JP6231295B2 - 反応装置 - Google Patents
反応装置 Download PDFInfo
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- JP6231295B2 JP6231295B2 JP2013101162A JP2013101162A JP6231295B2 JP 6231295 B2 JP6231295 B2 JP 6231295B2 JP 2013101162 A JP2013101162 A JP 2013101162A JP 2013101162 A JP2013101162 A JP 2013101162A JP 6231295 B2 JP6231295 B2 JP 6231295B2
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- Control Of High-Frequency Heating Circuits (AREA)
- Constitution Of High-Frequency Heating (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Description
U[W/m2.K]=P[W]÷ΔT0[K]÷A[m2]・・・式5
UA=P÷ΔT0・・・式11
Claims (5)
- 被加熱液を収容可能な反応容器と、
該反応容器を挿通可能な反応容器挿通孔を有する金属製の恒温槽と、
該恒温槽の対向する一対の側面に対向してそれぞれ設けられたマイクロ波導入口及びマイクロ波導出口と、
前記マイクロ波導入口に連結された入口側同軸導波管変換器及び前記マイクロ波導出口に連結された出口側同軸導波管変換器と、
マイクロ波発振器から出力されて前記入口側同軸導波管変換器を介して前記反応容器に導入されるマイクロ波の電力を測定する入口側電力検出手段と、
入口側同軸導波管変換器から導入されて反応容器を経て出口側同軸導波管変換器に導出されたマイクロ波の電力を測定する出口側電力検出手段と、
マイクロ波発振器まで戻ってきたマイクロ波の反射電力を測定する反射電力検出手段と、前記入口側電力検出手段で測定したマイクロ波の電力と出口側電力検出手段で測定したマイクロ波の電力と前記反射電力検出手段で測定したマイクロ波の電力とに基づいて前記被加熱液に吸収されたマイクロ波の電力を算出する吸収電力算出手段と、
前記反応容器内に反応薬液を注入する反応薬液注入部と、
前記反応容器内の被加熱液の温度を測定する被加熱液温度測定手段と、
前記恒温槽を加熱する加熱手段及び恒温槽を冷却する冷却手段及び恒温槽の温度を測定する恒温槽温度測定手段と、
前記被加熱液温度測定手段で測定した被加熱液の温度又は前記恒温槽温度測定手段で測定した恒温槽の温度に基づいて前記加熱手段及び冷却手段を制御する恒温槽温度制御手段と、
前記被加熱液温度測定手段で測定した被加熱液の温度に基づいて前記マイクロ波発振器から出力されるマイクロ波の電力を制御するマイクロ波出力制御手段とを備え、
マイクロ波シングルモードを熱源とし、
マイクロ波の進行波が恒温槽に吸収されずに被加熱液に1回だけ当たって通過することにより被加熱液にマイクロ波が直接照射され、被加熱液がマイクロ波シングルモードを吸収することを特徴とする反応装置。 - 前記恒温槽は、前記マイクロ波導入口及びマイクロ波導出口とは異なる恒温槽の側面に、前記反応容器内の状態を観察するための観察窓と明かり取り窓とが対向して設けられていることを特徴とする請求項1記載の反応装置。
- 前記マイクロ波は、2.45GHzであることを特徴とする請求項1又は2記載の反応装置。
- 前記入口側同軸導波管変換器は、前記マイクロ波導入口に向かって高さ寸法が一定で幅寸法が漸次幅狭となる形状を有し、出口側同軸導波管変換器は、前記マイクロ波導出口に向かって高さ寸法が一定で幅寸法が漸次幅狭となる形状を有していることを特徴とする請求項1乃至3のいずれか1項記載の反応装置。
- 前記反応容器は、該反応容器を保持する保持筒に保持された状態で前記反応容器挿通孔に挿通され、前記保持筒には、前記マイクロ波導入口及び前記マイクロ波導出口に対応した開口がそれぞれ設けられていることを特徴とする請求項1乃至4のいずれか1項記載の反応装置。
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Cited By (1)
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CN110876915A (zh) * | 2018-09-05 | 2020-03-13 | 捷微科技股份有限公司 | 光化学反应槽用温控光源装置及该光化学反应槽 |
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US5796080A (en) * | 1995-10-03 | 1998-08-18 | Cem Corporation | Microwave apparatus for controlling power levels in individual multiple cells |
WO2000072970A1 (en) * | 1999-05-28 | 2000-12-07 | Cepheid | Cartridge for conducting a chemical reaction |
JP2006302721A (ja) * | 2005-04-22 | 2006-11-02 | Idx Corp | マイクロ波による高圧加熱装置 |
WO2012153793A1 (ja) * | 2011-05-10 | 2012-11-15 | 独立行政法人産業技術総合研究所 | 物質の状態の測定、検出方法及び検出装置 |
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CN110876915A (zh) * | 2018-09-05 | 2020-03-13 | 捷微科技股份有限公司 | 光化学反应槽用温控光源装置及该光化学反应槽 |
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