JP7016468B2 - A fragrance composition, a sterilizing deodorant liquid using the fragrance composition, and a sterilizing deodorizing method. - Google Patents
A fragrance composition, a sterilizing deodorant liquid using the fragrance composition, and a sterilizing deodorizing method. Download PDFInfo
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Description
本発明は次亜塩素酸由来の塩素臭をマスキングする香料組成物の改良に関する。 The present invention relates to an improvement in a fragrance composition that masks the chlorine odor derived from hypochlorous acid.
弱酸性の次亜塩素酸水が優れた除菌消臭効果を備え、大気中へ噴霧してもその効果が維持されることが知られている。
次亜塩素酸水はインフルエンザ、ノロウィルス、大腸菌等による食中毒などの感染予防、体や衣服或いは自動車のシート等に付着した汗やタバコの臭い消しとして有効である。
しかしながら、次亜塩素酸水は塩素臭を伴うので、この塩素臭を香料を使ってマスキングすることが考えられる。
本発明に関連する技術を開示する先行文献として特許文献１を参照されたい。
It is known that weakly acidic hypochlorous acid water has an excellent sterilizing and deodorizing effect, and that effect is maintained even when sprayed into the atmosphere.
Hypochlorite water is effective for preventing infections such as food poisoning caused by influenza, norovirus, Escherichia coli, etc., and for eliminating the odor of sweat and tobacco adhering to the body, clothes, automobile seats, and the like.
However, since hypochlorite water is accompanied by a chlorine odor, it is conceivable to mask this chlorine odor with a fragrance.
Please refer to Patent Document 1 as a prior document that discloses a technique related to the present invention.
しかしながら、次亜塩素酸はそもそも消臭効果を備えるので、香料が次亜塩素酸の作用で分解され、期待通りに香り付けができないおそれがある。これはまた、次亜塩素酸が香料分解に消費されて減少し、本来の除菌消臭能力を発揮できなくなるおそれも意味する。 However, since hypochlorous acid has a deodorizing effect in the first place, there is a possibility that the fragrance is decomposed by the action of hypochlorous acid and the fragrance cannot be scented as expected. This also means that hypochlorous acid may be consumed and reduced in the decomposition of fragrances, and the original sterilizing and deodorizing ability may not be exhibited.
したがって、次亜塩素酸水と併用される香料は、次亜塩素酸に対する耐久性に優れかつ次亜塩素酸の除菌消臭能力に悪影響を与えず、さらには、次亜塩素酸水とともに大気中に噴霧されたときに塩素臭を抑制しつつ好適な香り付けができなければならない。
本発明者はかかる課題を達成すべく鋭意検討を重ねた結果、下記の香料組成物を見出した。
即ち、この発明の第１の局面の香料組成物は、
アルコール：２～８質量％、
香料成分：０．１～１．０質量％、
水及び必要に応じて配合される助剤：残部とからなり、
前記香料成分はシネオールとメントールと含む、ことを特徴とする香料組成物である。
Therefore, the fragrance used in combination with hypochlorous acid water has excellent durability against hypochlorous acid, does not adversely affect the sterilizing and deodorizing ability of hypochlorous acid, and further, the atmosphere together with hypochlorous acid water. When sprayed inside, it must be possible to give a suitable fragrance while suppressing the chlorine odor.
As a result of diligent studies to achieve this problem, the present inventor has found the following fragrance composition.
That is, the fragrance composition according to the first aspect of the present invention is:
Alcohol: 2-8% by mass,
Fragrance component: 0.1-1.0% by mass,
Water and auxiliaries to be added as needed: consisting of the balance
The fragrance composition is characterized by containing cineole and menthol as the fragrance component.
ここに、シネオールとメントールの配合比は香料組成物に含まれる香料成分の全質量を１００質量％としたとき、５６～８０質量％：７．５～２０質量％とすることが好ましく、更に好ましい配合比は６０～７０質量％：１０～２０質量％である。
ここに、シネオールとメントールはともに次亜塩素酸に対して安定である。その結果、次亜塩素酸の除菌消臭機能が長時間維持される。また、上記の範囲でシネオールとメントールとを併用して次亜塩素酸水とともに大気中へ噴霧したとき、次亜塩素酸の塩素臭が上手くマスキングされるとともに、付けられた香りも使用者に何ら不快感を与えることがない。
シネオールとメントールとの配合比が上記の範囲を逸脱したときには、塩素臭に対するマスキング効果が不充分になったり、一方の香が強調されすぎて室内空間の香りとして不適なものとなったりする。
Here, the blending ratio of cineole and menthol is preferably 56 to 80% by mass: 7.5 to 20% by mass, more preferably, when the total mass of the fragrance components contained in the fragrance composition is 100% by mass. The blending ratio is 60 to 70% by mass: 10 to 20% by mass.
Here, both cineole and menthol are stable against hypochlorous acid. As a result, the sterilizing and deodorizing function of hypochlorous acid is maintained for a long time. In addition, when cineole and menthol are used in combination in the above range and sprayed into the atmosphere together with hypochlorous acid water, the chlorine odor of hypochlorous acid is well masked, and the attached scent is also given to the user. Does not cause discomfort.
When the blending ratio of cineole and menthol deviates from the above range, the masking effect on chlorine odor becomes insufficient, or one of the scents is overemphasized and becomes unsuitable as the scent of the interior space.
シネオールにはユーカリ油由来の１－８シネオールが好ましい。
メントールにはペパーミント油やハッカ油などから抽出した天然由来のものや合成されたものを用いることができる。
以上より、香料成分はその全質量１００質量％としたとき、質量比で、
ユーカリ油：７０～９０質量％、
ペパーミント油：２５～５質量％、
メントール：残部
とすることが好ましい。
かかる配合比を採用することによりマスキング効果が十分に発揮されるとともに、付される香りもより好適なものとなる。
上記３種以外に意図しない微量な香料が含まれることを何ら阻害するものでない。
更に好ましい香料成分の配合比は、香料成分の全質量を１００質量％としたとき、次の通りである。
ユーカリ油：７５～８５質量％、
ペパーミント油：２０～７質量％、
メントール：残部
The cineole is preferably 1-8 cineole derived from eucalyptus oil.
As the menthol, naturally derived or synthesized menthol extracted from peppermint oil, peppermint oil, or the like can be used.
From the above, when the total mass of the fragrance component is 100% by mass, the mass ratio is
Eucalyptus oil: 70-90% by mass,
Peppermint oil: 25-5% by mass,
Menthol: Preferably the balance.
By adopting such a blending ratio, the masking effect is sufficiently exhibited and the scent to be attached becomes more suitable.
It does not prevent the inclusion of unintended trace amounts of fragrances other than the above three types.
A more preferable blending ratio of the fragrance component is as follows when the total mass of the fragrance component is 100% by mass.
Eucalyptus oil: 75-85% by mass,
Peppermint oil: 20-7% by mass,
Menthol: the rest
かかる香料成分はアルコールに溶解後、水、好ましくは精製水へ分散される。
アルコール、香料成分及び水の配合比は、香料組成物の全質量を１００質量％としたとき、アルコール：２～８質量％、香料成分：０．１～１．０質量％、水：残部とする。
香料成分の配合比を上記の範囲内のものにすれば、塩素臭をマスキングしつつ、次亜塩素酸水を噴霧したとき室内へ好適な香り付けを行える。香料成分の配合量が０．１質％未満になると、塩素臭に対するマスキング効果が不充分になる。他方、香料成分の配合量が１．０質量％を超えると香料成分の香が強調されすぎるので好ましくない。
アルコールの配合量は２～８質量％とする。このアルコールは香料成分を溶解できれば特に限定されず、エタノールの他にメタノールやプロパノールを用いることもできる。
なお、香料組成物には、その使用条件や使用目的等の必要に応じて、防腐剤、酸化防止剤、着色料など助剤の必要量が添加されることは言うまでもない。
The fragrance component is dissolved in alcohol and then dispersed in water, preferably purified water.
The blending ratio of alcohol, fragrance component and water is as follows: alcohol: 2 to 8% by mass, fragrance component: 0.1 to 1.0% by mass, water: balance when the total mass of the fragrance composition is 100% by mass. do.
If the blending ratio of the fragrance component is within the above range, it is possible to give a suitable scent to the room when spraying hypochlorite water while masking the chlorine odor. When the blending amount of the fragrance component is less than 0.1%, the masking effect on the chlorine odor becomes insufficient. On the other hand, if the blending amount of the fragrance component exceeds 1.0% by mass, the fragrance of the fragrance component is overemphasized, which is not preferable.
The blending amount of alcohol is 2 to 8% by mass. This alcohol is not particularly limited as long as it can dissolve the fragrance component, and methanol or propanol can be used in addition to ethanol.
Needless to say, a necessary amount of an auxiliary agent such as a preservative, an antioxidant, and a coloring agent is added to the fragrance composition according to the needs such as the conditions of use and the purpose of use.
この発明の香料組成物は次のように調製される。
最初に香料成分とアルコールとを混和させ、これを精製水に加え、更に混和させる。なお、助剤はその特性に応じて、香料成分とともにアルコールに混和したり、精製水に混和したりする。かかる混和が完了した後、溶液をフィルター濾過して不溶成分を除去する。
The fragrance composition of the present invention is prepared as follows.
First, the perfume component and alcohol are mixed, and this is added to purified water and further mixed. The auxiliary agent may be miscible with alcohol or purified water together with the fragrance component, depending on its characteristics. After such mixing is complete, the solution is filtered to remove insoluble components.
このよう調製された香料組成物を次亜塩素酸水へ撹拌により混合する。香料組成物と次亜塩素酸水との配合比は１：５～１０００（質量比）、好ましくは１：５～２０（質量比）の範囲で使用目的や使用条件に応じて適宜選択されるが、次亜塩素酸の濃度（質量）が１０～１００ｐｐｍとなるようにする。
この発明の香料組成物を混合した次亜塩素酸水を、高周波利用などの周知な方法で、大気中へ噴霧することで環境の除菌消臭を行える。上記の配合比を維持して、次亜塩素酸水とこの香料組成物とを独立して噴霧してもよい。その場合、大気中に噴霧された全霧滴に含まれる次亜塩素酸の濃度（質量）を１０～１００ｐｐｍとする。
The fragrance composition thus prepared is mixed with hypochlorite water by stirring. The blending ratio of the fragrance composition and the hypochlorous acid water is appropriately selected in the range of 1: 5 to 1000 (mass ratio), preferably 1: 5 to 20 (mass ratio) according to the purpose of use and the conditions of use. However, the concentration (mass) of hypochlorous acid should be 10 to 100 ppm.
By spraying the hypochlorite water mixed with the fragrance composition of the present invention into the atmosphere by a well-known method such as the use of high frequency, the environment can be sterilized and deodorized. The hypochlorite water and the fragrance composition may be independently sprayed while maintaining the above compounding ratio. In that case, the concentration (mass) of hypochlorous acid contained in all the mist droplets sprayed into the atmosphere is 10 to 100 ppm.
次に、この発明の実施例について説明する。
表１にこの発明の実施例１～３及び比較例１～８の香料組成物を示す。各香料組成物を構成する香料成分、エタノール及び精製水の配合比（質量％）を固定して、香料成分（ユーカリ油、ペパーミント油及びメント―ル）の配合比（質量％）を変化させた。
Table 1 shows the fragrance compositions of Examples 1 to 3 and Comparative Examples 1 to 8 of the present invention. The compounding ratio (mass%) of the perfume components (eucalyptus oil, peppermint oil and menthol) constituting each perfume composition was fixed by fixing the compounding ratio (mass%) of the perfume components, ethanol and purified water. ..
次亜塩素酸の濃度測定はＡＤＶＡＮＴＥＣ社製のクロール試験紙を用いて行った。
官能試験は除菌消臭液を大気中に噴霧して、そのときの香りの良し悪しを、複数のオペレータが主観的に判断した。◎は複数のオペレータが全て良い香り付けと判定した場合を示す。○は少なくとも１名のオペレータが良い香り付けと判定した場合を示す。×は全てのオペレータが香り付けに満足しなかった場合を示す。
表１の結果より、ユーカリ油、ペパーミント油及びメントールの配合はユーカリ油：７０～９０質量％、ペパーミント油：２５～５質量％、メントール：残部とすることが好ましいことがわかる。
The concentration of hypochlorous acid was measured using a chlor test paper manufactured by ADVANTEC.
In the sensory test, the disinfectant deodorant was sprayed into the air, and a plurality of operators subjectively judged whether the scent was good or bad at that time. ⊚ indicates a case where a plurality of operators all judge that the fragrance is good. ◯ indicates the case where at least one operator determines that the scent is good. X indicates a case where all operators were not satisfied with the scenting.
From the results in Table 1, it can be seen that the composition of eucalyptus oil, peppermint oil and menthol is preferably eucalyptus oil: 70 to 90% by mass, peppermint oil: 25 to 5% by mass, and menthol: the balance.
ユーカリ油には約８０質量％のシネオールが含まれ、ペパーミント油には約５０質量％メントールが含まれている。従って、香料成分として、シネオールとメントールとを採用することが好ましいことがわかる。また、それらの配合比は香料成分の全質量を１００質量％としたとき、５６～８０質量％のシネオール、７．５～２０質量％のメントールを含ませることが好ましい。 Eucalyptus oil contains about 80% by weight cineole and peppermint oil contains about 50% by weight menthol. Therefore, it can be seen that it is preferable to use cineole and menthol as the fragrance component. Further, it is preferable to include 56 to 80% by mass of cineole and 7.5 to 20% by mass of menthol when the total mass of the fragrance component is 100% by mass.
香料成分の配合比を実施例１に示したものに固定して、香料組成物における香料成分の配合比を変化させたときの結果を表２に示す。
表２の結果から、香料組成物における香料成分の配合比は０．１～１．０質量％とすることが好ましことがわかる。
From the results in Table 2, it can be seen that it is preferable that the blending ratio of the fragrance components in the fragrance composition is 0.1 to 1.0% by mass.
この発明は、上記発明の実施の形態及び実施例の説明に何ら限定されるものではない。特許請求の範囲の記載を逸脱せず、当業者が容易に想到できる範囲で種々の変形態様もこの発明に含まれる。
例えば、この発明の香料組成物は、漂白剤その他の次亜塩素酸を含む薬剤の塩素臭をマスキングする際にも利用可能である。
以下に、本発明の実施形態を列挙する。
１．
次亜塩素酸と組み合わせて使用するための香料組成物であって、
前記香料組成物は、
アルコール：２～８質量％、
香料成分：０．１～１．０質量％、
水及び必要に応じて配合される助剤：残部、とを含み、
前記香料成分はシネオールとメントールと含み、該香料成分の全質量を１００質量％としたとき、前記シネオールは５６～８０質量％、前記メントールは７．５～２０質量％である香料組成物。
２．
次亜塩素酸と組み合わせて使用するための香料組成物であって、
前記香料組成物は、
アルコール：２～８質量％、
香料成分：０．１～１．０質量％、
水及び必要に応じて配合される助剤：残部、とを含み、
前記香料成分はその全質量を１００質量％としたとき、
ユーカリ油：７０～９０質量％、
ペパーミント油：２５～５質量％、
メントール：５～２５質量％
である香料組成物。
３．
前記香料成分はその全質量１００質量％としたとき、
ユーカリ油：７５～８５質量％、
ペパーミント油：２０～７質量％、
メントール：５～１８質量％
である前記２に記載の香料組成物。
４．
前記１～３の何れかに記載の香料組成物と次亜塩素酸とを含む除菌消臭液であって、前記次亜塩素酸の濃度が１０～１００ｐｐｍ（質量）である、除菌消臭液。
５．
前記４に記載の除菌消臭液を大気中に噴霧する、除菌消臭方法。
６．
次亜塩素酸水を大気中に噴霧するステップと、
前記１～３の何れかに記載の香料組成物を大気中に噴霧するステップと、を含み、
前記両ステップで噴霧された霧滴に含まれる次亜塩素酸の濃度が１０～１００ｐｐｍ（質量）である、除菌消臭方法。
７．
次亜塩素酸の塩素臭を抑制またはマスキングするための前記１～３の何れかに記載の香料組成物の使用。
The present invention is not limited to the description of the embodiments and examples of the above invention. Various modifications are also included in the present invention to the extent that those skilled in the art can easily conceive without departing from the description of the scope of claims.
For example, the perfume composition of the present invention can also be used to mask the chlorine odor of bleaching agents and other agents containing hypochlorous acid.
The embodiments of the present invention are listed below.
1. 1.
A fragrance composition for use in combination with hypochlorous acid.
The fragrance composition is
Alcohol: 2-8% by mass,
Fragrance component: 0.1-1.0% by mass,
Including water and auxiliaries to be added as needed: the balance, and
A fragrance composition containing cineole and menthol, and when the total mass of the fragrance component is 100% by mass, the cineole is 56 to 80% by mass and the menthol is 7.5 to 20% by mass.
2. 2.
A fragrance composition for use in combination with hypochlorous acid.
The fragrance composition is
Alcohol: 2-8% by mass,
Fragrance component: 0.1-1.0% by mass,
Including water and auxiliaries to be added as needed: the balance, and
When the total mass of the fragrance component is 100% by mass,
Eucalyptus oil: 70-90% by mass,
Peppermint oil: 25-5% by mass,
Menthol: 5-25% by mass
A fragrance composition that is.
3. 3.
When the total mass of the fragrance component is 100% by mass,
Eucalyptus oil: 75-85% by mass,
Peppermint oil: 20-7% by mass,
Menthol: 5-18% by mass
The fragrance composition according to 2 above.
4.
A sterilizing deodorant containing the fragrance composition according to any one of 1 to 3 and hypochlorous acid, wherein the concentration of the hypochlorous acid is 10 to 100 ppm (mass). Air freshener.
5.
A sterilizing and deodorizing method for spraying the sterilizing and deodorizing liquid according to 4 into the atmosphere.
6.
The step of spraying hypochlorite water into the atmosphere,
The step comprising spraying the fragrance composition according to any one of 1 to 3 into the atmosphere.
A sterilizing and deodorizing method in which the concentration of hypochlorous acid contained in the mist droplets sprayed in both steps is 10 to 100 ppm (mass).
7.
Use of the fragrance composition according to any one of 1 to 3 above for suppressing or masking the chlorine odor of hypochlorous acid.
Claims (7)
前記香料組成物は、
アルコール：２～８質量％、
香料成分：０．１～１．０質量％、
水及び必要に応じて配合される助剤：残部、とを含み、
前記香料成分はシネオールとメントールと含み、該香料成分の全質量を１００質量％としたとき、前記シネオールは５６～８０質量％、前記メントールは７．５～２０質量％である香料組成物。 A fragrance composition for use in combination with hypochlorous acid .
The fragrance composition is
Alcohol: 2-8% by mass,
Fragrance component: 0.1-1.0% by mass,
Including water and auxiliaries to be added as needed: the balance, and
A fragrance composition containing cineole and menthol, and when the total mass of the fragrance component is 100% by mass, the cineole is 56 to 80% by mass and the menthol is 7.5 to 20% by mass.
前記香料組成物は、
アルコール：２～８質量％、
香料成分：０．１～１．０質量％、
水及び必要に応じて配合される助剤：残部、とを含み、
前記香料成分はその全質量を１００質量％としたとき、
ユーカリ油：７０～９０質量％、
ペパーミント油：２５～５質量％、
メントール：５～２５質量％
である香料組成物。 A fragrance composition for use in combination with hypochlorous acid .
The fragrance composition is
Alcohol: 2-8% by mass,
Fragrance component: 0.1-1.0% by mass,
Including water and auxiliaries to be added as needed: the balance, and
When the total mass of the fragrance component is 100% by mass,
Eucalyptus oil: 70-90% by mass,
Peppermint oil: 25-5% by mass,
Menthol: 5-25 % by mass
A fragrance composition that is.
ユーカリ油：７５～８５質量％、
ペパーミント油：２０～７質量％、
メントール：５～１８質量％
である請求項２に記載の香料組成物。 When the total mass of the fragrance component is 100% by mass,
Eucalyptus oil: 75-85% by mass,
Peppermint oil: 20-7% by mass,
Menthol: 5-18 % by mass
The fragrance composition according to claim 2.
請求項１～３の何れかに記載の香料組成物を大気中に噴霧するステップと、を含み、
前記両ステップで噴霧された霧滴に含まれる次亜塩素酸の濃度が１０～１００ｐｐｍ（質量）である、除菌消臭方法。 The step of spraying hypochlorite water into the atmosphere,
A step of spraying the fragrance composition according to any one of claims 1 to 3 into the atmosphere.
A sterilizing and deodorizing method in which the concentration of hypochlorous acid contained in the mist droplets sprayed in both steps is 10 to 100 ppm (mass).
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2017057026A JP7016468B2 (en) | 2017-03-23 | 2017-03-23 | A fragrance composition, a sterilizing deodorant liquid using the fragrance composition, and a sterilizing deodorizing method. |
| PCT/JP2018/011323 WO2018174136A1 (en) | 2017-03-23 | 2018-03-22 | Fragrance composition, and disinfecting and deodorizing solution and disinfecting and deodorizing method each utilizing same |
| JP2022000294A JP2022048167A (en) | 2017-03-23 | 2022-01-04 | Method of producing fragrance composition and method of producing disinfectant/deodorant liquid |
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| JP2017057026A JP7016468B2 (en) | 2017-03-23 | 2017-03-23 | A fragrance composition, a sterilizing deodorant liquid using the fragrance composition, and a sterilizing deodorizing method. |
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| JP2022000294A Division JP2022048167A (en) | 2017-03-23 | 2022-01-04 | Method of producing fragrance composition and method of producing disinfectant/deodorant liquid |
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| JP2022000294A Pending JP2022048167A (en) | 2017-03-23 | 2022-01-04 | Method of producing fragrance composition and method of producing disinfectant/deodorant liquid |
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| WO (1) | WO2018174136A1 (en) |
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| KR102411534B1 (en) * | 2021-08-06 | 2022-06-22 | 장민석 | Disinfectant Composition Comprising an perfume material and Disinfectant comprising the same |
| WO2023190598A1 (en) * | 2022-03-31 | 2023-10-05 | アース製薬株式会社 | Composition |
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| JP2003040766A (en) | 2001-07-26 | 2003-02-13 | Kao Corp | Tool for cleaning nasal cavity |
| JP2004224918A (en) | 2003-01-23 | 2004-08-12 | Zebra Pen Corp | Water-based ink for ballpoint pen, having viscosity reduced by shear |
| JP2005272399A (en) | 2004-03-25 | 2005-10-06 | Kao Corp | Hair cosmetic |
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| JP2015530124A (en) | 2012-10-08 | 2015-10-15 | インターコンチネンタル グレート ブランズ エルエルシー | Hard confectionery and its manufacturing method |
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|---|---|---|---|---|
| JPH0725735A (en) * | 1993-07-08 | 1995-01-27 | Kowa Co | Gargling agent |
| CA2192818C (en) * | 1994-07-25 | 2011-04-05 | D. Scott Harper | Antiseptic dentifrice comprising essential oils |
| JP2003246744A (en) * | 2002-02-25 | 2003-09-02 | Nippon Tenganyaku Kenkyusho:Kk | Nandina fruit component-containing solution |
| JP2007297719A (en) * | 2006-04-27 | 2007-11-15 | Lion Corp | Liquid finishing agent composition for fiber product |
| JP4971713B2 (en) * | 2006-07-28 | 2012-07-11 | 株式会社ダイゾー | Aerosol composition and aerosol product comprising the aerosol composition |
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- 2018-03-22 WO PCT/JP2018/011323 patent/WO2018174136A1/en active Application Filing
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2003040766A (en) | 2001-07-26 | 2003-02-13 | Kao Corp | Tool for cleaning nasal cavity |
| JP2004224918A (en) | 2003-01-23 | 2004-08-12 | Zebra Pen Corp | Water-based ink for ballpoint pen, having viscosity reduced by shear |
| JP2006518339A (en) | 2003-02-21 | 2006-08-10 | パー・ウォーター・ピュリフィケイション・プロダクツ・インコーポレイテッド | Water treatment composition having masking agent |
| JP2005272399A (en) | 2004-03-25 | 2005-10-06 | Kao Corp | Hair cosmetic |
| JP2015530124A (en) | 2012-10-08 | 2015-10-15 | インターコンチネンタル グレート ブランズ エルエルシー | Hard confectionery and its manufacturing method |
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| JP2022048167A (en) | 2022-03-25 |
| JP2018158998A (en) | 2018-10-11 |
| WO2018174136A1 (en) | 2018-09-27 |
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