JPH06105654A - Production of fancy beverage - Google Patents

Production of fancy beverage

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Publication number
JPH06105654A
JPH06105654A JP32481792A JP32481792A JPH06105654A JP H06105654 A JPH06105654 A JP H06105654A JP 32481792 A JP32481792 A JP 32481792A JP 32481792 A JP32481792 A JP 32481792A JP H06105654 A JPH06105654 A JP H06105654A
Authority
JP
Japan
Prior art keywords
solvent
extraction
beverage
extracting
nitrogen gas
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP32481792A
Other languages
Japanese (ja)
Inventor
Soichiro Tanaka
創一郎 田中
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kanebo Ltd
Original Assignee
Kanebo Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kanebo Ltd filed Critical Kanebo Ltd
Priority to JP32481792A priority Critical patent/JPH06105654A/en
Publication of JPH06105654A publication Critical patent/JPH06105654A/en
Pending legal-status Critical Current

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  • Tea And Coffee (AREA)

Abstract

PURPOSE:To obtain a fancy beverage excellent in flavor, aroma retentivity and color tone, suitable as a tea product by extracting active ingredients from a material to be extracted while blowing nitrogen gas into an extracting solvent to replace the dissolved oxygen with the nitrogen to prevent turbidity and precipitation. CONSTITUTION:In extracting active ingredients such as caffeine or tannins from a material to be extracted such as tea leaves or coffee beans, nitrogen gas is blown into an extraction solvent such as pure water at a rate of e.g. 0.25-10l/min based on 1000l of the solvent to replace the dissolved oxygen in the solvent with the nitrogen so as to come to <=3ppm in oxygen level, thus obtaining the objective fancy beverage.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明は、茶製品、コーヒー等の
嗜好飲料の製造方法に関する。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method for producing a favorite beverage such as tea products and coffee.

【0002】[0002]

【従来の技術】一般に、カフェイン、タンニン類を含有
する嗜好飲料としては、缶又は瓶入りの茶製品やコーヒ
ー等が挙げられ、その中で、透明度を有する飲料として
は、レモンティーやストレートティー等の紅茶、緑茶、
ウーロン茶、ストレートコーヒー等がある。これらの中
で、例えば、紅茶製品は、紅茶を熱水抽出した後、濾過
を経て甘味料等と調合し製造されている。これら透明感
のある嗜好飲料の製造においては、製品の冷却、保存時
に発生する濁り、沈殿をいかに抑止、防止するかが、大
きな長年の課題である。上記嗜好飲料で、冷却時に認め
られる濁り、沈殿は、飲料に含有されるカフェインとタ
ンニン類との相互作用により生じることは広く知られて
いる。
2. Description of the Related Art Generally, as a favorite beverage containing caffeine and tannins, canned or bottled tea products, coffee and the like can be cited. Among them, beverages having transparency include lemon tea and straight tea. Black tea, green tea, etc.
There are oolong tea and straight coffee. Among these, for example, black tea products are manufactured by extracting black tea with hot water and then filtering and blending it with a sweetener or the like. In the production of these beverages with a transparent feeling, it has been a long-standing problem how to prevent or prevent turbidity and precipitation that occur during cooling and storage of the product. It is widely known that, in the above-mentioned beverage of preference, the turbidity and the precipitation observed upon cooling are caused by the interaction between caffeine and tannins contained in the beverage.

【0003】そこで、この濁りを抑止する方法として、
蔗糖を過剰に添加して抽出する方法、pHを上げて抽出
する方法、タンナーゼ等によって酵素処理する方法、抽
出液冷却後の濾過強化にて濁りを沈殿として機械的に分
離する方法、あるいは高分子樹脂,シリカゲル等に接触
させ、タンニン類を吸着,除去する方法等が提案されて
いる。
Therefore, as a method of suppressing this turbidity,
Extraction by adding sucrose in excess, extraction by raising pH, enzymatic treatment with tannase, etc., mechanical separation of turbidity as precipitate by filtration enhancement after cooling the extract, or polymer A method of adsorbing and removing tannins by contacting with resin or silica gel has been proposed.

【0004】ところが、蔗糖を過剰に添加して抽出する
方法は、効果を発揮するのに20重量%以上添加するこ
とが必要であり、これは、風味上、甘味が強すぎ、実用
的でない。また、pH調整剤を用いて抽出する方法は、
添加量が多くなると塩味を感じ、風味上、好ましくな
く、低添加量では効果がなく、更に、非常に狭い領域で
のpH管理を要し、工程上好ましいものではない。更
に、タンナーゼ処理、濾過強化及びタンニン類の吸着,
除去等を行う方法は、それぞれ工程の複雑化、原料価格
の高騰を招くばかりでなく、嗜好飲料本来の風味を損な
うという問題が残されており、風味の点まで考慮した濁
りの防止方法は、未だ見い出されていないのが実情であ
った。
However, in the method of extracting by adding sucrose in excess, it is necessary to add 20% by weight or more in order to exert the effect, and this is not practical because of its too sweet taste. In addition, the method of extraction using a pH adjusting agent is
If the added amount is too large, a salty taste is felt, which is not preferable in terms of flavor, and if the added amount is too small, it is not effective. Further, pH control is required in a very narrow region, which is not preferable in the process. Furthermore, tannase treatment, filtration enhancement and adsorption of tannins,
The method of removing, etc. not only invites a complicated process and a rise in raw material prices, respectively, but there is still a problem that the flavor of the favorite beverage is impaired, and the method of preventing turbidity in consideration of the flavor is The reality is that it has not been found yet.

【0005】また、従来、コーヒーは、コーヒー豆を熱
水で浸漬抽出したものを、そのまま、あるいは、糖類等
を加えて飲用されている。コーヒーの抽出液の香り保持
手段としては、これまで、コーヒー豆の凍結粉砕処理等
のコーヒー豆を処理方法による保香性改善を始め、水出
し抽出等の抽出手段の検討、抗酸化剤の添加、あるい
は、容器に充填する際の液体窒素滴下、窒素による容器
内ヘッドスペースの酸素置換等の充填方法の検討が行わ
れてきた。しかしながら、コーヒーを抽出、製造する
際、コーヒーの持つ本来の香りを最大限に生かしながら
抽出を行うことは難しく、エキス、香料の付与に頼って
いるのが現状である。
Conventionally, coffee has been drunk by extracting coffee beans with hot water and drinking them as they are or by adding sugars and the like. As means for maintaining the scent of coffee extract, we have started to improve the aroma-retaining property of coffee beans by freeze-grinding the coffee beans, studying extraction methods such as water extraction, and adding antioxidants. Alternatively, investigations have been conducted on a filling method such as dropping liquid nitrogen at the time of filling the container, and replacing oxygen in the head space in the container with nitrogen. However, when extracting and manufacturing coffee, it is difficult to perform extraction while making the best use of the original scent of coffee, and it is the current situation to rely on the addition of extracts and flavors.

【0006】[0006]

【発明が解決しようとする課題】本発明は、このような
事情に鑑みなされたものであって、その目的とするとこ
ろは、冷却、保存時の濁り、沈殿を防止すると共に、嗜
好飲料本来の風味に効くカフェイン,タンニン類の含有
量を低下させることなく、また、組成物の構造変化をき
たすことなく、保香性、風味、色調上も望ましい嗜好飲
料の製造方法を提供することにある。
SUMMARY OF THE INVENTION The present invention has been made in view of such circumstances, and an object thereof is to prevent turbidity and precipitation during cooling and storage, and to prevent the natural taste of a favorite beverage. An object of the present invention is to provide a method for producing a favorite beverage which is desirable in terms of aroma retention, flavor and color tone without lowering the contents of caffeine and tannins which have an effect on flavor and without causing structural changes in the composition. .

【0007】[0007]

【課題を解決するための手段】上記の目的は、被抽出物
から有効成分を抽出するに当たり、抽出溶媒中に、窒素
ガスを吹き込み、溶媒中に溶存している酸素を置換しな
がら抽出を行うことを特徴とする嗜好飲料の製造方法に
よって達成される。
[Means for Solving the Problems] The above object is to extract the active ingredient from the substance to be extracted by blowing nitrogen gas into the extraction solvent and displacing oxygen dissolved in the solvent. This is achieved by a method for producing a favorite beverage characterized by the following.

【0008】すなわち、本発明者は、窒素ガスを、抽出
溶媒中へ吹き込みながら抽出を行い、溶媒中の溶存酸素
を低減することによって、濁り、沈殿の要因となるカフ
ェインとタンニン類との複合体形成、被抽出物より溶媒
中に溶出したタンニン類の会合とそれに伴うタンニンの
高分子量化とを抑止でき、また、保香性も良好とするこ
とができることを見い出し、本発明を完成した。
That is, the present inventor carried out extraction while blowing nitrogen gas into the extraction solvent to reduce dissolved oxygen in the solvent, thereby forming a complex of caffeine and tannins which causes turbidity and precipitation. It was found that the formation of a body, the association of tannins eluted in the solvent from the substance to be extracted and the accompanying increase in the molecular weight of tannin can be suppressed, and the fragrance retaining property can be improved, and the present invention was completed.

【0009】次に、本発明を詳しく説明する。本発明に
係る嗜好飲料としては、カフェインとタンニン類とを含
有する、レモンティー,ストレートティー等の紅茶、緑
茶、ウーロン茶、ストレートコーヒー等のコーヒー等が
挙げられる。
Next, the present invention will be described in detail. Examples of the favorite beverage according to the present invention include teas such as lemon tea and straight tea, which include caffeine and tannins, coffee such as green tea, oolong tea, and straight coffee.

【0010】本発明の製造方法は、例えば、次のように
して行う。すなわち、まず、被抽出物を準備し、抽出溶
媒にて有効成分を抽出する工程において、抽出溶媒中
に、窒素ガスを吹き込み、溶媒中に溶存している酸素を
窒素ガスに置換しつつ、抽出を行う。次に、得られた抽
出液を濾過した後、必要に応じて、甘味料、レモン果
汁、乳成分、pH調整剤、乳化剤、安定剤等の諸原料を
添加し、嗜好飲料を得る。
The manufacturing method of the present invention is performed as follows, for example. That is, first, in the step of preparing the substance to be extracted and extracting the active ingredient with the extraction solvent, nitrogen gas is blown into the extraction solvent, while the oxygen dissolved in the solvent is replaced with nitrogen gas, the extraction is performed. I do. Next, the obtained extract is filtered, and if necessary, various raw materials such as a sweetener, lemon juice, milk components, a pH adjuster, an emulsifier, and a stabilizer are added to obtain a favorite beverage.

【0011】上記被抽出物から有効成分を抽出する工程
において、窒素ガスは、抽出溶媒1000リットルに対
して、好ましくは0.25〜10リットル/分、更に好
ましくは1〜10リットル/分となるように吹き込むこ
とが好適である。また、窒素ガスを吹き込むことによ
り、溶媒中に溶存する酸素量を、好ましくは3ppm以
下、更に好ましくは1ppm以下に低減させる。
In the step of extracting the active ingredient from the substance to be extracted, the nitrogen gas content is preferably 0.25 to 10 liters / minute, and more preferably 1 to 10 liters / minute with respect to 1000 liters of the extraction solvent. It is preferable to blow in. By blowing nitrogen gas, the amount of oxygen dissolved in the solvent is reduced to preferably 3 ppm or less, more preferably 1 ppm or less.

【0012】窒素ガス量が0.25リットル/分未満で
は、溶存酸素の低減が不充分となる傾向にあり、製造後
の冷却保存時に濁りが発生し易くなる。また、呈味の劣
化が生じ易くなる。逆に、10リットル/分を超える
と、吹き込み時に発泡が生じ、操業性の低下を招く傾向
にある。また、溶媒中の溶存酸素量は0.75ppm程
度で飽和状態となり、それ以上は低減され難い。また、
窒素ガスの吹き込みは、抽出中、常時行ってもよく、断
続的に行ってもよい。また、抽出工程は、密閉系でも、
開放系でもよい。
When the amount of nitrogen gas is less than 0.25 liter / minute, the dissolved oxygen tends to be insufficiently reduced, and turbidity is likely to occur during storage after cooling after production. In addition, the taste is likely to deteriorate. On the other hand, when it exceeds 10 liters / minute, foaming occurs during blowing, which tends to cause deterioration in operability. Further, the dissolved oxygen amount in the solvent is saturated at about 0.75 ppm, and it is difficult to reduce it further. Also,
The blowing of the nitrogen gas may be performed constantly during the extraction or may be intermittently performed. In addition, the extraction process, even in a closed system,
It may be an open system.

【0013】また、茶類を抽出する際の温度は、好まし
くは20℃以下、より好ましくは5〜10℃の低温とす
る。20℃以下の低温で抽出することにより、茶葉中に
含まれる低分子量のタンニン類のみを抽出液中に溶出さ
せることができ、カフェインとの複合体形成後も溶解度
の減少をきたさず、更に、濁りの防止に顕著な効果が得
られる。更に、5〜10℃の低温度で抽出することによ
り、一層濁り防止効果が得られる。また、20℃以下の
低温で抽出することにより、抽出液は、マイルドで優し
い味わいとなり、ティーウォーター様の新規な風味を提
供することができる。
The temperature for extracting tea is preferably 20 ° C. or lower, more preferably 5 to 10 ° C. By extracting at a low temperature of 20 ° C. or lower, only the low molecular weight tannins contained in the tea leaves can be eluted in the extract, the solubility does not decrease even after the complex formation with caffeine, and A remarkable effect can be obtained in preventing turbidity. Furthermore, by extracting at a low temperature of 5 to 10 ° C., a more turbidity preventing effect can be obtained. Moreover, by extracting at a low temperature of 20 ° C. or lower, the extract has a mild and gentle taste, and can provide a novel flavor like tea water.

【0014】また、コーヒーを抽出する際の温度は、7
0℃以下が好ましく、温度と抽出時間との関係は、下記
式を満足する範囲内であることが望ましい。
The temperature for extracting coffee is 7
The temperature is preferably 0 ° C. or lower, and the relationship between the temperature and the extraction time is preferably within the range that satisfies the following formula.

【0015】[0015]

【数1】 [Equation 1]

【0016】10≦T≦70 (式中、Tは抽出温度、tは抽出時間を表す。)10≤T≤70 (where T is the extraction temperature and t is the extraction time)

【0017】また、図1のグラフに示す斜線で表された
部分がより好適な範囲である。また、抽出の際用いる溶
媒は、純水とし、必要に応じて、他の添加物を含有させ
てもよい。特に、低温(30℃以下)抽出の場合、糖濃
度25重量%以下の糖水溶液を用いると、更に濁り防止
効果が得られ、また、コーヒー豆からの有機酸等の呈味
成分の抽出を促進でき、更に保香性が良好となる。
Further, the hatched portion shown in the graph of FIG. 1 is a more preferable range. The solvent used in the extraction is pure water, and may contain other additives as necessary. In particular, in the case of low temperature extraction (30 ° C or lower), the use of an aqueous sugar solution having a sugar concentration of 25% by weight or less can further improve the turbidity-preventing effect, and accelerates extraction of taste components such as organic acids from coffee beans It is possible and the fragrance retaining property becomes good.

【0018】[0018]

【発明の効果】以上のように、本発明の嗜好飲料の製造
方法では、抽出工程において、窒素ガスを溶媒中に吹き
込みながら抽出を行うことから、製造後、冷却保存した
ときに発生する嗜好飲料の濁り、沈殿を防止することが
できる。更に、本発明の製造方法によれば、飲料本来の
風味を造っているカフェイン、タンニン類が会合するこ
とによってその含量が低下し、飲料本来の風味低下をき
たすことがない。また、本発明の製造方法によれば、保
香性、色調も良好な嗜好飲料を製造することができる。
As described above, in the method for producing a beverage of preference of the present invention, in the extraction step, the extraction is carried out while blowing nitrogen gas into the solvent. It is possible to prevent turbidity and precipitation. Further, according to the production method of the present invention, the content of caffeine and tannin, which make up the original flavor of the beverage, is reduced to reduce the content thereof, and the original flavor of the beverage is not deteriorated. Further, according to the production method of the present invention, it is possible to produce a favorite beverage having good aroma retention and good color tone.

【0019】次に、本発明を実施例を挙げて具体的に説
明する。 (実施例1〜5、比較例1)表1に示す抽出条件にて、
1000mlの純水を用いて、紅茶葉40gを抽出し
た。その後、20メッシュ及び150メッシュのフィル
ターで濾過を行って得られた紅茶液を、5℃で72時間
保冷後、風味、保香性及び目視にて濁りの状態を評価し
た。また、濁りについては、分光光度計(日立(株)
製)にて抽出液の波長660nmにおける光透過率を測
定し、評価指標とした。その結果を表1にあわせて示
す。
Next, the present invention will be specifically described with reference to examples. (Examples 1 to 5, Comparative Example 1) Under the extraction conditions shown in Table 1,
40 g of black tea leaves were extracted using 1000 ml of pure water. Then, the black tea liquor obtained by filtering with a 20-mesh filter and a 150-mesh filter was kept at 5 ° C. for 72 hours, and then evaluated for flavor, aroma-preserving property and visually turbid state. For turbidity, a spectrophotometer (Hitachi, Ltd.)
Manufactured) to measure the light transmittance of the extract at a wavelength of 660 nm as an evaluation index. The results are also shown in Table 1.

【0020】(実施例6)表1に示す抽出条件にて、1
000mlの純水を用いて、コーヒー豆100gを抽出
した(抽出時間30分間)。その後、綿の濾布で濾過を
行い、得られたコーヒー抽出液を、5℃で72時間保冷
後、風味、保香性及び濁りの状態を実施例1と同様にし
て評価した。その結果を表1にあわせて示す。
(Example 6) Under the extraction conditions shown in Table 1, 1
100 g of coffee beans were extracted using 000 ml of pure water (extraction time 30 minutes). Then, the mixture was filtered with a cotton filter cloth, and the coffee extract thus obtained was kept at 5 ° C. for 72 hours, and then evaluated for flavor, aroma retention and turbidity in the same manner as in Example 1. The results are also shown in Table 1.

【0021】(実施例7)表1に示す抽出条件にて、1
00gの焙煎コーヒー豆を、20℃で濃度15重量%の
砂糖水1000mlに4時間浸漬し、抽出液を調製した
(抽出時間4時間)。得られたコーヒー抽出液を、5℃
で72時間保冷後、風味、保香性及び濁りの状態を実施
例1と同様にして評価した。その結果を表1にあわせて
示す。
(Embodiment 7) Under the extraction conditions shown in Table 1, 1
00 g of roasted coffee beans was dipped in 1000 ml of sugar water having a concentration of 15% by weight at 20 ° C. for 4 hours to prepare an extract (extraction time 4 hours). The coffee extract obtained is 5 ° C
After being kept cold for 72 hours, the flavor, fragrance and turbidity were evaluated in the same manner as in Example 1. The results are also shown in Table 1.

【0022】[0022]

【表1】 [Table 1]

【0023】表1の結果より、実施例1〜5は、窒素ガ
スを吹き込みながら、抽出を行っているため、紅茶抽出
液の濁りが防止されていると共に、保香性の向上が認め
られた。また、実施例6のコーヒー抽出液も、紅茶抽出
液と同様、濁りが防止されていると共に、保香性の向上
が認められた。更に、実施例7のコーヒー抽出液は、濁
りが防止されていると共に、風味、保香性、色調の維持
に優れ、コーヒー本来の風味、香りを生かしたコーヒー
であった。
From the results shown in Table 1, in Examples 1 to 5, the extraction was carried out while blowing the nitrogen gas, so that the black tea extract was prevented from becoming turbid and the aroma retention was improved. . In addition, the coffee extract of Example 6 was found to have the same turbidity as that of the black tea extract and improved aroma retention. Furthermore, the coffee extract of Example 7 was a coffee in which turbidity was prevented and the flavor, aroma retention, and color tone were excellently maintained, and the original flavor and aroma of coffee were utilized.

【図面の簡単な説明】[Brief description of drawings]

【図1】コーヒーの好適な抽出温度と時間との関係を示
す線図。
FIG. 1 is a diagram showing a relationship between a suitable extraction temperature of coffee and time.

Claims (2)

【特許請求の範囲】[Claims] 【請求項1】 被抽出物から有効成分を抽出するに当た
り、抽出溶媒中に、窒素ガスを吹き込み、溶媒中に溶存
している酸素を置換しながら抽出を行うことを特徴とす
る嗜好飲料の製造方法。
1. Production of a beverage of preference characterized in that, when extracting an active ingredient from a substance to be extracted, nitrogen gas is blown into an extraction solvent to carry out extraction while substituting oxygen dissolved in the solvent. Method.
【請求項2】 抽出溶媒1000リットルに対して、窒
素ガスを、0.25〜10リットル/分となるよう液中
に吹き込み、溶媒中に溶存する酸素量が3ppm以下と
なるようにすることを特徴とする請求項1記載の嗜好飲
料の製造方法。
2. Nitrogen gas is blown into the liquid at a rate of 0.25 to 10 liters / min with respect to 1000 liters of the extraction solvent so that the amount of oxygen dissolved in the solvent is 3 ppm or less. The method for producing a favorite beverage according to claim 1, which is characterized in that.
JP32481792A 1992-08-11 1992-11-09 Production of fancy beverage Pending JPH06105654A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP32481792A JPH06105654A (en) 1992-08-11 1992-11-09 Production of fancy beverage

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP4-236491 1992-08-11
JP23649192 1992-08-11
JP32481792A JPH06105654A (en) 1992-08-11 1992-11-09 Production of fancy beverage

Publications (1)

Publication Number Publication Date
JPH06105654A true JPH06105654A (en) 1994-04-19

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Family Applications (1)

Application Number Title Priority Date Filing Date
JP32481792A Pending JPH06105654A (en) 1992-08-11 1992-11-09 Production of fancy beverage

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JP (1) JPH06105654A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009106162A (en) * 2007-10-26 2009-05-21 Meicha Midoriya:Kk Method and apparatus for extracting green tea
JP2009167176A (en) * 2007-12-18 2009-07-30 Kao Corp Method of deodorizing organic solvent
JP5547965B2 (en) * 2007-09-03 2014-07-16 サントリー食品インターナショナル株式会社 Container stuffed coffee drinks

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5547965B2 (en) * 2007-09-03 2014-07-16 サントリー食品インターナショナル株式会社 Container stuffed coffee drinks
JP2009106162A (en) * 2007-10-26 2009-05-21 Meicha Midoriya:Kk Method and apparatus for extracting green tea
JP2009167176A (en) * 2007-12-18 2009-07-30 Kao Corp Method of deodorizing organic solvent

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