JPH05296655A - Device for drying quartz jig - Google Patents

Device for drying quartz jig

Info

Publication number
JPH05296655A
JPH05296655A JP11832492A JP11832492A JPH05296655A JP H05296655 A JPH05296655 A JP H05296655A JP 11832492 A JP11832492 A JP 11832492A JP 11832492 A JP11832492 A JP 11832492A JP H05296655 A JPH05296655 A JP H05296655A
Authority
JP
Japan
Prior art keywords
quartz jig
quartz
vacuum tank
vacuum
vacuum chamber
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
JP11832492A
Other languages
Japanese (ja)
Inventor
Hiroyuki Inoue
博之 井上
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Steel Corp
Original Assignee
Nippon Steel Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Steel Corp filed Critical Nippon Steel Corp
Priority to JP11832492A priority Critical patent/JPH05296655A/en
Publication of JPH05296655A publication Critical patent/JPH05296655A/en
Withdrawn legal-status Critical Current

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  • Constitution Of High-Frequency Heating (AREA)
  • Drying Of Solid Materials (AREA)

Abstract

PURPOSE:To provide a device for drying a quartz jig capable of performing a rapid drying process for a quartz jig having a complex shape within clean atmosphere. CONSTITUTION:A dry vacuum pump 12 is connected to a vacuum tank 10 and an upper part of the vacuum tank is provided with a microwave oscillator 14 for use in radiating micro-wave within the vacuum tank. As a quartz jig 16 is inserted into the vacuum tank and the tank is sealingly closed, an inside part of the vacuum tank 10 is drawn with vacuum by the dry vacuum pump to cause its pressure to be reduced and then cleaning liquid remained on the surface of the quartz jig is rapidly gasified. At this time, the gasification is rapidly promoted to cause gasification heat to be deprived through thermal insulated expansion, resulting in that its temperature is decreased, so that a micro-wave is radiated from the micro-wave oscillator into the vacuum tank to perform a heating operation there, the deprived heat is restored from outside and coagulation of the cleaning liquid is prevented.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明は、半導体製造工程におい
てシリコンなどの半導体材料を取り扱うための石英治具
の乾燥装置に関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a quartz jig drying apparatus for handling semiconductor materials such as silicon in a semiconductor manufacturing process.

【0002】[0002]

【従来の技術】半導体製造工程で各種の半導体材料に対
して所定の処理を行う際に使用される治具は、半導体材
料への不純物の混入を防止するために石英製のものが使
用されている。そして、実際に半導体材料の処理に使用
する前に、石英治具の表面から不純物を除去するために
所定の洗浄液によって石英治具を洗浄するが、洗浄後の
石英治具の表面には洗浄液が残っているので、洗浄後直
ちにその石英治具を半導体の処理に使用することはでき
ず、石英治具の表面に付着した洗浄液を蒸発させるため
の乾燥処理が必要となる。
2. Description of the Related Art A jig used for performing a predetermined process on various semiconductor materials in a semiconductor manufacturing process is made of quartz in order to prevent impurities from being mixed into the semiconductor material. There is. Then, before actually using it for the processing of the semiconductor material, the quartz jig is cleaned with a predetermined cleaning liquid to remove impurities from the surface of the quartz jig. Since it remains, the quartz jig cannot be used for semiconductor processing immediately after cleaning, and a drying process for evaporating the cleaning liquid adhering to the surface of the quartz jig is required.

【0003】図3は従来の石英治具の乾燥装置の一例の
概略断面図である。この乾燥装置は、まず上部に設けら
れた送風機26によって乾燥空気を乾燥槽(ドラフタ
ー)24の中に下に向かって送風し、乾燥槽24の内部
にこの乾燥空気を充填する。そして、この中に下から石
英治具22を挿入し、乾燥空気を吹き付けることによっ
て石英治具22の表面に残っている洗浄液を蒸発する。
更に、上部中央に設けられたハロゲンランプ28から光
を照射して加熱することにより、洗浄液の蒸発を促進す
る。
FIG. 3 is a schematic sectional view of an example of a conventional quartz jig drying apparatus. In this drying device, first, a blower 26 provided at the upper portion blows dry air downward into a drying tank (drafter) 24, and the inside of the drying tank 24 is filled with the dry air. Then, the quartz jig 22 is inserted into the quartz jig 22 from below, and the cleaning liquid remaining on the surface of the quartz jig 22 is evaporated by blowing dry air.
Further, the halogen lamp 28 provided at the center of the upper portion is irradiated with light to heat the halogen lamp 28 to accelerate evaporation of the cleaning liquid.

【0004】[0004]

【発明が解決しようとする課題】しかしながら、石英治
具の中には石英炉芯管などのように細い枝管を持つもの
もある。このような石英治具は表面積が非常に大きく、
また、形状も複雑である。このような石英炉芯管を乾燥
槽の中に入れても、複雑に入り組んだ細部まで乾燥空気
を行き渡らせるのは困難であり、かかる石英治具を完全
に乾燥させるためには長時間を要する。このように石英
治具の乾燥に長い時間がかかると、半導体製造工程全体
の生産性が低下するという問題がある。
However, some quartz jigs have a thin branch tube such as a quartz furnace core tube. Such a quartz jig has a very large surface area,
Moreover, the shape is also complicated. Even if such a quartz furnace core tube is put in a drying tank, it is difficult to spread the dry air to the complicated and complicated details, and it takes a long time to completely dry such a quartz jig. . If it takes a long time to dry the quartz jig as described above, there is a problem that the productivity of the entire semiconductor manufacturing process decreases.

【0005】また、送風機によって普通の空気を石英治
具に吹き付けると、空気中に含まれる細かいゴミが石英
治具に付着することがあり、このような石英治具を使っ
て半導体材料の処理を行うと、半導体材料に不純物が混
入したり、製造後の短絡欠陥などの原因となる。
Further, when ordinary air is blown onto the quartz jig by a blower, fine dust contained in the air may adhere to the quartz jig, and such quartz jig is used to process semiconductor materials. Doing so may cause impurities to be mixed into the semiconductor material and short-circuit defects after manufacturing.

【0006】本発明は上記事情に基づいてなされたもの
であり、複雑な形状の石英治具の乾燥処理を清浄な雰囲
気のもとで迅速に行うことのできる石英治具の乾燥装置
を提供することを目的とするものである。
The present invention has been made in view of the above circumstances, and provides a quartz jig drying apparatus capable of rapidly performing a drying treatment of a quartz jig having a complicated shape in a clean atmosphere. The purpose is that.

【0007】[0007]

【課題を解決するための手段】上記の目的を達成するた
めの本発明は、石英治具を配置する真空槽と、該真空槽
の内部を減圧する減圧手段と、前記真空槽の内部を加熱
するための加熱手段とを具備することを特徴とするもの
である。
In order to achieve the above object, the present invention provides a vacuum chamber in which a quartz jig is arranged, a decompression means for decompressing the inside of the vacuum chamber, and a heating inside the vacuum chamber. It is characterized by comprising a heating means for heating.

【0008】[0008]

【作用】本発明は前記の構成によって、加熱手段によっ
て加熱し、断熱膨張によって奪われる気化熱を外部から
与えながら減圧手段で真空槽を減圧することにより、石
英治具の表面に付着している洗浄液などの液体は急速に
蒸発する。また、真空槽の内部で乾燥させることによ
り、清浄な雰囲気の中で乾燥処理を行うことができ、石
英治具の表面に不純物が付着することもない。
According to the present invention, with the above-mentioned structure, the vacuum chamber is decompressed by the decompressing means while being heated by the heating means and externally providing the heat of vaporization that is deprived by adiabatic expansion, and adheres to the surface of the quartz jig. Liquids such as cleaning liquids evaporate rapidly. Further, by drying inside the vacuum chamber, the drying process can be performed in a clean atmosphere, and impurities do not adhere to the surface of the quartz jig.

【0009】[0009]

【実施例】以下に図面を参照して本発明の実施例につい
て説明する。図1は本発明の第一実施例である石英治具
の乾燥装置を示す概略断面図、図2は本発明の第二実施
例石英治具の乾燥装置を示す概略断面図である。
Embodiments of the present invention will be described below with reference to the drawings. FIG. 1 is a schematic sectional view showing a quartz jig drying apparatus according to a first embodiment of the present invention, and FIG. 2 is a schematic sectional view showing a quartz jig drying apparatus according to a second embodiment of the present invention.

【0010】図1において、真空槽10には減圧手段で
あるドライ真空ポンプ12が接続されている。このドラ
イ真空ポンプ12としては例えばルーツポンプやソープ
ションポンプなどが使用でき、このドライ真空ポンプに
よって真空槽10の内部は10-3Torr以下の真空状態に
することができる。真空槽10の上部には、真空槽10
の内部にマイクロ波を放射するためのマイクロ波発振器
14が設けられている。また、真空槽10の内部下側に
は、乾燥すべき石英治具16を載置するための載置台1
8が設けられている。
In FIG. 1, a dry vacuum pump 12 as a pressure reducing means is connected to the vacuum chamber 10. As the dry vacuum pump 12, for example, a roots pump or a sorption pump can be used, and the inside of the vacuum chamber 10 can be brought to a vacuum state of 10 −3 Torr or less by this dry vacuum pump. At the top of the vacuum chamber 10, the vacuum chamber 10
A microwave oscillator 14 for radiating a microwave is provided inside the. A mounting table 1 for mounting a quartz jig 16 to be dried is provided on the lower side inside the vacuum chamber 10.
8 are provided.

【0011】石英治具16は、洗浄が済むと載置台18
上に載置されて真空槽10の下部より真空槽の内部へ挿
入される。なお、乾燥を行う際の石英治具の汚染を防止
するという観点から、載置台18も石英製とすることが
望ましい。石英治具16が真空槽10の内部に挿入され
真空槽10が密閉されると、ドライ真空ポンプ12によ
って真空槽10の内部が真空に引かれて減圧される。真
空槽10の内部の気圧が低下するに従って、水や洗浄液
のうち蒸気圧の高いものから順次蒸発して気化する。こ
のとき石英治具16が石英炉芯管のような細い枝管を持
つ複雑な形状のものであっても、この減圧の効果は石英
治具16のすみずみにまで及び、石英治具16の全ての
表面から洗浄液等を蒸発させることができる。また、真
空に引くことによって、不純物が石英治具に付着するこ
とも防止できる。
The quartz jig 16 is placed on the mounting table 18 after cleaning.
It is placed on top and inserted into the vacuum chamber from the bottom of the vacuum chamber 10. From the viewpoint of preventing contamination of the quartz jig during drying, it is desirable that the mounting table 18 also be made of quartz. When the quartz jig 16 is inserted into the vacuum chamber 10 and the vacuum chamber 10 is sealed, the inside of the vacuum chamber 10 is evacuated by the dry vacuum pump 12 to reduce the pressure. As the atmospheric pressure in the vacuum chamber 10 decreases, water and cleaning liquid having a higher vapor pressure are sequentially evaporated and vaporized. At this time, even if the quartz jig 16 has a complicated shape with a thin branch tube such as a quartz furnace core tube, the effect of this depressurization extends to every corner of the quartz jig 16 and Cleaning liquid and the like can be evaporated from all surfaces. Further, it is possible to prevent impurities from adhering to the quartz jig by drawing a vacuum.

【0012】しかしこのとき、蒸発が急速に進むと断熱
膨張によって気化熱が奪われ、温度が低下する。このた
め水や洗浄液の一部は凝結し、却って蒸発速度が遅くな
る場合がある。かかる事態を防止するため、ドライ真空
ポンプ12によって真空槽10の内部を減圧しながら、
マイクロ波発振器14から真空槽10の内部にマイクロ
波を放射して100℃〜200℃に加熱する。これによ
り石英治具の表面に残された洗浄液に外部から断熱膨張
によって奪われた熱を与えることができ、洗浄液の蒸発
速度の低下を防止することができる。このように真空槽
の内部を真空にすることと加熱とを組み合わせることに
よって、石英治具16の乾燥処理を迅速に行うことが可
能となる。
However, at this time, when the evaporation proceeds rapidly, the heat of vaporization is removed by adiabatic expansion, and the temperature drops. For this reason, a part of water or the cleaning liquid is condensed, and the evaporation rate may be slowed down. In order to prevent such a situation, while reducing the pressure inside the vacuum chamber 10 by the dry vacuum pump 12,
A microwave is radiated from the microwave oscillator 14 to the inside of the vacuum chamber 10 to heat it to 100 ° C to 200 ° C. This makes it possible to apply heat deprived from the outside by adiabatic expansion to the cleaning liquid left on the surface of the quartz jig, and prevent the evaporation rate of the cleaning liquid from decreasing. By thus combining the vacuuming of the inside of the vacuum chamber and the heating, the quartz jig 16 can be dried quickly.

【0013】図2に示した第二実施例では、図1のマイ
クロ波発振器14の代わりに、従来の乾燥装置と同様の
ハロゲンランプ20を使用している。その他の構成は第
一実施例と同様であるので、図1に示すものと同一の機
能を有するものには、同一の符号を付することにより、
その詳細な説明を省略する。第二の実施例は、ハロゲン
ランプ20によって真空槽10の内部に光を照射するこ
とにより、石英治具の表面に残った洗浄液に熱を供給す
ることができ、図1に示す第一実施例の場合と同様の効
果を得ることができる。その他の加熱手段としては、例
えば赤外線加熱の方法を使用することも有効である。
In the second embodiment shown in FIG. 2, instead of the microwave oscillator 14 of FIG. 1, a halogen lamp 20 similar to that of a conventional drying device is used. Since other configurations are similar to those of the first embodiment, the same reference numerals are given to those having the same functions as those shown in FIG.
Detailed description thereof will be omitted. In the second embodiment, heat can be supplied to the cleaning liquid remaining on the surface of the quartz jig by irradiating the interior of the vacuum chamber 10 with light by the halogen lamp 20, and the first embodiment shown in FIG. The same effect as in the case of can be obtained. As other heating means, it is also effective to use an infrared heating method, for example.

【0014】[0014]

【発明の効果】以上説明したように本発明によれば、真
空槽の内部を真空にし、かつ、マイクロ波発振器などの
加熱手段によって加熱することにより、洗浄液や水分な
どを急速に蒸発させることができるので、従来は非常に
長い時間を要していた石英治具の乾燥処理を短時間で迅
速に、かつ清浄な雰囲気の下で行うことができる石英治
具の乾燥装置を提供することができる。
As described above, according to the present invention, the inside of the vacuum chamber is evacuated and heated by a heating means such as a microwave oscillator, whereby the cleaning liquid, water and the like can be rapidly evaporated. Therefore, it is possible to provide a quartz jig drying device capable of performing a drying process of a quartz jig, which conventionally takes a very long time, in a short time, quickly and in a clean atmosphere. ..

【図面の簡単な説明】[Brief description of drawings]

【図1】本発明の第一実施例である石英治具の乾燥装置
を示す概略断面図である。
FIG. 1 is a schematic cross-sectional view showing a quartz jig drying apparatus according to a first embodiment of the present invention.

【図2】本発明の第二実施例である石英治具の乾燥装置
を示す概略断面図である。
FIG. 2 is a schematic sectional view showing a quartz jig drying apparatus according to a second embodiment of the present invention.

【図3】従来の石英治具の乾燥装置の概略断面図であ
る。
FIG. 3 is a schematic cross-sectional view of a conventional quartz jig drying device.

【符号の説明】[Explanation of symbols]

10 真空槽 12 ドライ真空ポンプ 14 マイクロ波発振器 16,22 石英治具 18 載置台 20,28 ハロゲンランプ 24 乾燥槽 26 送風機 10 Vacuum tank 12 Dry vacuum pump 14 Microwave oscillator 16,22 Quartz jig 18 Mounting table 20,28 Halogen lamp 24 Drying tank 26 Blower

Claims (2)

【特許請求の範囲】[Claims] 【請求項1】 石英治具を配置する真空槽と、該真空槽
の内部を減圧する減圧手段と、前記真空槽の内部を加熱
するための加熱手段とを具備することを特徴とする石英
治具の乾燥装置。
1. A quartz curing apparatus comprising: a vacuum chamber for arranging a quartz jig; a decompression unit for decompressing the interior of the vacuum chamber; and a heating unit for heating the interior of the vacuum chamber. Equipment drying equipment.
【請求項2】 前記加熱手段は、マイクロ波発振器又は
ハロゲンランプを用いたものである請求項1記載の石英
治具の乾燥装置。
2. The apparatus for drying a quartz jig according to claim 1, wherein the heating means uses a microwave oscillator or a halogen lamp.
JP11832492A 1992-04-10 1992-04-10 Device for drying quartz jig Withdrawn JPH05296655A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP11832492A JPH05296655A (en) 1992-04-10 1992-04-10 Device for drying quartz jig

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP11832492A JPH05296655A (en) 1992-04-10 1992-04-10 Device for drying quartz jig

Publications (1)

Publication Number Publication Date
JPH05296655A true JPH05296655A (en) 1993-11-09

Family

ID=14733858

Family Applications (1)

Application Number Title Priority Date Filing Date
JP11832492A Withdrawn JPH05296655A (en) 1992-04-10 1992-04-10 Device for drying quartz jig

Country Status (1)

Country Link
JP (1) JPH05296655A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009053036A (en) * 2007-08-27 2009-03-12 Rigaku Industrial Co Sample drier
JP2016070515A (en) * 2014-09-26 2016-05-09 ヤマト科学株式会社 Vacuum dryer
CN109378355A (en) * 2018-08-24 2019-02-22 曾杰 Non-traditional photovoltaic silicon wafer based on microwave treatment is cleaned and dried technique
CN111895651A (en) * 2020-06-19 2020-11-06 青岛海尔新能源电器有限公司 Vertical water tank and water heater

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009053036A (en) * 2007-08-27 2009-03-12 Rigaku Industrial Co Sample drier
JP2016070515A (en) * 2014-09-26 2016-05-09 ヤマト科学株式会社 Vacuum dryer
CN109378355A (en) * 2018-08-24 2019-02-22 曾杰 Non-traditional photovoltaic silicon wafer based on microwave treatment is cleaned and dried technique
CN109378355B (en) * 2018-08-24 2020-05-05 曾杰 Non-traditional photovoltaic silicon wafer cleaning and drying process based on microwave treatment
CN111895651A (en) * 2020-06-19 2020-11-06 青岛海尔新能源电器有限公司 Vertical water tank and water heater
CN111895651B (en) * 2020-06-19 2022-09-13 青岛海尔新能源电器有限公司 Vertical water tank and water heater

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Effective date: 19990706