JPH04122427A - Continuous treatment apparatus of highly viscous material - Google Patents

Continuous treatment apparatus of highly viscous material

Info

Publication number
JPH04122427A
JPH04122427A JP2239841A JP23984190A JPH04122427A JP H04122427 A JPH04122427 A JP H04122427A JP 2239841 A JP2239841 A JP 2239841A JP 23984190 A JP23984190 A JP 23984190A JP H04122427 A JPH04122427 A JP H04122427A
Authority
JP
Japan
Prior art keywords
rod
stirring blades
square frames
rotating shafts
rotary
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
JP2239841A
Other languages
Japanese (ja)
Inventor
Takatoshi Kinoshita
木下 高年
Keishin Furukawa
古川 敬信
Kazuo Ihara
井原 一夫
Atsumitsu Kanzaki
神崎 淳光
Chikao Oda
親生 小田
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hitachi Ltd
Hitachi Plant Technologies Ltd
Original Assignee
Hitachi Techno Engineering Co Ltd
Hitachi Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hitachi Techno Engineering Co Ltd, Hitachi Ltd filed Critical Hitachi Techno Engineering Co Ltd
Priority to JP2239841A priority Critical patent/JPH04122427A/en
Priority to KR1019910015419A priority patent/KR920006397A/en
Priority to DE4129669A priority patent/DE4129669A1/en
Publication of JPH04122427A publication Critical patent/JPH04122427A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/60Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis
    • B01F27/70Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms
    • B01F27/701Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms comprising two or more shafts, e.g. in consecutive mixing chambers
    • B01F27/702Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms comprising two or more shafts, e.g. in consecutive mixing chambers with intermeshing paddles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18Details relating to the spatial orientation of the reactor
    • B01J2219/182Details relating to the spatial orientation of the reactor horizontal

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)
  • Other Resins Obtained By Reactions Not Involving Carbon-To-Carbon Unsaturated Bonds (AREA)
  • Polymerisation Methods In General (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

PURPOSE:To lessen the whole sagging degree of a rotator even if the capacity of an apparatus becomes high to drive the apparatus safely without stirring blades touching a container main body by installing a reinforcing beam in the stirring blades which have rod-like square frames. CONSTITUTION:Two rotary shafts 2b are put in parallel in the longitudinal direction in a cylindrical container 1 put horizontally and both ends are fixed by a bearing 5. A plurality of stirring blades connected with rod-like square frames 3a, 3b, 4a, 4b are attached between rotary shafts in both ends and the rotary shafts 2a, 2b put in parallel are held in the way that the tip parts of the rod-like square frames of one corresponding stirring blade may pass close to the rotary center of the other stirring blade. Then, one or a plurality of parts 7a, 7b which are joined in the direction of the rotary axis between the axial center and the square frames 3a, 3b in the longitudinal direction are installed between a plurality of the square frames 4a, 4b in the radial direction installed between the rotary shafts 2a, 2b. As a result, the stirring blades do not touch the container main body and the apparatus is driven safely.

Description

【発明の詳細な説明】 [梁上の利用分野〕 本発明は高粘性液を攪拌処理するM続処理装置に係わり
、特に塊状重合法によりポリマーを製造したり、高粘性
物質からの低分子の溶剤等を脱揮する連続処理装置に関
するものである。
Detailed Description of the Invention [Field of Application on the Beam] The present invention relates to an M-subsequent treatment device for agitating and treating highly viscous liquids, and particularly for producing polymers by bulk polymerization and for producing low molecules from highly viscous substances. This invention relates to a continuous processing device that devolatilizes solvents and the like.

〔従来の技術〕[Conventional technology]

一般に、高粘性物質の混練、反応等の連続処理において
は、装置内でのデッドスペースをできるだけ少な(シ、
かつ、押し出し流れに近いことが要求される。そのため
横長円筒状容器を用い、攪拌翼を取付けた2本の回転軸
を長手方向に設置されたものが種々採用されている。例
えば第3図に示されるように円板形の翼10を多段に配
列し、容器l内面を全面に亘って掻き取れる構造として
デッドスペースを少なくしたものであるが、被処理液が
敵方ポアズ以上の高粘性となった場合、回転軸2m、2
bの表面や翼10表面に付着して流動しな(なる。運転
が長(なるにつれ、その量も増大し、スケーリングを起
こして製品の品質に悪影響を与える。
In general, in continuous processing such as kneading and reaction of high viscosity substances, the dead space within the equipment should be kept as small as possible.
In addition, it is required that the flow be close to that of extrusion. For this reason, various types of containers have been adopted in which a horizontally elongated cylindrical container is used and two rotating shafts with stirring blades are installed in the longitudinal direction. For example, as shown in Fig. 3, a structure in which disk-shaped blades 10 are arranged in multiple stages and the inner surface of the container l can be scraped over the entire surface is used to reduce dead space. If the viscosity becomes higher than
It adheres to the surface of the blade b and the surface of the blade 10 and becomes fluid.The longer the operation, the more the amount increases, causing scaling and adversely affecting the quality of the product.

そこで、この回転軸をなくし、攪拌翼も平板から線状の
部材で形成した特開昭62−112624号に記載され
た装置がある。本装置においては従来の装置と比べ付着
量をかなり軽減することができる。
Therefore, there is an apparatus described in JP-A-62-112624 in which this rotating shaft is eliminated and the stirring blades are also formed from a flat plate or a linear member. With this device, the amount of adhesion can be significantly reduced compared to conventional devices.

本装置においては回転体両端をベアリングで固定させて
いるが、装置が大型化すると、攪拌効力も太き(なるた
め、強度の面でも部材を大きくしなければならず、回転
体のMikも増えてくる。その結果、上下方向の回転体
の自重による回転体の全体たわみも増え、運転中はさら
に負荷がかかるためたわみ量がさらに太き(なる。容器
本体と翼の間は本体壁に付着した被処理物を翼で掻き取
ってクリーニングするため最小の隙間を設けている。
In this device, both ends of the rotating body are fixed with bearings, but as the device becomes larger, the stirring effect also increases (this means that the members must be made larger in terms of strength, and the Mik of the rotating body also increases. As a result, the overall deflection of the rotating body due to its own weight in the vertical direction increases, and the amount of deflection becomes even larger due to the additional load applied during operation. A minimum gap is provided in order to scrape and clean the processed material with blades.

そのため回転体のたわみが大きくなると、本体壁と接触
する問題がある。
Therefore, when the rotating body becomes deflected greatly, there is a problem that it comes into contact with the main body wall.

〔発明が解決しようとする問題〕[Problem that the invention seeks to solve]

上記従来技術は、攪拌翼の構造においては、装置を大型
化する上で攪拌翼の先端が容器本体に接触する欠点があ
った。
The above-mentioned conventional technology has a disadvantage in that the structure of the stirring blade makes the device larger and the tip of the stirring blade comes into contact with the container body.

本発明の目的は装置8′量が大きくなっても従来装置と
混合特性は度わらず、しかも棒状矩形枠を連結した攪拌
翼から構成される回転体に従来同様中心軸を設けないで
、ポリマーの付着量をできるだけ軽減させ、容器本体内
面に翼が接触することなく運転できる連続処理装置を提
供することにある。
The purpose of the present invention is to maintain the mixing characteristics of the conventional device even when the amount of the device 8' becomes large, and to produce polymers without having a central axis in the rotating body composed of stirring blades connected to rod-shaped rectangular frames. It is an object of the present invention to provide a continuous processing device which can reduce the amount of adhesion as much as possible and can operate without the blades coming into contact with the inner surface of the container body.

〔課題を解決するだめの手段〕[Failure to solve the problem]

上記目的を達成するために、棒状矩形枠の攪拌翼に補強
ビームを取り付け、剛性アlプを図ったものである。
In order to achieve the above object, a reinforcing beam is attached to the stirring blade of the rod-shaped rectangular frame to increase the rigidity.

〔作  用〕[For production]

第5図、第6図において、二つの半径方向部材4a、4
bと二つの長手方向部材3a、3bで一つの矩形枠を形
成したものを一つの攪拌翼3,4と称する。
In FIGS. 5 and 6, two radial members 4a, 4
b and the two longitudinal members 3a, 3b forming one rectangular frame is referred to as one stirring blade 3, 4.

第5図、第6図に示す回転軸28間の棒状矩形枠(攪拌
翼3,4)の位置において、回転軸中心を通る左右水平
線回りの断面二次モーメントはB断面よりA断面の方が
はるかに小さ(変形し易い。
At the position of the rod-shaped rectangular frame (stirring blades 3, 4) between the rotating shafts 28 shown in FIGS. 5 and 6, the moment of inertia of area around the left and right horizontal lines passing through the center of the rotating shaft is higher for cross-section A than for cross-section B. Much smaller (easier to deform).

従って、Aの位置でのlF?而二面モーメントを上げる
ために、両隣の翼の半径方向部材4a、4b開に、回転
軸2aの軸中心と長手方向部材3a。
Therefore, IF at position A? In order to increase the dihedral moment, the radial members 4a, 4b of the adjacent blades are separated from the axial center of the rotating shaft 2a and the longitudinal member 3a.

3bの中間位置に長手方向部材3a、3bと平行して単
一もしくは複数の補強ビームで接続したものである。
3b is connected in parallel with the longitudinal members 3a and 3b by a single or plural reinforcing beams.

〔実 施 例〕〔Example〕

以下、本発明の一実施例を第1図、第2図により説明す
る。図において、■は処理装置の容器本体で、第2図に
示す断面をもつ横長円筒状容器で水平に設置されている
。一般に容器本体l外周は加熱のだめのジャケット(図
示せず)で覆われている。2a、2bは容器本体lの長
手方向両端部に左右水平に並設された回転軸で、容器本
体lの側面に固定した軸受5で支持されている。左右い
ずれか、一方の回転軸2aもしくは2bは駆動装置N(
図示せず)に連結されている。両軸の回転軸2a、2b
間にはそれぞれ隣接する二つの長手方向部材3a、3b
と二つの半径方向部材4a、4bとで形成された矩形枠
の攪拌翼3,4が軸方向に90度の位相角をもって複数
個取り付けられてている。
An embodiment of the present invention will be described below with reference to FIGS. 1 and 2. In the figure, ■ is the container body of the processing device, which is a horizontally long cylindrical container with a cross section shown in FIG. 2, and is installed horizontally. Generally, the outer periphery of the container body l is covered with a jacket (not shown) for heating. Reference numerals 2a and 2b are rotating shafts arranged horizontally and horizontally at both ends of the container body l in the longitudinal direction, and are supported by bearings 5 fixed to the side surfaces of the container body l. Either the left or right rotating shaft 2a or 2b is driven by a drive device N (
(not shown). Both rotating shafts 2a, 2b
There are two adjacent longitudinal members 3a, 3b in between.
A plurality of rectangular stirring blades 3, 4 formed by two radial members 4a, 4b are attached with a phase angle of 90 degrees in the axial direction.

また両軸の攪拌翼3,4の半径方向部材4a。Also, the radial member 4a of the stirring blades 3, 4 having both shafts.

4bは回転軸28.2bの方向からみて相互に45度の
位相角で設けられている。
4b are provided at a phase angle of 45 degrees from each other when viewed from the direction of the rotation axis 28.2b.

また、一方の軸の半径方向部材4a又は4bが、他方の
軸中心に回転によりできるだけ近接して通過するように
軸rwj距離が設定されている。丈だ、両軸の半径方向
部材4a、4bが容器本体lの内壁面に近接して液を内
側で持ち上げるように内側から外側へ向って回転する。
Further, the axis rwj distance is set so that the radial member 4a or 4b of one axis passes as close as possible to the center of the other axis by rotation. The radial members 4a, 4b of both shafts are close to the inner wall surface of the container body l and rotate from the inside to the outside so as to lift the liquid inside.

両軸の攪拌翼3,4において、軸方向に両側にある攪拌
翼の半径方向部材4a、4b間に回転軸2a、2bの中
心と長手方向部材3a、3bの中間の半径方向位置に補
強ビーム7a又は7bが取り付けられている。各軸の両
端の攪拌翼にあってはL形の補強アームが使われ、他端
は回転軸2a又は2bと接続されている。
In the stirring blades 3 and 4 having both shafts, a reinforcing beam is installed between the radial members 4a and 4b of the stirring blades on both sides in the axial direction at a radial position between the center of the rotating shafts 2a and 2b and the longitudinal members 3a and 3b. 7a or 7b is attached. L-shaped reinforcing arms are used for the stirring blades at both ends of each shaft, and the other end is connected to the rotating shaft 2a or 2b.

6および9は容器本体lの下部に長手方向の一端および
他端部に設けられた被処理液の入口ノズルおよび出口ノ
ズル、8は容器本体lの他端上部に設けられた揮発物の
出口ノズルである。
6 and 9 are inlet and outlet nozzles for the liquid to be treated, which are provided at one longitudinal end and the other end of the lower part of the container body l; 8 is an outlet nozzle for volatile matter, which is provided at the upper part of the other end of the container body l. It is.

本実施例は一つの攪拌翼に補強ビーム7a又は7bを2
本設けた事例であるが、他の実施例として2本を超えを
複数の補強ビームを設けた攪拌翼を有する処理装置があ
る。
In this embodiment, two reinforcing beams 7a or 7b are attached to one stirring blade.
Although this is the present example, there is another example of a processing apparatus having stirring blades provided with more than two reinforcing beams.

〔発明の効果〕〔Effect of the invention〕

本発明によれば、装置!!!′量が大さ(なっても、回
転体の全体たわみ量を少なくすることができ、攪拌翼が
容器本体に接することなく、安全に運転することができ
る。
According to the invention, the device! ! ! Even if the amount is large, the overall amount of deflection of the rotating body can be reduced, and the stirring blades can be operated safely without coming into contact with the container body.

【図面の簡単な説明】[Brief explanation of the drawing]

第1図および第2図は本発明による高粘性物質の連続処
理装置の一実施例を示すもので、第1図は装置の上側か
らみた一部断面平面図、第2図は第1図の1−1線断面
図を示す。 第3図および第4図は従来装置の一実施例であり、第3
図は軸方向の容器本体断面図であり、第4図は第3図の
1−■線断面図を示す。 第5図、第6図は従来の処理装置の一実施例であり、第
5図は装置の上側からみた一部断面平面図、第6図は第
5(8)のト」線断面図を示す。 1・・・・・・容器本体、2a、2b・・・・・・回転
軸、3a。
Figures 1 and 2 show an embodiment of a continuous processing apparatus for highly viscous substances according to the present invention. A sectional view taken along the line 1-1 is shown. Figures 3 and 4 show an example of a conventional device;
The figure is a cross-sectional view of the main body of the container in the axial direction, and FIG. 4 shows a cross-sectional view taken along the line 1--■ in FIG. Figures 5 and 6 show an example of a conventional processing device, with Figure 5 being a partially sectional plan view seen from the top of the device, and Figure 6 being a sectional view taken along the line 5 (8). show. 1... Container body, 2a, 2b... Rotating shaft, 3a.

Claims (1)

【特許請求の範囲】 1、水平に設置された円筒状容器内の長手方向に2本の
回転軸を並設し、回転軸は長手に両端を軸受で固定され
、両端の回転軸間は複数個の棒状矩形枠を連結した攪拌
翼を取付け、前記並設した回転軸を相対応する一方の攪
拌翼の棒状矩形枠の先端が他方の攪拌翼の回転中心に近
接して通過するように保持した高粘性物質の連続処理装
置において、 前記回転軸間に設けられた複数個の棒状矩形枠の半径方
向部材間に単一若しくは複数個、軸中心と矩形枠の長手
方向部材との間で回転軸方向に接続する部材を設けたこ
とを特徴とする高粘性物質の連続処理装置。
[Claims] 1. Two rotating shafts are arranged in parallel in the longitudinal direction in a cylindrical container installed horizontally, the rotating shafts are fixed with bearings at both longitudinal ends, and there are multiple rotating shafts between the rotating shafts at both ends. Attach agitating blades in which two rod-shaped rectangular frames are connected, and hold the rotary shafts arranged in parallel so that the tips of the rod-shaped rectangular frames of one of the corresponding agitating blades pass close to the center of rotation of the other stirring blade. In the continuous processing apparatus for highly viscous substances, one or more rotary members are rotated between the radial members of a plurality of rod-shaped rectangular frames provided between the rotating shafts, and between the shaft center and the longitudinal members of the rectangular frames. A continuous processing device for highly viscous substances, characterized in that a member is provided that connects in the axial direction.
JP2239841A 1990-09-12 1990-09-12 Continuous treatment apparatus of highly viscous material Pending JPH04122427A (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
JP2239841A JPH04122427A (en) 1990-09-12 1990-09-12 Continuous treatment apparatus of highly viscous material
KR1019910015419A KR920006397A (en) 1990-09-12 1991-09-04 Continuous processing device of high viscosity material
DE4129669A DE4129669A1 (en) 1990-09-12 1991-09-06 Stirrer assembly, for reactor - formed as interacting rectangular frames by parallel rotating shafts, for high viscosity bulk polymerisation e.g. polyethylene terephthalate

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2239841A JPH04122427A (en) 1990-09-12 1990-09-12 Continuous treatment apparatus of highly viscous material

Publications (1)

Publication Number Publication Date
JPH04122427A true JPH04122427A (en) 1992-04-22

Family

ID=17050666

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2239841A Pending JPH04122427A (en) 1990-09-12 1990-09-12 Continuous treatment apparatus of highly viscous material

Country Status (3)

Country Link
JP (1) JPH04122427A (en)
KR (1) KR920006397A (en)
DE (1) DE4129669A1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007297359A (en) * 2006-05-08 2007-11-15 Central Glass Co Ltd Method for producing fluoroalkylsulfonic anhydride

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4339628C2 (en) * 1993-11-20 2003-04-10 Ismar Maschinen Gmbh kneading

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007297359A (en) * 2006-05-08 2007-11-15 Central Glass Co Ltd Method for producing fluoroalkylsulfonic anhydride

Also Published As

Publication number Publication date
DE4129669A1 (en) 1992-03-19
KR920006397A (en) 1992-04-27

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