JP6970016B2 - 抗付着支持体への接着性パターン印刷 - Google Patents
抗付着支持体への接着性パターン印刷 Download PDFInfo
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- C09J5/00—Adhesive processes in general; Adhesive processes not provided for elsewhere, e.g. relating to primers
- C09J5/02—Adhesive processes in general; Adhesive processes not provided for elsewhere, e.g. relating to primers involving pretreatment of the surfaces to be joined
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- B01J19/0046—Sequential or parallel reactions, e.g. for the synthesis of polypeptides or polynucleotides; Apparatus and devices for combinatorial chemistry or for making molecular arrays
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- B01J19/08—Processes employing the direct application of electric or wave energy, or particle radiation; Apparatus therefor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D1/00—Processes for applying liquids or other fluent materials
- B05D1/18—Processes for applying liquids or other fluent materials performed by dipping
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B05—SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D3/00—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials
- B05D3/06—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by exposure to radiation
- B05D3/061—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by exposure to radiation using U.V.
- B05D3/065—After-treatment
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- B05D3/00—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials
- B05D3/06—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by exposure to radiation
- B05D3/061—Pretreatment of surfaces to which liquids or other fluent materials are to be applied; After-treatment of applied coatings, e.g. intermediate treating of an applied coating preparatory to subsequent applications of liquids or other fluent materials by exposure to radiation using U.V.
- B05D3/065—After-treatment
- B05D3/067—Curing or cross-linking the coating
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- B05D—PROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
- B05D5/00—Processes for applying liquids or other fluent materials to surfaces to obtain special surface effects, finishes or structures
- B05D5/10—Processes for applying liquids or other fluent materials to surfaces to obtain special surface effects, finishes or structures to obtain an adhesive surface
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
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- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12Q—MEASURING OR TESTING PROCESSES INVOLVING ENZYMES, NUCLEIC ACIDS OR MICROORGANISMS; COMPOSITIONS OR TEST PAPERS THEREFOR; PROCESSES OF PREPARING SUCH COMPOSITIONS; CONDITION-RESPONSIVE CONTROL IN MICROBIOLOGICAL OR ENZYMOLOGICAL PROCESSES
- C12Q1/00—Measuring or testing processes involving enzymes, nucleic acids or microorganisms; Compositions therefor; Processes of preparing such compositions
- C12Q1/68—Measuring or testing processes involving enzymes, nucleic acids or microorganisms; Compositions therefor; Processes of preparing such compositions involving nucleic acids
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- C—CHEMISTRY; METALLURGY
- C40—COMBINATORIAL TECHNOLOGY
- C40B—COMBINATORIAL CHEMISTRY; LIBRARIES, e.g. CHEMICAL LIBRARIES
- C40B50/00—Methods of creating libraries, e.g. combinatorial synthesis
- C40B50/14—Solid phase synthesis, i.e. wherein one or more library building blocks are bound to a solid support during library creation; Particular methods of cleavage from the solid support
- C40B50/18—Solid phase synthesis, i.e. wherein one or more library building blocks are bound to a solid support during library creation; Particular methods of cleavage from the solid support using a particular method of attachment to the solid support
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00583—Features relative to the processes being carried out
- B01J2219/00596—Solid-phase processes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00274—Sequential or parallel reactions; Apparatus and devices for combinatorial chemistry or for making arrays; Chemical library technology
- B01J2219/00709—Type of synthesis
- B01J2219/00711—Light-directed synthesis
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2301/00—Additional features of adhesives in the form of films or foils
- C09J2301/40—Additional features of adhesives in the form of films or foils characterized by the presence of essential components
- C09J2301/416—Additional features of adhesives in the form of films or foils characterized by the presence of essential components use of irradiation
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2471/00—Presence of polyether
- C09J2471/006—Presence of polyether in the substrate
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2483/00—Presence of polysiloxane
- C09J2483/006—Presence of polysiloxane in the substrate
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/48—Biological material, e.g. blood, urine; Haemocytometers
- G01N33/50—Chemical analysis of biological material, e.g. blood, urine; Testing involving biospecific ligand binding methods; Immunological testing
- G01N33/53—Immunoassay; Biospecific binding assay; Materials therefor
- G01N33/543—Immunoassay; Biospecific binding assay; Materials therefor with an insoluble carrier for immobilising immunochemicals
- G01N33/54353—Immunoassay; Biospecific binding assay; Materials therefor with an insoluble carrier for immobilising immunochemicals with ligand attached to the carrier via a chemical coupling agent
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- Application Of Or Painting With Fluid Materials (AREA)
- Apparatus Associated With Microorganisms And Enzymes (AREA)
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Description
以下の定義が本出願に適用される。
−前記層を、ベンゾフェノンを含有する第1の水溶液に接触させる工程と、
−その後に、前記パターンに応じて且つ表面エネルギーに応じて、前記ベンゾフェノンの吸収スペクトル内の波長の放射線で前記層を照射する工程とを含む。
本方法の変形例では、
−前記層の厚さは、1nm〜20nmであり、
−前記波長は、300nm〜400nmの範囲で選択され、
−前記ポリマーは、ポリエチレングリコール(PEG)であり、
−前記ポリマーは、ポリ(N−イソプロピルアクリルアミド)(ポリNIPAM)であり、
−前記支持体は、ガラスであり、
−前記支持体は、ポリジメチルシロキサン(PDMS)であり、
−前記ポリエチレングリコールに伝達される前記照射の前記表面エネルギーは、10mJ/mm2〜1000mJ/mm2であり、
−前記ポリ(N−イソプロピルアクリルアミド)に伝達される前記照射の前記表面エネルギーは、100mJ/mm2〜10000mJ/mm2であり、
−前記PDMS支持体のヤング率は、15kPa未満である。
本発明はまた、前記ポリマーブラシ上に対象の分子又は分子集合のパターンを印刷するための上記方法に関し、
本方法は、
−すすぐことにより、前記層と前記第1の溶液との間の接触を除去する工程と、
−その後に、前記層を、前記対象の分子又は分子集合を含有する第2の水溶液と接触させる工程とをさらに含む。
本発明はまた、前記ポリマーブラシ上にナノシェルのパターンを印刷する上記方法に関し、
本方法は、
−すすぐことにより、前記層と前記第1の水溶液との間の接触を除去する工程と、
−前記層を、前記ナノシェルを含有する第2の溶液に接触させる工程とをさらに含む。
本発明はまた、前記ポリマーブラシ上にDNA鎖のパターンを印刷するための上記方法に関し、
本方法は、
−すすぐことにより、前記層と前記第1の水溶液との間の接触を除去する工程と、
−前記層を、前記DNA鎖を含有する第2の溶液に接触させる工程とをさらに含む。
前記層への照射の表面エネルギーを空間的に変化させることによって、前記支持体(1)の表面に接着勾配を有する接着性パターンを製造する。
本発明は、以下の図面の一覧に関連してさらに理解される。
めに従来技術で既知の技術で当該分子による像を生成することができる。
Claims (15)
- ナノメートルサイズの抗付着層(2)を形成して、支持体(1)の表面に広がるポリマーブラシ上に接着性パターンを印刷する方法であって、
前記層(2)を、ベンゾフェノンを含有する第1の水溶液(4)に接触させる工程と、
その後に、前記パターンに応じて、前記ベンゾフェノンの吸収スペクトル内の波長の放射線(3)で前記層を照射する工程と
を含む方法。 - 請求項1に記載の方法であって、
前記層(2)の厚さは、1nm〜20nmであることを特徴とする方法。 - 請求項2に記載の方法であって、
前記波長は、300nm〜400nmの範囲で選択されることを特徴とする方法。 - 請求項3に記載の方法であって、
前記ポリマーは、ポリエチレングリコール(PEG)であることを特徴とする方法。 - 請求項3に記載の方法であって、
前記ポリマーは、ポリ(N−イソプロピルアクリルアミド)であることを特徴とする方法。 - 請求項3に記載の方法であって、
前記支持体(1)は、ガラスであることを特徴とする方法。 - 請求項3に記載の方法であって、
前記支持体(1)はポリジメチルシロキサン(PDMS)であることを特徴とする方法。 - 請求項4に記載の方法であって、
前記ポリエチレングリコールに伝達される前記照射の表面エネルギーは、10mJ/mm2〜1000mJ/mm2であることを特徴とする方法。 - 請求項5に記載の方法であって、
前記ポリ(N−イソプロピルアクリルアミド)に伝達される前記照射の表面エネルギーは、100mJ/mm2〜10000mJ/mm2であることを特徴とする方法。 - ナノメートルサイズの抗付着層(2)を形成して、支持体(1)の表面に広がるポリマーブラシ上に、対象の分子又は分子集合のパターンを印刷する方法であって、
請求項1〜9の何れか1項に記載の方法により前記ポリマーブラシ上に接着性パターンを印刷する工程と、
すすぐことにより、前記層(2)と前記第1の水溶液(4)との間の接触を除去する工
程と、
前記層(2)を、前記対象の分子又は分子集合を含有する第2の水溶液と接触させる工程とを
この順で行うことを含む方法。 - 請求項10に記載の方法であって、
前記対象の分子又は分子集合がタンパク質である方法。 - 請求項10に記載の方法であって、
前記対象の分子又は分子集合がナノシェルである方法。 - 請求項10に記載の方法であって、
前記対象となる分子又は分子集合がDNA鎖である方法。 - 請求項10に記載の方法であって、
前記層が前記対象の分子又は分子集合と接触したときに、前記対象の分子又は分子集合は、前記接着性パターン上に吸着され、この吸着は光エネルギーが供給されることなく起こる方法。 - 。
請求項1に記載の方法であって、
前記層への照射の表面エネルギーを空間的に変化させることによって、前記支持体(1)の表面に接着勾配を有する接着性パターンを製造する方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR1459497 | 2014-10-03 | ||
FR1459497A FR3026742B1 (fr) | 2014-10-03 | 2014-10-03 | Impression d'un motif adhesif sur un support anti-salissures |
PCT/EP2015/072874 WO2016050980A1 (fr) | 2014-10-03 | 2015-10-02 | Impression d'un motif adhesif sur un support anti-salissures |
Publications (2)
Publication Number | Publication Date |
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JP2018500608A JP2018500608A (ja) | 2018-01-11 |
JP6970016B2 true JP6970016B2 (ja) | 2021-11-24 |
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JP2017537015A Active JP6970016B2 (ja) | 2014-10-03 | 2015-10-02 | 抗付着支持体への接着性パターン印刷 |
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Country | Link |
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US (1) | US10941319B2 (ja) |
EP (1) | EP3201282A1 (ja) |
JP (1) | JP6970016B2 (ja) |
KR (1) | KR102421564B1 (ja) |
CN (1) | CN107109141B (ja) |
AU (1) | AU2015326803B2 (ja) |
BR (1) | BR112017006839A2 (ja) |
CA (1) | CA2963167C (ja) |
FR (1) | FR3026742B1 (ja) |
MX (1) | MX2017004272A (ja) |
RU (1) | RU2702559C2 (ja) |
WO (1) | WO2016050980A1 (ja) |
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CN106932846B (zh) * | 2017-05-08 | 2019-11-05 | 京东方科技集团股份有限公司 | 一种光学增亮结构及其制作方法 |
EP3536402A1 (de) | 2018-03-09 | 2019-09-11 | Ibidi Gmbh | Probenkammer |
FR3079233B1 (fr) * | 2018-03-20 | 2022-04-01 | Alveole | Substrat pour l'impression de proteines |
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US5677196A (en) * | 1993-05-18 | 1997-10-14 | University Of Utah Research Foundation | Apparatus and methods for multi-analyte homogeneous fluoro-immunoassays |
CA2319587C (en) * | 1998-02-11 | 2004-09-21 | University Of Houston | Method and apparatus for chemical and biochemical reactions using photo-generated reagents |
EP1208126B1 (en) * | 1999-07-02 | 2006-04-12 | Symyx Technologies, Inc. | Polymer brushes for immobilizing molecules to a surface or substrate, where the polymers have water-soluble or water-dispersible segments and probes bonded thereto |
US7147687B2 (en) * | 2001-05-25 | 2006-12-12 | Nanosphere, Inc. | Non-alloying core shell nanoparticles |
DE60226736D1 (de) * | 2002-09-17 | 2008-07-03 | Kalachev Alexey | Verfahren zum Anordnen einem Polymer-Molekül |
KR100561842B1 (ko) * | 2003-08-25 | 2006-03-16 | 삼성전자주식회사 | 단량체 광산발생제 조성물, 상기 조성물로 코팅된 기판,상기 단량체 광산발생제 조성물을 이용하여 기판상에서화합물을 합성하는 방법 및 상기 방법에 의하여 제조된마이크로어레이 |
CA2596807A1 (en) * | 2005-02-10 | 2006-08-17 | Commissariat A L'energie Atomique | Method for the photochemical attachment of biomolecules to a substrate |
US7397232B2 (en) * | 2005-10-21 | 2008-07-08 | The University Of Akron | Coulter counter having a plurality of channels |
US8349410B2 (en) * | 2006-08-17 | 2013-01-08 | University of Pittsburgh—of the Commonwealth System of Higher Education | Modification of surfaces with polymers |
FR2988093B1 (fr) * | 2012-03-14 | 2014-04-25 | Alveole | Dispositif de greffage micro-structure de proteines sur un substrat |
US9171720B2 (en) * | 2013-01-19 | 2015-10-27 | Rohm And Haas Electronic Materials Llc | Hardmask surface treatment |
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- 2014-10-03 FR FR1459497A patent/FR3026742B1/fr active Active
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- 2015-10-02 MX MX2017004272A patent/MX2017004272A/es unknown
- 2015-10-02 BR BR112017006839-7A patent/BR112017006839A2/pt active Search and Examination
- 2015-10-02 WO PCT/EP2015/072874 patent/WO2016050980A1/fr active Application Filing
- 2015-10-02 CA CA2963167A patent/CA2963167C/en active Active
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- 2015-10-02 JP JP2017537015A patent/JP6970016B2/ja active Active
- 2015-10-02 EP EP15785060.3A patent/EP3201282A1/fr active Pending
- 2015-10-02 RU RU2017114966A patent/RU2702559C2/ru active
- 2015-10-02 CN CN201580053960.7A patent/CN107109141B/zh active Active
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Also Published As
Publication number | Publication date |
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RU2702559C2 (ru) | 2019-10-08 |
RU2017114966A3 (ja) | 2019-04-05 |
CN107109141B (zh) | 2020-08-14 |
WO2016050980A1 (fr) | 2016-04-07 |
AU2015326803A1 (en) | 2017-04-20 |
BR112017006839A2 (pt) | 2018-06-19 |
KR20170095813A (ko) | 2017-08-23 |
RU2017114966A (ru) | 2018-11-06 |
AU2015326803B2 (en) | 2019-07-18 |
CA2963167C (en) | 2023-03-14 |
CN107109141A (zh) | 2017-08-29 |
JP2018500608A (ja) | 2018-01-11 |
CA2963167A1 (en) | 2016-04-07 |
FR3026742A1 (fr) | 2016-04-08 |
EP3201282A1 (fr) | 2017-08-09 |
US20170218230A1 (en) | 2017-08-03 |
KR102421564B1 (ko) | 2022-07-15 |
US10941319B2 (en) | 2021-03-09 |
FR3026742B1 (fr) | 2016-12-23 |
MX2017004272A (es) | 2017-10-02 |
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