JP7008928B1 - Substrate cleaning vacuum drying equipment - Google Patents

Substrate cleaning vacuum drying equipment Download PDF

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JP7008928B1
JP7008928B1 JP2021093145A JP2021093145A JP7008928B1 JP 7008928 B1 JP7008928 B1 JP 7008928B1 JP 2021093145 A JP2021093145 A JP 2021093145A JP 2021093145 A JP2021093145 A JP 2021093145A JP 7008928 B1 JP7008928 B1 JP 7008928B1
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substrate
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vacuum drying
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義治 山本
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ヤマトテクノス有限会社
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Abstract

【課題】本発明は1つの処理室2内で基板11を洗浄及び真空乾燥が出来る装置で清浄さを保ちながら洗浄し洗浄時間の短縮と洗浄液の残留のないクリーンな真空乾燥で乾燥時間の短縮ができ汚染もなく効率よく出来る基板洗浄真空乾燥装置を得ることにある。【解決手段】処理室2内の基板11に気体ノズル28から窒素ガス等を充円錐形噴射すると清浄さを保ち洗浄工程の時間は短縮する。また処理室カバー4の内側48の形状を円錐と、ベース中央54を中高にして傾斜させ飛び散った洗浄液は傾斜で排液溝53に流し排液溝53も傾斜で排液口15に流すのと、基板11から気体を流れやすくした真空排気口23は基板11より高い位置で処理室カバー4の内側48に真空排気口23を設けると乾燥時間を短縮するのとで、一つの処理室2内で効率よく汚染もなく洗浄と真空乾燥の時間を短縮する事ができる基板洗浄真空乾燥装置を構成している。【選択図】 図1PROBLEM TO BE SOLVED: To shorten the cleaning time by cleaning the substrate 11 in one processing chamber 2 while maintaining the cleanliness with a device capable of cleaning and vacuum drying, and to shorten the drying time by clean vacuum drying without residual cleaning liquid. The purpose is to obtain a substrate cleaning vacuum drying device that can be used efficiently without contamination. SOLUTION: When a substrate 11 in a processing chamber 2 is filled with nitrogen gas or the like from a gas nozzle 28 in a conical shape, cleanliness is maintained and the time of the cleaning step is shortened. Further, the shape of the inner 48 of the processing chamber cover 4 is a cone, and the cleaning liquid that is inclined by tilting the center 54 of the base to a medium height is inclined and flows into the drainage groove 53, and the drainage groove 53 is also inclined and flows into the drainage port 15. The vacuum exhaust port 23, which facilitates the flow of gas from the substrate 11, is located higher than the substrate 11, and if the vacuum exhaust port 23 is provided inside 48 of the processing chamber cover 4, the drying time is shortened. It constitutes a substrate cleaning vacuum drying device that can efficiently shorten the cleaning and vacuum drying time without contamination. [Selection diagram] Fig. 1

Description

本発明は、半導体の基板等の精密基板の洗浄及び乾燥の基板洗浄真空乾燥装置に関する。 The present invention relates to a substrate cleaning vacuum drying apparatus for cleaning and drying precision substrates such as semiconductor substrates.

従来は、特許文献1に記載のように半導体基板を一枚ずつ回転洗浄して真空乾燥する装置として図1(以下、従来例における説明の図番と符号は特許文献1の記載内容である。)の洗浄装置1と図4に示す洗浄装置1がある。これらの洗浄装置1の図1と図4はどちらも容器によって囲まれた一つの処理室内において、洗浄処理及び乾燥処理がなされる。その装置は容器の上部に切換弁を介して洗浄液より発生する蒸気又はN2雰囲気に置換の為に排出する容器の上部に排気口を設けている。そして外気を遮断して密閉された容器の中の処理室部の下でカバーより内側にN2の供給口を設けた処理室内にN2を導入するのに切換弁を開きN2雰囲気に置換した後にテーブルに支持されている半導体基板を回転させて高周波液体噴射器で洗浄する。その後半導体基板を移動する事無くカバーを下降させてカバーの下端に気密可能なシールでテーブル及び半導体基板を閉じこめて密閉された空間にしてから処理室の下部に供給口を設けて切換弁を介して真空ポンプで減圧して半導体基板を真空乾燥処理するように構成されていた。 Conventionally, as a device for rotating and cleaning semiconductor substrates one by one and vacuum-drying them as described in Patent Document 1, FIG. 1 (hereinafter, reference numerals and reference numerals in the description in the conventional example are the contents described in Patent Document 1. ) And the cleaning device 1 shown in FIG. Both FIGS. 1 and 4 of these cleaning devices 1 perform cleaning treatment and drying treatment in one processing chamber surrounded by a container. The device is provided with an exhaust port on the upper part of the container, which discharges the steam generated from the cleaning liquid or the N2 atmosphere for replacement through the switching valve on the upper part of the container. Then, the switching valve is opened to introduce N2 into the processing chamber provided with the N2 supply port inside the cover under the processing chamber in the sealed container by shutting off the outside air, and then the table is replaced with the N2 atmosphere. The semiconductor substrate supported by the is rotated and cleaned with a high-frequency liquid injector. After that, the cover is lowered without moving the semiconductor substrate, and the table and the semiconductor substrate are closed with an airtight seal at the lower end of the cover to create a sealed space, and then a supply port is provided at the bottom of the processing chamber via a switching valve. The semiconductor substrate was vacuum-dried by reducing the pressure with a vacuum pump.

しかしながら、従来の特許文献1の洗浄及び真空乾燥に関しては図1と図4に示す洗浄装置1では、どちらも容器内は外気を遮断して密閉された室内で洗浄処理及乾燥処理する。そして終了後はテーブルに装着された半導体基板を出し入れする開閉トビラから待機している搬送ロボットで半導体基板を搬出して、次に洗浄する半導体基板を搬入する。そして外気が容器内に入り込むので、開閉トビラを閉じて切換弁を介してN2の導入を続けながら容器内の気体を切換弁から排出しN2雰囲気に置換した後に半導体基板の洗浄を行うので、洗浄前にN2を導入してN2雰囲気に置換する時間が要するので洗浄待ち時間を必要とし洗浄工程の時間が長く成るという問題がある。さらに真空乾燥時に洗浄液体が平面の床面及び排水溝に残留があり乾燥する時間が長く成るという問題もある。また真空排気口が床面にあり半導体基板より下に有り半導体基板のパターン溝の中は間接的な吸引になり効率が悪く乾燥時間が長くなる。一部のメモリでは微細化により高アスペクト比(パターン深さ/パターン幅)では、たとえばフラッシュメモリ(不揮発性メモリ)はアスペクト比が十倍を越えてパターン溝の深さは、他のメモリより深くなりパターン倒れを起こさず効率よく吸引が難度に成る。その乾燥においてはリンス液としてIPA(イソプロピルアルコール)を使用してのスピン乾燥(回転乾燥)が主流である。また、容器内のカバーはエアーシリンダー及び動作機構によりテーブルと垂直方向に昇降されているのでカバーを上下するエアーシリンダーの可動部及び動作機構部の摺動摩擦で金属等が容器内に発生した汚染やパーテイクルが処理室内に侵入し半導体基板に付着する等という問題がある。 However, regarding the conventional cleaning and vacuum drying of Patent Document 1, in both the cleaning apparatus 1 shown in FIGS. 1 and 4, the inside of the container is shut off from the outside air and the cleaning treatment and the drying treatment are performed in a closed room. Then, after the completion, the semiconductor substrate is carried out by the transfer robot waiting from the opening / closing door for taking in and out the semiconductor board mounted on the table, and then the semiconductor board to be cleaned is carried in. Then, since the outside air enters the container, the semiconductor substrate is washed after the gas in the container is discharged from the switching valve and replaced with the N2 atmosphere while the opening / closing door is closed and N2 is continuously introduced through the switching valve. Since it takes time to introduce N2 before and replace it with the N2 atmosphere, there is a problem that a waiting time for washing is required and the time of the washing step becomes long. Further, there is a problem that the cleaning liquid remains on the flat floor surface and the drainage groove during vacuum drying, and the drying time becomes long. Further, the vacuum exhaust port is on the floor surface and below the semiconductor substrate, and the inside of the pattern groove of the semiconductor substrate is indirect suction, which is inefficient and prolongs the drying time. With high aspect ratio (pattern depth / pattern width) due to miniaturization in some memories, for example, flash memory (nonvolatile memory) has an aspect ratio of more than 10 times and the depth of the pattern groove is deeper than other memories. It becomes difficult to suck efficiently without causing the pattern to collapse. In the drying, spin drying (rotational drying) using IPA (isopropyl alcohol) as a rinsing liquid is the mainstream. In addition, since the cover inside the container is moved up and down in the direction perpendicular to the table by the air cylinder and the operating mechanism, metal etc. may be contaminated inside the container due to the sliding friction of the moving part and the operating mechanism part of the air cylinder that moves up and down the cover. There is a problem that the particle invades the processing chamber and adheres to the semiconductor substrate.

特許第4902091号公報Japanese Patent No. 4902091

本発明は、以上のような従来の欠点に鑑み、従来は中央部が周縁部より窪んだ平面の上にシールするフランジ(Oリング付)を介して取り付けられた金属製の回転軸は処理室内部に露出するテーブルとその動作部品等とフランジ(Oリング付)を締め付けるボルトは薬液対応樹脂で製作する。そこで処理室内部の上からテーブルの下面の中心にフランジ(Oリング付)の付いた回転軸4が固着している。そしてフランジ(Oリング付)により洗浄液漏れや真空漏れを防止出来るが、回転軸4はフランジ(Oリング付)を介して固定する締め付けボルトは薬液を含む洗浄液に侵されない樹脂製のボルトで締め付ける。その回転軸は駆動モータが取り付けているので振動も有り樹脂製ボルトでは緩みも発生する恐れも有り強度的に不十分である。それ故、処理室ベースの下に回転部本体に取り付けたフランジAを金属製の取付ボルトで処理室ベースの下部に設置すると強度の補強をして緩みが発生する事がない。 In view of the above-mentioned conventional drawbacks, in the present invention, the metal rotating shaft conventionally attached via a flange (with an O-ring) whose central portion is sealed on a flat surface recessed from the peripheral portion is a processing chamber. The table exposed inside, its moving parts, and the bolts that tighten the flange (with O-ring) are made of chemical-compatible resin. Therefore, a rotating shaft 4 with a flange (with an O-ring) is fixed to the center of the lower surface of the table from above the inside of the processing chamber. The flange (with O-ring) can prevent leakage of cleaning liquid and vacuum, but the rotating shaft 4 is fixed via the flange (with O-ring), and the tightening bolt is tightened with a resin bolt that is not affected by the cleaning liquid containing the chemical solution. Since the drive motor is attached to the rotating shaft, there is vibration, and resin bolts may loosen, which is insufficient in terms of strength. Therefore, if the flange A attached to the rotating portion main body is installed under the processing chamber base with a metal mounting bolt at the lower part of the processing chamber base, the strength is reinforced and loosening does not occur.

また、従来の半導体基板の洗浄は処理室で行なうが繋がっている容器も含んだ中でN2雰囲気の中で洗浄をする。そして乾燥は処理室内で行なう。その容器は容積大きいので洗浄する前にN2雰囲気に置換するのに時間がかかる問題が有る。それ故、処理室2は処理室ベース3に隔壁8を接合し隔壁蓋9は隔壁8に固定し隔壁蓋9との間に間隙を持って昇降する処理室カバー4で囲まれた中の処理室2内を窒素ガスに置換してから洗浄するのは容積が小さく成っているので洗浄前の窒素ガスに置換される待ち時間は短縮されるが。それ故、基板11の全面に当たるように窒素ガスを基板11に包括的噴射を行いながら洗浄する事により洗浄前の待ち時間を無くする事が出来る基板洗浄真空乾燥装置を提供する事を目的としている。 Further, although the conventional semiconductor substrate is washed in the processing chamber, it is washed in an N2 atmosphere including the connected container. And drying is done in the processing room. Since the container has a large volume , there is a problem that it takes time to replace it with an N2 atmosphere before cleaning. Therefore, in the processing chamber 2, the partition wall 8 is joined to the processing chamber base 3, the partition wall lid 9 is fixed to the partition wall 8, and the processing chamber is surrounded by the processing chamber cover 4 which moves up and down with a gap between the processing chamber lid 9 and the partition wall lid 9. Cleaning after replacing the inside of the chamber 2 with nitrogen gas has a small volume, so the waiting time for replacement with nitrogen gas before cleaning is shortened. Therefore, it is an object of the present invention to provide a substrate cleaning vacuum drying apparatus capable of eliminating the waiting time before cleaning by cleaning the substrate 11 while comprehensively injecting nitrogen gas onto the substrate 11 so as to hit the entire surface of the substrate 11. ..

また、従来の半導体基板を出し入れ口は容器に開閉トビラは基板用の密閉可能で高額な角型真空ゲートバルブを設置している。それ故、基板11が通過する基板出入口41を設けて開閉トビラ42とそれを上下するトビラ上下シリンダー43で処理室2内の窒素ガスの圧力で開閉トビラ42の隙間から漏れる簡単な構造の基板洗浄真空乾燥装置を提供する事を目的としている。 In addition, a conventional semiconductor substrate is opened and closed in a container at the entrance and exit, and a sealable and expensive square vacuum gate valve for the substrate is installed in the door. Therefore, a substrate entrance / exit 41 through which the substrate 11 passes is provided, and the opening / closing door 42 and the upper / lower cylinder 43 of the door that moves it up and down are used to clean the substrate with a simple structure that leaks from the gap between the opening / closing door 42 due to the pressure of nitrogen gas in the processing chamber 2. It is intended to provide a vacuum drying device.

また、従来の真空乾燥は容器の中で処理室のカバーを下降させて洗浄した場所で半導体基板を真空乾燥する。それ故、真空乾燥は洗浄した場所で処理室カバー4と隔壁8と隔壁蓋9で囲まれた処理室2で処理室カバー4を下降させて処理室ベース3側に装着した処理室ベース用Oリング18が蜜着して出来た真空室50内で基板11を真空乾燥する。その処理室2の1室で囲まれた容積も小さくして洗浄も真空乾燥もする事が出来る基板洗浄真空乾燥装置を提供する事を目的としている。 Further, in the conventional vacuum drying, the semiconductor substrate is vacuum dried in a place where the cover of the processing chamber is lowered and cleaned in the container. Therefore, in vacuum drying, the processing chamber cover 4 is lowered in the processing chamber 2 surrounded by the processing chamber cover 4, the partition wall 8 and the partition wall lid 9 at the washed place, and the processing chamber base 3 side is mounted on the processing chamber base O. The substrate 11 is vacuum-dried in the vacuum chamber 50 formed by the ring 18 being squeezed. It is an object of the present invention to provide a substrate cleaning vacuum drying apparatus capable of performing cleaning and vacuum drying by reducing the volume surrounded by one of the processing chambers 2.

更に、従来の容器内の処理室部の床面は平坦である為に洗浄液はすむうすに排水溝に流れないのと排水溝に一旦集めて切換弁を開いて洗浄液を排出するので待機するのと、洗浄液が残留のまま真空乾燥するのも乾燥工程の時間が長くなる。それ故、処理室2内の処理室ベース3のベース中央54を中高にして真空室50の容積を小さくするのと、その中高の傾斜で飛び散った洗浄液は素早く排液溝53に流し排液口15に排出させ洗浄液の残留がなく成る様にすると基板11の乾燥工程の時間を短縮する事ができる基板洗浄真空乾燥装置を提供する事を目的としている。 Furthermore, since the floor surface of the treatment chamber inside the conventional container is flat, the cleaning liquid does not easily flow into the drainage ditch, and once it is collected in the drainage ditch, the switching valve is opened and the cleaning liquid is discharged, so it stands by. In addition, vacuum drying with the cleaning liquid remaining also increases the time required for the drying process. Therefore, the volume of the vacuum chamber 50 is reduced by setting the center 54 of the base 3 of the processing chamber base 3 in the processing chamber 2 to a medium height, and the cleaning liquid scattered due to the inclination of the medium height is quickly drained to the drainage groove 53 and the drainage port. It is an object of the present invention to provide a substrate cleaning vacuum drying apparatus capable of shortening the time of the drying step of the substrate 11 by discharging the substrate 11 to eliminate the residual cleaning liquid.

更に、従来は真空乾燥する半導体基板の一般的なメモリのパターンはアスペクト比(パターン深さ/パターン幅)が三から四倍であつたが近年のフラッシユメモリ(不揮発性メモリ)では微細化により高アスペクト比(パターン深さ/パターン幅)は十倍を越えさらに進化し溝はさらに深くなる。そこで、パターンの倒れにくい乾燥するには乾燥部の機能の向上と、そのパターンに合わせた表面張力のリンス液体を活用する。そこで従来の真空排気口は半導体基板より低い位置であるのと床面にあり気体は側面にぶつかり屈折して流れて抵抗が発生して排気効率が悪いと言う問題がある。それ故、リンス液体は蒸気及び気体にして初期段階から効率よく吸引するには基板11より高い位置で直接的に真空排気口23に流れるように設ける基板洗浄真空乾燥装置を提供する事を目的としている。 Furthermore, in the past, the aspect ratio (pattern depth / pattern width) of a general memory pattern of a semiconductor substrate that was vacuum-dried was three to four times, but in recent years flash memory (nonvolatile memory) has become finer. The high aspect ratio (pattern depth / pattern width) exceeds 10 times and further evolves, and the groove becomes deeper. Therefore, in order to dry the pattern so that it does not fall over, the function of the dried part is improved and a rinse liquid with a surface tension that matches the pattern is used. Therefore, there is a problem that the conventional vacuum exhaust port is located at a lower position than the semiconductor substrate and is located on the floor surface, and the gas collides with the side surface and is refracted to flow to generate resistance, resulting in poor exhaust efficiency. Therefore, in order to convert the rinse liquid into steam and gas and efficiently suck it from the initial stage, it is an object of the present invention to provide a substrate cleaning vacuum drying device provided so as to flow directly to the vacuum exhaust port 23 at a position higher than the substrate 11. There is.

上記目的を達成するために、この発明の基板洗浄真空乾燥装置の請求項1の発明では、
処理室2の外部で処理室ベース3の下側からフッ素樹脂又は塩化ビニール樹脂、等の薬液対応用樹脂のフランジA51を介して金属製の回転部本体10取り付けてそのフランジA51から処理室ベース3の下側に金属製の取付ボルト52を装着してその取付ボルト52の強度の補強と腐食対策をするのと、処理室2内の処理室ベース3に隔壁8を接合し隔壁蓋9は隔壁8に固定し隔壁蓋9との間に間隙を持って移動する処理室カバー4で囲まれた処理室2の中で、処理室カバー4の凹状の内側48より窒素ガスを基板11の全面に当たるように気体ノズル28から噴射するのと、隔壁8に基板出入口41を設けてトビラ上下シリンダー43で開閉トビラ42を開閉するのと、回転部本体10に取り付けた駆動モータ20で回転しうる基板掴み軸14に掴まれた基板11を揺動運動する旋回軸38に取り付けたノズル37で回転洗浄した後に処理室カバー4が下降して処理室ベース3側に装着した処理室ベース用Oリング18に密閉された真空室50で真空切換弁24を介して真空ポンプ26で真空室50を減圧する手段をも処理室2内に設けることを特徴とする。
In order to achieve the above object, the invention of claim 1 of the substrate cleaning vacuum drying apparatus of the present invention
Outside the processing chamber 2, a metal rotating part main body 10 is attached from the lower side of the processing chamber base 3 via a flange A51 of a resin for chemicals such as fluororesin or vinyl chloride resin, and the processing chamber base 3 is attached from the flange A51. A metal mounting bolt 52 is attached to the lower side to reinforce the strength of the mounting bolt 52 and prevent corrosion, and the partition 8 is joined to the processing chamber base 3 in the processing chamber 2 so that the partition lid 9 is a partition. In the processing chamber 2 surrounded by the processing chamber cover 4 fixed to 8 and moving with a gap between the partition wall lid 9, nitrogen gas hits the entire surface of the substrate 11 from the concave inner side 48 of the processing chamber cover 4. As described above, the gas nozzle 28 is used to inject the gas, the partition 8 is provided with the substrate inlet / outlet 41, and the opening / closing tobira 42 is opened / closed by the upper and lower cylinders 43 of the tobira. The processing chamber cover 4 is lowered to the O-ring 18 for the processing chamber base mounted on the processing chamber base 3 side after the substrate 11 gripped by the shaft 14 is rotationally cleaned by the nozzle 37 attached to the swirling shaft 38 that swings. A means for depressurizing the vacuum chamber 50 by the vacuum pump 26 via the vacuum switching valve 24 in the closed vacuum chamber 50 is also provided in the processing chamber 2.

更に、この発明の基板洗浄真空乾燥装置の請求項2の発明では、処理室2の樹脂で出来た処理室カバー4の内側48の形状を円錐又は円球にして、中心から内周に向かって下げると内側48の内周部の肉厚が厚くして真空圧で中央部の凹みを抑え、かつ容積が小さくするのと、処理室2内の処理室ベース3のベース中央54を中高にして真空室50の容積をさらに小さくするのと、ベース中央54の中高の傾斜で飛び散った洗浄液は素早く排液溝53に流れ排液口15に速やかに排出し洗浄液の残留がなく成るのとで基板11を乾燥する手段を設ける事を特徴とする Further, in the invention of claim 2 of the substrate cleaning vacuum drying apparatus of the present invention, the shape of the inner 48 of the processing chamber cover 4 made of the resin of the processing chamber 2 is made into a cone or a sphere, and the shape is made into a cone or a sphere from the center to the inner circumference. When lowered, the wall thickness of the inner peripheral portion of the inner 48 is increased to suppress the dent in the central portion by vacuum pressure, and the volume is reduced. The volume of the vacuum chamber 50 is further reduced, and the cleaning liquid scattered at the middle and high inclinations of the base center 54 quickly flows into the drainage groove 53 and is quickly discharged to the drainage port 15, so that the cleaning liquid does not remain on the substrate. It is characterized by providing a means for drying the eleven.

更に、この発明の基板洗浄真空乾燥装置の請求項3の発明では、真空室50内を真空乾燥するには基板11のパターン溝の深い中の液体は蒸気から気化するので初期段階から効率よく真空排気口23に吸引するには基板11より上部の方に蒸気及び気体の流れにするのと、その真空排気口23は基板11より高い位置で処理室カバー4の内側48に真空排気口23を設ける事を特徴とする。 Further, in the invention of claim 3 of the substrate cleaning vacuum drying apparatus of the present invention, in order to vacuum dry the inside of the vacuum chamber 50, the liquid in the deep pattern groove of the substrate 11 is vaporized from the steam, so that the vacuum is efficiently vacuumed from the initial stage. In order to suck into the exhaust port 23, the flow of steam and gas is made to flow toward the upper part of the substrate 11, and the vacuum exhaust port 23 is located higher than the substrate 11 and the vacuum exhaust port 23 is provided inside 48 of the processing chamber cover 4. It is characterized by being provided.

以上の説明から明らかなように、本発明にあっては次に列拳する効果得られる。
請求項1の発明では、図1、図2、図3の処理室2内で洗浄と真空乾燥を行う。その処理室ベース3の下側から薬液対応用樹脂のフランジA51を介して金属製の回転部本体10を取り付ける。そのフランジA51は処理室ベース3の下側に金属製の取付ボルト52により構成されているので、緩みと強度の補強と腐食の防止ができるように構成されている。
また、処理室カバー4の凹状の内側48の気体ノズル28から窒素ガスを充円錐形噴射すると基板11の全面に直接当たり基板11の上面は窒素ガスで包囲した状態の中での洗浄ノズル37が基板11の洗浄を行なうようになっているが基板11の上面の洗浄を行いながら途中から窒素ガスが容積の小さくなった処理室2が置換された中で洗浄を行うように構成されているので自然酸化膜の付着の予防ができる。さらに処理室2内を窒素ガスで置換されるのを待つことなく洗浄するように構成されているので洗浄工程の時間の短縮ができる。
また、隔壁8に基板出入口41を設けてエアスライドテイブル型のトビラ上下シリンダー43一個と樹脂板の開閉トビラ42が上下するガイド溝を隔壁8に設けて基板出入口41の開閉ができるように構成されているので安価でできる。
また、従来は蜜閉された容器に囲まれた処理室であつたが本方法では容積も小さくした処理室で洗浄も真空乾燥もできるように成っているので接置面積を小さくして、さらに真空乾燥はリンス液にIPA(イソプロピルアルコール)を使用せずに純水で乾燥が出来るように成っているので揮発性有機化合物(VOC)の排出の規制ができる。
As is clear from the above explanation, in the present invention, the effect of row fisting can be obtained next.
In the invention of claim 1, washing and vacuum drying are performed in the processing chamber 2 of FIGS. 1, 2, and 3. A metal rotating portion main body 10 is attached from the lower side of the processing chamber base 3 via a flange A51 of a resin for dealing with chemicals. Since the flange A51 is configured by a metal mounting bolt 52 on the lower side of the processing chamber base 3, it is configured to be able to reinforce looseness and strength and prevent corrosion.
Further, when nitrogen gas is injected in a conical shape from the concave inner 48 gas nozzle 28 of the processing chamber cover 4, the cleaning nozzle 37 directly hits the entire surface of the substrate 11 and the upper surface of the substrate 11 is surrounded by the nitrogen gas . Although the substrate 11 is cleaned, the upper surface of the substrate 11 is cleaned while the processing chamber 2 having a small volume of nitrogen gas is replaced from the middle of the cleaning. It is possible to prevent the adhesion of the natural oxide film. Further, since the inside of the processing chamber 2 is configured to be cleaned without waiting for being replaced with nitrogen gas , the time of the cleaning step can be shortened.
Further, the partition wall 8 is provided with a substrate inlet / outlet 41, and a guide groove for opening / closing the resin plate opening / closing cylinder 42 and one air slide table upper / lower cylinder 43 is provided in the partition wall 8 so that the substrate inlet / outlet 41 can be opened and closed. Because it is cheap, it can be done.
In addition, in the past, the treatment chamber was surrounded by a tightly closed container, but in this method, the treatment chamber has a smaller volume and can be washed and vacuum dried, so the placement area can be reduced and further. Vacuum drying is such that it can be dried with pure water without using IPA (isopropyl alcohol) as the rinsing liquid, so it is possible to regulate the emission of volatile organic compounds (VOC).

請求項2の発明では、図1,図3の処理室カバー4の内側48の形状を円錐にして、中心から内周に向かって下げると内側48の内周部の肉厚が厚くする事により真空圧による耐圧で中央部の凹みを抑えられて容積も小さくなり、かつ処理室ベース3のベース中央54を中高にしたので真空室50の容積は小さくなるのと、そのベース中央54の中高部に飛び散った洗浄液は排液溝53に向かって素早く流れ、その排液溝53は排液口15に向かって傾斜により速やかに排出できるので飛び散った洗浄液は残留がなくなるように構成されているのとで乾燥時間の短縮ができる。 In the invention of claim 2, the shape of the inner 48 of the processing chamber cover 4 of FIGS. The pressure resistance due to the vacuum pressure suppresses the dent in the central part and the volume becomes smaller, and the volume of the vacuum chamber 50 becomes smaller because the base center 54 of the processing chamber base 3 is made medium and high. The splattered cleaning liquid quickly flows toward the drainage groove 53, and the drainage groove 53 can be quickly discharged by tilting toward the drainage port 15, so that the splattered cleaning liquid is configured to have no residue. The drying time can be shortened.

請求項3の発明では、図1、図3の真空室50内の基板11を真空乾燥するには真空機能を活用して真空排気口23は基板11より高い位置にして障害物なしで流れ、その真空排気口23は処理室カバー4の内側48に配置した事により基板11のパターン溝の中を結露すること無く効率よく吸引するように構成されているので乾燥時間の短縮ができる。 In the invention of claim 3, in order to vacuum dry the substrate 11 in the vacuum chamber 50 of FIGS. 1 and 3, the vacuum exhaust port 23 is set higher than the substrate 11 and flows without obstacles by utilizing the vacuum function. Since the vacuum exhaust port 23 is arranged inside 48 of the processing chamber cover 4 so as to efficiently suck the inside of the pattern groove of the substrate 11 without dew condensation, the drying time can be shortened.

本発明の実施するための最良の第1の形態の基板洗浄真空乾燥装置の正面の断面図である。It is sectional drawing of the front of the substrate cleaning vacuum drying apparatus of the best 1st embodiment for carrying out this invention. 本発明の実施するための最良の第2の形態の基板洗浄真空乾燥装置の右側面の一部断面図である。It is a partial cross-sectional view of the right side surface of the substrate washing vacuum drying apparatus of the best 2nd embodiment for carrying out this invention. 本発明の実施するための最良の第4の形態の基板洗浄真空乾燥装置の真空室を形成した時の断面図である。It is sectional drawing at the time of forming the vacuum chamber of the substrate cleaning vacuum drying apparatus of the best 4th embodiment for carrying out this invention.

以下、本発明の実施の形態を図に基づいて説明する。 Hereinafter, embodiments of the present invention will be described with reference to the drawings.

(実施例1)
本発明の基板洗浄真空乾燥装置の実施例1では図1、図2、図3は真空室の断面図であって、その装置の処理室2内で洗浄と真空乾燥を行う。本装置は金属製の取り付けボルトで引張り強さが約500MPaで樹脂製ボルトの5倍の強さの取付ボルト52を回転部本体10に取り付けた樹脂製のフランジA51を処理室ベース3の下側で金属製の取付ボルト52で締め付ける事により緩まず正常な運転が行なえる。そのフランジA51は回転部用Oリング19により洗浄液漏れや真空漏れの防止が出来る。また回転部本体10のメンテナンスの時は処理室カバー4を上下するアーム5に取り付いたスライド軸6およびシリンダー39のロット56等を解体せずに回転部本体10を取り外す事が出来る。それはメンテナンス蓋47を外して基板掴み軸14の取り付け部品を外した後に処理室ベース3の下側の取付ボルト52を取り外すので処理室2内への汚染を抑えてメンテナンスも容易である。
(Example 1)
In Example 1 of the substrate cleaning vacuum drying apparatus of the present invention, FIGS. 1, 2, and 3 are cross-sectional views of a vacuum chamber, and cleaning and vacuum drying are performed in the processing chamber 2 of the apparatus. This device is a metal mounting bolt with a tensile strength of about 500 MPa and a mounting bolt 52 that is five times stronger than a resin bolt. By tightening with the metal mounting bolt 52, normal operation can be performed without loosening. The flange A51 can prevent cleaning liquid leakage and vacuum leakage by the rotating O-ring 19. Further, at the time of maintenance of the rotating portion main body 10, the rotating portion main body 10 can be removed without disassembling the slide shaft 6 attached to the arm 5 that raises and lowers the processing chamber cover 4, the lot 56 of the cylinder 39, and the like. Since the maintenance lid 47 is removed and the mounting parts of the board gripping shaft 14 are removed and then the mounting bolt 52 on the lower side of the processing chamber base 3 is removed, contamination inside the processing chamber 2 is suppressed and maintenance is easy.

また、処理室ベース3に隔壁8を接合し隔壁蓋9は隔壁8に固定し隔壁蓋9との間に間隙を持って移動する処理室カバー4で囲まれた中で処理室カバー4の凹状の内側48の中心部に装着した気体ノズル28から充円錐形噴射すると窒素ガスを基板11の全面に直接当たり基板11の上面は窒素ガスで包囲した状態の中で発泡性の洗浄薬液対応用の洗浄ノズル37(特許第5610360と特許第4368351号に説明されている)洗浄液は常温で超音波洗浄して基板11の状況に合わせて洗浄角度を自動で変えて洗浄を行なうので付着汚染物質及びパーテイクルの付着の除去洗浄が出来る。そして基板11を処理室2内に搬入は基板出入口41を設けてトビラ上下シリンダー43で隔壁8のガイド溝に沿って開閉トビラ42を開いた後に基板掴み軸14に基板11を挿入後に開閉トビラ42をトビラ上下シリンダー43で閉じた後に基板11に気体ノズル28から充円錐形噴射すると窒素ガスが基板11の全面に直接当たり基板11の上面は窒素ガスで包囲した状態と成り、その基板11を回転可能にした回転部本体10に設置された駆動モータ20で運転をして、次に旋回軸38を駆動モータ(図省略)で洗浄ノズル37を原点位置から待機位置に移動してからカップ用シリンダー13でカップ12を下から上に移動した後に洗浄ノズル37から洗浄液を噴射して待機位置から基板11の中心に向かって洗浄を行い、中心から折り返し待機位置まで洗浄する。次の洗浄が無ければ旋回軸38を駆動モータ(図省略)で洗浄ノズル37を原点位置に移動すると洗浄工程は完了する。 Further, the partition 8 is joined to the processing chamber base 3, and the partition lid 9 is fixed to the partition 8 and is surrounded by the processing chamber cover 4 which moves with a gap between the partition lid 9 and the partition lid 9. When a gas nozzle 28 mounted in the center of the inner 48 of the substrate is used to inject a filled cone, the nitrogen gas directly hits the entire surface of the substrate 11, and the upper surface of the substrate 11 is surrounded by the nitrogen gas . The cleaning nozzle 37 (described in Patent No. 5610360 and Patent No. 4368351) is ultrasonically cleaned at room temperature, and the cleaning angle is automatically changed according to the situation of the substrate 11 to perform cleaning. Can be cleaned by removing the adhesion of gas. Then, the substrate 11 is carried into the processing chamber 2 by providing a substrate inlet / outlet 41, opening the opening / closing door 42 along the guide groove of the partition wall 8 with the door upper / lower cylinder 43, inserting the substrate 11 into the board gripping shaft 14, and then opening / closing the door 42. When the gas nozzle 28 injects the gas into the substrate 11 in a conical shape after the gas is closed by the upper and lower cylinders 43 of the door, the nitrogen gas directly hits the entire surface of the substrate 11 and the upper surface of the substrate 11 is surrounded by the nitrogen gas , and the substrate 11 is rotated. The drive motor 20 installed in the enabled rotating part main body 10 is operated, and then the swivel shaft 38 is moved by the drive motor (not shown) to move the cleaning nozzle 37 from the origin position to the standby position, and then the cup cylinder. After moving the cup 12 from the bottom to the top in 13, the cleaning liquid is sprayed from the cleaning nozzle 37 to perform cleaning from the standby position toward the center of the substrate 11, and the cleaning is performed from the center to the folded standby position. If there is no next cleaning, the cleaning process is completed when the swivel shaft 38 is moved to the origin position by the drive motor (not shown).

その後に処理室カバー4が横移動して隔壁蓋9に接触して擦れた粉塵で処理室2内を汚染すること無く垂直に昇降するようにヘット側ネジ付シリンダー39とスライド軸6とアーム5に取り付けたL字のアーム5が中心に向かった先端位置に接続ロット49と繋がっている処理室カバー4を下降させると処理室ベース3側に処理室ベース用Oリング18を装着すると処理室ベース用Oリング18は下側に成るので浮く事も無くより蜜着して真空室50で真空乾燥の準備ができた。その真空室50内で基板11を真空乾燥するには基板11を無回転真空乾燥か回転真空乾燥を選択してから電磁弁B25を通電すると真空切換弁24が開くまでは気体ノズル28から窒素ガスを噴射する。その通電で真空切換弁24を開いて真空ポンプ26で減圧して基板11はIPA(イソプロピルアルコール)を使用しない真空乾燥でリンス液は純水で行なうので揮発性有機化合物(VOC)の排出規制を実施した真空乾燥する事が出来る。そしてパターンがさらに微細に成り高アスペクト比になればパターンに合わせた表面張力の低いリンス液を使用して洗浄を行う。 After that, the cylinder 39 with screws on the head side, the slide shaft 6, and the arm 5 are moved so that the processing chamber cover 4 moves laterally and moves up and down vertically without contaminating the inside of the processing chamber 2 with dust rubbed against the partition wall lid 9. When the processing chamber cover 4 connected to the connection lot 49 is lowered to the tip position where the L-shaped arm 5 attached to the center is directed toward the center, the processing chamber base O-ring 18 is attached to the processing chamber base 3 side. Since the O-ring 18 for use is on the lower side, it does not float and is more closely attached, and is ready for vacuum drying in the vacuum chamber 50. To vacuum dry the substrate 11 in the vacuum chamber 50, select non-rotational vacuum drying or rotary vacuum drying of the substrate 11 and then energize the solenoid valve B25. Nitrogen gas is emitted from the gas nozzle 28 until the vacuum switching valve 24 opens. Is sprayed. The vacuum switching valve 24 is opened by the energization, the pressure is reduced by the vacuum pump 26, the substrate 11 is vacuum dried without using IPA (isopropyl alcohol), and the rinse liquid is pure water. The vacuum drying performed can be performed. Then, when the pattern becomes finer and has a high aspect ratio, cleaning is performed using a rinse solution having a low surface tension that matches the pattern.

また、隔壁蓋9は隔壁8に取り付けて、その隔壁蓋9の内径は処理室カバー4に添った形状にして間隙を保つ、その間隙は処理室2内が気体ノズル28からの噴射で処理室2内が大気圧より上がった時に隙間から自然放出する。さらに、基板出入口41の開閉トビラ42の隙間からも自然放出する。そして処理室2内の気体の置換は必要に応じて排気口33より電磁弁D35を介して排気電磁弁34を開き排気フアン36で強制放出する。また、その処理室2内で洗浄も真空乾燥もできるのである。 Further, the partition wall lid 9 is attached to the partition wall 8, and the inner diameter of the partition wall lid 9 is shaped to fit the processing chamber cover 4 to maintain a gap. The gap is formed in the processing chamber 2 by injection from a gas nozzle 28. 2 When the inside of 2 rises above the atmospheric pressure, it is naturally released from the gap. Further, it is naturally discharged from the gap of the opening / closing door 42 of the substrate entrance / exit 41. Then, the gas in the processing chamber 2 is replaced by opening the exhaust solenoid valve 34 from the exhaust port 33 via the solenoid valve D35 and forcibly discharging the gas by the exhaust fan 36 as needed. In addition, cleaning and vacuum drying can be performed in the processing chamber 2.

(実施例2)
更に、図2,図3で示されるように真空室50での乾燥時間をより短縮するには、樹脂で出来た処理室カバー4の内側48の形状を円錐にして中心から内周に向かって下げると内側48の内周部の肉厚が厚くなり真空による耐圧で中央部の凹みを無くし、かつ容積を小さくする。さらに処理室ベース3のベース中央54を中高にする事により真空室50の容積をさらに小さくする。そのベース中央54の中高にした事により傾斜部に飛び散った洗浄液は素早く排液溝53に流れて、その排液溝53から排液口15に向かって傾斜しているので、より速やかに排液口15に排出し洗浄液の残留がなく成り基板11の乾燥時間を短縮する事ができるのである。
(Example 2)
Further, as shown in FIGS. 2 and 3, in order to further shorten the drying time in the vacuum chamber 50, the shape of the inner 48 of the processing chamber cover 4 made of resin is made conical and is directed from the center to the inner circumference. When lowered, the wall thickness of the inner peripheral portion of the inner 48 becomes thicker, and the pressure resistance due to the vacuum eliminates the dent in the central portion and reduces the volume. Further, the volume of the vacuum chamber 50 is further reduced by setting the base center 54 of the processing chamber base 3 to a medium height. The cleaning liquid scattered on the inclined portion due to the middle height of the base center 54 quickly flows into the drainage groove 53 and is inclined from the drainage groove 53 toward the drainage port 15, so that the drainage liquid can be discharged more quickly. It is possible to shorten the drying time of the substrate 11 because it is discharged to the mouth 15 and the cleaning liquid does not remain.

(実施例3)
更に、図1、図3で示されるように真空室50の真空乾燥する時は基板11のパターンはアスペクト比(パターン深さ/パターン幅)が大きく成るとそれに伴ってパターン溝は深く成る。そのパターン溝内の液体は蒸気及び気体と成るので初期段階から効率よく吸引するには、パターンに合わせた表面張力のリンス液を使用して表面張力の力と装置の機能を活用して真空乾燥をする。そこで真空排気口23は基板11より高い位置で処理室カバー4の内側48に真空排気口23から効率よく吸引して基板11の乾燥時間を短縮する事ができるのである。
(Example 3)
Further, as shown in FIGS. 1 and 3, when the vacuum chamber 50 is vacuum-dried, the pattern of the substrate 11 becomes deeper as the aspect ratio (pattern depth / pattern width) increases. Since the liquid in the pattern groove becomes steam and gas, in order to suck efficiently from the initial stage, vacuum dry using the surface tension force and the function of the device using a surface tension rinse liquid that matches the pattern. do. Therefore, the vacuum exhaust port 23 can efficiently suck the inside 48 of the processing chamber cover 4 from the vacuum exhaust port 23 at a position higher than the substrate 11 to shorten the drying time of the substrate 11.

本発明は、半導体の基板を洗浄及び乾燥する装置を製造する産業で利用される。 The present invention is used in the industry of manufacturing devices for cleaning and drying semiconductor substrates.

1 基板洗浄真空乾燥装置
2 処理室
3 処理室ベース
4 処理室カバー
5 アーム
6 スライド軸
7 真空ホース
8 隔壁
9 隔壁蓋
10 回転部本体
11 基板
12 カップ
13 カップ用シリンダー
14 基板掴み軸
15 排液口
16 排液切換弁
17 電磁弁A
18 処理室ベース用Oリング
19 回転部用Oリング
20 駆動モータ
21 真空用Oリング
22 排液用Oリング
23 真空排気口
24 真空切換弁
25 電磁弁B
26 真空ポンプ
27 エアー源
28 気体ノズル
29 気体導入源
30 切換弁
31 電磁弁C
32 気体用Oリング
33 排気口
34 排気切換弁
35 電磁弁D
36 排気フアン
37 洗浄ノズル
38 旋回軸
39 ヘッド側ネジ付シリンダー
40 真空フランジ
41 基板出入口
42 開閉トビラ
43 トビラ上下シリンダー
44 上スライドガイド
45 下スライドガイド
46 排液処理タンク
47 メンテ蓋
48 内側
49 接続ロット
50 真空室
51 フランジA
52 取付ボルト
53 排液溝
54 ベース中央
55 ネジ部
56 ロット
1 Substrate cleaning vacuum drying device 2 Processing chamber 3 Processing chamber base 4 Processing chamber cover 5 Arm 6 Slide shaft 7 Vacuum hose 8 Partition 9 Partition lid 10 Rotating part main body 11 Board 12 Cup 13 Cup cylinder 14 Board grip shaft 15 Drainage port 16 Drainage switching valve 17 Solenoid valve A
18 O-ring for processing chamber base 19 O-ring for rotating part 20 Drive motor 21 O-ring for vacuum 22 O-ring for drainage 23 Vacuum exhaust port 24 Vacuum switching valve 25 Solenoid valve B
26 Vacuum pump 27 Air source 28 Gas nozzle 29 Gas introduction source 30 Switching valve 31 Solenoid valve C
32 O-ring for gas 33 Exhaust port 34 Exhaust switching valve 35 Solenoid valve D
36 Exhaust fan 37 Cleaning nozzle 38 Swing shaft 39 Head side screwed cylinder 40 Vacuum flange 41 Board entrance / exit 42 Opening / closing Tobira 43 Tobira upper / lower cylinder 44 Upper slide guide 45 Lower slide guide 46 Drainage treatment tank 47 Maintenance lid 48 Inner 49 Connection lot 50 Vacuum chamber 51 Flange A
52 Mounting bolt 53 Drainage groove 54 Base center 55 Threaded part 56 Lot

Claims (3)

処理室2の外部で処理室ベース3の下側からフッ素樹脂又は塩化ビニール樹脂、等の薬液対応用樹脂のフランジA51を介して金属製の回転部本体10取り付けてそのフランジA51から処理室ベース3の下側に金属製の取付ボルト52を装着してその取付ボルト52の強度の補強と腐食対策をするのと、処理室2内の処理室ベース3に隔壁8を接合し隔壁蓋9は隔壁8に固定し隔壁蓋9との間に間隙を持って移動する処理室カバー4で囲まれた処理室2の中で、処理室カバー4の凹状の内側48より窒素ガスを基板11の全面に当たるように気体ノズル28から噴射するのと、隔壁8に基板出入口41を設けてトビラ上下シリンダー43で開閉トビラ42を開閉するのと、回転部本体10に取り付けた駆動モータ20で回転しうる基板掴み軸14に掴まれた基板11を揺動運動する旋回軸38に取り付けたノズル37で回転洗浄した後に処理室カバー4が下降して処理室ベース3側に装着した処理室ベース用Oリング18に密閉された真空室50で真空切換弁24を介して真空ポンプ26で真空室50を減圧する手段をも処理室2内に設ける事を特徴とする基板洗浄真空乾燥装置。 Outside the processing chamber 2, a metal rotating part main body 10 is attached from the lower side of the processing chamber base 3 via a flange A51 of a resin for chemicals such as fluororesin or vinyl chloride resin, and the processing chamber base 3 is attached from the flange A51. A metal mounting bolt 52 is mounted on the lower side to reinforce the strength of the mounting bolt 52 and prevent corrosion, and the partition wall 8 is joined to the processing chamber base 3 in the processing chamber 2 so that the partition wall lid 9 is a partition wall. In the processing chamber 2 surrounded by the processing chamber cover 4 fixed to 8 and moving with a gap between the partition wall lid 9, nitrogen gas hits the entire surface of the substrate 11 from the concave inner side 48 of the processing chamber cover 4. As described above, the gas nozzle 28 is used to inject the gas, the partition wall 8 is provided with the substrate inlet / outlet 41, and the opening / closing door 42 is opened / closed by the door upper / lower cylinder 43. The processing chamber cover 4 is lowered to the O-ring 18 for the processing chamber base mounted on the processing chamber base 3 side after the substrate 11 gripped by the shaft 14 is rotationally cleaned by the nozzle 37 attached to the swirling shaft 38 that swings. A substrate cleaning vacuum drying apparatus, characterized in that a means for depressurizing the vacuum chamber 50 by a vacuum pump 26 via a vacuum switching valve 24 in the closed vacuum chamber 50 is also provided in the processing chamber 2. 処理室2の樹脂で出来た処理室カバー4の内側48の形状を円錐又は円球にして、中心から内周に向かって下げると内側48の内周部の肉厚が厚くして真空圧で中央部の凹みを抑え、かつ容積が小さくするのと、処理室2内の処理室ベース3のベース中央54を中高にして真空室50の容積をさらに小さくするのと、ベース中央54の中高の傾斜で飛び散った洗浄液は素早く排液溝53に流れ排液口15に速やかに排出し洗浄液の残留がなく成るのとで基板11を乾燥する手段を設ける事を特徴とする請求項1に記載の基板洗浄真空乾燥装置。 When the shape of the inner 48 of the processing chamber cover 4 made of the resin of the processing chamber 2 is made into a cone or a sphere and lowered from the center toward the inner circumference, the wall thickness of the inner peripheral portion of the inner 48 becomes thicker and vacuum pressure is applied. Suppressing the dent in the central part and reducing the volume, making the base center 54 of the processing chamber base 3 in the processing chamber 2 medium and high to further reduce the volume of the vacuum chamber 50, and making the volume of the vacuum chamber 50 medium and high. The first aspect of claim 1, wherein the cleaning liquid scattered due to the inclination quickly flows into the drainage groove 53 and is quickly discharged to the drainage port 15 to eliminate the residual cleaning liquid, so that a means for drying the substrate 11 is provided. Substrate cleaning Vacuum drying equipment. 真空室50内を真空乾燥するには基板11のパターン溝の深い中の液体は蒸気から気化するので初期段階から効率よく真空排気口23に吸引するには基板11より上部の方に蒸気及び気体の流れにするのと、その真空排気口23は基板11より高い位置で処理室カバー4の内側48に真空排気口23を設ける事を特徴とする請求項1又は2に記載の基板洗浄真空乾燥装置。 To vacuum dry the inside of the vacuum chamber 50, the liquid in the deep pattern groove of the substrate 11 is vaporized from the steam, so to efficiently suck it into the vacuum exhaust port 23 from the initial stage, steam and gas are directed toward the upper part of the substrate 11. The substrate cleaning vacuum drying according to claim 1 or 2, wherein the vacuum exhaust port 23 is provided on the inner side 48 of the processing chamber cover 4 at a position higher than the substrate 11. Device.
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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001319915A (en) * 2000-05-08 2001-11-16 Tokyo Electron Ltd System and method for liquid treatment
JP2019012824A (en) * 2017-06-30 2019-01-24 株式会社Screenホールディングス Substrate processing device and substrate processing method

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001319915A (en) * 2000-05-08 2001-11-16 Tokyo Electron Ltd System and method for liquid treatment
JP2019012824A (en) * 2017-06-30 2019-01-24 株式会社Screenホールディングス Substrate processing device and substrate processing method

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