JPH02253895A - Production of brewing water for refined sake - Google Patents
Production of brewing water for refined sakeInfo
- Publication number
- JPH02253895A JPH02253895A JP7617389A JP7617389A JPH02253895A JP H02253895 A JPH02253895 A JP H02253895A JP 7617389 A JP7617389 A JP 7617389A JP 7617389 A JP7617389 A JP 7617389A JP H02253895 A JPH02253895 A JP H02253895A
- Authority
- JP
- Japan
- Prior art keywords
- water
- tank
- hardness
- carbon dioxide
- limestone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 88
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims abstract description 43
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 29
- 229910002092 carbon dioxide Inorganic materials 0.000 claims abstract description 20
- 239000001569 carbon dioxide Substances 0.000 claims abstract description 20
- 235000019738 Limestone Nutrition 0.000 claims abstract description 19
- 239000006028 limestone Substances 0.000 claims abstract description 18
- 238000007664 blowing Methods 0.000 claims abstract description 12
- 238000001914 filtration Methods 0.000 claims abstract description 10
- 238000010828 elution Methods 0.000 abstract description 17
- 150000002500 ions Chemical class 0.000 abstract description 2
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 239000007789 gas Substances 0.000 description 13
- 235000020681 well water Nutrition 0.000 description 8
- 239000002349 well water Substances 0.000 description 8
- 239000000126 substance Substances 0.000 description 6
- -1 1)I)l of about 200 Chemical compound 0.000 description 4
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 3
- 235000011089 carbon dioxide Nutrition 0.000 description 3
- 230000002378 acidificating effect Effects 0.000 description 2
- 235000010216 calcium carbonate Nutrition 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- WZFUQSJFWNHZHM-UHFFFAOYSA-N 2-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperazin-1-yl]-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)N1CCN(CC1)CC(=O)N1CC2=C(CC1)NN=N2 WZFUQSJFWNHZHM-UHFFFAOYSA-N 0.000 description 1
- 238000013124 brewing process Methods 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- NKWPZUCBCARRDP-UHFFFAOYSA-L calcium bicarbonate Chemical compound [Ca+2].OC([O-])=O.OC([O-])=O NKWPZUCBCARRDP-UHFFFAOYSA-L 0.000 description 1
- 229910000020 calcium bicarbonate Inorganic materials 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- 229910001424 calcium ion Inorganic materials 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000013505 freshwater Substances 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
Abstract
Description
【発明の詳細な説明】 [産業上の利用分野J この発明は清酒醸造水の製造法に関するものである。[Detailed description of the invention] [Industrial Application Field J This invention relates to a method for producing sake brewed water.
[従来の技術]
一般に、清酒の醸造水は、灘の官本のように全硬度(以
下、単に硬度という。)CaCO3の1)I)lが、例
えば200程度の高いものが良いとされている。そして
従来は宮水に近いなるべく硬度の高い水を選択して用い
ている。[Prior Art] In general, it is said that sake brewing water should have a high total hardness (hereinafter simply referred to as hardness) of CaCO3, such as 1)I)l of about 200, as shown in Nada Kanbon. There is. Conventionally, water with the highest possible hardness, which is close to Miyamizu, is selected and used.
[発明が解決しようとする課題]
しかしながら、清酒醸造工場においては希望する硬度の
醸造水が得にくい問題があった。そこで、本発明の課題
はたとえばCaCO360ppmの硬度の低い醸造水を
、CaC03200ppm程ri (7)高い硬度に簡
単に改質し得る清酒醸造水の製造法を提供することにあ
る。[Problems to be Solved by the Invention] However, there has been a problem in sake brewing factories that it is difficult to obtain brewed water with a desired hardness. Therefore, an object of the present invention is to provide a method for producing sake brewed water that can easily modify brewed water with a low hardness of, for example, 360 ppm of CaCO to a hardness of about 200 ppm of CaCO (7).
[課題を解決するための手段]
上記した課題を解決するための本発明の手段は、清酒の
醸造用とする硬度の低い水に炭酸ガスの吹込みと、石灰
石の接触とを行ない、必要により炭酸ガスの吹込みと石
灰石の接触とを繰返し、しかる後、この水を活性炭濾過
して処理水を得るようにした8IWAs造水の製造法と
される。[Means for Solving the Problems] The means of the present invention for solving the above-mentioned problems includes blowing carbon dioxide gas into low-hardness water used for brewing sake and bringing it into contact with limestone, and, if necessary, It is said to be a method for producing 8IWAs water, in which the blowing of carbon dioxide gas and contact with limestone are repeated, and then the water is filtered with activated carbon to obtain treated water.
[作 用] 硬度の低い水は炭酸ガスの吹込みにより弱酸性になる。[Work] Water with low hardness becomes slightly acidic by blowing carbon dioxide gas into it.
弱酸性の水は石灰石との接触においてCa++イオンを
含有する水となる。活性炭濾過により主として有機物が
吸着除去される。When the slightly acidic water comes into contact with limestone, it becomes water containing Ca++ ions. Activated carbon filtration mainly removes organic substances by adsorption.
[試験例] 次に本発明に係わる試験Fを説明する。[Test example] Next, Test F according to the present invention will be explained.
まず、第1図に示す小規模な試験装置を用意し、醸造水
とする井水Wの硬度を上げる試験をした。First, a small-scale test apparatus shown in FIG. 1 was prepared, and a test was conducted to increase the hardness of well water W used as brewing water.
試験装置において1は石灰石2〜2を入れた溶出槽、3
は通水ポンプ、4は濾過粒度が1μのカートリッジ式の
濾過器、5は繊維状活性炭を入れたカートリッジ式の活
性炭濾過器、6.7.8は開閉弁である。溶出槽1は通
水ポンプ4を介して接続管9,10にて第1図の如く接
続しである。In the test equipment, 1 is an elution tank containing 2 to 2 limestones, 3
4 is a water pump, 4 is a cartridge type filter with a filtration particle size of 1 μm, 5 is a cartridge type activated carbon filter containing fibrous activated carbon, and 6.7.8 is an on-off valve. The elution tank 1 is connected via a water pump 4 to connecting pipes 9 and 10 as shown in FIG.
溶出槽1の井水Wが通水ポンプ3及び濾過器4及び活性
炭濾過器5を経て貯留槽11に至る経1路に)と、溶出
槽1の井水Wが通水ポンプ3及び濾過器4を経て溶出槽
1に循環される経路口とを設けた。The well water W from the elution tank 1 passes through the water pump 3, the filter 4, and the activated carbon filter 5 to reach the storage tank 11), and the well water W from the elution tank 1 passes through the water pump 3 and the filter. 4 and a path opening for circulation to the elution tank 1.
なお、試験に用いた井水Wは京都市松尾大社の境内に湧
出している「亀ノ井」より採取した水を用いた。In addition, the well water W used in the test was water collected from "Kamenoi" which gushes out in the precincts of Matsuo Taisha Shrine, Kyoto City.
試験例1
2C11ブロツクの石灰石を18μ入れた溶出槽1内に
井水Wを51入れ、前記した経路口にて室温で2時間処
理(通水12541 /sin、) L、た貯留槽11
に導入して処理水NQI(処理水WA)を得た。Test Example 1 51 well water W was put into elution tank 1 containing 18μ of 2C11 block limestone, and treated at room temperature for 2 hours at the above-mentioned channel opening (water flow 12541/sin) L, storage tank 11
to obtain treated water NQI (treated water WA).
試験例2
試験例1にて、得た処理水Nα1を貯留槽11にて24
時間放置後に溶出槽1に移し、更に室温にて2時間経路
むにより循環させた後、貯留槽11に戻して処理水N0
2(処理水WA)を得た。Test Example 2 The treated water Nα1 obtained in Test Example 1 was stored in the storage tank 11 for 24 hours.
After standing for a while, the treated water was transferred to the elution tank 1, and after being circulated for 2 hours at room temperature, it was returned to the storage tank 11 and the treated water N0
2 (treated water WA) was obtained.
試験例3
試験装置の溶出槽1にドライアイスを100g投入し、
蒸発完了した15分後に経路(へ)にて1時間循環させ
た後、貯留槽11に導入して処理水Nα3(処理水WA
>を得た。Test Example 3 100g of dry ice was put into the elution tank 1 of the test device,
After 15 minutes after the completion of evaporation, the water is circulated for 1 hour through the path (to), and then introduced into the storage tank 11 where the treated water Nα3 (treated water WA
> obtained.
前記各処理水WAのpH及び全硬度(CaCO3ppm
)は第1表に示す通りであった。pH and total hardness (CaCO3ppm
) were as shown in Table 1.
第1表より、処理水Nα1、処理水NQ 2は石灰石か
らのCa+Fイオンの溶出が定常状態ではほとんどない
ことがわかる。ただし、長時間にわたり循環を行なうと
若干硬度は上がるが、pH値が僅かに下がっていること
から空気中の炭酸ガスを吸収して炭酸水素カルシウムの
形で溶出したものと考えられる。処理水No、 3はp
H値がやや下がり過ぎたが、硬度は非常に高められたこ
とが認められる。From Table 1, it can be seen that in the treated water Nα1 and the treated water NQ2, there is almost no elution of Ca+F ions from limestone in a steady state. However, when circulating for a long time, the hardness increases slightly, but the pH value decreases slightly, which suggests that carbon dioxide gas in the air was absorbed and eluted in the form of calcium hydrogen carbonate. Treated water No. 3 is p
Although the H value decreased a little too much, it was recognized that the hardness was greatly increased.
試験例4
上記した各試験例に基づき、第2図の実用装置を用意し
て試験した。実用装置において、21は溶出槽、22は
水循環用の通水ポンプ、23は濾過粒度が1μの濾過器
、24は活性炭濾過槽、25は処理水WAの貯留槽であ
る。貯留槽25は冷却器26に接続され処理水を冷却保
持可能にされている。前記溶出槽21の上部にはl造水
となる井水の給水管27が配置され、槽内の底部には槽
内の貯水28に炭酸ガスを吹込む炭酸ガス吹込み手段2
9が設けられている。なお、前記した試験例3はドライ
アイスにて炭酸ガスを供給したが、ドライアイスは溶解
ωの制御がし難いので、直接に炭酸ガスを吹込む手段2
9を採用した。槽内の貯水28は槽外の通水ポンプ22
を介して溶出槽21上部より槽内に落下されるようにさ
れている。Test Example 4 Based on the above-mentioned test examples, the practical device shown in FIG. 2 was prepared and tested. In the practical device, 21 is an elution tank, 22 is a water pump for water circulation, 23 is a filter with a filtration particle size of 1 μm, 24 is an activated carbon filtration tank, and 25 is a storage tank for treated water WA. The storage tank 25 is connected to a cooler 26 so that the treated water can be kept cool. At the top of the elution tank 21, a well water supply pipe 27 for producing fresh water is arranged, and at the bottom of the tank there is a carbon dioxide gas blowing means 2 for blowing carbon dioxide into the water stored in the tank.
9 is provided. In addition, in Test Example 3 described above, carbon dioxide gas was supplied using dry ice, but since it is difficult to control the dissolution ω of dry ice, means 2 for directly blowing carbon dioxide gas was used.
9 was adopted. Water storage 28 inside the tank is handled by a water pump 22 outside the tank.
The liquid is dropped into the elution tank 21 from the upper part of the tank through the elution tank 21.
30は槽内の上部に配設された案内板、31は案内板3
0下方に配置された石灰石層である。各装置部は接続管
32,33.34を介して第2図の如く接続されている
。30 is a guide plate arranged at the upper part of the tank, 31 is a guide plate 3
It is a limestone layer located below 0. Each device section is connected through connecting pipes 32, 33, and 34 as shown in FIG.
すなわち、溶出槽21に供給された醸造用の井水Wは石
灰石層31を通過し、槽底部で貯水28となる。貯水2
8には炭酸ガスが吹込まれる。That is, the well water W for brewing supplied to the elution tank 21 passes through the limestone layer 31 and becomes the water storage 28 at the bottom of the tank. Water storage 2
Carbon dioxide gas is blown into 8.
方、貯水28は通水ポンプ22にて溶出槽21の頂部に
汲み上げられ槽内に落下され、石灰石層31と接触し貯
水28となり、炭酸ガスの吹込みと、石灰石の接触が所
定時間繰返され、Ca++イオンが含有された硬度18
0〜220 pf)Ill稈度の水となる。しかる後、
貯水28すなわち処理水は給送ポンプ35を介して濾過
機23に送られ、異物が除去された後、活性炭濾過槽2
4の活性炭層にて有機物が除去され、この濾過水WAは
貯留槽25に導入される。貯留W425の処理水WAは
冷却され、10℃以下に保持される。貯留槽25の冷却
された処理水W△は必要に応じ醸造水として清酒の仕込
み工程に送られる。On the other hand, the water reservoir 28 is pumped up to the top of the elution tank 21 by the water pump 22 and dropped into the tank, and comes into contact with the limestone layer 31 to become the reservoir water 28, and the blowing of carbon dioxide gas and the contact with the limestone are repeated for a predetermined period of time. , hardness 18 containing Ca++ ions
0 to 220 pf) The water will have a culm degree of Ill. After that,
The stored water 28, that is, the treated water, is sent to the filter 23 via the feed pump 35, and after foreign substances are removed, it is transferred to the activated carbon filtration tank 2.
Organic matter is removed in the activated carbon layer No. 4, and this filtered water WA is introduced into the storage tank 25. The treated water WA in the storage W425 is cooled and maintained at 10° C. or lower. The cooled treated water WΔ in the storage tank 25 is sent to the sake brewing process as brewing water if necessary.
しかして、前記した実用装置にて第1表の井水を第2表
の条件1及び条件2にて処理し、第3表の処理水Nα4
−1、及び処理水Nα4−2を得た。Therefore, the well water shown in Table 1 was treated with the above-mentioned practical equipment under conditions 1 and 2 shown in Table 2, and the treated water Nα4 shown in Table 3 was
-1 and treated water Nα4-2 were obtained.
第3表にて明らかなように試験例4にて得た処理氷島4
−1及び処理水No、4−2は清酒のWA造水として好
ましい硬度のものである。As shown in Table 3, the treated ice island 4 obtained in Test Example 4
-1 and treated water No. 4-2 have hardness preferable as WA water production for sake.
本試験例4の実用装置によれば、硬度の低い醸造水は任
意の高硬度の水に改質される。なお、実用装置における
濾過機23は省略し、活性炭濾過槽24にて異物除去と
有機物除去を兼備させてもよい。また、実用装置におい
て、炭酸ガス流山、循環水量、循環時間は適宜に定める
ことができる。According to the practical device of Test Example 4, brewed water with low hardness is reformed into water with any high hardness. Note that the filter 23 in the practical device may be omitted, and the activated carbon filtration tank 24 may be used to remove foreign substances and organic substances. In addition, in a practical device, the flow rate of carbon dioxide gas, the amount of circulating water, and the circulation time can be determined as appropriate.
[発明の効果1
本発明は清酒醸造用の硬度の低い水に炭酸ガスの吹込み
と石灰石の接触とを行なうようにしたので、石灰石の成
分であるCa++イオンが処理水に含有される。そして
Ca イオンの含有層は炭酸ガスの吹込みと石灰石の接
触とを繰返すことにより増すことができ、CCaCO3
200pp程度の高硬度の醸造水となし得る。[Effect of the Invention 1] In the present invention, carbon dioxide gas is blown into low-hardness water for sake brewing and contact with limestone is carried out, so that Ca++ ions, which are a component of limestone, are contained in the treated water. The layer containing Ca ions can be increased by repeating the injection of carbon dioxide gas and contact with limestone,
It can be made into brewed water with a high hardness of about 200 pp.
また、本発明の処理水は活性炭濾過した濾過水であるの
で、異物及び有機物が除去されていて清酒の醸造水とし
て好ましいものである。なお、本発明は特別な処理工程
を必要としないので実施し易い。Furthermore, since the treated water of the present invention is filtered water that has been filtered with activated carbon, foreign substances and organic substances have been removed, making it preferable as brewing water for sake. Note that the present invention is easy to implement because it does not require any special processing steps.
第1図は試験装置の概略図、第2図は実用装置の構′?
l説明図である。
21 ・・・溶 出 槽
22・・・通水ポンプ
23・・・濾 過 機
24・・・活性炭濾過槽
25・・・貯 留 槽
28・・・貯 水
29・・・炭酸ガス吹込み手段
31・・・石灰石層Figure 1 is a schematic diagram of the test equipment, and Figure 2 is the structure of the practical equipment.
1 is an explanatory diagram. 21... Elution tank 22... Water pump 23... Filtration machine 24... Activated carbon filtration tank 25... Storage tank 28... Water storage 29... Carbon dioxide gas blowing means 31...limestone layer
Claims (1)
込みと、石灰石の接触とを行ない、必要により炭酸ガス
の吹込みと石灰石の接触とを繰返し、しかる後、この水
を活性炭濾過して処理水を得ることを特徴とした清酒醸
造水の製造法。(1) Blow in carbon dioxide gas and contact with limestone into low-hardness water used for brewing sake, repeat the blowing of carbon dioxide gas and contact with limestone if necessary, and then pour this water into activated carbon. A method for producing sake brewing water characterized by obtaining treated water through filtration.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP7617389A JPH02253895A (en) | 1989-03-28 | 1989-03-28 | Production of brewing water for refined sake |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP7617389A JPH02253895A (en) | 1989-03-28 | 1989-03-28 | Production of brewing water for refined sake |
Publications (1)
Publication Number | Publication Date |
---|---|
JPH02253895A true JPH02253895A (en) | 1990-10-12 |
Family
ID=13597702
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP7617389A Pending JPH02253895A (en) | 1989-03-28 | 1989-03-28 | Production of brewing water for refined sake |
Country Status (1)
Country | Link |
---|---|
JP (1) | JPH02253895A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110981099A (en) * | 2019-12-18 | 2020-04-10 | 江南大学 | Method for producing ethanol by recycling biogas slurry and vinasse clear liquid and reusing |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS58159892A (en) * | 1982-03-19 | 1983-09-22 | Sumitomo Heavy Ind Ltd | Treatment of fresh water |
JPS6157292A (en) * | 1984-08-29 | 1986-03-24 | Mitsubishi Heavy Ind Ltd | Method for converting fresh water to drinking water |
JPS6238292A (en) * | 1985-08-09 | 1987-02-19 | Hitachi Ltd | Method and apparatus for forming calcium ion water |
JPS6274483A (en) * | 1985-09-30 | 1987-04-06 | Ebara Infilco Co Ltd | Method for improving water quality |
-
1989
- 1989-03-28 JP JP7617389A patent/JPH02253895A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS58159892A (en) * | 1982-03-19 | 1983-09-22 | Sumitomo Heavy Ind Ltd | Treatment of fresh water |
JPS6157292A (en) * | 1984-08-29 | 1986-03-24 | Mitsubishi Heavy Ind Ltd | Method for converting fresh water to drinking water |
JPS6238292A (en) * | 1985-08-09 | 1987-02-19 | Hitachi Ltd | Method and apparatus for forming calcium ion water |
JPS6274483A (en) * | 1985-09-30 | 1987-04-06 | Ebara Infilco Co Ltd | Method for improving water quality |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110981099A (en) * | 2019-12-18 | 2020-04-10 | 江南大学 | Method for producing ethanol by recycling biogas slurry and vinasse clear liquid and reusing |
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