JPH06127965A - Apparatus for production of optical fiber preform - Google Patents

Apparatus for production of optical fiber preform

Info

Publication number
JPH06127965A
JPH06127965A JP27981392A JP27981392A JPH06127965A JP H06127965 A JPH06127965 A JP H06127965A JP 27981392 A JP27981392 A JP 27981392A JP 27981392 A JP27981392 A JP 27981392A JP H06127965 A JPH06127965 A JP H06127965A
Authority
JP
Japan
Prior art keywords
optical fiber
fiber preform
reaction vessel
burner
exhaust pipe
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP27981392A
Other languages
Japanese (ja)
Other versions
JP3287618B2 (en
Inventor
Yukio Komura
幸夫 香村
Yasuhiro Naka
恭宏 仲
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Furukawa Electric Co Ltd
Original Assignee
Furukawa Electric Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Furukawa Electric Co Ltd filed Critical Furukawa Electric Co Ltd
Priority to JP27981392A priority Critical patent/JP3287618B2/en
Publication of JPH06127965A publication Critical patent/JPH06127965A/en
Application granted granted Critical
Publication of JP3287618B2 publication Critical patent/JP3287618B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03BMANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
    • C03B37/00Manufacture or treatment of flakes, fibres, or filaments from softened glass, minerals, or slags
    • C03B37/01Manufacture of glass fibres or filaments
    • C03B37/012Manufacture of preforms for drawing fibres or filaments
    • C03B37/014Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means, e.g. vapour phase deposition of bulk porous glass either by outside vapour deposition [OVD], or by outside vapour phase oxidation [OVPO] or by vapour axial deposition [VAD]
    • C03B37/0144Means for after-treatment or catching of worked reactant gases

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Glass Melting And Manufacturing (AREA)
  • Manufacture, Treatment Of Glass Fibers (AREA)

Abstract

PURPOSE:To provide the apparatus for production of the optical fiber preform which can correctly create the conc. distribution of the refractive index imparting agent in the optical fiber base material. CONSTITUTION:The optical fiber preform 6 is formed by depositing glass particles synthesized in flames 2a, 3a of a core burner 2 and a clad burner 3 at the front end of a seed rod 5 in a reaction vessel 1. The unnecessary gas in the reaction vessel 1 is discharged outside the reaction vessel 1 by a discharge pipe 4. A swirling flow generating unit 8 which generates swirling flow like tornade is provided around the inlet of the discharge pipe 4 in the reaction vessel 1.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明は、反応容器の中でバーナ
で合成したガラス微粒子を種棒の先端に堆積させて光フ
ァイバ母材を形成する光ファイバ母材製造装置に関する
ものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to an optical fiber preform producing apparatus for depositing glass fine particles synthesized by a burner in a reaction vessel on the tip of a seed rod to form an optical fiber preform.

【0002】[0002]

【従来の技術】図4は、従来の光ファイバ母材製造装置
の例を示したものである。該光ファイバ母材製造装置
は、反応容器1にコアバーナ2,クラッドバーナ3と排
気管4とを図示のように対向配置し,反応容器1の開口
部からその内部に種棒5を下向きに挿入し、コアバーナ
2の火炎2a中で合成したコア用のガラス微粒子とクラ
ッドバーナ3の火炎3a中で合成したクラッド用のガラ
ス微粒子とを、回転しつつ引上げる種棒5の下端に堆積
させて光ファイバ母材6の製造を行っていた。光ファイ
バ母材6として付着しないガラス微粒子及びHCl等
は、光ファイバ母材6を間にしてコアバーナ2及びクラ
ッドバーナ3の反対側に存在する排気管4より排気させ
ていた。
2. Description of the Related Art FIG. 4 shows an example of a conventional optical fiber preform manufacturing apparatus. In the optical fiber preform manufacturing apparatus, a core burner 2, a clad burner 3 and an exhaust pipe 4 are arranged to face each other in a reaction vessel 1, and a seed rod 5 is inserted downward from the opening of the reaction vessel 1 into the reaction vessel 1. Then, the glass particles for the core synthesized in the flame 2a of the core burner 2 and the glass particles for the clad synthesized in the flame 3a of the clad burner 3 are deposited on the lower end of the seed rod 5 that is pulled up while rotating, and light is emitted. The fiber preform 6 was manufactured. The glass particles, HCl, and the like that do not adhere as the optical fiber base material 6 were exhausted from the exhaust pipe 4 existing on the opposite side of the core burner 2 and the clad burner 3 with the optical fiber base material 6 in between.

【0003】この場合、コアバーナ2の先端での反応
は、次の通りである。 SiCl4 +2H2 O→SiO2 +4HCl GeCl4 +2H2 O→GeO2 +4HCl ここで、H2 Oは水素ガスと酸素ガスを原料ガスと共に
コアバーナ2に供給して、酸水素火炎2aを作ることに
より形成される。
In this case, the reaction at the tip of the core burner 2 is as follows. SiCl 4 + 2H 2 O → SiO 2 + 4HCl GeCl 4 + 2H 2 O → GeO 2 + 4HCl Here, H 2 O is formed by supplying hydrogen gas and oxygen gas together with the source gas to the core burner 2 to form an oxyhydrogen flame 2a. To be done.

【0004】このような光ファイバ母材製造装置では、
屈折率付与剤であるGeO2 をSiO2 からなる光ファ
イバ母材6内に設計通りに分布させることが必要であ
る。即ち、図5(A)に示すようにコア部(SiO2
GeO2 )6aとクラッド部(SiO2 )6bとからな
る光ファイバ母材6内に、図5(B)に示すようにGe
2 の濃度分布を正確に決めることが、シングルモード
光ファイバの屈折率のプロファイルを決定する上で必要
である。光ファイバ母材6内のGeO2 の濃度分布が正
しく形成されないと、例えば図6に示すように該GeO
2 の濃度分布の裾部及び上部がだれてしまうことにな
る。
In such an optical fiber preform manufacturing apparatus,
It is necessary to distribute GeO 2 which is a refractive index imparting agent in the optical fiber preform 6 made of SiO 2 as designed. That is, as shown in FIG. 5 (A), the core portion (SiO 2 +
As shown in FIG. 5 (B), the GeO 2 ) 6a and the cladding (SiO 2 ) 6b are placed in the optical fiber preform 6 as shown in FIG.
Accurate determination of the O 2 concentration distribution is necessary for determining the profile of the refractive index of the single mode optical fiber. If the concentration distribution of GeO 2 in the optical fiber preform 6 is not properly formed, for example, as shown in FIG.
The bottom and the top of the concentration distribution of 2 will be dripping.

【0005】[0005]

【発明が解決しようとする課題】しかしながら、従来の
光ファイバ母材製造装置では、図4及び図7に示すよう
に各火炎2a,3aの周囲及び排気管4の入口の周囲等
で無数のガスの渦7等による乱れがあり、ガス等の流れ
が時間的,空間的に安定しないため、コアバーナ2から
供給されるGeO2 の流れが乱れて、光ファイバ母材6
のコア部6aに正しく堆積せず、該光ファイバ母材6内
のGeO2 の濃度分布を正しく作ることができない問題
点があった。
However, in the conventional optical fiber preform manufacturing apparatus, as shown in FIGS. 4 and 7, innumerable gases are present around the flames 2a and 3a and around the inlet of the exhaust pipe 4. There is turbulence due to the vortex 7 and the like, and the flow of gas and the like is not stable in time and space, so the flow of GeO 2 supplied from the core burner 2 is disturbed, and the optical fiber preform 6
However, there was a problem that the GeO 2 concentration distribution in the optical fiber preform 6 could not be made correctly because it was not correctly deposited on the core portion 6a.

【0006】反応容器1内のガスの流れを安定させるた
め、(イ)種棒5の上部からダウンフローを与える、
(ロ)バーナ2,3の周囲からエアーを供給する、
(ハ)排気管4の吸引風量を大きくする等の対策が考え
られているが、いずれも問題があり、光ファイバ母材6
内のGeO2 の濃度分布を正しく作ることができる光フ
ァイバ母材製造装置の開発が望まれている。
In order to stabilize the gas flow in the reaction vessel 1, (a) downflow is applied from the upper part of the seed rod 5.
(B) Air is supplied from around the burners 2 and 3.
(C) Measures such as increasing the suctioned air volume of the exhaust pipe 4 have been considered, but all have problems, and the optical fiber preform 6
It is desired to develop an optical fiber preform manufacturing apparatus capable of accurately forming the GeO 2 concentration distribution in the inside.

【0007】本発明の目的は、光ファイバ母材内の屈折
率付与剤の濃度分布を正しく作ることができる光ファイ
バ母材製造装置を提供することにある。
An object of the present invention is to provide an optical fiber preform manufacturing apparatus capable of accurately forming the concentration distribution of the refractive index imparting agent in the optical fiber preform.

【0008】[0008]

【課題を解決するための手段】上記の目的を達成する本
発明の構成を説明すると、本発明はバーナの火炎中で合
成したガラス微粒子を反応容器の中で種棒の先端に堆積
させて光ファイバ母材を形成し、前記反応容器内の不要
ガスを排気管で該反応容器の外に排出させる光ファイバ
母材製造装置において、前記反応容器内の前記排気管の
入口の周囲に、旋回流を発生させる旋回流発生ユニット
が設けられていることを特徴とする。
The structure of the present invention which achieves the above-mentioned object will be described. The present invention is that the glass fine particles synthesized in the flame of a burner are deposited on the tip of a seed rod in a reaction vessel to emit light. In an optical fiber preform manufacturing apparatus that forms a fiber preform and discharges unnecessary gas in the reaction vessel to the outside of the reaction vessel by an exhaust pipe, a swirling flow around the inlet of the exhaust pipe in the reaction vessel. It is characterized in that a swirling flow generating unit for generating is generated.

【0009】[0009]

【作用】このように反応容器内の排気管の入口の周囲
に、旋回流を発生させる旋回流発生ユニットを設ける
と、該反応容器内の排気管の入口の周囲に龍巻のような
旋回流が発生し、この旋回流で排気管の吸引能力が高ま
る。その結果、反応容器内で浮遊している不要なガス等
がこの旋回流により吸引されて除去され、該反応容器内
のガス等の流れが安定し、コアバーナから供給される屈
折率付与剤が光ファイバ母材のコア部に正しく堆積し、
光ファイバ母材内に屈折率付与剤の濃度分布を正しく形
成することができる。
When a swirl flow generating unit for generating a swirl flow is provided around the inlet of the exhaust pipe in the reaction container as described above, a swirl-like swirl flow is formed around the inlet of the exhaust pipe in the reaction container. Occurs, and the swirling flow enhances the suction capability of the exhaust pipe. As a result, unnecessary gas floating in the reaction container is sucked and removed by this swirling flow, the flow of gas etc. in the reaction container is stabilized, and the refractive index imparting agent supplied from the core burner emits light. Accurately deposited on the core of the fiber base material,
It is possible to correctly form the concentration distribution of the refractive index imparting agent in the optical fiber preform.

【0010】[0010]

【実施例】図1及び図3は、本発明に係る光ファイバ母
材製造装置の一実施例を示したものである。なお、前述
した図4と対応する部分には、同一符号を付けて示して
いる。
1 and 3 show one embodiment of an optical fiber preform manufacturing apparatus according to the present invention. The parts corresponding to those in FIG. 4 described above are denoted by the same reference numerals.

【0011】本実施例では、反応容器1内の排気管4の
入口の周囲に、龍巻のような旋回流を発生させる旋回流
発生ユニット8を設けている。該旋回流発生ユニット8
は、所定間隔で同軸配置された内筒8aと外筒8bの両
端が端板8c,8dで閉塞され、内筒8aと外筒8bと
の間にはオリフィス8eが設けられ、外筒8bの先端外
周には複数のノズル8fが設けられ、外筒8bの基端に
はインレット部8gが設けられた構造になっている。
In this embodiment, a swirl flow generating unit 8 for generating a swirl flow like a tornado is provided around the inlet of the exhaust pipe 4 in the reaction vessel 1. The swirl flow generation unit 8
Both ends of an inner cylinder 8a and an outer cylinder 8b coaxially arranged at a predetermined interval are closed by end plates 8c and 8d, and an orifice 8e is provided between the inner cylinder 8a and the outer cylinder 8b. A plurality of nozzles 8f are provided on the outer circumference of the tip, and an inlet portion 8g is provided on the base end of the outer cylinder 8b.

【0012】このような旋回流発生ユニット8を備えた
光ファイバ母材製造装置においては、コアバーナ2の火
炎2a中で合成したコア用のガラス微粒子とクラッドバ
ーナ3の火炎3a中で合成したクラッド用のガラス微粒
子とを、回転しつつ引上げる種棒5の下端に堆積させて
光ファイバ母材6の製造を行う際に、旋回流発生ユニッ
ト8のインレット部8gからエアーを供給すると、該旋
回流発生ユニット8の先端外周の各ノズル8fからエア
ーが図3に示すように渦状の旋回流として放出される。
これにより排気管4の入口の周囲に龍巻のような旋回流
が発生し、排気管4の吸引能力が高まり、反応容器1内
の不要なガス等がこの旋回流により吸引されて除去さ
れ、該反応容器1内のガス等の流れが安定し、コアバー
ナ2aから供給される屈折率付与剤であるGeO2 が光
ファイバ母材6のコア部6aに正しく堆積し、該光ファ
イバ母材6内にGeO2 の濃度分布を正しく形成するこ
とができる。
In the optical fiber preform manufacturing apparatus equipped with such a swirling flow generating unit 8, the glass particles for core synthesized in the flame 2a of the core burner 2 and the clad synthesized in the flame 3a of the clad burner 3 are used. When the optical particles are deposited on the lower end of the seed rod 5 that is pulled up while rotating to manufacture the optical fiber preform 6, when air is supplied from the inlet portion 8g of the swirling flow generating unit 8, the swirling flow is generated. Air is discharged from each nozzle 8f on the outer periphery of the tip of the generation unit 8 as a swirling swirl flow as shown in FIG.
As a result, a swirling flow like a tornado is generated around the inlet of the exhaust pipe 4, the suction capacity of the exhaust pipe 4 is increased, and unnecessary gas and the like in the reaction vessel 1 is sucked and removed by the swirling flow, The flow of gas or the like in the reaction vessel 1 is stabilized, and GeO 2 which is the refractive index imparting agent supplied from the core burner 2a is correctly deposited on the core portion 6a of the optical fiber preform 6, Thus, the GeO 2 concentration distribution can be correctly formed.

【0013】実験例 コアバーナ2 H2 :5 l/min O2 :5 l/min SiCl4 :300 cc/min GeCl4 :20〜30 cc/min クラッドバーナ3 H2 :10 l/min O2 :10 l/min SiCl4 :300 cc/min 排気管4内の圧力:−2mmH2 O 種棒5の上部からのエアーの流量:150 l/min 旋回流発生ユニット8へのエアー供給量:5〜30 l/min ノズル8fの口径:1〜3mmφ ノズル8fの個数:16個 上記実施例では、旋回流発生ユニット8にエアーを供給
したが、エアーの代わりにN2 やAr等を用いることも
できる。
Experimental Example Core burner 2 H 2 : 5 l / min O 2 : 5 l / min SiCl 4 : 300 cc / min GeCl 4 : 20-30 cc / min Clad burner 3 H 2 : 10 l / min O 2 : 10 l / min SiCl 4 : 300 cc / min Pressure in exhaust pipe 4: -2 mmH 2 O Air flow rate from upper part of seed rod 5: 150 l / min Air supply amount to swirl flow generation unit 8: 5 30 l / min Diameter of nozzle 8f: 1-3 mmφ Number of nozzles 8f: 16 In the above embodiment, air was supplied to the swirl flow generating unit 8, but N 2 or Ar may be used instead of air. .

【0014】ノズル8fの口径は、もっと小さくするこ
ともできる。また、ノズル8fの個数は16個に限定され
るものではなく、旋回流を作れる個数であれば何個でも
よい。更に、ノズル8fは端板8cに設けることもでき
る。
The diameter of the nozzle 8f can be made smaller. Further, the number of nozzles 8f is not limited to 16 and may be any number as long as a swirl flow can be created. Further, the nozzle 8f may be provided on the end plate 8c.

【0015】旋回流発生ユニット8は、ガラスや表面に
防食処理を施した金属等で形成することができる。
The swirl flow generating unit 8 can be formed of glass or a metal whose surface is anticorrosive.

【0016】該旋回流発生ユニット8へのガスの供給量
は、少なくても多くてもよくないので、適性範囲の供給
量を適宜決める必要がある。
The amount of gas supplied to the swirl flow generating unit 8 may be either small or large, so that it is necessary to appropriately determine the amount of gas supplied in an appropriate range.

【0017】[0017]

【発明の効果】以上説明したように本発明に係る光ファ
イバ母材製造装置においては、反応容器内の排気管の入
口の周囲に、旋回流を発生させる旋回流発生ユニットを
設けるので、該反応容器内の排気管の入口の周囲に龍巻
のような旋回流が発生し、この旋回流で排気管の吸引能
力が高まり、反応容器内の不要なガス等がこの旋回流に
より吸引されて除去され、該反応容器内のガス等の流れ
が安定し、コアバーナから供給される屈折率付与剤が光
ファイバ母材のコア部に正しく堆積し、光ファイバ母材
内に屈折率付与剤の濃度分布を正しく形成することがで
きる。
As described above, in the optical fiber preform manufacturing apparatus according to the present invention, since the swirl flow generating unit for generating the swirl flow is provided around the inlet of the exhaust pipe in the reaction vessel, the reaction A tornado-like swirling flow is generated around the inlet of the exhaust pipe in the vessel, and this swirling flow enhances the suction capacity of the exhaust pipe, and unnecessary gas in the reaction vessel is sucked and removed by this swirling flow. The flow of gas or the like in the reaction vessel is stabilized, the refractive index imparting agent supplied from the core burner is correctly deposited on the core portion of the optical fiber preform, and the concentration distribution of the refractive index imparting agent in the optical fiber preform. Can be formed correctly.

【図面の簡単な説明】[Brief description of drawings]

【図1】本発明に係る光ファイバ母材製造装置の概略構
成を示す縦断面図である。
FIG. 1 is a longitudinal sectional view showing a schematic configuration of an optical fiber preform manufacturing apparatus according to the present invention.

【図2】本実施例で用いている旋回流発生ユニットの縦
断面図である。
FIG. 2 is a vertical cross-sectional view of a swirl flow generation unit used in this embodiment.

【図3】図1のX−X線矢視図である。FIG. 3 is a view taken along line XX of FIG.

【図4】従来の光ファイバ母材製造装置の概略構成を示
す縦断面図である。
FIG. 4 is a vertical sectional view showing a schematic configuration of a conventional optical fiber preform manufacturing apparatus.

【図5】(A)は光ファイバ母材の横断面図、(B)は
光ファイバ母材内におけるGeO2 の正しい濃度分布の
一例を示す濃度分布図である。
5A is a cross-sectional view of an optical fiber preform, and FIG. 5B is a concentration distribution diagram showing an example of a correct GeO 2 concentration distribution in the optical fiber preform.

【図6】光ファイバ母材内における不適正なGeO2
濃度分布図である。
FIG. 6 is an inappropriate GeO 2 concentration distribution diagram in the optical fiber preform.

【図7】図4のY−Y線矢視図である。7 is a view taken along the line YY of FIG.

【符号の説明】[Explanation of symbols]

1 反応容器 2 コアバーナ 2a 火炎 3 クラッドバーナ 3a 火炎 4 排気管 5 種棒 6 光ファイバ母材 7 渦 8 旋回流発生ユニット 8a 内筒 8b 外筒 8c,8d 端板 8e オリフィス 8f ノズル 8g インレット部 1 Reaction Vessel 2 Core Burner 2a Flame 3 Clad Burner 3a Flame 4 Exhaust Pipe 5 Type Rod 6 Optical Fiber Preform 7 Vortex 8 Swirling Flow Generation Unit 8a Inner Cylinder 8b Outer Cylinder 8c, 8d End Plate 8e Orifice 8f Nozzle 8g Inlet Part

Claims (1)

【特許請求の範囲】[Claims] 【請求項1】 バーナの火炎中で合成したガラス微粒子
を反応容器の中で種棒の先端に堆積させて光ファイバ母
材を形成し、前記反応容器内の不要ガスを排気管で該反
応容器の外に排出させる光ファイバ母材製造装置におい
て、 前記反応容器内の前記排気管の入口の周囲に、旋回流を
発生させる旋回流発生ユニットが設けられていることを
特徴とする光ファイバ母材製造装置。
1. A glass fiber fine particle synthesized in a flame of a burner is deposited on a tip of a seed rod in a reaction vessel to form an optical fiber preform, and unnecessary gas in the reaction vessel is exhausted through the reaction vessel. In the apparatus for producing an optical fiber preform for discharging to the outside of the optical fiber preform, a swirl flow generation unit for generating a swirl flow is provided around the inlet of the exhaust pipe in the reaction vessel. Manufacturing equipment.
JP27981392A 1992-10-19 1992-10-19 Optical fiber preform manufacturing equipment Expired - Fee Related JP3287618B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP27981392A JP3287618B2 (en) 1992-10-19 1992-10-19 Optical fiber preform manufacturing equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP27981392A JP3287618B2 (en) 1992-10-19 1992-10-19 Optical fiber preform manufacturing equipment

Publications (2)

Publication Number Publication Date
JPH06127965A true JPH06127965A (en) 1994-05-10
JP3287618B2 JP3287618B2 (en) 2002-06-04

Family

ID=17616281

Family Applications (1)

Application Number Title Priority Date Filing Date
JP27981392A Expired - Fee Related JP3287618B2 (en) 1992-10-19 1992-10-19 Optical fiber preform manufacturing equipment

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