JPH0378925B2 - - Google Patents

Info

Publication number
JPH0378925B2
JPH0378925B2 JP18834883A JP18834883A JPH0378925B2 JP H0378925 B2 JPH0378925 B2 JP H0378925B2 JP 18834883 A JP18834883 A JP 18834883A JP 18834883 A JP18834883 A JP 18834883A JP H0378925 B2 JPH0378925 B2 JP H0378925B2
Authority
JP
Japan
Prior art keywords
tank
chemical
tanks
processing tank
chemical liquid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
JP18834883A
Other languages
Japanese (ja)
Other versions
JPS6080737A (en
Inventor
Kunihisa Nakamura
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Choda Seisakusho Kk
Original Assignee
Choda Seisakusho Kk
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Choda Seisakusho Kk filed Critical Choda Seisakusho Kk
Priority to JP18834883A priority Critical patent/JPS6080737A/en
Publication of JPS6080737A publication Critical patent/JPS6080737A/en
Publication of JPH0378925B2 publication Critical patent/JPH0378925B2/ja
Granted legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/36Embedding or analogous mounting of samples

Landscapes

  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Or Analysing Biological Materials (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Microscoopes, Condenser (AREA)

Description

【発明の詳細な説明】 (技術分野) この発明は、顕微鏡標本を作成する為に、生物
組織片を種々の薬液に順次浸漬処理してパラフイ
ンで固めるのに使用される一槽式包埋装置に於い
て、浸漬処理を繰り返す事により劣化した薬液を
能率良く入れ換える方法に関する。
[Detailed Description of the Invention] (Technical Field) The present invention relates to a one-tank embedding device used for sequentially immersing biological tissue pieces in various chemical solutions and solidifying them with paraffin in order to create microscopic specimens. The present invention relates to a method for efficiently replacing chemical solutions that have deteriorated through repeated immersion treatments.

(発明の背景) 病理検査の為、患部等から切り取つた生物組織
片を、脱水、脱脂した後パラフインを浸透して固
化させ、ミクロトーム刀で薄切して顕微鏡標本と
する事が行なわれている。
(Background of the invention) For pathological examinations, biological tissue pieces cut from affected areas, etc. are dehydrated, degreased, soaked in paraffin to solidify them, and then sliced with a microtome to obtain microscopic specimens. .

この様な作業を行なう包埋装置の一種として、
処理しようとする生物組織片を、薬液を出入させ
る事の出来る1個の処理槽内に入れ、この処理槽
に順次一連の処理用薬液(例えばアルコール、キ
シレン等)のタンク及び溶融パラフインのタンク
を連通させ、これらの薬液及び溶融パラフイン
を、定められたプログラムにより順次処理槽内に
送り込んで所要時間ずつ組織を処理する一槽式包
埋装置が知られている。
As a type of embedding device that performs this kind of work,
A piece of biological tissue to be processed is placed in a single processing tank through which chemical solutions can be introduced and removed, and a series of tanks for processing chemicals (e.g., alcohol, xylene, etc.) and a tank for molten paraffin are sequentially placed in this processing tank. A one-tank embedding apparatus is known in which these chemical solutions and molten paraffin are communicated with each other and are sequentially sent into a processing tank according to a predetermined program to process tissues for a required period of time.

図面は一般的な一槽式包埋装置の概要を示して
いる。1はロータリ弁で、このロータリ弁1は、
複数の薬液タンク2a,2b及びパラフインタン
ク3,3に入れた薬液や溶融パラフインを、これ
より高い位置に設けられた処理槽4へ順次送る為
のものである。
The drawing shows an overview of a typical single-vessel embedding device. 1 is a rotary valve, and this rotary valve 1 is
This is for sequentially sending the chemical liquid and molten paraffin contained in the plurality of chemical liquid tanks 2a, 2b and paraffin tanks 3, 3 to a processing tank 4 provided at a higher position.

上記各タンク2a,2b,3に挿入された管
5,6は、ロータリ弁1の弁座1aに接続されて
いる。そして上記各管5,6は、弁板1bの回動
による通路切り換えにより、管7を介して、順次
処理槽4の底部に通じる。パラフインタンク3,
3やパラフインの通る通路、処理槽4には、ヒー
タや断熱材を取付けて、加熱、保温をする。
The pipes 5, 6 inserted into the respective tanks 2a, 2b, 3 are connected to the valve seat 1a of the rotary valve 1. The pipes 5 and 6 are sequentially connected to the bottom of the processing tank 4 via the pipe 7 by switching the passages by rotating the valve plate 1b. Parafine tank 3,
A heater and a heat insulating material are attached to the passage through which the paraffin and paraffin pass through and the processing tank 4 to heat and keep warm.

処理槽4内には、生物組織片を入れた通液性の
篭8が挿入される。処理槽4には気密蓋9が施さ
れ、処理槽4の上部は管10により三方弁11を
経て、管12を通り真空ポンプ13に、又は管1
4を通り大気に、選択的に通じる様になつてい
る。
A liquid-permeable cage 8 containing biological tissue pieces is inserted into the processing tank 4 . The processing tank 4 is equipped with an airtight lid 9, and the upper part of the processing tank 4 is connected to a pipe 10 through a three-way valve 11, a pipe 12 to a vacuum pump 13, or a pipe 1.
4 and selectively communicates with the atmosphere.

この様な一槽式包埋装置により、生物組織片の
包埋処理を行なう場合には、先ず、三方弁11を
切り換える事により、処理槽4内を真空ポンプ1
3に通じさせ、この処理槽4内を減圧する。
When embedding biological tissue pieces using such a one-tank embedding device, first, by switching the three-way valve 11, the inside of the processing tank 4 is controlled by the vacuum pump 1.
3, and the pressure inside this processing tank 4 is reduced.

この結果、ロータリ弁1により管7と連通する
管5の一つを通り、管5に挿入された薬液タンク
2a1の薬液が処理槽4に吸込まれて、篭8を浸漬
し、篭8内の生物組織片を処理する。
As a result, the chemical liquid in the chemical liquid tank 2a1 inserted into the pipe 5 passes through one of the pipes 5 communicating with the pipe 7 by the rotary valve 1, is sucked into the processing tank 4, immerses the basket 8, and enters the inside of the basket 8. processing biological tissue pieces.

所定時間の処理が終つたならば、三方弁11を
大気側に切り換える。この切り換えにより、処理
槽4に大気が進入し、この処理槽4内の薬液は管
7,5を流下して、元の薬液タンク2a1戻る。
When the processing for a predetermined period of time is completed, the three-way valve 11 is switched to the atmosphere side. By this switching, the atmosphere enters the processing tank 4, and the chemical liquid in the processing tank 4 flows down the pipes 7 and 5 and returns to the original chemical liquid tank 2a1 .

そこでロータリ弁1を切り換え、次の薬液タン
ク2a2を処理槽4に接続して同様に操作し、最後
にパラフインタンク3から溶融パラフインを、同
様にして処理槽4に給排し、パラフイン包埋をす
る。
Therefore, the rotary valve 1 is switched, the next chemical tank 2a 2 is connected to the processing tank 4, and the same operation is performed.Finally, the molten paraffin is supplied and discharged from the paraffin tank 3 to the processing tank 4 in the same manner, and the paraffin embedding process is carried out. do.

この例は、薬液、パラフインの排出を大気圧に
よる自然流下により行なうものであるが、図面に
鎖線で示した様に、三方弁11の大気側にコンプ
レツサ15を接続し、加圧空気により薬液等をタ
ンクに押戻す様にしても良い。この場合は、処理
槽4をタンク2a,2b,3よりも低い位置に設
ける事が出来る。
In this example, the chemical liquid and paraffin are discharged by gravity under atmospheric pressure.As shown by the chain line in the drawing, a compressor 15 is connected to the atmosphere side of the three-way valve 11, and the chemical liquid and paraffin are discharged using pressurized air. It is also possible to push it back into the tank. In this case, the processing tank 4 can be provided at a lower position than the tanks 2a, 2b, and 3.

ところで、上述の様に構成され作用する一槽式
包埋装置に於いて、処理槽4に薬液を供給する為
の薬液タンク2a,2bには、総て異なる種類の
薬液を貯溜しておくのではない。
By the way, in the one-tank embedding apparatus constructed and operated as described above, the chemical liquid tanks 2a and 2b for supplying the chemical liquid to the processing tank 4 store different types of chemical liquids. isn't it.

例えば、包埋装置の初期行程時に、処理槽4内
に薬液を供給する薬液タンク2a1〜2a7には、何
れも脱水、脱脂用のアルコールを貯溜しておき、
次の行程に於いて処理槽4内に薬液を供給する薬
液タンク2b1〜2b3には、処理槽内洗滌用のキシ
レンを貯溜しておく。
For example, during the initial process of the embedding device, alcohol for dehydration and degreasing is stored in the chemical liquid tanks 2a 1 to 2a 7 that supply the chemical liquid to the processing tank 4.
Xylene for cleaning the inside of the processing tank is stored in the chemical tanks 2b 1 to 2b 3 that supply the chemical into the processing tank 4 in the next step.

同一の薬液であるアルコールを貯溜した、薬液
タンク2a1〜2a7に於いては、最初に処理槽4内
と連通される薬液タンク2a1に貯溜されたアルコ
ールの純度が最も低く、2a2,2a3と次第に純度
の高いものとなり、アルコールを貯溜した薬液タ
ンク2aの中では最後に処理槽4と連通される、
最後尾の薬液タンク2a7に、最も純度の高い無水
アルコールが貯溜される。
Among the chemical liquid tanks 2a 1 to 2a 7 that store alcohol, which is the same chemical liquid, the alcohol stored in the chemical liquid tank 2a 1 that communicates with the inside of the processing tank 4 first has the lowest purity, 2a 2 , 2a to 3 , the purity gradually increases, and in the chemical tank 2a storing alcohol, it is finally communicated with the processing tank 4.
Anhydrous alcohol of the highest purity is stored in the last chemical tank 2a7 .

これは、各薬液タンク2a1〜2a7内のアルコー
ルを処理槽4内に送り込んで、この処理槽4内の
生物組織片を処理すると、この組織片中の水分及
び脂肪がアルコール中に混入する為で、包埋装置
に於いては脱水及び脱脂が完全に行なわれる様
に、次第に純度の高くなる複数(通常は図示の例
の様に7個)の薬液タンク2a1〜2a7から、順次
処理槽4にアルコールを給排する。
This is because when the alcohol in each chemical solution tank 2a 1 to 2a 7 is sent into the processing tank 4 and the biological tissue pieces in this processing tank 4 are processed, the water and fat in the tissue pieces mix into the alcohol. Therefore, in order to ensure complete dehydration and degreasing in the embedding device, chemical solutions are sequentially added from multiple (usually seven as in the illustrated example) tanks 2a 1 to 2a 7 of increasing purity. Alcohol is supplied to and discharged from the processing tank 4.

薬液タンク2b1〜2b3に貯溜されたキシレン
も、同様に、最初に処理槽4に連通される薬液タ
ンク2b1内のものが最も純度が低く、キシレンを
貯溜した薬液タンク2bの中では最後に処理槽4
に連通される、最後尾の薬液タンク2b3内のもの
が、最も純度が高くなつている。
Regarding the xylene stored in the chemical liquid tanks 2b 1 to 2b 3 , the purity of the chemical liquid tank 2b 1 that is first communicated with the processing tank 4 is the lowest, and the lowest purity of the chemical liquid tank 2b that stores xylene. processing tank 4
The chemical liquid in the last chemical liquid tank 2b3, which is communicated with the chemical liquid tank 2b3 , has the highest purity.

この様に各薬液タンク2a,2b内に貯溜され
た薬液は、包埋処理を繰り返し行なう事により次
第に純度が低下し、良好な包埋処理を行なえなく
なる為、或る程度処理作業を行なつた後は、薬液
を入れ換えなければならない。
As described above, the purity of the chemical liquid stored in each chemical liquid tank 2a, 2b gradually decreases as the embedding process is repeated, making it impossible to perform a good embedding process. After that, you have to replace the chemical solution.

この際、全部の薬液を新しいものと交換したの
では、薬液が無駄となり、費用が嵩む為、例えば
アルコールを貯溜した薬液タンク2aの場合、最
も純度が低いタンク2a1内のアルコールのみを廃
棄してから、少し純度の高いアルコールを貯溜し
た薬液タンク2a2をタンク2a1の位置に移し、以
下同様にして、タンク2a7をタンク2a6の位置に
移し、タンク2a7の位置には新しい無水アルコー
ルを貯溜したタンクを装着する様にしている。キ
シレンを貯溜したタンク2bの場合も同様であ
る。
At this time, replacing all the chemical solutions with new ones would waste the chemical solutions and increase costs. For example, in the case of the chemical solution tank 2a that stores alcohol, only the alcohol in the tank 2a 1 , which has the lowest purity, should be discarded. After that, move the chemical solution tank 2a 2 containing alcohol with a slightly higher purity to the tank 2a 1 position, and in the same way, move the tank 2a 7 to the tank 2a 6 position, and place a new anhydrous liquid in the tank 2a 7 position. It is equipped with a tank that stores alcohol. The same applies to the tank 2b storing xylene.

ところが、従来は総ての薬液タンク2a,2b
を取り外して、1個ずつ隣りに移し換える作業を
行なつていた為、薬液の入れ換え作業が面倒であ
つた。特に管5,5は各薬液タンク2a,2bの
奥に迄挿し込まれている為、この管5,5を各薬
液タンク2a,2b内から抜き出す作業は、包埋
装置が狭い場所に設置されている場合は行ない難
く、管5内に残留した薬液が滴下して作業者の衣
服を汚したり、或は薬液がクロロホルム等の場合
は、床にこぼれて異臭を放つ等、周囲の環境を悪
化する事になり好ましくない。
However, conventionally, all chemical liquid tanks 2a, 2b
The work of replacing the chemical solution was troublesome, as it involved removing the chemical solution and transferring it one by one to the adjacent one. In particular, since the tubes 5, 5 are inserted deep into each chemical solution tank 2a, 2b, the work of extracting these tubes 5, 5 from each drug solution tank 2a, 2b is difficult if the embedding device is installed in a narrow space. It is difficult to do so if the chemical solution remaining in the pipe 5 drips and stains the clothes of the worker, or if the chemical solution is chloroform or the like, it spills on the floor and gives off a strange odor, worsening the surrounding environment. I don't like it because I have to do it.

(本発明の目的) 本発明は上述の様な不都合を解消し、薬液の入
れ換えを、衣服等を汚す事なく容易に行なえる、
一槽式包埋装置に於ける薬液の入れ換え方法を提
供する事を目的としている。
(Object of the present invention) The present invention solves the above-mentioned inconveniences, and makes it possible to easily replace the chemical solution without staining clothes, etc.
The purpose is to provide a method for replacing chemical solutions in a single-tank embedding device.

(本発明の構成) 本発明の一槽式包埋装置に於ける薬液の入れ換
え方法は、同一種の薬液を貯溜した複数の薬液タ
ンクの内、包埋処理時に最初に処理槽と連通され
る、最も純度の低い薬液を貯溜した第一の薬液タ
ンク内の薬液を廃棄した後、隣りの第二の薬液タ
ンク内に貯溜された少し純度の高い薬液を処理槽
に移してから、上記複数の薬液タンクと処理槽と
を結ぶ管路の途中に設けた弁を切り換えて、処理
槽内の薬液を上記空になつた第一の薬液タンク内
に移し替え、次いで空になつた第二の薬液タンク
内に、隣りの第三の薬液タンク内の、更に少し純
度の高い薬液を同様の操作により移し換える操作
を繰り返し行なつて、同一種の薬液を貯溜した上
記複数の薬液タンクの内、包埋処理時に最後に処
理槽と連通される最後尾の薬液タンクが空になつ
た後、この最後尾の薬液タンク内に新しい薬液を
注入する。
(Structure of the present invention) In the method for exchanging chemical solutions in the single-tank embedding device of the present invention, among a plurality of chemical solution tanks storing the same type of drug solution, the one that communicates with the processing tank first during the embedding process is After discarding the chemical solution in the first chemical tank storing the lowest purity chemical solution, the slightly higher purity chemical solution stored in the adjacent second chemical tank is transferred to the processing tank, and then the above-mentioned multiple By switching the valve installed in the middle of the pipe connecting the chemical tank and the processing tank, the chemical liquid in the processing tank is transferred to the empty first chemical tank, and then transferred to the empty second chemical tank. By repeating the same operation to transfer a slightly higher purity chemical from an adjacent third chemical tank into the tank, one of the plurality of chemical liquid tanks storing the same type of chemical liquid was packaged. After the last chemical liquid tank that communicates with the processing tank is finally emptied during burial treatment, a new chemical liquid is injected into this last chemical liquid tank.

(実施例) 次に、図示の一槽式包埋装置を参照しつつ本発
明を更に詳しく説明する。
(Example) Next, the present invention will be described in more detail with reference to the illustrated one-tank embedding apparatus.

薬液の入れ換えを行なう場合には、先ず、同一
種の薬液を貯溜した複数個ずつの薬液タンク2
a,2bの内、包埋処理時に最初に処理槽4に連
通する、それぞれ最も純度の低いアルコール、キ
シレンを貯溜した薬液タンク2a1,2b1を外し、
内部のアルコール、キシレンを廃棄する。
When replacing the chemical solution, first, the chemical solution tanks 2 each containing the same type of chemical solution are replaced.
Of a and 2b, remove the chemical tanks 2a 1 and 2b 1 , which store the lowest purity alcohol and xylene, respectively, and which communicate with the processing tank 4 first during the embedding process.
Discard the alcohol and xylene inside.

次いで、ロータリ弁1が薬液タンク2a1と処理
槽4とを通過させた状態で、真空ポンプ13を運
転する。タンク2a1は空である為、管5から処理
槽4へは空気が自由に流入し、処理槽4内の圧力
は低下しない為、適当な場所に圧力スイツチを設
ければ、真空ポンプ13を一定時間運転する事に
より、タンク2a1内が空である事が確かめられ
る。
Next, the vacuum pump 13 is operated with the rotary valve 1 allowing the chemical solution tank 2a 1 and the processing tank 4 to pass through. Since the tank 2a1 is empty, air freely flows into the processing tank 4 from the pipe 5, and the pressure inside the processing tank 4 does not decrease. Therefore, if a pressure switch is installed at an appropriate location, the vacuum pump 13 can be turned on. By operating for a certain period of time, it can be confirmed that the tank 2a1 is empty.

タンク2a1に薬液が残つていると、次の操作で
タンク2a2の薬液をタンク2a1に移す事が出来な
い(溢れる)為、警報により注意を促す。タンク
2a1が空である事を確認出来たならば、ロータリ
弁1を切り換えて、タンク2a2を処理槽4に通じ
させ、真空ポンプ13を駆動して、このタンク2
a2内のアルコールを処理槽4内に吸引する。
If the chemical solution remains in the tank 2a 1 , the chemical solution in the tank 2a 2 cannot be transferred to the tank 2a 1 in the next operation (overflow), so an alarm is issued to call for attention. After confirming that the tank 2a 1 is empty, switch the rotary valve 1 to make the tank 2a 2 communicate with the processing tank 4, drive the vacuum pump 13, and drain the tank 2.
The alcohol in a 2 is sucked into the processing tank 4.

タンク2a2内のアルコールを総て処理槽4内に
吸引したならば、ロータリ弁1を切り換えて再び
タンク2a1の処理槽4とを通じさせると共に、三
方弁11を切り換えて管10と管14とを連通さ
せ、この処理槽4内のアルコールをタンク2a1
に移し換える。
Once all the alcohol in the tank 2a 2 has been sucked into the processing tank 4, switch the rotary valve 1 to make the tank 2a 1 communicate with the processing tank 4 again, and switch the three-way valve 11 to connect the pipe 10 and the pipe 14. The alcohol in the processing tank 4 is transferred to the tank 2a1 .

この操作により、タンク2a2が空になるので、
次いでタンク2a2のアルコールをタンク2a1に移
したのと同様の手順で、タンク2a3内のアルコー
ルをタンク2a2に移し換え、以下同様の作業を繰
り返し行なつて、タンク2a7内のアルコールをタ
ンク2a6に移し換える。
This operation empties tank 2a 2 , so
Next, in the same manner as the alcohol in tank 2a 2 was transferred to tank 2a 1 , the alcohol in tank 2a 3 is transferred to tank 2a 2 , and the same process is repeated to remove the alcohol in tank 2a 7 . Transfer to tank 2a 6 .

タンク2a7内のアルコールをタンク2a6に移し
換え、このタンク2a7と隣りのタンク2b1とが空
である事を確認したならば、前記したアルコール
の場合と同様にして、タンク2b2内のキシレンを
タンク2b1内に移し換え、次いでタンク2b3内の
キシレンをタンク2b2内に移し換える。
After transferring the alcohol in tank 2a 7 to tank 2a 6 and confirming that this tank 2a 7 and the adjacent tank 2b 1 are empty, transfer the alcohol in tank 2b 2 in the same manner as in the case of alcohol described above. xylene in tank 2b 1 is transferred, and then xylene in tank 2b 3 is transferred into tank 2b 2 .

以上の操作が完了した時点で、アルコール、キ
シレンは、それぞれ1個ずつ前のタンクに移し換
えられ、それぞれ最後尾のタンク2a7,2b3は空
になる為、タンク2a7には新しい無水アルコール
を、タンク2b3には純粋なキシレンを、それぞれ
注入して、薬液の入れ換え作業を完了する。
When the above operations are completed, alcohol and xylene are transferred one by one to the previous tank, and the last tanks 2a 7 and 2b 3 are empty, so new anhydrous alcohol is placed in tank 2a 7 . Pure xylene is injected into tanks 2b and 3 , respectively, to complete the chemical replacement work.

以上の操作の内、タンク2a1,2b1の薬液廃棄
と、タンク2a7,2b3への新たな薬液注入とを除
く操作、即ちロータリ弁1の切り換え、三方弁1
1の切り換え、真空ポンプ13の運転、停止は、
マイクロコンピユータにより予め定められた順序
に従つて、自動的に行なわれる。
Among the above operations, operations excluding the disposal of the chemical liquid in the tanks 2a 1 and 2b 1 and the injection of new chemical liquid into the tanks 2a 7 and 2b 3 , i.e., the switching of the rotary valve 1 and the three-way valve 1
1, operation and stop of the vacuum pump 13 are as follows:
This is done automatically according to a predetermined order by a microcomputer.

従つて、操作者は最初にタンク2a1,2b1内の
薬液を廃棄し、最後にタンク2a7,2b3内に新た
な薬液を注入するだけで良い。
Therefore, the operator only needs to first discard the chemical liquid in the tanks 2a 1 and 2b 1 and finally inject new chemical liquid into the tanks 2a 7 and 2b 3 .

尚、ロータリ弁のボートを薬液タンク2a,2
bとパラフインタンク3,3との合計量よりも多
くし、この余分のポートに接続した管を、廃棄さ
れる薬液を貯溜する廃棄タンクに連通すれば、タ
ンク2a1,2b1の着脱作業も不要となる。
In addition, the boat of the rotary valve is connected to the chemical tank 2a, 2.
b and the paraffin tanks 3 and 3, and connect the pipe connected to this extra port to the waste tank that stores the chemical solution to be discarded, the work of attaching and detaching the tanks 2a 1 and 2b 1 is also possible. No longer needed.

更に、タンク2a7,2b3に新しい薬液を注入す
る場合、処理槽4に注入した薬液を管7、ロータ
リ弁1、管5を通じて各タンク2a7,2b3に移す
様にすれば、タンク2a7,2b3の着脱も不要とな
る、但し、この場合は、タンク2a7に注入する無
水アルコールにキシレンが混入しない様にする
為、タンク2aのアルコールをタンク2a6に移し
てタンク2a7が空になつたならば、タンク2bの
キシレン移し換えをする前に処理槽4に無水アル
コールを注入し、この無水アルコールをタンク2
a7に移し換える。この操作も、補充用の無水アル
コールを貯溜した補充タンクとロータリ弁とを管
で接続しておけば、マイクロコンピユータのプロ
グラムに従つて自動的に行なわれる。タンク2b3
への純粋なキシレンの注入も同様に行なう事が出
来る。
Furthermore, when injecting a new chemical solution into the tanks 2a 7 and 2b 3 , if the chemical solution injected into the processing tank 4 is transferred to each tank 2a 7 and 2b 3 through the pipe 7, rotary valve 1, and pipe 5, the tank 2a 7 and 2b 3 are no longer required. However, in this case, in order to prevent xylene from being mixed with the absolute alcohol injected into tank 2a 7 , the alcohol in tank 2a is transferred to tank 2a 6 , and tank 2a 7 is Once the tank 2b is empty, pour absolute alcohol into the treatment tank 4 before transferring the xylene from the tank 2b, and pour this absolute alcohol into the tank 2.
Transfer to a 7 . This operation can also be performed automatically according to the microcomputer program if the replenishment tank containing absolute alcohol for replenishment is connected to the rotary valve through a pipe. tank 2b 3
Injection of pure xylene into can be performed in a similar manner.

(発明の効果) 本発明の一槽式包埋装置に於ける薬液の入れ換
え方法は、以上に述べた様に構成される為、薬液
の入れ換え時に付け外ししなければならない薬液
タンクの数が少なくて済み、或は付け外しが不要
となり、作業が容易でしかも衣服や床を汚損する
事も少なくて済む。
(Effects of the Invention) Since the method for exchanging chemical solutions in the one-tank embedding device of the present invention is configured as described above, the number of chemical solution tanks that must be attached and removed when exchanging chemical solutions is reduced. There is no need to attach or remove the device, making the work easier and reducing the chance of staining clothes or the floor.

【図面の簡単な説明】[Brief explanation of drawings]

図面は一槽式包埋装置の構成を略示する図であ
る。 1:ロータリ弁、1a:弁座、1b:弁板、2
a,2b:薬液タンク、3:パラフインタンク、
4:処理槽、5,6,7:管、8:篭、9:気密
蓋、10:管、11:三方弁、12:管、13:
真空ポンプ、14:管、15:コンプレツサ。
The drawing is a diagram schematically showing the configuration of a single-tank embedding device. 1: Rotary valve, 1a: Valve seat, 1b: Valve plate, 2
a, 2b: chemical tank, 3: paraffin tank,
4: Processing tank, 5, 6, 7: Pipe, 8: Basket, 9: Airtight lid, 10: Pipe, 11: Three-way valve, 12: Pipe, 13:
Vacuum pump, 14: pipe, 15: compressor.

Claims (1)

【特許請求の範囲】[Claims] 1 同一種の薬液を貯溜した複数の薬液タンクの
内、包埋処理時に最初に処理槽と連通される、最
も純度の低い薬液を貯溜した第一の薬液タンク内
の薬液を廃棄した後、隣りの第二の薬液タンク内
に貯溜された少し純度の高い薬液を処理槽に移し
てから、上記複数の薬液タンクと処理槽とを結ぶ
管路の途中に設けた弁を切り換えて、処理槽内の
薬液を上記空になつた第一の薬液タンク内に移し
替え、次いで空になつた第二の薬液タンク内に、
隣りの第三の薬液タンク内の、更に少し純度の高
い薬液を同様の操作により移し換える操作を繰り
返し行なつて、同一種の薬液を貯溜した上記複数
の薬液タンクの内、包埋処理時に最後に処理槽と
連通される最後尾の薬液タンクが空になつた後、
この最後尾の薬液タンク内に新しい薬液を注入す
る、一槽式包埋装置に於ける薬液の入れ換え方
法。
1 Among multiple chemical liquid tanks storing the same type of chemical liquid, the first chemical liquid tank that stores the lowest purity chemical liquid, which is communicated with the processing tank first during the embedding process, is disposed of, and then The slightly higher purity chemical solution stored in the second chemical solution tank is transferred to the processing tank, and then the valve installed in the middle of the pipe connecting the plurality of chemical solution tanks and the processing tank is switched to remove the inside of the processing tank. Transfer the chemical solution into the empty first chemical tank, and then into the empty second chemical tank,
By repeating the same operation to transfer a slightly higher purity chemical from the adjacent third chemical tank, the last one of the plurality of chemical tanks storing the same kind of chemical was transferred during the embedding process. After the last chemical tank connected to the treatment tank is emptied,
A method for replacing the chemical solution in a single-tank embedding device, in which a new drug solution is injected into the last drug tank.
JP18834883A 1983-10-11 1983-10-11 Process for exchanging liquid chemical in single tank type enbedding apparatus Granted JPS6080737A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP18834883A JPS6080737A (en) 1983-10-11 1983-10-11 Process for exchanging liquid chemical in single tank type enbedding apparatus

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP18834883A JPS6080737A (en) 1983-10-11 1983-10-11 Process for exchanging liquid chemical in single tank type enbedding apparatus

Publications (2)

Publication Number Publication Date
JPS6080737A JPS6080737A (en) 1985-05-08
JPH0378925B2 true JPH0378925B2 (en) 1991-12-17

Family

ID=16222045

Family Applications (1)

Application Number Title Priority Date Filing Date
JP18834883A Granted JPS6080737A (en) 1983-10-11 1983-10-11 Process for exchanging liquid chemical in single tank type enbedding apparatus

Country Status (1)

Country Link
JP (1) JPS6080737A (en)

Also Published As

Publication number Publication date
JPS6080737A (en) 1985-05-08

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