JPH03127638A - Vibrating and stirring ball mil - Google Patents

Vibrating and stirring ball mil

Info

Publication number
JPH03127638A
JPH03127638A JP2267516A JP26751690A JPH03127638A JP H03127638 A JPH03127638 A JP H03127638A JP 2267516 A JP2267516 A JP 2267516A JP 26751690 A JP26751690 A JP 26751690A JP H03127638 A JPH03127638 A JP H03127638A
Authority
JP
Japan
Prior art keywords
stirring
pulverizing
vibrating
ball mill
stirring ball
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
JP2267516A
Other languages
Japanese (ja)
Other versions
JP2901332B2 (en
Inventor
Dieter Steidl
ディーター・シュタイドル
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hoechst AG
Original Assignee
Hoechst AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst AG filed Critical Hoechst AG
Publication of JPH03127638A publication Critical patent/JPH03127638A/en
Application granted granted Critical
Publication of JP2901332B2 publication Critical patent/JP2901332B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/16Mills in which a fixed container houses stirring means tumbling the charge
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/14Mills in which the charge to be ground is turned over by movements of the container other than by rotating, e.g. by swinging, vibrating, tilting

Abstract

PURPOSE: To activate an area of stagnation by connecting a stirrer via an articulated shaft to a drive assembly. CONSTITUTION: Pulverizing media are supplied in a loosened state from a supply pipe 4. A pulverizing pipe 1 is mounted at a bearing 16 installed to the eccentric drive assembly 5. The articulated shaft 6 absorbs the vibration of both the pulverizing pipe 1 and a stirrer shaft 2. The product to be pulverized is admitted from a supply port 12 in a dry state or suspended state and is discharged from the ball mill through a discharge port 13. As a result, the pulverizing efficiency is improved.

Description

【発明の詳細な説明】 (産業上の利用分野) 本発明は撹はん型のボールミルに関し、その粉砕システ
ムが更に振動動作をも行うように構成された、振動・撹
はん型ボールミルに関するものである。
[Detailed Description of the Invention] (Industrial Application Field) The present invention relates to a stirring type ball mill, and more particularly, to a vibrating/stirring type ball mill in which the grinding system is configured to also perform a vibration operation. It is.

(従来の技術) 振動型のミルや撹はん型のボールミルは粉砕装置として
公知である。
(Prior Art) Vibratory mills and stirring ball mills are well-known as grinding devices.

(発明が解決しようとする問題点) これらのミルの欠点は、被粉砕物の細かさを低下させ、
かつ、時空的な収率を損なう、よどみの区域(被粉砕物
が動かない区域)が比較的大きいことにある。本発明は
この欠点を除去することを目的とする。
(Problems to be Solved by the Invention) The disadvantages of these mills are that they reduce the fineness of the material to be crushed;
Another problem is that the stagnation area (area where the material to be crushed does not move) is relatively large, which impairs the spatiotemporal yield. The present invention aims to eliminate this drawback.

(問題点を解決するための手段) 上述の目的を達成するため、本発明の振動・撹はん型ボ
ールミルは次のような構成を採る。すなわち、偏心駆動
装置に装着された軸受に取り付けられた、振動・撹はん
型ボールミルであって、撹はん装置が関節式の軸を介し
て撹はん装置用の駆動装置に連結されている、振動・撹
はん型ボールミルである。
(Means for Solving the Problems) In order to achieve the above-mentioned object, the vibrating/stirring ball mill of the present invention has the following configuration. vibrating and stirring ball mills mounted on bearings mounted on an eccentric drive, the stirring device being connected to the drive for the stirring device via an articulated shaft; This is a vibration/stirring ball mill.

(作用) 本発明の振動・撹はん型ボールミルのように、上述の二
つの粉砕システムを一つの装置として一体化すると、個
別のシステムに比べ前述したよどみの区域が活性化され
、より大きな収率で被粉砕物の細かさが向上する。
(Function) When the above-mentioned two grinding systems are integrated as one device like the vibration/stirring ball mill of the present invention, the stagnation area mentioned above is activated and the yield is increased compared to separate systems. The fineness of the material to be crushed is improved at a higher rate.

(実施例) 本発明の詳細を以下に図に従って説明するが、これは本
発明の一実施例を示すにすぎない。
(Example) The details of the present invention will be described below with reference to the drawings, but this merely shows one example of the present invention.

両側を据え付けられ、撹はん要素3を有する撹はん軸2
が粉砕管1の内部に置かれている。被粉砕物を粉砕する
ための粉砕媒体(図示せず)は、ばらばらにされた状態
で供給管4から供給される。
a stirring shaft 2 mounted on both sides and having a stirring element 3;
is placed inside the crushing tube 1. A grinding medium (not shown) for grinding the object to be ground is supplied from the supply pipe 4 in a separated state.

粉砕管1は偏心駆動装置5に装着された軸受け16に取
り付けられている。図示されていない撹はん装置用の駆
動装置が関節式の軸6を介して撹はん装置に連結してお
り、関節式の軸6が粉砕管1と撹はん軸2の振動を吸収
する。土泥の駆動装置は両方とも無限に調節可能なギア
ボックスに取り付けることができる。撹はん要素3とし
ては、棒や円盤のようなものが適当である。粉砕管1に
は2重のジャケット7.7aを装着することができ、冷
却剤や加熱用媒体を開口8.9.10.11を通してジ
ャケット7.7aに送ったり、そこから排出したりする
ことができる。
The grinding tube 1 is mounted on a bearing 16 mounted on an eccentric drive 5. A drive for the stirring device (not shown) is connected to the stirring device via an articulated shaft 6, which absorbs the vibrations of the grinding tube 1 and the stirring shaft 2. do. Both mud drives can be mounted on an infinitely adjustable gearbox. As the stirring element 3, something like a rod or a disk is suitable. The grinding tube 1 can be fitted with a double jacket 7.7a, through which coolant or heating medium can be conveyed to and discharged from the jacket 7.7a through the openings 8.9.10.11. Can be done.

この撹はん型ボールミルは連続的にも断続的にも操作し
つる。前述の粉砕媒体によって粉砕される製品(被粉砕
物)は、乾燥状態あるいは懸濁した状態で(in a 
5uspension)供給口12から入れられ、排出
口13を通してミルから排出される。
This stirred ball mill can be operated continuously or intermittently. The product to be ground by the above-mentioned grinding media may be in a dry or suspended state (in a
5uspension) is entered through the feed port 12 and discharged from the mill through the discharge port 13.

14.15は測定部を示す。偏心駆動装置5によって、
撹はん型ボールミルは同時に振動ミルとして作動する。
14.15 shows the measurement part. By the eccentric drive device 5,
The stirred ball mill simultaneously operates as a vibratory mill.

振動の大きさは1分間に200ないし1500の振動で
4ないし12mmである。
The magnitude of the vibrations is 4 to 12 mm at 200 to 1500 vibrations per minute.

(発明の効果) 周知の振動ミルや撹はん型ミルに比べ本発明の粉砕装置
の有利な点を下記の試験を参照しながら示す。それぞれ
異なるD5゜の粒子寸法を有する3種類の物質を本発明
の粉砕装置に送り込んで、異なる操作で粉砕を行った。
(Effects of the Invention) The advantages of the grinding device of the present invention compared to known vibrating mills and stirrer mills will be illustrated with reference to the following tests. Three materials, each with a different particle size of D5°, were fed into the milling apparatus of the invention and milled in different operations.

粒子の分析は、C11as製の、レーザーの原理で作動
する粒度測定器で行った。粉砕した物質は測定前に水中
で拡散させた。
The analysis of the particles was carried out with a particle sizer manufactured by C11as and operating on the laser principle. The ground material was dispersed in water before measurements.

この拡散は1分間の超音波処理で行った。サンプルは3
つ計測した。
This diffusion was performed by ultrasonication for 1 minute. The sample is 3
One measurement was made.

試験結果は以下の表に示される。この表中、数字は平均
粒度Dso[μm]を示し、1の欄は粉砕処理していな
い場合、2の欄は純粋に振動ミル動作のみによって粉砕
した場合、3の欄は純粋に撹はんミル動作のみによって
粉砕した場合、4の欄は本発明に従って撹はんミル動作
と振動ミル動作を同時にして粉砕した場合を示す。
The test results are shown in the table below. In this table, the numbers indicate the average particle size Dso [μm]. Column 1 indicates the case where no pulverization treatment was performed, column 2 indicates the case where the pulverization was performed purely by vibration mill operation, and column 3 indicates the case where the pulverization was performed purely by stirring. In the case of pulverization by only mill operation, column 4 shows the case of pulverization by simultaneous stirring mill operation and vibration mill operation according to the present invention.

表 供給物質      1 2 3 4 石灰石       100  5.0 3.5 2.
0ペンゾクサゾール   16.9 5.1 4.4 
2.7ボルアクリロニト リル          42.036.3 37.2
 24.5
Surface supply material 1 2 3 4 Limestone 100 5.0 3.5 2.
0 Penzoxazole 16.9 5.1 4.4
2.7boracrylonitrile 42.036.3 37.2
24.5

【図面の簡単な説明】[Brief explanation of the drawing]

図は、被粉砕物の存在しない状態で表された本発明の一
実施例のミルの断面図である。 1・・・粉砕管 2・・・撹はん軸 3・・・撹はん要素 4・・・粉砕媒体の供給管 5・・・偏心駆動装置 6・・・関節式の軸 7.7a・・・ジャケット 8.9.10.11・・・開口 12・・・被粉砕物の供給口 13.14.15・・・排出口 16・・・軸受
The figure is a cross-sectional view of a mill according to an embodiment of the present invention, shown in the absence of objects to be crushed. 1... Grinding tube 2... Stirring shaft 3... Stirring element 4... Grinding media supply pipe 5... Eccentric drive device 6... Articulated shaft 7.7a. ... Jacket 8.9.10.11 ... Opening 12 ... Supply port for crushed material 13.14.15 ... Discharge port 16 ... Bearing

Claims (1)

【特許請求の範囲】[Claims] 1、偏心駆動装置(5)に装着された軸受(16)に取
り付けられた、振動・撹はん型ボールミルであって、撹
はん装置が関節式の軸(6)を介して撹はん装置用の駆
動装置に連結されている、振動・撹はん型ボールミル。
1. A vibration/stirring ball mill mounted on a bearing (16) mounted on an eccentric drive (5), in which the stirring device stirs through an articulated shaft (6). A vibrating/stirring ball mill connected to a driving device for the equipment.
JP2267516A 1989-10-04 1990-10-04 Vibration / stirring type ball mill Expired - Lifetime JP2901332B2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE3933097A DE3933097A1 (en) 1989-10-04 1989-10-04 SWINGING AGITATOR BALL MILL
DE3933097.4 1989-10-04

Publications (2)

Publication Number Publication Date
JPH03127638A true JPH03127638A (en) 1991-05-30
JP2901332B2 JP2901332B2 (en) 1999-06-07

Family

ID=6390798

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2267516A Expired - Lifetime JP2901332B2 (en) 1989-10-04 1990-10-04 Vibration / stirring type ball mill

Country Status (9)

Country Link
EP (1) EP0421318B1 (en)
JP (1) JP2901332B2 (en)
KR (1) KR0181493B1 (en)
BR (1) BR9004948A (en)
CA (1) CA2026821A1 (en)
DE (2) DE3933097A1 (en)
ES (1) ES2055841T3 (en)
MX (1) MX174613B (en)
PT (1) PT95499B (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2014124617A (en) * 2012-12-27 2014-07-07 Equos Research Co Ltd Thermally crushing device
JP2014124618A (en) * 2012-12-27 2014-07-07 Equos Research Co Ltd Thermally crushing device
CN107199102A (en) * 2017-07-26 2017-09-26 太仓市山姆绿丰农产品专业合作社 A kind of Highefficientpulverizer

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107716002B (en) * 2017-11-06 2023-03-28 齐鲁工业大学 Device and method for preparing hexagonal boron nitride nanosheet through pure shear ball milling and ultrasonic cooperation
CN114653438B (en) * 2022-05-06 2022-11-22 淄博市淄川金龙磨料磨具有限公司 Ball-milling equipment for producing and processing superfine white corundum micropowder

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1116980A (en) * 1965-03-16 1968-06-12 Southwestern Eng Co Machine for pulverizing or surface-treating material
DE2631826A1 (en) * 1975-09-10 1977-03-24 Chamber Of Mines Services Ltd CENTRIFUGAL MILL

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2014124617A (en) * 2012-12-27 2014-07-07 Equos Research Co Ltd Thermally crushing device
JP2014124618A (en) * 2012-12-27 2014-07-07 Equos Research Co Ltd Thermally crushing device
CN107199102A (en) * 2017-07-26 2017-09-26 太仓市山姆绿丰农产品专业合作社 A kind of Highefficientpulverizer

Also Published As

Publication number Publication date
ES2055841T3 (en) 1994-09-01
JP2901332B2 (en) 1999-06-07
EP0421318A3 (en) 1991-07-24
KR910007581A (en) 1991-05-30
CA2026821A1 (en) 1991-04-05
DE3933097A1 (en) 1991-04-11
EP0421318B1 (en) 1994-06-08
KR0181493B1 (en) 1999-04-15
EP0421318A2 (en) 1991-04-10
PT95499A (en) 1992-07-31
BR9004948A (en) 1991-09-10
PT95499B (en) 1998-07-31
DE59006016D1 (en) 1994-07-14
MX174613B (en) 1994-05-30

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