JPH05202380A - Sedative essential oil and cosmetic containing the same essential oil - Google Patents
Sedative essential oil and cosmetic containing the same essential oilInfo
- Publication number
- JPH05202380A JPH05202380A JP4037041A JP3704192A JPH05202380A JP H05202380 A JPH05202380 A JP H05202380A JP 4037041 A JP4037041 A JP 4037041A JP 3704192 A JP3704192 A JP 3704192A JP H05202380 A JPH05202380 A JP H05202380A
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- essential oil
- sedative
- oil
- column
- cosmetic containing
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Abstract
Description
【０００１】[0001]
【産業上の利用分野】本発明は、ローズ油より後記特定
の性質を有する高沸点成分を除き鎮静効果及びその効果
の持続性に優れた鎮静用精油及び該精油を含む香粧品に
関する。BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a sedative essential oil excellent in sedative effect and long-lasting effect except rose oil having a high boiling point component having specific properties described below and a cosmetic containing the essential oil.
【０００２】[0002]
【従来の技術及び発明が解決しようとする課題】従来よ
り、香料などの芳香物質の吸入、又は塗布による芳香治
療、いわゆる「アロマテラピー」が行われてきている。
又その中で気分を穏やかにし、安定した爽やかな状態に
させる効果、すなわち鎮静効果に関しては、特開平０３
−２８３００号公報，特開平０３−１１１４９３号公報
にサンダルウッド油及びラベンダー油から高沸点成分を
除いた精油で試みられている。2. Description of the Related Art Heretofore, aroma treatment by inhalation or application of a fragrance substance such as a fragrance, so-called "aromatherapy" has been performed.
Further, regarding the effect of calming the mood and making it into a stable and refreshing state, that is, the sedative effect, there is disclosed in JP-A-03-03
-28300 and Japanese Patent Application Laid-Open No. 03-111493 have tried an essential oil obtained by removing high boiling point components from sandalwood oil and lavender oil.
【０００３】しかしながら、これらの精油は鎮静効果及
びその効果の持続性の面において必ずしも満足出来る物
ではなかった。However, these essential oils are not always satisfactory in terms of sedative effect and sustainability of the effect.
【０００４】本発明者らはこの様な事情に鑑み、鋭意検
討を重ねた結果、後記特定の鎮静用精油及び該精油を含
有して成る香粧品が優れた鎮静効果を有し、しかもその
効果の持続性に優れる事をみいだし、本発明を完成し
た。In view of such circumstances, the inventors of the present invention have conducted extensive studies, and as a result, the specific sedative essential oils described below and the cosmetics containing the essential oils have an excellent sedative effect and the effect thereof. The present invention has been completed by finding that it has excellent sustainability.
【０００５】即ち、本発明の目的は鎮静効果とその効果
の持続性に優れた鎮静用精油及び該精油を含有して成る
香粧品を提供する事にある。That is, an object of the present invention is to provide an essential oil for sedation which is excellent in sedative effect and its lasting effect, and a cosmetic containing the essential oil.
【０００６】[0006]
【課題を解決するための手段】上述の目的はローズ油よ
り高沸点成分を除いた下記の性質を有する鎮静用精油
と、該精油を含む香粧品によって達成される。Means for Solving the Problems The above object is achieved by a sedative essential oil having the following properties obtained by removing high boiling components from rose oil, and a cosmetic containing the essential oil.
【０００７】ガスクロマトグラフィーのクロマトグラム
において、リテンションタイムが０分から５０分以内で
あること。 機種：ヒューレット・パッカード社 ５８９０Ａ カラム：ジェー・アンド・ダブル社 ＤＢ−ＷＡＸ（内
径０．２５ｍｍ×長さ６０ｍ） キャリアガス：ヘリウム キャリアガス流量：１ml／分 カラム温度：７０℃〜２００℃ カラム昇温速度：２℃／分 検出器：Ｆ．Ｉ．Ｄ．In the chromatogram of gas chromatography, the retention time is within 0 to 50 minutes. Model: Hewlett-Packard Company 5890A Column: J & Double Company DB-WAX (inner diameter 0.25 mm x length 60 m) Carrier gas: Helium Carrier gas flow rate: 1 ml / min Column temperature: 70 ° C to 200 ° C Column temperature increase Speed: 2 ° C / min Detector: F.I. I. D.
【０００８】本発明において使用されるローズ油とは、
従来から使用されている公知の天然精油でローザ・セン
チフォーリア・エル（Ｒｏｓａｃｅｎｔｉｆｏｌｉａ
Ｌ．）又はローザ・ダマセニア・ミル（Ｒｏｓａｄａｍ
ａｓｃｅｎｉａ Ｍｉｌｌ．）の花を、水蒸気蒸留して
得られるローズオイルもしくは石油エーテル等の有機溶
剤で抽出して得られるローズアブソリュートをさすが、
水蒸気蒸留して得られるローズオイルの方が、より好ま
しい。The rose oil used in the present invention is
A well-known natural essential oil that has been used in the past, Rosa centifolia L (Rosacentifolia)
L. ) Or Rosa Damasenia Mill (Rosadam)
ascenia Mill. ) Flowers are extracted with an organic solvent such as rose oil or petroleum ether obtained by steam distillation.
Rose oil obtained by steam distillation is more preferable.
【０００９】本発明の鎮静用精油は、例えば次のように
して得ることができる。The sedative essential oil of the present invention can be obtained, for example, as follows.
【００１０】丸型フラスコにローズ油を入れ、減圧蒸留
装置を取り付け、０．５〜１．０ｍｍＨｇの範囲で減圧
し、オイルバス中で温度２５℃から７０℃までゆっくり
と昇温させ、低沸点成分を採取する。Rose oil was placed in a round flask, a vacuum distillation apparatus was attached, the pressure was reduced in the range of 0.5 to 1.0 mmHg, and the temperature was slowly raised from 25 ° C to 70 ° C in an oil bath to obtain a low boiling point. Collect the ingredients.
【００１１】採取した低沸点成分は、下記のガスクロマ
トグラフィーにおけるリテンションタイムが０分から５
０分以内の物質であるが、本発明においてはその成分全
てを用いる必要はなく、例えば０〜３０分の成分を用い
ても鎮静効果が得られる。The collected low boiling point component has a retention time in the following gas chromatography of 0 minute to 5 minutes.
Although it is a substance within 0 minutes, it is not necessary to use all of its components in the present invention, and for example, a sedative effect can be obtained even if components of 0 to 30 minutes are used.
【００１２】機種：ヒューレット・パッカード社 ５８
９０Ａ カラム：ジェー・アンド・ダブル社 ＤＢ−ＷＡＸ（内
径０．２５ｍｍ×長さ６０ｍ） キャリアガス：チッソ キャリアガス流量：１ml／分 カラム温度：７０℃〜２００℃ カラム昇温速度：２℃／分 検出器：Ｆ．Ｉ．Ｄ．Model: Hewlett-Packard Company 58
90A column: DB & WAX (J-and-Double) (inner diameter 0.25 mm x length 60 m) Carrier gas: Chisso Carrier gas flow rate: 1 ml / min Column temperature: 70 ° C-200 ° C Column heating rate: 2 ° C / min Detector: F.I. I. D.
【００１３】ローズ油よりローズ油高沸点成分を除いた
鎮静用精油は無色透明な物質であり、比重がｄ20 20＝
０．８００〜０．９５０であり、リナロール，ネロー
ル，シトロネロール，ゲラニオール等を主成分とするも
のである。The sedative essential oil obtained by removing the high boiling point component of rose oil from rose oil is a colorless and transparent substance having a specific gravity of d 20 20 =
It is 0.800 to 0.950, and contains linalool, nerol, citronellol, geraniol and the like as main components.
【００１４】また他の製造方法としては、吸着剤にシリ
カゲル、展開溶媒にヘキサンを用いたカラムクロマトグ
ラフィーによって、ヘキサン留出分を濃縮して得る方法
もあるが若干ではあるが高沸点成分が残留するので前者
の方が好ましい。Another method is to obtain the hexane distillate by concentrating the hexane distillate by column chromatography using silica gel as the adsorbent and hexane as the developing solvent, but some high boiling components remain. Therefore, the former is preferable.
【００１５】また、上記の精油を含有してなる香粧品の
調製方法は、特に限定されることがなく、一般的な方法
で良いが、例えば次の様にして調合香料を調製すること
ができる。The method for preparing a cosmetic product containing the above essential oil is not particularly limited and may be a general method. For example, a prepared perfume can be prepared as follows. .
【００１６】前述の方法によって得られた鎮静用精油
に、調和する香料成分を加えて変調し、保留性やこくな
どを加えて仕上げをしてトップノート，ボディノート，
ラストノートをうまく組合わせて経時的にも魅力ある香
りとしてミューゲ，カーネーション，ジャスミン等のシ
ングルフローラル，フロラールブーケ，シプレー，オリ
エンタル，シトラス等の特徴を持った調合香料組成物を
組立てる。The sedative essential oil obtained by the above-mentioned method is added with a harmonizing fragrance component to modulate it, and a retaining property or body is added to finish it.
Assemble a blended fragrance composition with the characteristics of single floral such as muguet, carnation, jasmine, floral bouquet, sypree, oriental, citrus, etc. as an attractive scent even with the last note.
【００１７】本発明のローズ油より高沸点成分を除いた
鎮静用精油を香粧品に配合するときの配合量は、形態に
よっても異なるが、例えば香水・オーデコロンなどのフ
レグランス製品には約０．０１〜５０重量％，スキンロ
ーションには約０．００１〜１．０重量％，シャンプー
には約０．０１〜０．５０重量％，室温芳香剤には約
０．０５〜３０重量％などが好適である。The amount of the essential oil for soothing, which is obtained by removing the high boiling point component from the rose oil of the present invention, in a cosmetic composition varies depending on the form, but is about 0.01 for a fragrance product such as perfume and cologne. -50% by weight, about 0.001-1.0% by weight for skin lotion, about 0.01-0.50% by weight for shampoo, about 0.05-30% by weight for room temperature fragrance, etc. Is.
【００１８】また本発明で得られる精油をトリメチルシ
トレート，トリエチルシトレート，トリブチルシトレー
ト，ジメチルフタレート，ジエチルフタレート，ジプロ
ピルフタレート，ジブチルフタレート，フィノキシエタ
ノール，ジプロピレングリコール，ベンジルベンゾエー
ト，ベンジルサリシレート等の保留剤のうち少なくとも
一種と組み合わせて、芳香を持続的に揮散し、かつ長時
間鎮静効果を持続させることができる。The essential oil obtained according to the present invention may be trimethyl citrate, triethyl citrate, tributyl citrate, dimethyl phthalate, diethyl phthalate, dipropyl phthalate, dibutyl phthalate, finoxyethanol, dipropylene glycol, benzyl benzoate, benzyl salicylate, etc. In combination with at least one of the above retention agents, the aroma can be continuously volatilized and the sedative effect can be maintained for a long time.
【００１９】これらの保留剤の中では特にトリメチルシ
トレート，トリエチルシトレート，トリブチルシトレー
ト，フェノキシエタノールが好適であり効果及びその効
果の持続性に優れた精油及び該精油を含む香粧品を提供
することができる。Among these retaining agents, trimethyl citrate, triethyl citrate, tributyl citrate and phenoxyethanol are particularly preferable, and to provide an essential oil and a cosmetic containing the essential oil which are excellent in the effect and the sustainability of the effect. You can
【００２０】また、これらの保留剤の配合量は、香粧品
の総量を基準として約０．００１〜１５重量％の範囲が
好適である。The amount of these holding agents to be compounded is preferably in the range of about 0.001 to 15% by weight, based on the total amount of the cosmetic product.
【００２１】その他、本発明の香粧品には、必要に応じ
てアルコール類，水，油，界面活性剤，着色剤，防腐
剤，酸化防止剤等を加えることができる。In addition, alcohols, water, oils, surfactants, colorants, preservatives, antioxidants and the like can be added to the cosmetics of the present invention as required.
【００２２】本発明の香粧品としては、香水，オードト
ワレ，オーデコロン，室内芳香剤，室内芳香エアゾー
ル，ピローシートなどの芳香製品、石鹸，シャンプー，
リンス等のトイレタリー製品、クリーム，ローション等
の基礎化粧品、頭髪化粧品、仕上化粧品等があげられ
る。Perfumes, eau de toilette, cologne, indoor fragrances, indoor fragrance aerosols, fragrance products such as pillow sheets, soaps, shampoos, and the like.
Examples include toiletry products such as rinses, basic cosmetics such as creams and lotions, hair cosmetics, and finish cosmetics.
【００２３】[0023]
【実施例】以下、実施例及び比較例によって本発明を詳
説するが、本発明は実施例の記載に限定される物ではな
い。なお、実施例に記載した鎮静効果の官能評価試験を
下記の通り行った。The present invention will be described in detail below with reference to examples and comparative examples, but the present invention is not limited to the description of the examples. In addition, the sensory evaluation test of the sedative effect described in the Example was performed as follows.
【００２４】官能評価試験 試料０．５ｇを匂い紙（６×１５０ｍｍ）に取り出し、
１０分後，３０分後，９０分後の香りの鎮静効果につい
て評価した。Sensory evaluation test 0.5 g of a sample was taken out to an odor paper (6 × 150 mm),
After 10 minutes, 30 minutes, and 90 minutes, the sedative effect of the scent was evaluated.
【００２５】なお、ここで言う鎮静効果とは、具体的に
は香りを与えた事により気分が落ち着いてくることを指
し、表１の鎮静効果判断基準にしたがって２０名の被験
者によって評価し、その結果を２０名の評価点の平均値
で示した。The sedative effect here means that the mood is calmed down by giving a scent, and the sedative effect is evaluated by 20 test subjects according to the sedative effect evaluation criteria in Table 1, and The results are shown as the average value of the evaluation points of 20 people.
【００２６】[0026]
【表１】 [Table 1]
【００２７】実施例には、下記製造例によって調製した
本発明の鎮静用精油を用いた。In the examples, the sedative essential oils of the present invention prepared by the following production examples were used.
【００２８】（製造例）丸型フラスコにローズ油５００
ｇを入れ、減圧蒸留装置を取り付ける。０．２ｍｍＨｇ
〜０．３ｍｍＨｇの範囲で減圧し、オイルバス中で温度
２５℃から７０℃まで昇温させ、その間毎分約１〜２ml
の留出速度で初留分を採取する。最終的にはローズ油よ
り高沸点成分を除いた鎮静用精油が約３９０ｇ（収率約
７８％）採取される。(Production Example) Rose oil 500 in a round flask.
g, and attach a vacuum distillation apparatus. 0.2 mmHg
Depressurize in the range of ~ 0.3mmHg, raise the temperature from 25 ℃ to 70 ℃ in an oil bath, and about 1-2mL / min during that time.
The first fraction is collected at the distillation rate of. Finally, about 390 g (yield about 78%) of essential oil for soothing, which is obtained by removing high boiling point components from rose oil, is collected.
【００２９】実施例１，比較例１〜２（精油） 実施例１には、前記製造例で調製された本発明の鎮静用
精油を用いた。Example 1, Comparative Examples 1-2 (Essential oil) In Example 1, the sedative essential oil of the present invention prepared in the above Production Example was used.
【００３０】比較例１には、前記製造例にて得られるロ
ーズ油高沸点成分（蒸留残渣）を用い、比較例２には、
一般に用いられているローズ油（未蒸留）を用いた。In Comparative Example 1, the high boiling point component of rose oil (distillation residue) obtained in the above Production Example was used, and in Comparative Example 2,
The commonly used rose oil (undistilled) was used.
【００３１】これらについて前述の機器評価及び官能評
価試験を行った。その結果を表２に示した。The above-mentioned device evaluation and sensory evaluation test were performed on these. The results are shown in Table 2.
【００３２】[0032]
【表２】 [Table 2]
【００３３】この結果、ローズ油低沸点成分に鎮静効果
があり、それよりも高沸点成分（蒸留残渣）は、鎮静効
果に何等寄与していないばかりでなく、ローズ油とは反
対の興奮方向への効果を持つという全く新しい事実を見
出した。As a result, the low boiling point component of rose oil has a soothing effect, and the high boiling point component (distillation residue) higher than that contributes not only to the soothing effect but also in the direction of excitement opposite to that of rose oil. Has found a whole new fact that has the effect of.
【００３４】また、官能的にも低沸点成分はローズ油特
有のフレッシュでスウィートな香りを持ち拡散性に富む
が、高沸点成分はスパイシィ・ウッディな重く拡散性の
悪い香りであった。Also, the low-boiling point component has a fresh and sweet scent unique to rose oil and is rich in diffusivity, while the high-boiling point component is a spicy, woody, heavy and poorly diffusing scent.
【００３５】実施例２〜４，比較例３〜５（オーデコロ
ン，香水） 実施例２〜４においては、製造例で得た本発明の鎮静用
精油を用い、また比較例３〜５では、通常の天然精油で
あるローズ油又は、前記のローズ油高沸点成分（蒸留残
渣）を用いて、表３の処方に於いて、（１）〜（６）を
（７）で希釈してオーデコロン（実施例２及び４，比較
例３〜４），香水（実施例３，比較例５）を調製し、前
記官能評価試験を行った。その結果を表４に示した。Examples 2-4, Comparative Examples 3-5 (Cologne, Perfume) In Examples 2-4, the sedative essential oil of the present invention obtained in Production Example is used, and in Comparative Examples 3-5, it is usually used. In the formulation of Table 3, (1) to (6) were diluted with (7) using rose oil which is a natural essential oil of the above or the above-mentioned high boiling point component of rose oil (distillation residue) to obtain cologne (implemented). Examples 2 and 4, Comparative Examples 3 to 4) and perfumes (Example 3, Comparative Example 5) were prepared, and the sensory evaluation test was performed. The results are shown in Table 4.
【表３】 [Table 3]
【００３６】実施例５〜７，比較例６〜７（スキンロー
ション） 表５の処方に於いて（１）〜（１３）を混合してスキン
ローションを調製し、前記官能評価試験を行った。その
結果を表４に示した。Examples 5 to 7 and Comparative Examples 6 to 7 (skin lotion) In the formulation of Table 5, (1) to (13) were mixed to prepare a skin lotion, and the sensory evaluation test was conducted. The results are shown in Table 4.
【００３７】[0037]
【表４】 [Table 4]
【００３８】[0038]
【表５】 [Table 5]
【００３９】表４からわかるように、製造例の鎮静用精
油を含有してなる実施例２〜７のオーデコロン，香水，
スキンローションは、各試験とも優れた結果を示した。As can be seen from Table 4, cologne, perfume, and colognes of Examples 2 to 7 containing the essential oil for soothing of the production example.
The skin lotion showed excellent results in each test.
【００４０】また、製造例の鎮静用精油と保留剤とを組
み合わせてなる実施例４のオーデコロン，実施例７のス
キンローションは、９０分後の香りにおいても鎮静効果
において優れた結果を示した。The eau de cologne of Example 4 and the skin lotion of Example 7 in which the essential oil for soothing of the production example and the retaining agent were combined showed excellent results in the soothing effect even in the scent after 90 minutes.
【００４１】一方、ローズ油高沸点成分を含有してなる
比較例３，６のオーデコロン及びスキンローションは、
鎮静効果がなく、全く良いものではなかった。On the other hand, the colognes and skin lotions of Comparative Examples 3 and 6 containing a high boiling point component of rose oil were:
There was no sedative effect and it was not good at all.
【００４２】また、単なるローズ油を含有してなる比較
例４，５，７のオーデコロン，香水，スキンローション
についても、経時と共に鎮静効果があると答えた人数が
少なくなっていった。Also, with respect to the colognes, perfumes, and skin lotions of Comparative Examples 4, 5, and 7 containing mere rose oil, the number of people who answered that they had a soothing effect decreased with time.
【００４３】[0043]
【発明の効果】以上記載の如く、本発明の鎮静用精油及
び該精油を含む香粧品は、鎮静効果に優れ、効果の持続
性も優れていることは明らかである。As described above, it is clear that the sedative essential oil of the present invention and the cosmetics containing the essential oil are excellent in sedative effect and excellent in sustaining effect.
【００４４】[0044]
【図１】製造例によって得られた本発明の鎮静用精油の
ガスクロマトグラムである。たて軸は含有成分ピークの
相対強度を示し、よこ軸はリテンションタイム（単位：
分）を示す。FIG. 1 is a gas chromatogram of the essential oil for sedation of the present invention obtained by a production example. The vertical axis shows the relative intensity of the peaks of the contained components, and the horizontal axis shows the retention time (unit:
Minutes).
Claims (2)
の性質を有する鎮静用精油。下記のガスクロマトグラフ
ィーのクロマトグラムにおいて、リテンションタイムが
０分から５０分以内であること。 機種：ヒューレット・パッカード社 ５８９０Ａ カラム：ジェー・アンド・ダブル社 ＤＢ−ＷＡＸ（内
径０．２５ｍｍ×長さ６０ｍ） キャリアガス：ヘリウム キャリアガス流量：１ml／分 カラム温度：７０℃〜２００℃ カラム昇温速度：２℃／分 検出器：Ｆ．Ｉ．Ｄ．1. A soothing essential oil having the following properties, which is obtained by removing high-boiling components from rose oil. In the chromatogram of the following gas chromatography, the retention time must be within 0 to 50 minutes. Model: Hewlett-Packard Company 5890A Column: J & Double Company DB-WAX (inner diameter 0.25 mm x length 60 m) Carrier gas: Helium Carrier gas flow rate: 1 ml / min Column temperature: 70 ° C to 200 ° C Column temperature increase Speed: 2 ° C / min Detector: F.I. I. D.
品。2. A cosmetic product containing the sedative essential oil according to claim 1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP4037041A JPH05202380A (en) | 1992-01-27 | 1992-01-27 | Sedative essential oil and cosmetic containing the same essential oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP4037041A JPH05202380A (en) | 1992-01-27 | 1992-01-27 | Sedative essential oil and cosmetic containing the same essential oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| JPH05202380A true JPH05202380A (en) | 1993-08-10 |
Family
ID=12486524
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP4037041A Pending JPH05202380A (en) | 1992-01-27 | 1992-01-27 | Sedative essential oil and cosmetic containing the same essential oil |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH05202380A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2006001186A1 (en) * | 2004-06-23 | 2006-01-05 | Nature Technology Inc. | Composition for antianxiety drug containing vegetable essence ingredient as active ingredient, percutaneous-absorption-type antianxiety drug employing the composition, and processes for producing these |
| EP1424071A4 (en) * | 2001-08-08 | 2006-06-07 | Shiseido Co Ltd | Perfume compositions |
| JP2010065234A (en) * | 2001-08-08 | 2010-03-25 | Shiseido Co Ltd | Use of specific perfume component for preparing perfume composition for mental sedation and method of providing mental sedation effect in perfume composition |
-
1992
- 1992-01-27 JP JP4037041A patent/JPH05202380A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1424071A4 (en) * | 2001-08-08 | 2006-06-07 | Shiseido Co Ltd | Perfume compositions |
| US7169746B2 (en) | 2001-08-08 | 2007-01-30 | Shiseido Co., Ltd. | Perfume composition |
| KR100910728B1 (en) * | 2001-08-08 | 2009-08-05 | 가부시키가이샤 시세이도 | Perfume compositions |
| JP2010065234A (en) * | 2001-08-08 | 2010-03-25 | Shiseido Co Ltd | Use of specific perfume component for preparing perfume composition for mental sedation and method of providing mental sedation effect in perfume composition |
| WO2006001186A1 (en) * | 2004-06-23 | 2006-01-05 | Nature Technology Inc. | Composition for antianxiety drug containing vegetable essence ingredient as active ingredient, percutaneous-absorption-type antianxiety drug employing the composition, and processes for producing these |
| JPWO2006001186A1 (en) * | 2004-06-23 | 2008-04-17 | ネイチャーテクノロジー株式会社 | Composition for anti-anxiety drug containing plant essential oil component as active ingredient, percutaneous absorption type anxiolytic drug containing the composition, and production method thereof |
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