is pressed against a magnetic disk substrate and rinsed with water, wherein a scrub made of polyvinyl acetal resin is used, and a scrub rotation speed of 1400 to 1600 rpm is used. , Rinse water amount 2 liter / min or more, rinse water shower time 1
A method for cleaning a substrate for a magnetic disk, wherein the cleaning is performed in 0 to 30 seconds.
JP8207069A 1996-08-06 1996-08-06 Cleaning method for substrate for magnetic disk Pending JPH1049868A (en)

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JP8207069A JPH1049868A (en) 1996-08-06 1996-08-06 Cleaning method for substrate for magnetic disk

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JPH1049868A true JPH1049868A (en) 1998-02-20

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2018535172A (en) * 2015-10-02 2018-11-29 コーニング インコーポレイテッド Removable glass surface treatment and method for reducing particle adhesion
CN109037106A (en) * 2013-10-03 2018-12-18 株式会社荏原制作所 Base plate cleaning device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109037106A (en) * 2013-10-03 2018-12-18 株式会社荏原制作所 Base plate cleaning device
JP2018535172A (en) * 2015-10-02 2018-11-29 コーニング インコーポレイテッド Removable glass surface treatment and method for reducing particle adhesion

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