JPH05156366A - Manufacture of surface treated original plate by continuous annealing - Google Patents

Manufacture of surface treated original plate by continuous annealing

Info

Publication number
JPH05156366A
JPH05156366A JP34409091A JP34409091A JPH05156366A JP H05156366 A JPH05156366 A JP H05156366A JP 34409091 A JP34409091 A JP 34409091A JP 34409091 A JP34409091 A JP 34409091A JP H05156366 A JPH05156366 A JP H05156366A
Authority
JP
Japan
Prior art keywords
annealing
heating
temperature
cooling
continuous annealing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP34409091A
Other languages
Japanese (ja)
Other versions
JP3040569B2 (en
Inventor
Teruaki Yamada
輝昭 山田
Masahiko Oda
昌彦 織田
Kazuya Ezure
和哉 江連
Masahiro Doi
雅博 土井
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Steel Corp
Original Assignee
Nippon Steel Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Steel Corp filed Critical Nippon Steel Corp
Priority to JP3344090A priority Critical patent/JP3040569B2/en
Publication of JPH05156366A publication Critical patent/JPH05156366A/en
Application granted granted Critical
Publication of JP3040569B2 publication Critical patent/JP3040569B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Abstract

PURPOSE:To provide the method for manufacturing a surface treated original plate by continuous annealing capable of high temp. annealing and capable of manufacturing T-3 to T-4 by compact super rapid heating short time annealing and that is low in equipment cost. CONSTITUTION:This cover is (1) the method in which a slab constituted of 0.020 to 0.070% C, 0.05 to 0.60% Mn, 0.001 to 0.025% P, 0.001 to 0.025% S, 0.012 to 0.090% solAl, <=0.0035% N, <=0.0070% T.O and the balance iron with inevitable impurities is subjected to heating and hot rolling under ordinary hot rolling conditions and is coiled into a hot rolled steel strip, which is subjected to cold rolling of >=85 draft and is thereafter subjected to continuous annealing of heating it in the temp. range of at least >=500 deg.C to 650 to 850 deg.C at 300 to 2000 deg.C/s heating rate, holding it <=3sec, cooling it to <=550 deg.C at 40 to 550 deg.C/s cooling rate, staying it at 550 to 400 deg.C for 2 to 15sec and executing cooling to a room temp. and is (2) the method in which C.T is regulated to 660 to 750 deg.C, and the regulation value of C and N is widen.

Description

【発明の詳細な説明】Detailed Description of the Invention

【0001】[0001]

【産業上の利用分野】本発明は錫メッキやクロム酸処理
などの表面処理が施される表面処理原板の硬さレベルが
テンパー度で3〜4の表面処理用原板を連続焼鈍で製造
する方法に関するものである。
BACKGROUND OF THE INVENTION 1. Field of the Invention The present invention relates to a method of continuously annealing a surface-treating original plate having a hardness level of 3 to 4 in terms of temper degree, which is subjected to a surface treatment such as tin plating or chromic acid treatment. It is about.

【0002】[0002]

【従来の技術】錫メッキやクロム酸処理などの表面処理
が施される表面処理原板の硬さレベルがテンパー度で3
〜4の表面処理用原板(以下それぞれT−3,T−4と
記す)は、従来は10〜40℃/sの加熱速度で加熱し
600〜700℃で20〜30sec均熱し10〜20
℃/sで500℃まで冷却し20〜40℃/sで室温ま
で冷却するような焼鈍時間が約2分も掛かる連続焼鈍炉
により製造されていたが、この場合は(1)焼鈍時間が
長く焼鈍炉内に滞留するコイルの長さが1000m以上
にもおよび設備長が長くなり連続焼鈍装置の建設費が高
くなる,(2)このような炉は、設備の設置スペースを
短くするためハースロールを上下に配置しその間を鋼帯
が上下しながら通過する縦パス型炉が採用されている。
そのため、より軟質なメッキ原板を製造するのに効果的
な例えば700℃を越えるような高温焼鈍では鋼板の強
度が大きく低下し絞り(しわ)が発生するようになり通
板出来なくなる。従って、高温焼鈍が出来ず、軟質な鋼
板の製造が難しくなる。(3)このような炉の場合は、
加熱、均熱帯には、高温の炉が用いられるので板厚が変
わった場合とか加熱均熱温度が変わった場合には温度の
追従が遅れ所定の温度になるまで時間が掛かるので調整
コイルを通過させ温度調整を行う必要が生じる。従っ
て、生産性のロスやエネルギーロス等を回避しようとす
れば板厚や設定温度の変化がなるべく少ないように通板
の順番をスケジューリングする必要があり製品の納期管
理や在庫増の問題が生じる。以上(1),(2),
(3)等の問題がある。
2. Description of the Related Art The hardness level of a surface-treated original plate to which a surface treatment such as tin plating or chromic acid treatment is applied is 3 in terms of temper degree.
The surface-treating original plates (hereinafter, referred to as T-3 and T-4) of Nos. 4 to 4 are conventionally heated at a heating rate of 10 to 40 ° C./s and uniformly soaked at 600 to 700 ° C. for 20 to 30 seconds to 10 to 20.
Although it was manufactured by a continuous annealing furnace in which it takes about 2 minutes to cool to 500 ° C. at 50 ° C./s and to room temperature at 20 to 40 ° C./s, in this case (1) the annealing time is long. The length of the coil staying in the annealing furnace is more than 1000 m and the equipment length becomes long, which increases the construction cost of the continuous annealing equipment. (2) Such a furnace has a hearth roll to shorten the installation space of the equipment. A vertical pass furnace is used in which the steel strips are placed vertically and the steel strip passes vertically between them.
Therefore, high-temperature annealing that exceeds 700 ° C., which is effective for producing a softer plated original plate, causes a large decrease in the strength of the steel plate, causing wrinkling, which makes it impossible to pass the plate. Therefore, high temperature annealing cannot be performed and it becomes difficult to manufacture a soft steel sheet. (3) In the case of such a furnace,
Since a high-temperature furnace is used for heating and soaking, if the plate thickness changes or if the heating soaking temperature changes, the temperature tracking will be delayed and it will take some time to reach the specified temperature, so it will pass through the adjustment coil. It becomes necessary to adjust the temperature. Therefore, in order to avoid productivity loss, energy loss, etc., it is necessary to schedule the order of sheet passing so that changes in sheet thickness and set temperature are as small as possible, which causes problems such as delivery management of products and inventory increase. Above (1), (2),
There are problems such as (3).

【0003】一方、短時間連続焼鈍法に付いても考案及
び研究がなされており、特公昭36−10052号公
報、特公昭36−21155号公報、特公昭40−30
20号公報、特公昭46−19781号公報、及び、
「Recrystallization ’90 Ed
ited by Chandra The Miner
als,Metals & Materials So
ciety,1990」の文献(以下文献1と記す。)
がある。しかし、特公昭36−21155号公報は20
0〜300℃でコイルとして巻き取らねばならず酸化の
問題、巻き取り設備の問題、巻き取ったコイルの冷却方
法或いは冷却時のコイル内外周の不均一冷却の問題があ
る。又、特公昭40−3020号公報はテンパー度が6
以上の製造方法で、特公昭46−19781号公報はH
R30Tが72以上の極めて硬質な材質の表面処理原板を製
造する方法で、これらの方法ではT−3〜T−4の製造
は不可能である。特公昭36−10052号公報は急速
加熱を行い均熱を殆ど行わず急冷する焼鈍時間が約15
secの短時間焼鈍法であるが、この方法の大きな問題
点は同公報の表1に示されているように得られる材質の
硬さがHR30Tで65とテンパー度が5(以下T−5と記
す)のものしか出来ないことである。
On the other hand, the short-time continuous annealing method has also been devised and studied, and Japanese Patent Publication No. 36-10052, Japanese Patent Publication No. 36-21115, and Japanese Patent Publication No. 40-30.
No. 20, Japanese Patent Publication No. 46-19781, and
"Recrystallization '90 Ed
ited by Chandra The Miner
als, Metals & Materials So
Citation, 1990 ”(hereinafter referred to as Document 1).
There is. However, Japanese Patent Publication No. 36-21155 discloses 20
It must be wound as a coil at 0 to 300 ° C., and there are problems of oxidation, winding equipment, cooling method of the wound coil, and uneven cooling of the inner and outer circumferences of the coil during cooling. Further, Japanese Patent Publication No. 40-3020 has a temper degree of 6
According to the above manufacturing method, Japanese Patent Publication No. 46-19781 discloses H
R 30 T is a method of producing a surface-treated original plate of extremely hard material having a value of 72 or more, and T-3 to T-4 cannot be produced by these methods. Japanese Examined Patent Publication No. Sho 36-10052 discloses that the annealing time for rapid heating and quenching with almost no soaking is about 15
Although it is a short time annealing method of sec, the major problem of this method is that the hardness of the obtained material is HR 30 T of 65 and the temper degree is 5 (hereinafter T-) as shown in Table 1 of the publication. It is the only thing that can be done.

【0004】又、文献1で紹介されている内容は、1)
リムド鋼の熱延板を脱炭焼鈍し、C含有量を0.005
%にした鋼を用い70%の冷間圧延を行い、0.2se
c(約3500℃/s)で加熱し0.1secの均熱を
行い水スプレーで急冷した結果、0.5sec,0.3
sec加熱(約2000℃/s〜3000℃/s)の場
合よりも顕著に再結晶温度が低下したことが、又、2)
0.5sec,0.3sec加熱(約2000℃/s〜
3000℃/s)の場合は、約830℃、800℃以上
にもなることが紹介されている。即ち、文献1の方法
は、熱延板を脱炭焼鈍し且つ加熱温度の温度制御が極め
て困難な0.2sec(約3500℃/s)の加熱速度
即ち0.01secの様な極めて微かな加熱時間のバラ
ツキで実に35℃もの温度バラツキとなるような実用化
が極めて困難な加熱速度条件とが必要であり、実用に供
するには適しない方法であることがわかる。以上のよう
に、コンパクトで高温焼鈍が可能で通板のスケジューリ
ングの自由度の大きい超急速加熱短時間焼鈍の従来法で
は、軟質材の製造が出来なかったり、実験室レベルでは
出来ても(文献1の方法)経済的にも工業的にも実機化
が不可能な方法しかまだ無いのである。
The contents introduced in the literature 1 are 1)
Decarburized annealing of hot rolled rimmed steel, C content 0.005
% Steel is cold-rolled to 70%, 0.2se
As a result of heating at c (about 3500 ° C./s), soaking for 0.1 sec, and quenching with a water spray, 0.5 sec, 0.3
2) that the recrystallization temperature was remarkably lowered as compared with the case of sec heating (about 2000 ° C / s to 3000 ° C / s).
0.5sec, 0.3sec heating (about 2000 ° C / s ~
In the case of 3000 ° C / s), it is introduced that the temperature can be about 830 ° C, 800 ° C or higher. That is, the method of Reference 1 is a decarburization annealing of a hot rolled sheet and a heating rate of 0.2 sec (about 3500 ° C./s) at which it is extremely difficult to control the heating temperature, that is, an extremely minute heating such as 0.01 sec. It can be seen that this method is not suitable for practical use because it requires a heating rate condition that makes it extremely difficult to put it into practical use, in which the temperature fluctuates as much as 35 ° C. due to time variations. As described above, the conventional method of ultra-rapid heating and short-time annealing, which is compact and capable of high-temperature annealing and has a high degree of freedom in threading scheduling, cannot produce soft materials or even at the laboratory level. Method 1) There is still only the method that cannot be put to practical use economically and industrially.

【0005】[0005]

【発明が解決しようとする課題】本発明で解決しようと
する課題は、高温焼鈍が可能で、通板のスケジューリン
グの自由度が大きく、コンパクトで設備費の小さい超急
速加熱短時間焼鈍設備で、T−3〜T−4の製造が可能
な連続焼鈍による表面処理原板の製造方法を提供する事
である。
The problem to be solved by the present invention is a super rapid heating and short time annealing equipment which is capable of high temperature annealing, has a high degree of freedom in the scheduling of sheet passing, is compact, and has a small equipment cost. It is to provide a method for producing a surface-treated original plate by continuous annealing capable of producing T-3 to T-4.

【0006】[0006]

【課題を解決するための手段】本発明者等は、上記課題
を解決するため、成分含有量、熱延条件、冷間圧延条
件、連続焼鈍条件について総合的に検討し、本発明の製
造方法を見いだしたものである。本発明の要旨は下記の
通りである。 (1)C :0.020〜0.070% Mn:0.05〜0.60% P :0.001〜0.025% S :0.001〜0.025% Sol Al:0.012〜0.090% N :≦0.0035% T.O:≦0.0070% 残部不可避的不純物及び鉄よりなる鋼片を、通常の熱間
圧延条件で加熱、熱間圧延を行い、巻き取り熱延鋼帯と
し、85%以上の冷間圧延を行い、その後、連続焼鈍に
て少なくとも500℃以上の温度域を300〜2000
℃/sで650〜850℃に加熱し3秒以下の保定を行
い、40〜500℃/sの冷却速度で550℃以下まで
冷却し、550〜400℃の間で2〜15秒間滞在せし
め、室温まで冷却する事を特徴とする連続焼鈍による表
面処理原板の製造方法。
In order to solve the above-mentioned problems, the present inventors comprehensively studied the content of components, hot rolling conditions, cold rolling conditions, and continuous annealing conditions, and the manufacturing method of the present invention. I found it. The gist of the present invention is as follows. (1) C: 0.020 to 0.070% Mn: 0.05 to 0.60% P: 0.001 to 0.025% S: 0.001 to 0.025% Sol Al: 0.012 0.090% N: ≤0.0035% TO: ≤0.0070% A steel slab consisting of the balance unavoidable impurities and iron is heated and hot-rolled under normal hot-rolling conditions, and the winding heat is applied. A steel strip is used, cold rolling is performed at 85% or more, and then continuous annealing is performed at a temperature range of at least 500 ° C. to 300 to 2000.
It is heated to 650 to 850 ° C. at 3 ° C./s and retained for 3 seconds or less, cooled to 550 ° C. or less at a cooling rate of 40 to 500 ° C./s, and allowed to stay at 550 to 400 ° C. for 2 to 15 seconds, A method for producing a surface-treated original plate by continuous annealing, which comprises cooling to room temperature.

【0007】(2)C :0.020〜0.080% Mn:0.05〜0.60% P :0.001〜0.025% S :0.001〜0.025% Sol Al:0.020〜0.100% N :≦0.0070% T.O:≦0.0070% 残部不可避的不純物及び鉄よりなる鋼片を、加熱し、熱
間圧延を行い、660℃〜750℃の範囲の巻き取り温
度(以下C.Tと記す)で巻き取り熱延鋼帯とし、85
%以上の冷間圧延を行い、その後、連続焼鈍にて少なく
とも500℃以上の温度域を300〜2000℃/sで
650〜850℃に加熱し3秒以下の保定を行い、40
〜500℃/sの冷却速度で550℃以下まで冷却し、
550〜400℃の間で2〜15秒間滞在せしめ、室温
まで冷却する事を特徴とする連続焼鈍による表面処理原
板の製造方法
(2) C: 0.020 to 0.080% Mn: 0.05 to 0.60% P: 0.001 to 0.025% S: 0.001 to 0.025% Sol Al: 0 0.020 to 0.100% N: ≤ 0.0070% TO: ≤ 0.0070% A steel slab composed of the balance unavoidable impurities and iron is heated and hot-rolled to a temperature of 660 ° C to 750 ° C. Rolling hot rolled steel strip at a winding temperature in the range (hereinafter referred to as CT)
% Cold-rolling is performed, and thereafter, a temperature range of at least 500 ° C. or higher is heated to 650-850 ° C. at 300-2000 ° C./s by continuous annealing, and retained for 3 seconds or less.
Cooling to 550 ° C or lower at a cooling rate of ~ 500 ° C / s,
A method for producing a surface-treated original plate by continuous annealing, characterized in that it is allowed to stay at 550 to 400 ° C. for 2 to 15 seconds and cooled to room temperature.

【0008】以下に本発明について詳細に述べる。本発
明者等は、前記課題を解決するため、その製造方法につ
いて、成分含有量、熱延条件、冷間圧延条件、連続焼鈍
条件について総合的に検討し、連続焼鈍の加熱に於い
て少なくとも500℃以上の温度域を300〜2000
℃/sで650〜850℃に加熱すること、再結晶焼
鈍後の結晶粒径を大きくするために、発明の(1)とし
てC:0.020〜0.070%,N:≦0.0035
%、とし、低温で巻き取ることを可能とする方法、発明
の(2)としてC:0.020〜0.0800%,so
lAl:0.020〜0.100%,N:≦0.007
0%,残部不可避的不純物及び鉄よりなる鋼片を、加熱
し、660℃〜750℃の範囲のC.Tで巻き取り熱延
鋼帯とするC,N含有量の規制を大幅に緩和させる方
法、均熱後の冷却を40〜500℃/sの冷却速度で
550℃以下まで冷却し、550〜400℃の間で2〜
15秒間滞在せしめ固溶のC含有量を低減させる方法、
の、、の3点を主ポイントとすることにより、C
含有量が発明の(1)としてC:0.020〜0.07
0%,発明の(2)としてC:0.020〜0.080
%と通常の製鋼法で容易に得られるC含有量の鋼に於い
ても極めてコンパクトな連続焼鈍設備でT−3〜T−4
の製造が可能となることを初めて見いだしたものであ
る。
The present invention will be described in detail below. In order to solve the above problems, the present inventors comprehensively examined the component content, hot rolling conditions, cold rolling conditions, and continuous annealing conditions for the production method thereof, and at least 500 in the heating of continuous annealing. 300 to 2000 in the temperature range above ℃
In order to increase the crystal grain size after recrystallization annealing by heating to 650 to 850 ° C. at C / s, C: 0.020 to 0.070%, N: ≦ 0.0035 as (1) of the invention.
%, And a method that enables winding at low temperature, C: 0.020 to 0.0800%, so as (2) of the invention.
Al: 0.020 to 0.100%, N: ≤ 0.007
A steel slab consisting of 0%, the balance unavoidable impurities, and iron was heated to form a C.C. A method of significantly relaxing the restrictions on the C and N contents of the hot-rolled steel strip taken up by T, cooling after soaking at a cooling rate of 40 to 500 ° C / s to 550 ° C or less, and 550 to 400 2 between ℃
A method of reducing the C content of solid solution by allowing it to stay for 15 seconds,
By using 3 points of, and
Content is C: 0.020 to 0.07 as (1) of the invention.
0%, C: 0.020 to 0.080 as (2) of the invention
% And a C content that can be easily obtained by an ordinary steelmaking method, T-3 to T-4 with extremely compact continuous annealing equipment.
It was the first time that it was possible to manufacture.

【0009】図1は、本発明のポイントの「連続焼鈍
の加熱に於いて少なくとも500℃以上の温度域を30
0〜200℃/sで650〜850℃に加熱すること」
の効果を示した図である。本発明の方法で製造したC含
有量が0.05%、90%の冷間圧延率で圧延した板厚
が0.25mmの冷延板を、図2に示すヒートサイクル
で加熱速度(αH)と均熱温度(T)を変え、時間(t)
を0.1sec、均熱後の冷却を300℃/sの冷却速
度で500℃まで冷却し、520〜450℃の間で5秒
間滞在せしめ、室温まで冷却した鋼板の組織を調査し、
再結晶の完了する温度を求め、その結果を示した図であ
る。
FIG. 1 shows that the temperature range of at least 500.degree.
Heating to 650-850 ° C at 0-200 ° C / s "
It is a figure showing the effect of. The C content was 0.05%, the cold-rolled sheet having a plate thickness of 0.25 mm rolled at a cold rolling rate of 90% produced by the method of the present invention was heated at a heating rate (αH) in the heat cycle shown in FIG. And soaking temperature (T) are changed, time (t)
For 0.1 sec, cooling after soaking was cooled to 500 ° C. at a cooling rate of 300 ° C./s, allowed to stay for 5 seconds between 520 and 450 ° C., and the structure of the steel sheet cooled to room temperature was investigated,
FIG. 6 is a diagram showing the result of finding the temperature at which recrystallization is completed.

【0010】図1から、加熱速度を300℃/s以上と
する事により再結晶完了温度が顕著に低下することがわ
かる。このことから、均熱時間が殆どないようなコンパ
クトな連続焼鈍設備でT−3〜T−4を製造するには、
本発明のポイントの連続焼鈍の加熱に於いて300℃
/s以上の超急速加熱することが極めて重要であること
がわかる。尚、文献1では、約1700℃/s(t1
0.5sec)程度の加熱速度では再結晶完了温度が8
00〜830℃と著しく上昇しているが、図1に示す結
果は、大きく異なった結果となっている。この理由に付
いては、今後の詳細な検討が必要であるが、冷間圧延率
が70%であるのに対し90%と大幅に高くなっている
こと、又、成分、特にT.O含有量が0.0375%と
高いリムド鋼の熱延板を脱炭焼鈍した素材を供試鋼とし
たこと、等の条件の違いによる影響によりこのように異
なったのではないかと考えられる。
It can be seen from FIG. 1 that the recrystallization completion temperature is remarkably lowered by setting the heating rate to 300 ° C./s or more. From this, in order to produce T-3 to T-4 with a compact continuous annealing equipment with almost no soaking time,
300 ° C in the heating of continuous annealing which is the point of the present invention
It can be seen that it is extremely important to perform ultra-rapid heating of not less than / s. Note that in Reference 1, about 1700 ° C./s (t 1 =
When the heating rate is about 0.5 sec, the recrystallization completion temperature is 8
Although it remarkably rises to 00 to 830 ° C., the result shown in FIG. 1 is a very different result. The reason for this is to be examined in detail in the future, but the cold rolling ratio is 70%, which is significantly higher than 90%, and the components, especially T.I. It is considered that the difference may be due to the influence of different conditions such as the fact that the material obtained by decarburizing and annealing a hot rolled sheet of rimmed steel having a high O content of 0.0375% was used as the test steel.

【0011】尚、このように300℃/s以上で加熱す
ることにより、従来の20℃/sより軟質な材質が得ら
れるメカニズムに付いては必ずしも充分に解明できてい
ないが、 A.超急速加熱の場合は、再結晶のスタート時に於ける
サブグレインの粒界の移動速度並びに粒成長時の粒界の
移動速度が極めて速いので、粒界への偏析元素の粒界へ
の移動が追従しなくなり粒界の移動を妨げる偏析元素が
少なくなる。その結果、超急速加熱を行うことにより再
結晶がより低温で起こるとともに粒成長も容易となりよ
り軟質材が得られるようになった。尚、冷間圧延率、成
分、等はこのサブグレインの生成並びに大きさ等に影響
を与えているのではないかと考えられる。
The mechanism by which a material softer than the conventional 20 ° C./s can be obtained by heating at 300 ° C./s or more as described above has not been sufficiently clarified. In the case of ultra-rapid heating, since the moving speed of the grain boundaries of the subgrains at the start of recrystallization and the moving speed of the grain boundaries during grain growth are extremely fast, the segregation elements move to the grain boundaries. The number of segregated elements that do not follow and hinder the movement of grain boundaries decreases. As a result, by performing ultra-rapid heating, recrystallization occurs at a lower temperature and grain growth becomes easier, and a softer material can be obtained. It is considered that the cold rolling rate, composition, etc. may affect the generation and size of this subgrain.

【0012】B.超急速加熱の場合は、再結晶〜粒成長
の間の時間があまりにも短いので再結晶前、途中、粒成
長の段階に於いてAlNの微細析出が殆ど起こらなくな
る。その結果、超急速加熱を行うことにより再結晶がよ
り低温であるとともに粒成長も容易となりより軟質材が
得られるようになった。等の効果によるものではないか
と推察される。尚、これらのA,Bの効果は、連続焼鈍
の加熱に於いて少なくとも500℃以上の温度域を30
0℃/s以上で650〜850℃に加熱することで得ら
れた。
B. In the case of ultra-rapid heating, the time between recrystallization and grain growth is so short that AlN fine precipitation hardly occurs before and during recrystallization during grain growth. As a result, by performing ultra-rapid heating, recrystallization was performed at a lower temperature, grain growth was facilitated, and a softer material was obtained. It is presumed that this is due to the effects of the above. The effects of A and B are 30 at least in the temperature range of 500 ° C. or higher during heating in continuous annealing.
It was obtained by heating to 650 to 850 ° C at 0 ° C / s or more.

【0013】本発明のポイントのは、ポイントの超
急速加熱効果を発揮させるための成分並びに熱延条件で
ある。発明の(1)としてC:0.020〜0.070
%,N:≦0.0035%、とすることを主要条件とす
る低温で巻き取ることを可能とする方法で、C含有量が
0.070%超になるとCの悪影響が大きくなりすぎ、
又、N含有量が0.0035%超になると超急速加熱で
も微細なAlNが析出し始めるようになる、等C,N含
有量を規制する必要がある。発明の(2)としてC:
0.020〜0.080%,sol Al:0.020
〜0.100%,N:≦0.0070%,残部不可避的
不純物及び鉄よりなる鋼片を、加熱し、660℃〜75
0℃の範囲のC.Tで巻き取り熱延鋼帯とする方法で、
660℃〜750℃の範囲のC.Tで巻き取ることによ
りCは粗大セメンタイトとして凝集析出させマトリック
スを純化させ、NをAlNとして粗大析出させ悪影響を
緩和させることにより、C,N含有量の規制を大幅に緩
和させることをポイントとする方法である。
The point of the present invention is the components and hot rolling conditions for exhibiting the ultra-rapid heating effect of the point. As (1) of the invention, C: 0.020 to 0.070.
%, N: ≤ 0.0035%, which is a method that enables winding at low temperature, the main condition being that the adverse effect of C becomes too large when the C content exceeds 0.070%.
Further, if the N content exceeds 0.0035%, fine AlN will begin to precipitate even with ultra-rapid heating, and it is necessary to regulate the C and N contents. As (2) of the invention, C:
0.020-0.080%, sol Al: 0.020
˜0.100%, N: ≦ 0.0070%, the balance unavoidable impurities and a steel slab composed of iron are heated to 660 ° C. to 75 ° C.
C. in the range of 0 ° C. With the method of winding hot rolled steel strip at T,
C. in the range of 660 ° C to 750 ° C. The point is to significantly relax the regulation of C and N contents by winding C at T to coagulate and precipitate as coarse cementite to purify the matrix and coarsely precipitate N as AlN to mitigate the adverse effect. Is the way.

【0014】本発明のポイントのは、本発明のポイン
ト、の方法等で再結晶焼鈍時加熱、均熱時に結晶粒
を充分に大きく成長させた後、引き続き行われる均熱後
の冷却を40〜500℃/sの冷却速度で550℃以下
まで冷却し、550〜400℃の間で2〜15秒間滞在
せしめることである。冷却条件をこのように規制するこ
とにより、均熱時に多量に再固溶していた固溶Cを約4
0〜50ppm以下にすることが可能となる。その結
果、、、の総合効果でT−3〜T−4の表面処理
原板の製造が可能となる。
The point of the present invention is that after the heating during recrystallization annealing and the crystal grains are grown sufficiently large during soaking by the method of the point of the present invention or the like, the subsequent cooling after soaking is 40 to 40 ° C. It is to cool to 550 ° C. or lower at a cooling rate of 500 ° C./s, and to make it stay between 550 to 400 ° C. for 2 to 15 seconds. By controlling the cooling conditions in this manner, a large amount of solid solution C that had been re-dissolved during soaking was about 4
It becomes possible to make it 0 to 50 ppm or less. As a result, it is possible to manufacture the surface-treated original plate of T-3 to T-4 with the total effect of.

【0015】以下に製造条件について詳細に述べる。C
は、前述のようにT−3〜T−4の硬度に大きく影響す
る元素で、超急速加熱焼鈍時の再結晶焼鈍後の結晶粒径
に影響を与える重要な元素である。発明の(1)の方法
では、C含有量が0.070%超になるとT−3〜T−
4の硬度が得られなくなるのでC含有量の上限を0.0
70%とし、発明の(2)の方法では、C含有量が0.
080%超になるとT−3〜T−4の硬度が得られなく
なるのでC含有量の上限を0.080%とした。尚、C
量が0.020%未満では転炉でのCの吹き下げが必要
となる。その結果、溶鋼中のT.O含有量が高くなり鋼
中の介在物が増加し製品の加工性が劣化するようにな
る。又、それを回避する方法として、製鋼工場での脱ガ
スによる脱炭処理方法があるが処理費が高くなりすぎる
等の問題があるので、下限のC含有量を0.020%と
した。
The manufacturing conditions will be described in detail below. C
Is an element that greatly affects the hardness of T-3 to T-4 as described above, and is an important element that affects the crystal grain size after recrystallization annealing during super rapid heating annealing. In the method (1) of the invention, when the C content exceeds 0.070%, T-3 to T-.
Since the hardness of 4 cannot be obtained, the upper limit of the C content is 0.0
70%, and in the method (2) of the invention, the C content is 0.
If it exceeds 080%, the hardness of T-3 to T-4 cannot be obtained, so the upper limit of the C content was made 0.080%. Incidentally, C
If the amount is less than 0.020%, it is necessary to blow down C in the converter. As a result, the T. The O content increases, the inclusions in the steel increase, and the workability of the product deteriorates. Further, as a method for avoiding this, there is a decarburization treatment method by degassing in a steelmaking plant, but there is a problem that the treatment cost becomes too high, so the lower limit C content was set to 0.020%.

【0016】Mn含有量は、0.60%超になるとT−
3〜T−4の硬度が得られなくなるので0.60%を上
限値とした。尚、0.05%未満は通常の製造法では得
られないので下限値を0.05%とした。P含有量は、
0.025%超になるとT−3〜T−4の硬度が得られ
なくなるので0.025%を上限値とした。尚、0.0
01%未満は通常の製造法では得られないので下限値を
0.001%とした。S含有量は、0.025%超にな
るとT−3〜T−4の硬度が得られなくなるので0.0
25%を上限値とした。尚、0.001%未満は通常の
製造法では得られないので下限値を0.001%とし
た。
If the Mn content exceeds 0.60%, T-
Since the hardness of 3 to T-4 cannot be obtained, 0.60% was made the upper limit. In addition, since less than 0.05% cannot be obtained by an ordinary manufacturing method, the lower limit value is set to 0.05%. P content is
If it exceeds 0.025%, the hardness of T-3 to T-4 cannot be obtained, so 0.025% was made the upper limit. In addition, 0.0
Since less than 01% cannot be obtained by an ordinary manufacturing method, the lower limit value was made 0.001%. If the S content exceeds 0.025%, the hardness of T-3 to T-4 cannot be obtained, so 0.0
25% was made the upper limit. In addition, since less than 0.001% cannot be obtained by an ordinary manufacturing method, the lower limit is set to 0.001%.

【0017】sol Alは、発明の(1)の方法で
は、sol Al含有量が0.090%超になると、超
急速加熱焼鈍を行ってもsol Alが多いため微細な
AlNが多く析出するようになるので0.090%を上
限値とした。尚、0.012%未満では、脱酸不足のた
めT.O含有量が高くなり0.0070%以下とする事
ができなくなるので下限値を0.012%とした。又、
本発明の(2)の方法では、高温巻き取りによりNをA
lNとして固定するために必要な元素であるので、so
l Al含有量が0.020%未満となるとsol Al
が不足しNを粗大なAlNとして十分に析出させること
が出来なくなり、微細なAlNが析出するようになり、
再結晶焼鈍時に結晶粒を微細化し材質を硬くしT−3〜
T−4の硬度が得られなくなるので、下限のsol A
l量を0.020%とした。又、0.100%超になる
と固溶強化により材質が硬化しT−3〜T−4の硬度が
得られなくなるので0.100%を上限値とした。
According to the method (1) of the invention, when the content of sol Al exceeds 0.090%, sol Al is large in sol Al even if ultra-rapid heating annealing is carried out, so that a large amount of fine AlN is precipitated. Therefore, 0.090% was set as the upper limit. If the content is less than 0.012%, the T. Since the O content becomes too high to be 0.0070% or less, the lower limit is set to 0.012%. or,
In the method (2) of the present invention, N is converted to A by high-temperature winding.
Since it is an element necessary for fixing as 1N, so
l When Al content is less than 0.020%, sol Al
Is insufficient and N cannot be sufficiently precipitated as coarse AlN, and fine AlN comes to be precipitated.
During recrystallization annealing, crystal grains are refined to harden the material and T-3
Since the hardness of T-4 cannot be obtained, the lower limit of sol A
The amount of 1 was 0.020%. On the other hand, if it exceeds 0.100%, the material is hardened by solid solution hardening and the hardness of T-3 to T-4 cannot be obtained, so 0.100% was made the upper limit.

【0018】N含有量は、発明の(1)の方法では、N
含有量が0.0035%超になると、超急速加熱焼鈍を
行ってもNが多いため微細なAlNが析出するようにな
るので0.0035%を上限値とした。又、本発明の
(2)の方法では、高温巻き取りによりNをAlNとし
て固定するためにN含有量が多くても軟質な材質が得ら
れるが、N含有量が0.0070%超になるとAlNの
析出量が多くなりすぎ材質を硬くしT−3〜T−4の硬
度が得られなくなるので0.0070%を上限値とし
た。尚、N含有量は低いほど軟質な鋼板が得られるので
特に下限値を規制する必要はない。
In the method (1) of the invention, the N content is N
If the content exceeds 0.0035%, fine AlN will be precipitated due to a large amount of N even after performing ultra-rapid heating annealing, so 0.0035% was made the upper limit. Further, in the method (2) of the present invention, since N is fixed as AlN by high-temperature winding, a soft material can be obtained even if the N content is large, but if the N content exceeds 0.0070%. Since the precipitation amount of AlN becomes too large and the material becomes hard and the hardness of T-3 to T-4 cannot be obtained, 0.0070% was made the upper limit value. It should be noted that the lower the N content, the softer the steel sheet can be obtained, so there is no need to regulate the lower limit value.

【0019】T.O含有量は、0.0070%超になる
とスラブの表層付近に気泡が発生し、メッキ原板の表面
傷などが増え良好な製品が得られなくなるので0.00
70%を上限値とした。尚、下限値は、特に規制する必
要がないので規制しなかった。熱延条件は、発明の
(1)の方法としては特に規制する必要がなく通常の熱
延条件でよい。発明の(2)の方法としたのは熱延の巻
き取り時にCとNを無害化する為の重要な工程で、C.
Tが660℃未満の巻き取り温度では材質が硬化しT−
3〜T−4の硬度が得られなくなるので660℃を下限
値とした。又、巻き取り温度が750℃超ではスケール
が異常に厚くなり酸洗性が大幅に劣化するようになるの
で750℃を上限値とした。尚、熱延の加熱条件は、特
に規制する必要がなく通常行われる加熱条件でよいが、
より軟質な鋼板を得るには、1150℃以下の加熱温度
(SRTと記す)が好ましい。
T. If the O content exceeds 0.0070%, air bubbles are generated near the surface layer of the slab, and scratches on the plating base plate increase, so that a good product cannot be obtained.
70% was made the upper limit. The lower limit is not regulated because it does not need to be regulated. The hot rolling conditions do not have to be particularly restricted as the method (1) of the invention, and ordinary hot rolling conditions may be used. The method (2) of the invention is an important step for rendering C and N harmless during winding of hot rolling.
At a winding temperature of T less than 660 ° C, the material is hardened and T-
Since a hardness of 3 to T-4 cannot be obtained, 660 ° C was set as the lower limit value. On the other hand, if the winding temperature exceeds 750 ° C, the scale becomes abnormally thick and the pickling property deteriorates significantly, so 750 ° C was set as the upper limit. The heating conditions for hot rolling do not need to be particularly restricted and may be those that are normally performed.
In order to obtain a softer steel plate, a heating temperature of 1150 ° C. or lower (referred to as SRT) is preferable.

【0020】冷間圧延時の冷間圧延率は、85%未満で
は再結晶焼鈍時の再結晶温度が高くなり材質が硬くなり
T−3〜T−4が得られ難くなると共にメッキ製品は板
厚が薄いので85%未満の冷間圧延率では熱延板の板厚
が薄くなりすぎ熱間圧延が困難となるので、下限値を8
5%とした。尚、上限値は特に規制する必要がないので
規制しなかった。連続焼鈍時の再結晶焼鈍の加熱速度
は、本発明の最も重要なポイントで、その効果並びにそ
のメカニズムは先に推察した通りである。加熱速度が3
00℃/s未満では超急速加熱効果が得られず材質が硬
化しT−3〜T−4の硬度が得られなくなるので300
℃/sを下限値とした。尚、2000℃/s超の加熱速
度ではあまりにも加熱速度が速すぎるため加熱の到達温
度の制御が不安定となり安定した品質が得難くなるので
2000℃/sを上限とした。
If the cold rolling ratio during cold rolling is less than 85%, the recrystallization temperature during recrystallization annealing becomes high and the material becomes hard, making it difficult to obtain T-3 to T-4, and the plated product becomes a plate. Since the thickness is thin, if the cold rolling ratio is less than 85%, the thickness of the hot-rolled sheet becomes too thin, which makes hot rolling difficult.
It was set to 5%. It should be noted that the upper limit value is not regulated because it does not need to be regulated. The heating rate of recrystallization annealing at the time of continuous annealing is the most important point of the present invention, and its effect and its mechanism are as previously inferred. Heating rate is 3
If it is less than 00 ° C./s, the effect of ultra-rapid heating cannot be obtained, the material is hardened, and the hardness of T-3 to T-4 cannot be obtained.
° C / s was set as the lower limit. If the heating rate is higher than 2000 ° C./s, the heating rate is too fast, and the control of the ultimate temperature of heating becomes unstable, and it becomes difficult to obtain stable quality. Therefore, the upper limit is 2000 ° C./s.

【0021】再結晶焼鈍時の焼鈍温度は、650℃未満
では超急速加熱焼鈍でも充分な再結晶が起こらずT−3
〜T−4の硬度が得られなくなるので650℃を下限値
とした。尚、焼鈍温度が850℃超になると均熱帯を通
過する時に鋼板が軟化し延び易くなり通板性が悪くなる
ので850℃を上限値とした。再結晶焼鈍時の均熱時間
は、超急速加熱焼鈍では均熱時間がなくとも充分な再結
晶と粒成長が生じT−3〜T−4の硬度が得られるので
均熱時間の下限値は規制する必要がない。尚、均熱時間
の上限を3secとしたのは、本発明の目的である「設
備費を大きく軽減し得る極めてコンパクトな連続焼鈍設
備でT−3〜T−4の製造が可能な連続焼鈍による表面
処理原板を製造する方法」の思想から外れるようになる
ので3secを上限値とした。
When the annealing temperature during the recrystallization annealing is less than 650 ° C., sufficient recrystallization does not occur even in the super rapid heating annealing, and T-3.
The hardness of ˜T-4 cannot be obtained, so 650 ° C. is set as the lower limit value. If the annealing temperature exceeds 850 ° C., the steel sheet is softened and easily spreads when passing through the soaking zone, and the stripability deteriorates. Therefore, 850 ° C. was set as the upper limit value. As for the soaking time during recrystallization annealing, in the ultra-rapid heating annealing, sufficient recrystallization and grain growth occur and hardness of T-3 to T-4 can be obtained even if there is no soaking time, so the lower limit of the soaking time is No need to regulate. The upper limit of the soaking time is set to 3 sec, which is the object of the present invention "due to the continuous annealing capable of producing T-3 to T-4 with an extremely compact continuous annealing equipment capable of greatly reducing the equipment cost. Therefore, the upper limit is set to 3 sec, because it deviates from the idea of "a method for producing a surface-treated original plate".

【0022】再結晶焼鈍後の冷却は、本発明の重要なポ
イントの1つで、T−3〜T−4を得るためには均熱後
の冷却時に、図3から、550〜400℃の間で2秒以
上の間滞在せしめる必要があることがわかる。尚、滞在
時間が15秒超では、設備長が長くなり過ぎ、本願の発
明の方法の主旨であるコンパクトな設備を提供すること
から外れるようになるので15秒以下とした。
Cooling after recrystallization annealing is one of the important points of the present invention, and in order to obtain T-3 to T-4, at the time of cooling after soaking, as shown in FIG. It turns out that it is necessary to stay for 2 seconds or more. If the staying time exceeds 15 seconds, the equipment length becomes too long, which is outside the provision of compact equipment, which is the gist of the method of the present invention.

【0023】図3は、本発明の方法で製造したC含有量
が0.05%、90%の冷間圧延率で圧延した板厚が
0.25mmの冷延板を、図2に示すヒートサイクルで
αH:1000℃/s、T1:710℃、t1:0.1s
ec、均熱後の冷却を300℃/sの冷却速度でT2
で冷却し、T2〜T3の温度域を10℃/sでtoa秒間
滞在せしめ、300℃/sで室温まで冷却して焼鈍した
鋼板に1.2%の調質圧延を施し表面処理原板を造り、
その鋼板のHR30Tを測定し、その結果を示した図であ
る。この図3から、均熱後の冷却に於いて、500〜4
00℃の間での2〜15秒の極短時間の間滞留させる効
果は極めて顕著で、微か2〜3秒の滞在でもHR30Tが大
きく低下している。又、T3の温度が300℃と本願の
発明の範囲を外れると殆ど軟化が生じないこともわか
る。このようにHR30Tが急激に低下するのは、再結晶焼
鈍の均熱時に多量に再固溶していた固溶Cが、550〜
400℃の間での2秒以上の滞留中に、顕著に低下する
ためである。
FIG. 3 shows a heat rolled sheet shown in FIG. 2 which is manufactured by the method of the present invention and has a C content of 0.05% and a cold rolling rate of 90% and a thickness of 0.25 mm. Cycle: αH: 1000 ° C / s, T 1 : 710 ° C, t 1 : 0.1s
ec, cooling after soaking is cooled to T 2 at a cooling rate of 300 ° C./s, the temperature range of T 2 to T 3 is kept at 10 ° C./s for toa seconds, and cooled to room temperature at 300 ° C./s. 1.2% temper rolling is applied to the annealed steel sheet to make a surface-treated original sheet,
Measured HR 30 T of the steel sheet is a diagram showing the results. From FIG. 3, in cooling after soaking, 500 to 4
The effect of staying at 00 ° C. for an extremely short time of 2 to 15 seconds is extremely remarkable, and the HR 30 T is greatly reduced even after a slight stay of 2 to 3 seconds. It is also understood that when the temperature of T 3 is 300 ° C., which is outside the range of the invention of the present application, softening hardly occurs. As described above, the HR 30 T sharply decreases because a large amount of solid solution C re-dissolved during soaking during recrystallization annealing is 550 to 550.
This is because during the retention of 400 ° C. for 2 seconds or more, the temperature is remarkably lowered.

【0024】尚、550℃までの冷却条件は、500℃
/s超では急速冷却の制御性が劣化するようになるの
で、又、40℃/s未満では冷却時間が長くなり設備長
が長くなるようになり、本願の発明の方法の主旨である
コンパクトな設備を提供することから外れるようになる
ので40〜500℃/sに規制した。更に、550〜4
00℃の間での2〜15秒の滞留後の冷却条件は、特に
規制する必要がなく速やかに冷却すれば良い。調質圧延
は通常行われている0.5〜2.0%を必要に応じ施せ
ばよい。
The cooling condition up to 550 ° C. is 500 ° C.
If it exceeds / s, the controllability of rapid cooling will deteriorate, and if it is less than 40 ° C / s, the cooling time will increase and the equipment length will increase, which is a compact feature of the method of the present invention. Since it will be out of provision of equipment, it was regulated to 40 to 500 ° C / s. Furthermore, 550-4
The cooling conditions after the retention of 2 to 15 seconds between 00 ° C do not need to be particularly limited, and the cooling may be performed promptly. The temper rolling may be performed at 0.5 to 2.0% which is usually performed, if necessary.

【0025】[0025]

【実施例】以下に本発明の効果を実施例により説明す
る。表1に示す成分、熱延条件で2.5mmの熱延鋼帯
を製造し、冷間圧延率90%で冷間圧延した0.25m
mの冷延鋼板を図2に示すヒートサイクルで表2に示す
温度、時間及びαc2が300℃/sの条件で連続焼鈍を
施し、1.2%の調質圧延を施し、表面処理原板を得
た。得られた表面処理原板の硬度(HR30T)を測定し、
その結果を表2に示す。鋼Aは、本願の発明の(1)の
方法での範囲内の製造条件のもので、鋼B,Cは本願の
発明の(2)での方法の範囲内の製造条件のもので、鋼
D,Eは本願の発明の方法の範囲外の製造条件のもので
ある。
EXAMPLES The effects of the present invention will be described below with reference to examples. The composition shown in Table 1 and a hot rolled steel strip of 2.5 mm were manufactured under the hot rolling conditions and cold rolled at a cold rolling ratio of 90% to 0.25 m.
The cold-rolled steel sheet of m was continuously annealed in the heat cycle shown in FIG. 2 under the conditions of temperature, time and αc 2 of 300 ° C./s shown in Table 2, and temper-rolled to 1.2% to obtain a surface-treated original sheet. Got The hardness (HR 30 T) of the obtained surface-treated original plate was measured,
The results are shown in Table 2. Steel A has manufacturing conditions within the range of the method (1) of the present invention, and steels B and C have manufacturing conditions within the range of the method of (2) of the present invention. D and E are manufacturing conditions outside the range of the method of the present invention.

【0026】[0026]

【表1】 [Table 1]

【0027】[0027]

【表2】 [Table 2]

【0028】試料1,2,3,4,5,6は、本発明の
方法の実施例で、何れもT−3〜T−4の硬度範囲(H
R30T=58±3〜61±3)のメッキ原板が得られてい
る。試料1は、表1に示すようにC,N量等の成分、熱
延条件、並びに焼鈍条件を本発明の(1)での方法の範
囲内での実施例である。本発明の(1)の方法であれば
HR30Tが59.0とT−3〜T−4の硬度範囲のメッキ
原板が得られることがわかる。試料2.3,4,5,
6,は、表1,2に示すように主としてC,N量並びに
焼鈍条件を本発明の(2)の方法の範囲内で変化させた
実施例である。本発明の(2)の方法の範囲内であれば
何れもT−3〜T−4の硬度範囲のメッキ原板が得られ
ることがわかる。試料7はC.Tが低い本発明の(1)
の方法のC,N量が高く外れた比較例で、T−3〜T−
4の硬度範囲のメッキ原板が得られなくなることがわか
る。
Samples 1, 2, 3, 4, 5, and 6 are examples of the method of the present invention, and all of them have a hardness range of T-3 to T-4 (H
A plated original plate of R 30 T = 58 ± 3 to 61 ± 3) is obtained. As shown in Table 1, sample 1 is an example in which components such as C and N contents, hot rolling conditions, and annealing conditions were within the range of the method (1) of the present invention. It is understood that according to the method (1) of the present invention, an original plating plate having an HR 30 T of 59.0 and a hardness range of T-3 to T-4 can be obtained. Samples 2.3, 4, 5,
As shown in Tables 1 and 2, 6 and 6 are examples in which the amounts of C and N and the annealing conditions were changed within the range of the method (2) of the present invention. It is understood that the plating original plate having the hardness range of T-3 to T-4 can be obtained within the range of the method (2) of the present invention. Sample 7 is C.I. (1) of the present invention having a low T
In the comparative example in which the amounts of C and N are high in the above method, T-3 to T-
It can be seen that a plating original plate having a hardness range of 4 cannot be obtained.

【0029】試料8は、本発明の(2)の方法の焼鈍後
の550〜400℃の間の滞在時間(toa)が1秒と
低く外れた比較例で、T−3〜T−4の硬度範囲のメッ
キ原板が得られなくなることがわかる。試料9は、本発
明の(2)の方法のC,N量が高く外れ且つ加熱速度が
20℃/sと従来法と同じレベルで更に焼鈍後の550
〜400℃の間の滞在時間(toa)も殆ど無かった比
較例で、T−3〜T−4の硬度範囲のメッキ原板が得ら
れなかった。試料10は、焼鈍時の均熱時間が30se
cと長い現在工業的に行われている連続焼鈍条件の従来
例である。
Specimen 8 is a comparative example in which the residence time (toa) between 550 and 400 ° C. after annealing in the method (2) of the present invention was as low as 1 second, and it was T-3 to T-4. It can be seen that the original plating plate in the hardness range cannot be obtained. Sample 9 has a high C and N content of the method (2) of the present invention and deviates, and the heating rate is 20 ° C./s, which is the same level as that of the conventional method and is 550 after further annealing.
In Comparative Example, there was almost no residence time (toa) between 400 ° C. and 400 ° C., and a plating original plate having a hardness range of T-3 to T-4 could not be obtained. Sample 10 has a soaking time of 30 se during annealing.
This is a conventional example of continuous annealing conditions that are currently industrially performed for a long time.

【0030】[0030]

【発明の効果】以上に本発明について詳細に説明した
が、本発明によれば、高温焼鈍が可能で、通板のスケジ
ューリングの自由度が大きく、コンパクトで設備費の小
さい超急速加熱短時間の連続焼鈍設備で、T−3〜T−
4の表面処理原板の製造が可能となり、その工業的価値
は大である。
Although the present invention has been described in detail above, according to the present invention, it is possible to perform high temperature annealing, have a high degree of freedom in the scheduling of sheet passing, be compact, and reduce the equipment cost for ultra-rapid heating in a short time. With continuous annealing equipment, T-3 to T-
The surface-treated original plate of No. 4 can be manufactured, and its industrial value is great.

【図面の簡単な説明】[Brief description of drawings]

【図1】連続焼鈍の加熱速度と硬度との関係を示す図、FIG. 1 is a diagram showing a relationship between a heating rate and hardness in continuous annealing,

【図2】調査実験並びに実施例に用いた連続焼鈍のヒー
トサイクルを示す図、
FIG. 2 is a diagram showing a heat cycle of continuous annealing used in investigation experiments and examples,

【図3】均熱後の冷却条件とHR30Tとの関係を示す図で
ある。
FIG. 3 is a diagram showing a relationship between cooling conditions after soaking and HR 30 T.

───────────────────────────────────────────────────── フロントページの続き (72)発明者 土井 雅博 兵庫県姫路市広畑区富士町1番地 新日本 製鐵株式会社広畑製鐵所内 ─────────────────────────────────────────────────── ─── Continuation of the front page (72) Inventor Masahiro Doi 1 Fuji-machi, Hirohata-ku, Himeji-shi, Hyogo Shin Nippon Steel Co., Ltd. Hirohata Works

Claims (2)

【特許請求の範囲】[Claims] 【請求項1】C :0.020〜0.070% Mn:0.05〜0.60% P :0.001〜0.025% S :0.001〜0.025% Sol Al:0.012〜0.090% N :≦0.0035% T.O:≦0.0070% 残部不可避的不純物及び鉄よりなる鋼片を、通常の熱間
圧延条件で加熱、熱間圧延を行い、巻き取り熱延鋼帯と
し、85%以上の冷間圧延を行い、その後、連続焼鈍に
て少なくとも500℃以上の温度域を300〜2000
℃/sで650〜850℃に加熱し3秒以下の保定を行
い、40〜500℃/sの冷却速度で550℃以下まで
冷却し、550〜400℃の間で2〜15秒間滞在せし
め、室温まで冷却する事を特徴とする連続焼鈍による表
面処理原板の製造方法
1. C: 0.020 to 0.070% Mn: 0.05 to 0.60% P: 0.001 to 0.025% S: 0.001 to 0.025% Sol Al: 0.0. 012 to 0.090% N: ≤ 0.0035% TO: ≤ 0.0070% A steel slab composed of the balance unavoidable impurities and iron is heated under normal hot rolling conditions, hot rolled, and wound. Hot-rolled steel strip, cold-rolled at 85% or more, and then continuously annealed at a temperature range of at least 500 ° C to 300-2000.
It is heated to 650 to 850 ° C. at 3 ° C./s and retained for 3 seconds or less, cooled to 550 ° C. or less at a cooling rate of 40 to 500 ° C./s, and allowed to stay at 550 to 400 ° C. for 2 to 15 seconds, Method for producing surface-treated original plate by continuous annealing characterized by cooling to room temperature
【請求項2】C :0.020〜0.080% Mn:0.05〜0.60% P :0.001〜0.025% S :0.001〜0.025% Sol Al:0.020〜0.100% N :≦0.0070% T.O:≦0.0070% 残部不可避的不純物及び鉄よりなる鋼片を、加熱し、熱
間圧延を行い、660℃〜750℃の範囲の巻き取り温
度で巻き取り熱延鋼帯とし、85%以上の冷間圧延を行
い、その後、連続焼鈍にて少なくとも500℃以上の温
度域を300〜2000℃/sで650〜850℃に加
熱し3秒以下の保定を行い、40〜500℃/sの冷却
速度で550℃以下まで冷却し、550〜400℃の間
で2〜15秒間滞在せしめ、室温まで冷却する事を特徴
とする連続焼鈍による表面処理原板の製造方法
2. C: 0.020 to 0.080% Mn: 0.05 to 0.60% P: 0.001 to 0.025% S: 0.001 to 0.025% Sol Al: 0.0. 020 to 0.100% N: ≤ 0.0070% TO: ≤ 0.0070% A steel slab composed of the balance unavoidable impurities and iron is heated and hot-rolled in the range of 660 ° C to 750 ° C. It is made into a hot rolled steel strip at a coiling temperature of 85%, cold rolled at 85% or more, and then heated at a temperature range of at least 500 ° C to 650 to 850 ° C at 300 to 2000 ° C / s by continuous annealing. Hold for 3 seconds or less, cool to 550 ° C or less at a cooling rate of 40 to 500 ° C / s, let it stay between 550 to 400 ° C for 2 to 15 seconds, and cool to room temperature. Method for manufacturing surface-treated original plate by annealing
JP3344090A 1991-12-03 1991-12-03 Manufacturing method of surface-treated original sheet by continuous annealing Expired - Fee Related JP3040569B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP3344090A JP3040569B2 (en) 1991-12-03 1991-12-03 Manufacturing method of surface-treated original sheet by continuous annealing

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP3344090A JP3040569B2 (en) 1991-12-03 1991-12-03 Manufacturing method of surface-treated original sheet by continuous annealing

Publications (2)

Publication Number Publication Date
JPH05156366A true JPH05156366A (en) 1993-06-22
JP3040569B2 JP3040569B2 (en) 2000-05-15

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Application Number Title Priority Date Filing Date
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Country Link
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