JPH09145560A - Filter device for oil concentration sensor - Google Patents

Filter device for oil concentration sensor

Info

Publication number
JPH09145560A
JPH09145560A JP32987195A JP32987195A JPH09145560A JP H09145560 A JPH09145560 A JP H09145560A JP 32987195 A JP32987195 A JP 32987195A JP 32987195 A JP32987195 A JP 32987195A JP H09145560 A JPH09145560 A JP H09145560A
Authority
JP
Japan
Prior art keywords
filter
housing
solvent
filter device
oil concentration
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP32987195A
Other languages
Japanese (ja)
Other versions
JP3522933B2 (en
Inventor
Takashi Kawamoto
隆司 川本
Kunio Terada
邦雄 寺田
Hiroshi Fujii
洋 藤井
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Horiba Ltd
Original Assignee
Horiba Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Horiba Ltd filed Critical Horiba Ltd
Priority to JP32987195A priority Critical patent/JP3522933B2/en
Publication of JPH09145560A publication Critical patent/JPH09145560A/en
Application granted granted Critical
Publication of JP3522933B2 publication Critical patent/JP3522933B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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  • Sampling And Sample Adjustment (AREA)
  • Investigating Or Analysing Materials By Optical Means (AREA)

Abstract

PROBLEM TO BE SOLVED: To provide an oil concentration sensor which is less contaminated even when the remaining amount of liquid after a sample is discharged is small and the using amount of a solvent is small and a contaminated state of which can be confirmed from outside. SOLUTION: In a filter apparatus 1, two housing blocks 2, 3 with liquid paths 2a, 3a and air paths 2b, 3b, and a filter 4 held between the two housing blocks 2 and 3 for separating water from a solvent are arranged. A projection 2c for holding the filter and a predetermined recessed part 2d are formed at the center of the housing block 2. A filter-retaining projection 3c, a predetermined recessed part 3d and a filter-retaining projection 3e in a peripheral edge part of the recessed part 3d are formed at the center of the other housing block 3. Moreover, a groove 3g is formed in the vicinity of the whole outer periphery of the recessed part 3d of the other housing block 3. The housing blocks 2 and 3 are transparent bodies.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【発明の属する技術分野】この発明は、水の中に存在す
る油分の濃度を測定する油分濃度計で使用される水と溶
媒分離用のフィルタ装置、特に使用する溶媒を極力少な
くし且つ測定回数を増やすことのできるフィルタ装置に
関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a filter device for separating water from a solvent used in an oil concentration meter for measuring the concentration of oil present in water, particularly to reduce the amount of solvent used and the number of measurements. The present invention relates to a filter device that can increase

【0002】[0002]

【従来の技術】水中に存在する油分濃度を測定する場合
には油分濃度計が使用される。測定に際しては、試料水
にフッ素系の溶媒を入れ、水と油分の溶解した溶媒とを
フィルタ装置で分離した後、溶媒を赤外線分析装置に導
入し、その吸収スペクトルを分析することにより行う。
2. Description of the Related Art An oil concentration meter is used to measure the concentration of oil contained in water. The measurement is carried out by adding a fluorine-based solvent to the sample water, separating the water and the solvent in which the oil component is dissolved by a filter device, introducing the solvent into an infrared analyzer, and analyzing the absorption spectrum.

【0003】即ち、油分濃度計では、図4に示すよう
に、試料水20ccと溶媒10cc程度の混合液を容器
30に入れ、バルブ32により一定量づつ水・溶媒分離
用のフィルタ装置1に送り、水と油分の溶解した溶媒と
を該フィルタ装置1で分離し、溶媒を試料セル31に導
き赤外線を照射する。そして溶媒中の油分を構成する炭
素や水素の結合により吸収された赤外線吸収スペクトル
を分析することにより油分濃度が測定される。33は分
離された水排出用のバルブ、34は分離された溶媒排出
用のバルブである。
That is, in the oil concentration meter, as shown in FIG. 4, a mixed solution of 20 cc of sample water and 10 cc of solvent is put in a container 30 and is sent by a valve 32 to the filter device 1 for water / solvent separation in fixed amounts. , The solvent in which water and oil are dissolved is separated by the filter device 1, and the solvent is guided to the sample cell 31 and irradiated with infrared rays. Then, the oil concentration is measured by analyzing the infrared absorption spectrum absorbed by the bond of carbon and hydrogen constituting the oil in the solvent. Reference numeral 33 is a separated water discharging valve, and 34 is a separated solvent discharging valve.

【0004】[0004]

【発明が解決しようとする課題】油分濃度計では、溶媒
の使用量を少なくすることが望まれているが、従来の水
・溶媒分離用のフィルタ装置ではフィルタを収容してい
るハウジング内部をできるだけ小さくすることで対処し
ていた。そのためフィルタとハウジングとの隙間が小さ
くなり、排出時表面張力等で内部のコ−ナ−周辺に液が
多く残りコンタミネ−ションが生じるという問題があっ
た。例えば、上記するように30cc程度の量を用いた
場合、1回の試料分析に対して大体3cc使用されてい
るが、こうしたコンタミネ−ションにより2回の分析が
可能な程度であった。また、ハウジングも不透明な材料
で製作されているためフィルタの汚れが確認できないと
いう不便があった。
In the oil concentration meter, it is desired to reduce the amount of solvent used, but in the conventional filter device for separating water and solvent, the inside of the housing containing the filter should be as small as possible. I was dealing with it by making it smaller. Therefore, there is a problem that the gap between the filter and the housing becomes small, and a large amount of liquid remains around the inner corner due to surface tension at the time of discharge, resulting in contamination. For example, when an amount of about 30 cc was used as described above, about 3 cc was used for one sample analysis, but such contamination allowed only two analyzes. In addition, since the housing is also made of an opaque material, there is an inconvenience that the dirt of the filter cannot be confirmed.

【0005】この発明は上記する課題に着目してなされ
たものであり、試料排出時の残量液が少なく、溶媒の使
用料が少なくてもコンタミネ−ションも少なく且つ外部
からも汚れの状態が確認できる油分濃度計用フィルタ装
置を提供することを目的としている。
The present invention has been made by paying attention to the above-mentioned problems. The residual liquid at the time of discharging the sample is small, the contamination is small even when the solvent usage fee is small, and the contamination state from the outside is small. It is an object of the present invention to provide a filter device for an oil concentration meter that can be confirmed.

【0006】[0006]

【課題を解決するための手段】即ち、この発明は上記す
る課題を解決するために、内部に液流通用の通路とエ
ア用通路を設けた二つのハウジングブロックと、これら
二つのハウジングブロックの間に挟持され水と溶媒とを
分離するフィルタとを配置してなる油分濃度計用フィル
タ装置において、前記二つのハウジングブロックの一方
のハウジングブロックの中央には所定の凹部が形成さ
れ、他方のハウジングブロックの中央には所定の凹部と
該凹部の周縁部にフィルタ押さえ用の突起が形成され、
更に、他方のハウジングブロックに形成された凹部外周
近傍には全周にわたって溝を形成したことを特徴とす
る。また、前記二つのハウジングブロックの中央には
それぞれフィルタ押さえ用突部を形成することを特徴と
する。或いは前記二つのハウジングブロックの一方若
しくは両方が透明体であることを特徴とする。
In order to solve the above-mentioned problems, the present invention provides two housing blocks having a passage for liquid flow and a passage for air therein, and between these two housing blocks. In a filter device for an oil concentration meter, which is sandwiched between and is provided with a filter for separating water and a solvent, a predetermined recess is formed in the center of one of the two housing blocks, and the other housing block. A predetermined concave portion in the center of the and a projection for pressing the filter is formed on the peripheral portion of the concave portion,
Further, a groove is formed over the entire circumference in the vicinity of the outer circumference of the recess formed in the other housing block. In addition, a filter pressing protrusion is formed at the center of each of the two housing blocks. Alternatively, one or both of the two housing blocks are transparent.

【0007】油分濃度計用フィルタ装置をの手段とす
れば、フィルタとハウジングブロックとの間の間隔及び
空間の容量は大きくなる。しかし、この溝による容量の
増加はフィルタの外周近傍だけであるため溶媒の使用量
を増大させることはない。また、の手段によれば、フ
ィルタは、試料液を濾過する際、いずれか一方のハウジ
ングブロックに全面的に付着することがなくなり、両側
に適切な空間を維持することができるため、フィルタ機
能を十分に発揮することができる。更に、の手段によ
れば、ハウジングブロック内部の汚れの状況も容易に確
認することができる。
If the filter device for the oil concentration meter is used as the means, the space between the filter and the housing block and the volume of the space are increased. However, the increase in capacity due to this groove does not increase the amount of solvent used because it is only in the vicinity of the outer periphery of the filter. Further, according to the means, when the sample liquid is filtered, the filter does not completely adhere to one of the housing blocks, and it is possible to maintain an appropriate space on both sides. It can be fully demonstrated. Further, according to the means (1), it is possible to easily confirm the state of dirt inside the housing block.

【0008】[0008]

【発明の実施の態様】以下、この発明の具体的実施の形
態を図面を参照しながら説明する。図1はこの発明の油
分濃度計用フィルタ装置の断面図、図2は図1のA−A
矢視図、図3は図2のP部拡大図である。油分濃度計で
使用される水・油分分離用のフィルタ装置1は、内部に
液流通用の通路2a,3aとエア用通路2b,3bを設
けた二つのハウジングブロック2,3と、これら二つの
ハウジングブロックの間に挟持され水と溶媒とを分離す
るフィルタ4と、前記液流通用の通路2a,3aに取り
付けられる管継手5,6と、エア用通路2b,3bに取
り付けられる管継手7,8と、で構成される。前記二つ
のハウジングブロック2,3の一方若しくは両方は透明
な合成樹脂或いはガラスの透明体で製作する。また、前
記フィルタ4はフッ素径樹脂の材料、例えばポリテトラ
フルオロエチレン(PTFE)で製作される。
DESCRIPTION OF THE PREFERRED EMBODIMENTS Specific embodiments of the present invention will be described below with reference to the drawings. FIG. 1 is a cross-sectional view of a filter device for an oil content meter of the present invention, and FIG. 2 is AA of FIG.
FIG. 3 is an enlarged view of part P in FIG. A filter device 1 for water / oil separation used in an oil concentration meter includes two housing blocks 2 and 3 having passages 2a and 3a for liquid flow and passages 2b and 3b for air therein, and two of these housing blocks. A filter 4 which is sandwiched between housing blocks to separate water and a solvent, pipe joints 5 and 6 attached to the liquid passages 2a and 3a, and pipe joints 7 attached to the air passages 2b and 3b. 8 and. One or both of the two housing blocks 2 and 3 are made of transparent synthetic resin or a transparent body of glass. Further, the filter 4 is made of a fluorine resin material, for example, polytetrafluoroethylene (PTFE).

【0009】前記一方のハウジングブロック2の中央に
はフィルタ押さえ用の突部2cが形成されると共に所定
半径の凹部2dが形成されている。また、他方のハウジ
ングブロック3の中央にもフィルタ押さえ用の突部3c
が形成されると共に所定半径の凹部3dが形成され、更
に、該凹部3dの周縁部にフィルタ4の外周縁近傍を押
さえるフィルタ押さえ用の突起3eが形成されている。
そして前記他方のハウジングブロック3の外周縁から内
径側には少し低い平坦部3fが形成され、前記一方のハ
ウジングブロック2には外周縁から内径側にかけて前記
平坦部3fに丁度嵌まり合う平坦凸部2eが形成され、
これらの平坦部3fと平坦凸部2eの間にはパッキン9
が挟持されている。
At the center of the one housing block 2, a protrusion 2c for pressing a filter is formed and a recess 2d having a predetermined radius is formed. Further, the protrusion 3c for pressing the filter is also provided in the center of the other housing block 3.
And a concave portion 3d having a predetermined radius are formed, and further, a filter pressing projection 3e for pressing the vicinity of the outer peripheral edge of the filter 4 is formed on the peripheral portion of the concave portion 3d.
A flat portion 3f that is slightly lower than the outer peripheral edge of the other housing block 3 is formed on the inner diameter side, and a flat convex portion that fits exactly on the flat portion 3f from the outer peripheral edge to the inner diameter side on the one housing block 2. 2e is formed,
A packing 9 is provided between the flat portion 3f and the flat convex portion 2e.
Is pinched.

【0010】前記フィルタ4は、ハウジングブロック
2,3中央の両側の突部2c,3cにより挟持されると
共に周縁部は他方のハウジングブロック3に設けたフィ
ルタ押さえ用の突起3eで押さえられる。こうしてフィ
ルタ4の両側には二つのハウジングブロック2,3に設
けられた凹部2d及び3dによる液溜め用の空間が形成
された状態となる。そして該フィルタ4は、試料液を濾
過する際、いずれか一方のハウジングブロックに全面的
に付着することがなくなり、両側に適切な空間を維持す
ることができる。即ち、フィルタ4は、前記二つのハウ
ジングブロック2,3の中央に設けた突部2c,3cに
より挟持すれば該フィルタ機能を十分に発揮することが
できる。尚、これらの突部2c,3cを設けず、フィル
タ押さえ用の突起3eのみでフィルタ4を押さえるよう
にしてもよい。
The filter 4 is sandwiched by the projections 2c, 3c on both sides of the center of the housing blocks 2, 3 and the peripheral edge is pressed by the filter pressing projection 3e provided on the other housing block 3. In this way, on both sides of the filter 4, a space for liquid storage is formed by the recesses 2d and 3d provided in the two housing blocks 2 and 3. When the sample solution is filtered, the filter 4 does not entirely adhere to one of the housing blocks, and it is possible to maintain an appropriate space on both sides. That is, if the filter 4 is sandwiched by the protrusions 2c and 3c provided at the center of the two housing blocks 2 and 3, the filter function can be sufficiently exhibited. It should be noted that the protrusions 2c and 3c may not be provided and the filter 4 may be held only by the filter holding protrusion 3e.

【0011】次に、前記他方のハウジングブロック3に
形成された凹部3dの外周近傍には全周にわたって溝3
gが形成されている。この溝3gにより前記フィルタ4
とハウジングブロック3との間の間隔及び凹部3dの容
量は大きくなる。しかし、この溝3gによる容量の増加
はフィルタ4の外周近傍だけであるため溶媒の使用量を
増大させることはない。
Next, in the vicinity of the outer periphery of the recess 3d formed in the other housing block 3, the groove 3 is formed over the entire periphery.
g is formed. This groove 3g allows the filter 4
The space between the housing and the housing block 3 and the capacity of the recess 3d are increased. However, since the capacity increase due to the groove 3g is only in the vicinity of the outer periphery of the filter 4, the amount of solvent used is not increased.

【0012】この発明の油分濃度計用フィルタ装置は以
上のような構成からなり、二つのハウジングブロック
2,3は間にフィルタ4とパッキン9を挟持した状態で
ボルト10,11により組み込まれる。試料液は管継手
5から導入され、通路二aを通って凹部2dに溜めら
れ、フィルタ4で水と油分を溶解させた溶媒とに分離さ
れ、分離された溶媒は通路3aを通って管継手6から排
出され、そして分析用セル31(図4参照)に導入さ
れ、ここで分析される。また、残った水分はバルブ33
を開けて排出される。この場合、ハウジングブロック3
に形成した溝3gにより表面張力による影響は少なくな
り溶媒の残量も少なくなる。
The filter device for an oil concentration meter according to the present invention has the above-described structure, and the two housing blocks 2 and 3 are assembled by the bolts 10 and 11 with the filter 4 and the packing 9 sandwiched therebetween. The sample liquid is introduced from the pipe joint 5, is accumulated in the recess 2d through the passage 2a, is separated into water and the solvent in which the oil is dissolved by the filter 4, and the separated solvent is passed through the passage 3a to form the pipe joint. 6 and is introduced into an analysis cell 31 (see FIG. 4) where it is analyzed. In addition, the remaining water is stored in the valve 33.
To be discharged. In this case, the housing block 3
By the groove 3g formed in the above, the influence of the surface tension is reduced and the residual amount of the solvent is also reduced.

【0013】[0013]

【発明の効果】以上詳述したように、この発明の油分濃
度計用フィルタ装置によれば、油分濃度を測定する際従
来と殆ど同量の溶媒で更に測定回数を増やすことができ
る。従って、それだけ油分濃度計の濃度測定の精度を向
上させることができる。また、ハウジング内に残留する
溶媒も少なくなり、且つコンタミネ−ションも大幅に少
なくすることができる。また、ハウジングブロックとし
て透明な材料を使用しているため内部の汚れの状況も容
易に確認することができる。
As described in detail above, according to the filter device for an oil content meter of the present invention, when measuring the oil content, the number of measurements can be further increased with almost the same amount of solvent as in the conventional case. Therefore, the accuracy of the concentration measurement of the oil concentration meter can be improved accordingly. Further, the amount of solvent remaining in the housing is reduced, and the contamination can be significantly reduced. In addition, since a transparent material is used for the housing block, it is possible to easily check the state of dirt inside.

【図面の簡単な説明】[Brief description of the drawings]

【図1】この発明の油分濃度計用フィルタ装置の断面図
である。
FIG. 1 is a cross-sectional view of a filter device for an oil concentration meter according to the present invention.

【図2】図1のA−A矢視図である。FIG. 2 is a view as viewed in the direction of arrows AA in FIG. 1;

【図3】図1のフィルタ装置の下部の拡大図である。FIG. 3 is an enlarged view of a lower portion of the filter device of FIG.

【図4】従来から行われている油分濃度計のブロック図
である。
FIG. 4 is a block diagram of a conventional oil concentration meter.

【符号の説明】[Explanation of symbols]

1 フィルタ装置 2 ハウジングブロック 2c 突部 2d 凹部 3 ハウジングブロック 3c 突部 3d 凹部 3e フィルタ押さえ用突起 3g 溝 4 フィルタ 1 Filter Device 2 Housing Block 2c Projection 2d Recess 3 Housing Block 3c Projection 3d Recess 3e Filter Holding Projection 3g Groove 4 Filter

Claims (3)

【特許請求の範囲】[Claims] 【請求項1】 内部に液流通用の通路とエア用通路を設
けた二つのハウジングブロックと、これら二つのハウジ
ングブロックの間に挟持され水と溶媒とを分離するフィ
ルタとを配置してなる油分濃度計用フィルタ装置におい
て、 前記二つのハウジングブロックの一方のハウジングブロ
ックの中央には所定の凹部が形成され、他方のハウジン
グブロックの中央には所定の凹部と該凹部の周縁部にフ
ィルタ押さえ用の突起が形成され、更に、他方のハウジ
ングブロックに形成された凹部外周近傍には全周にわた
って溝を形成したことを特徴とする油分濃度計用のフィ
ルタ装置。
1. An oil component comprising two housing blocks having a liquid passage and an air passage therein, and a filter sandwiched between the two housing blocks to separate water and a solvent. In the filter device for a densitometer, a predetermined concave portion is formed in the center of one of the two housing blocks, and a predetermined concave portion is formed in the center of the other housing block and a filter pressing member is provided at a peripheral portion of the concave portion. A filter device for an oil concentration meter, characterized in that a protrusion is formed and a groove is formed over the entire circumference in the vicinity of the outer periphery of the recess formed in the other housing block.
【請求項2】 二つのハウジングブロックの中央にはそ
れぞれフィルタ押さえ用突部を形成することを特徴とす
る請求項1に項記載の油分濃度計用フィルタ装置。
2. The filter device for an oil concentration meter according to claim 1, wherein a filter pressing protrusion is formed in the center of each of the two housing blocks.
【請求項3】 二つのハウジングブロックの一方若しく
は両方が透明体であることを特徴とする請求項2若しく
は請求項3に記載の油分濃度計用フィル装置。
3. The fill device for an oil concentration meter according to claim 2 or 3, wherein one or both of the two housing blocks is a transparent body.
JP32987195A 1995-11-24 1995-11-24 Filter device for oil concentration meter Expired - Fee Related JP3522933B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP32987195A JP3522933B2 (en) 1995-11-24 1995-11-24 Filter device for oil concentration meter

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP32987195A JP3522933B2 (en) 1995-11-24 1995-11-24 Filter device for oil concentration meter

Publications (2)

Publication Number Publication Date
JPH09145560A true JPH09145560A (en) 1997-06-06
JP3522933B2 JP3522933B2 (en) 2004-04-26

Family

ID=18226180

Family Applications (1)

Application Number Title Priority Date Filing Date
JP32987195A Expired - Fee Related JP3522933B2 (en) 1995-11-24 1995-11-24 Filter device for oil concentration meter

Country Status (1)

Country Link
JP (1) JP3522933B2 (en)

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JPS647909A (en) * 1987-06-29 1989-01-11 Kurita Water Ind Ltd Membrane separator
JPS6456104A (en) * 1987-06-11 1989-03-03 Millipore Corp Filter
JPH0165609U (en) * 1987-10-22 1989-04-26
JPH02125727U (en) * 1989-03-29 1990-10-17
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JPH0560507U (en) * 1992-01-20 1993-08-10 東陶機器株式会社 Strainer structure
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JPH07280799A (en) * 1994-04-11 1995-10-27 Kaiyo Bio Technol Kenkyusho:Kk Method and device for evaluating purification of sand-layer oil contamination
JPH07318466A (en) * 1994-05-27 1995-12-08 Shimadzu Corp Automatic sample preparing device

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