JPH0657670A - Flotator - Google Patents

Flotator

Info

Publication number
JPH0657670A
JPH0657670A JP21964992A JP21964992A JPH0657670A JP H0657670 A JPH0657670 A JP H0657670A JP 21964992 A JP21964992 A JP 21964992A JP 21964992 A JP21964992 A JP 21964992A JP H0657670 A JPH0657670 A JP H0657670A
Authority
JP
Japan
Prior art keywords
air
bubbles
raw material
zone
material liquid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
JP21964992A
Other languages
Japanese (ja)
Inventor
Kenzo Kato
賢造 加藤
Hiroshi Suzumura
鈴村  洋
Shunji Kasuga
俊二 春日
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsubishi Heavy Industries Ltd
Original Assignee
Mitsubishi Heavy Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsubishi Heavy Industries Ltd filed Critical Mitsubishi Heavy Industries Ltd
Priority to JP21964992A priority Critical patent/JPH0657670A/en
Publication of JPH0657670A publication Critical patent/JPH0657670A/en
Withdrawn legal-status Critical Current

Links

Classifications

    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/64Paper recycling

Abstract

PURPOSE:To improve the removing efficiency of fine ink particles by connecting a specific gas-injection apparatus to an air-feeding port of an aeration zone. CONSTITUTION:A gas-injection apparatus 5 having a channel 13 for raw material liquid at the center and a tubular porous material 6 connected to an air feeding port 12 at the back is connected to the air-feeding port 12 of an aeration zone. Fine bubbles can be generated in the injection of air to improve the dispersing effect and the number of bubbles can be controlled simply by changing the injection rate of air.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明は脱インキ装置等に利用で
きるフローテータに関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a floater that can be used in a deinking device or the like.

【0002】[0002]

【従来の技術】従来の加圧型脱インキモジュールを図6
について説明すると、円周方向に設けられた数個の空気
ノズルから圧縮空気1を吹き込み、ドーナツ状の空気室
を形成させる。供給空気の一部を加圧下で原料液2中に
溶解させると同時に、空気室に対する原料流の機械的な
剪断作用により、気泡を発生させる。また図6にはエア
を溶解させるエアレーションゾーンAに続いて、ミキシ
ングゾーンBと分離ゾーンCがある。ミキシングゾーン
Bには、図8に示すように数段の拡大急縮流路9が設け
られている。先ず拡大流路での圧力の急変によるキャビ
テーション作用により、原料中の溶解空気がインキ粒子
を核とした微細な気泡として析出する。次に数段の拡大
急縮流路での加減速流れとマイクロタービュレンス10
により、微細気泡を含む幅広いサイズ分布の気泡とイン
キ粒子の衝突と付着が高度に達成される。一方分離ゾー
ンCでは、インキ粒子を付着した気泡を界面に向けて上
昇させ、D範囲の液面上にインキを含有した泡を形成さ
せる。この時分離ゾーンCの原料のフローパターンを制
御して、適度な乱流を維持することで、繊維のフロスへ
の混入を抑制すると共に、繊維の沈澱を防止して繊維の
歩留りを向上させる。次いで界面上のフロスは、リジェ
クト3として排出され(Eの範囲)、他はアクセプト4
として次の段のPDM装置に導入される。
2. Description of the Related Art A conventional pressure type deinking module is shown in FIG.
The compressed air 1 is blown from several air nozzles provided in the circumferential direction to form a donut-shaped air chamber. At the same time as a part of the supply air is dissolved in the raw material liquid 2 under pressure, bubbles are generated by the mechanical shearing action of the raw material flow on the air chamber. Further, in FIG. 6, there are a mixing zone B and a separation zone C following the aeration zone A for dissolving air. In the mixing zone B, as shown in FIG. 8, several stages of expansion / contraction channels 9 are provided. First, the dissolved air in the raw material is deposited as fine bubbles with the ink particles as the nuclei by the cavitation action due to the sudden change in the pressure in the enlarged flow path. Next, acceleration / deceleration flow and micro turbulence in several stages of expansion / contraction flow
Due to this, collision and adhesion of ink particles with a wide size distribution of bubbles including fine bubbles are highly achieved. On the other hand, in the separation zone C, the bubbles having ink particles attached thereto are raised toward the interface to form bubbles containing the ink on the liquid surface in the D range. At this time, the flow pattern of the raw material in the separation zone C is controlled to maintain an appropriate turbulent flow, thereby suppressing the mixing of the fibers into the floss and preventing the precipitation of the fibers to improve the fiber yield. The floss on the interface is then ejected as reject 3 (range E) and the others are accept 4
Is introduced into the PDM device in the next stage.

【0003】[0003]

【発明が解決しようとする課題】近年回収故紙の上質紙
への再利用を目指すことが盛んになり、白色度を従来以
上に向上させることが望まれており、脱インキ装置にお
いて、特に10μm以下の微細なインキ粒子を除去する
必要が生じている。また浮選機にて微細な粒子を除去す
るためには、粒子の気泡への付着のチャンスを増大させ
ることが先ず必要であり、空気吹込量の増大、滞留時間
の延長、気泡の微細化などの対策がとられていた。また
気泡径がフローテーションに与える影響については、鉱
山に使用された時代から研究されており、気泡径が粒子
径の5倍の時に最も効果が大きいことが分かっている。
10μm以下のインキ粒子除去のためには、50μm以
下の気泡を発生させることが望ましいが、従来の装置で
は不充分であった。本発明は前記従来の課題を解決する
ために提案されたものである。
In recent years, it has become popular to aim to reuse recovered waste paper as high-quality paper, and it is desired to improve the whiteness more than ever before. Especially, in the deinking device, it is 10 μm or less. It is necessary to remove the fine ink particles of In addition, in order to remove fine particles with a flotation machine, it is first necessary to increase the chances of particles adhering to the bubbles, such as increasing the amount of air blown, extending the residence time, and making the bubbles finer. Was taken. The effect of bubble size on flotation has been studied since the time it was used in mines, and it has been found that the effect is greatest when the bubble size is 5 times the particle size.
In order to remove ink particles having a size of 10 μm or less, it is desirable to generate bubbles having a size of 50 μm or less, but it has been insufficient with the conventional apparatus. The present invention has been proposed to solve the above conventional problems.

【0004】[0004]

【課題を解決するための手段】このため本発明は、主と
して原料液に空気を吹込むエアレーションゾーン、原料
液中のインキ粒子を核として気泡を析出させるミキシン
グゾーン、前記気泡を浮上分離させる分離ゾーンから構
成されたフローテータにおいて、前記エアレーションゾ
ーンの空気供給口に、中央部に原料液通路を備え、背面
に空気供給口に通ずる管状多孔質体を設けた気体注入装
置を連通させてなるもので、これを課題解決のための手
段とするものである。
For this reason, the present invention is mainly directed to an aeration zone for blowing air into a raw material liquid, a mixing zone for precipitating bubbles with ink particles in the raw material liquid as nuclei, and a separation zone for floating and separating the bubbles. In the floatator constituted by, the air supply port of the aeration zone is provided with a raw material liquid passage in the central portion, and a gas injection device provided with a tubular porous body communicating with the air supply port on the back side is connected to the air supply port. , Is a means for solving the problems.

【0005】[0005]

【作用】本発明は中央部に原料液通路を有する管状多孔
質体を設けたので、従来型と比較して空気注入時におい
て微細な気泡を発生させることができ、分散効果も大き
くなる。また従来方式では、気体注入量を増加させれ
ば、気泡が合体して1〜2mmφの気泡となり易いが、
本発明では微細気泡となっているため合体しにくい。更
に空気注入量を変化させることによって微細粒径を保っ
たまま気泡数をコントロールすることが可能となる。
In the present invention, since the tubular porous body having the raw material liquid passage in the central portion is provided, fine bubbles can be generated at the time of injecting air as compared with the conventional type, and the dispersion effect is increased. Further, in the conventional method, if the gas injection amount is increased, the bubbles are likely to coalesce into a bubble of 1 to 2 mmφ,
In the present invention, since it is a fine bubble, it is difficult to unite. Furthermore, by changing the air injection amount, it becomes possible to control the number of bubbles while maintaining the fine particle size.

【0006】[0006]

【実施例】以下本発明を図面の実施例について説明する
と、図1〜図2は本発明の実施例を示し、図1は主とし
て原料液2に空気1を吹込むエアレーションゾーンA、
原料液2中のインキ粒子を核として気泡を析出させるミ
キシングゾーンB、前記気泡を浮上分離させる分離ゾー
ンCから構成されているフローテータを示す。また図2
の如く前記エアレーションゾーンAには空気供給口12
に通じる気体注入装置5を設けてあり、同装置5は中央
部に原料液2の通路13を備え、背面に同空気供給口1
2に通じる管状多孔質体6を設けた構造としてある。な
お、7はサポート、8は微細気泡である。次に図2によ
り作用を説明すると、図2は本発明の気体の注入手段を
示し、空気注入口12から供給された空気1は、管状多
孔質体6の微細孔(30〜50μmmφ)を通り、微細
気泡8となって通路13中の原料液2中に分散してい
く。図1は気体注入装置5を用いたフローテータの全体
図を示し、また図2に示す如く管状多孔質体6は、サポ
ート7によりフローテータの円管11の内側に固定され
ている。一方使用する多孔質体6としては、Al2 3
質の人工砥粒の焼結体などが先ず考えられるが、耐食性
があって加工可能な多孔質体であれば何でも十分利用可
能であり、金属、プラスチックなどの使用も考えられ
る。
DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS The present invention will be described below with reference to the accompanying drawings. FIGS. 1 and 2 show an embodiment of the present invention. FIG. 1 shows an aeration zone A in which air 1 is mainly blown into a raw material liquid 2.
1 shows a floater composed of a mixing zone B for precipitating air bubbles with ink particles in the raw material liquid 2 as nuclei, and a separation zone C for floating and separating the air bubbles. See also FIG.
As described above, the air supply port 12 is provided in the aeration zone A.
Is provided with a gas injecting device 5 which communicates with the air supply port 5.
2 has a structure in which a tubular porous body 6 leading to 2 is provided. In addition, 7 is a support and 8 is a fine bubble. Next, the operation will be described with reference to FIG. 2. FIG. 2 shows the gas injecting means of the present invention. The air 1 supplied from the air injecting port 12 passes through the fine pores (30 to 50 μmmφ) of the tubular porous body 6. The fine bubbles 8 are dispersed in the raw material liquid 2 in the passage 13. FIG. 1 shows an overall view of a floatator using a gas injection device 5, and as shown in FIG. 2, a tubular porous body 6 is fixed inside a circular tube 11 of the floatator by a support 7. On the other hand, the porous body 6 used is Al 2 O 3
First, a sintered body of artificial abrasive grains of high quality can be considered, but any porous body having corrosion resistance and capable of being processed can be sufficiently used, and use of metal, plastic or the like is also conceivable.

【0007】次に下記具体例について本発明を説明する
と、多孔質体の平均孔径は40μmで、同一の原料(新
聞古紙)、溶液(水800リットルに対し脱墨剤40
g、水酸化ナトリウム84.2g、珪酸ソーダ600
g、過酸化水素229g)で処理したものを、濃度1%
になるように希釈したものを用いた。また処理液量は、
285リットル/min、ガス液比=20%、入口圧力
=2kgf/cm2 の場合、PDMを6段直列につない
で、最終段で測定した脱インキ率を図3に示す。脱イン
キ率はJIS法に従い、手抄き紙により濾過し、その紙
を粒子アナライザーにより測定した値を用いた(JIS
−TAPPI 紙パルプ試験方法NO.39−82)。
その結果、本発明の場合は従来法よりも、特に10μm
以下の粒子径インキの除去性能が高いことが分かった。
次に前記具体例と同様の条件で、ガス量を増やしてガス
/液=30%の場合のテスト結果を図4に示す。また前
記2つの具体例と同様の条件下において、多孔質体の平
均孔径と平均気泡径の関係のテスト結果を図5に示す。
この時の多孔率の条件は30%とし、気泡径50μm以
下を多量に発生させる平均孔径は40μmであった。ま
た気泡径50μmを保つためには、多孔質体の平均孔径
を40μm以下にすることが望ましい。
The present invention will be described with reference to the following specific examples. The average pore size of the porous body is 40 μm, and the same raw material (newspaper waste) and solution (800 liters of water to 40 parts of the deinking agent) are used.
g, sodium hydroxide 84.2 g, sodium silicate 600
g, hydrogen peroxide 229 g) treated with a concentration of 1%
What was diluted so that it became The amount of processing liquid is
In the case of 285 liter / min, gas-liquid ratio = 20%, and inlet pressure = 2 kgf / cm 2 , PDM is connected in six stages in series and the deinking rate measured at the final stage is shown in FIG. For the deinking rate, a value obtained by filtering with hand-made paper according to the JIS method and measuring the paper with a particle analyzer was used (JIS
-TAPPI paper pulp test method NO. 39-82).
As a result, in the case of the present invention, especially 10 μm
It was found that the following particle size ink removal performance is high.
Next, FIG. 4 shows the test results when the amount of gas was increased and gas / liquid = 30% under the same conditions as in the above specific example. Further, FIG. 5 shows the test results of the relationship between the average pore diameter and the average cell diameter of the porous body under the same conditions as the above two specific examples.
At this time, the porosity was set to 30%, and the average pore size for generating a large amount of bubbles having a diameter of 50 μm or less was 40 μm. Further, in order to maintain the bubble diameter of 50 μm, it is desirable that the average pore diameter of the porous body be 40 μm or less.

【0008】[0008]

【発明の効果】以上詳細に説明した如く本発明は構成さ
れているので、従来方式に比べて微細径の気泡を多く発
生させることにより、細かい(10μm以下)インキ粒
子の除去性を向上させることができる。また本発明は加
圧型であるため、液中に空気を溶解させることができ、
従って溶解空気が減圧された時に発生する未溶解(析
出)空気を利用することができる。更に本発明は空気注
入時において微細径の気泡を発生させるため、空気注入
量の加減により微細径の気泡を保ったまま気泡数をコン
トロールできる。
As described in detail above, the present invention is constituted, and therefore, the removal of fine (10 μm or less) ink particles is improved by generating a large number of bubbles having a fine diameter as compared with the conventional method. You can Further, since the present invention is a pressure type, it is possible to dissolve air in the liquid,
Therefore, undissolved (precipitated) air generated when the dissolved air is depressurized can be used. Further, according to the present invention, bubbles having a small diameter are generated at the time of injecting air. Therefore, the number of bubbles can be controlled while maintaining the bubbles having a small diameter by adjusting the injection amount of air.

【図面の簡単な説明】[Brief description of drawings]

【図1】本発明の実施例に係るフローテータ全体の1部
断面側面図である。
FIG. 1 is a partial cross-sectional side view of an entire floatator according to an embodiment of the present invention.

【図2】本発明の実施例を示すフローテータの気体注入
装置の詳細断面図である。
FIG. 2 is a detailed cross-sectional view of a gas injector for a floater showing an embodiment of the present invention.

【図3】本発明と従来におけるインキ粒子サイズとイン
キ除去率との関係を示す線図である。
FIG. 3 is a diagram showing the relationship between the ink particle size and the ink removal rate in the present invention and the related art.

【図4】本発明と従来における図3と異なるインキ粒子
サイズとインキ除去率との関係を示す線図である。
FIG. 4 is a diagram showing a relationship between an ink particle size and an ink removal rate, which is different from that of FIG. 3 in the present invention and the related art.

【図5】本発明における多孔質体の平均孔径と平均気泡
径との関係を示す線図である。
FIG. 5 is a diagram showing the relationship between the average pore diameter and the average cell diameter of the porous body in the present invention.

【図6】従来のフローテータの全体を示す1部断面側面
図である。
FIG. 6 is a partial sectional side view showing the entire conventional floater.

【図7】従来のフローテータの気体注入口を示す断面図
である。
FIG. 7 is a cross-sectional view showing a gas inlet of a conventional floatator.

【図8】従来のフローテータにおけるミキシングゾーン
を示す断面図である。
FIG. 8 is a sectional view showing a mixing zone in a conventional floater.

【符号の説明】[Explanation of symbols]

1 空気 2 原料液 3 リジェクト 4 アクセプト 5 気体注入装置 6 管状多孔質体 7 サポート 8 微細化された空気 11 円管 12 空気供給口 13 原料液の通路 A エアレーションゾーン B ミキシングゾーン C 分離ゾーン D 気泡分離 E フロス分離 1 Air 2 Raw Material Liquid 3 Reject 4 Accept 5 Gas Injector 6 Tubular Porous Body 7 Support 8 Micronized Air 11 Circular Tube 12 Air Supply Port 13 Raw Material Passage A Aeration Zone B Mixing Zone C Separation Zone D Bubble Separation E floss separation

Claims (1)

【特許請求の範囲】[Claims] 【請求項1】 主として原料液に空気を吹込むエアレー
ションゾーン、原料液中のインキ粒子を核として気泡を
析出させるミキシングゾーン、前記気泡を浮上分離させ
る分離ゾーンから構成されたフローテータにおいて、前
記エアレーションゾーンの空気供給口に、中央部に原料
液通路を備え、背面に空気供給口に通ずる管状多孔質体
を設けた気体注入装置を連通させたことを特徴とするフ
ローテータ。
1. A floater comprising mainly an aeration zone for blowing air into a raw material liquid, a mixing zone for precipitating bubbles with ink particles in the raw material liquid as nuclei, and a separation zone for floating and separating the bubbles. A floater, characterized in that a gas injection device having a raw material liquid passage in the center and a tubular porous body communicating with the air supply port on the back is connected to the air supply port of the zone.
JP21964992A 1992-07-28 1992-07-28 Flotator Withdrawn JPH0657670A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP21964992A JPH0657670A (en) 1992-07-28 1992-07-28 Flotator

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP21964992A JPH0657670A (en) 1992-07-28 1992-07-28 Flotator

Publications (1)

Publication Number Publication Date
JPH0657670A true JPH0657670A (en) 1994-03-01

Family

ID=16738827

Family Applications (1)

Application Number Title Priority Date Filing Date
JP21964992A Withdrawn JPH0657670A (en) 1992-07-28 1992-07-28 Flotator

Country Status (1)

Country Link
JP (1) JPH0657670A (en)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH08106503A (en) * 1994-10-05 1996-04-23 Focus Syst:Kk Document processing system
WO2005012632A1 (en) * 2003-07-31 2005-02-10 Nippon Paper Industries Co., Ltd. Process for producing recycled pulp, method of modifying pulp fiber surface and contaminant, and pulp treating apparatus
WO2006085598A1 (en) * 2005-02-09 2006-08-17 Nippon Paper Industries Co., Ltd. Method for beating of pulp, method for treatment of process water, and process for producing pulp and paper
JP2006249648A (en) * 2005-02-09 2006-09-21 Nippon Paper Industries Co Ltd Method for beating pulp
JP2006257621A (en) * 2005-02-18 2006-09-28 Nippon Paper Industries Co Ltd Book printing paper
JP2006283204A (en) * 2005-03-31 2006-10-19 Nippon Paper Industries Co Ltd Method for treating process water, and method for producing pulp, paper
WO2007052760A1 (en) * 2005-11-04 2007-05-10 Nippon Paper Industries Co., Ltd. Apparatus for treating papermaking feedstock
JP2008544098A (en) * 2005-06-17 2008-12-04 メトソ ペーパー インク Flotation cell
KR20180028322A (en) * 2016-09-08 2018-03-16 서울대학교산학협력단 Separationg method of particles

Cited By (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH08106503A (en) * 1994-10-05 1996-04-23 Focus Syst:Kk Document processing system
JPWO2005012632A1 (en) * 2003-07-31 2007-09-27 日本製紙株式会社 Method for producing recycled pulp, method for modifying pulp fiber surface and impurities, and pulp processing apparatus
WO2005012632A1 (en) * 2003-07-31 2005-02-10 Nippon Paper Industries Co., Ltd. Process for producing recycled pulp, method of modifying pulp fiber surface and contaminant, and pulp treating apparatus
US7727355B2 (en) 2003-07-31 2010-06-01 Nippon Paper Industries Co., Ltd. Methods for producing recycled pulp and methods for modifying pulp fiber surfaces using liquid jet cavitation
KR100926819B1 (en) * 2003-07-31 2009-11-12 니뽄 세이시 가부시끼가이샤 Process for producing recycled pulp, method of modifying pulp fiber surface and contaminant, and pulp treating apparatus
US7967947B2 (en) 2005-02-09 2011-06-28 Nippon Paper Industries Co., Ltd. Methods for beating pulp, methods for treating process waters, and methods for producing pulp and paper
WO2006085598A1 (en) * 2005-02-09 2006-08-17 Nippon Paper Industries Co., Ltd. Method for beating of pulp, method for treatment of process water, and process for producing pulp and paper
NO340824B1 (en) * 2005-02-09 2017-06-26 Jujo Paper Co Ltd Method of painting pulp, and method of preparing pulp
US8784608B2 (en) 2005-02-09 2014-07-22 Nippon Paper Industries Co., Ltd. Methods for beating pulp, methods for treating process waters, and methods for producing pulp and paper
JP4546936B2 (en) * 2005-02-09 2010-09-22 日本製紙株式会社 Pulp beating method
JP2006249648A (en) * 2005-02-09 2006-09-21 Nippon Paper Industries Co Ltd Method for beating pulp
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