JP6164889B2 - Granulated granules and method for producing the same - Google Patents

Granulated granules and method for producing the same Download PDF

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JP6164889B2
JP6164889B2 JP2013070959A JP2013070959A JP6164889B2 JP 6164889 B2 JP6164889 B2 JP 6164889B2 JP 2013070959 A JP2013070959 A JP 2013070959A JP 2013070959 A JP2013070959 A JP 2013070959A JP 6164889 B2 JP6164889 B2 JP 6164889B2
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友哉 上野
友哉 上野
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Yaizu Suisan Kagaku Kogyo Co Ltd
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Description

本発明は、水への沈降性、分散性等の溶解適性に優れた造粒顆粒及びその製造方法に関する。   The present invention relates to a granulated granule excellent in solubility suitability such as sedimentation in water and dispersibility, and a method for producing the same.

一般に、粉末の造粒加工の目的には、多種原料が混合される際の均一性を高めたり、粉末充填機に適した高速計量性(流動性)をもたせたり、表面積を減少させることで吸湿速度を低減させたり、粉末の飛散や容器への付着を防止したり、外観上の付加価値の向上など、様々であるが、水への溶解適性を向上させるためにも、しばしば造粒加工が用いられる。   Generally, the purpose of granulating powder is to increase the uniformity when various raw materials are mixed, to provide high-speed meterability (fluidity) suitable for powder filling machines, or to reduce the surface area to absorb moisture. Various methods such as reducing the speed, preventing powder scattering and adhesion to the container, and improving the added value of the appearance, are often used to improve the solubility in water. Used.

粉末を水に溶かす際には、まま粉の形成という問題がある。まま粉の形成とは、粉末自体が水へ分散する速度よりも、水と粉体の接触面での水和が早い場合に、接触面のみの水和が生じ、溶解していない粉体が内部に残る現象をいう。まま粉が形成されると、内部に残る粉体が分散せずに、溶けにくくなる。   When the powder is dissolved in water, there is a problem of powder formation as it is. In the powder formation, when the hydration at the contact surface of water and powder is faster than the speed at which the powder itself disperses in water, hydration of only the contact surface occurs and the undissolved powder A phenomenon that remains inside. If the powder is formed as it is, the powder remaining inside does not disperse and becomes difficult to melt.

造粒加工の対象となる粉末の1つとして、スプレードライ乾燥品が知られている。しかし、スプレードライ乾燥品は、微粉末状で表面積が大きいために水和が早く、まま粉を形成しやすい。また、粒子が中空構造をとり、空気を抱いているため、造粒加工を施しても水面上に浮く傾向があり、水面付近からの沈み込みが遅いという問題がある。   A spray-dried product is known as one of powders to be granulated. However, spray-dried products are finely powdered and have a large surface area, so that they are hydrated quickly and easily form powder. In addition, since the particles have a hollow structure and hold air, there is a problem that even if granulation is performed, the particles tend to float on the water surface, and the sinking from the vicinity of the water surface is slow.

このような問題に関し、例えば下記特許文献1には、粉末原料をポリソルベートで処理することによって、飛散性、水への溶解性・分散性が改善された粉末組成物を得る方法が記載されている。また、特許文献2では、予め、まま粉形成性成分と乳化剤とを混合して乳化剤-まま粉形成性成分混合物を調製し、次いで残りの成分を乳化剤-まま粉形成性成分混合物と混合し、造粒することにより、溶解性を改善した顆粒状組成物を得る方法が記載されている。   Regarding such a problem, for example, the following Patent Document 1 describes a method of obtaining a powder composition with improved scattering properties, water solubility and dispersibility by treating a powder raw material with polysorbate. . In Patent Document 2, a powder-forming component and an emulsifier are mixed in advance to prepare an emulsifier-powder-forming component mixture, and then the remaining components are mixed with the emulsifier-powder-forming component mixture. A method is described for obtaining a granular composition with improved solubility by granulation.

しかしながら、これらの方法では、水へ溶解して用いるタイプの混合調味料や粉末食品等であって、特に油脂を多く含むものについては、水に溶かす際の沈降性や湿潤性に優れず、必ずしも溶解適性の改善には繋がらなかった。   However, in these methods, mixed seasonings and powdered foods of the type used by dissolving in water, especially those that contain a large amount of fats and oils are not excellent in sedimentation and wettability when dissolved in water, and are not necessarily It did not lead to improvement of dissolution suitability.

一方、特許文献3には、ドラム乾燥法によって得られた非多孔質で薄片状のコラーゲンペプチド粉末と結着剤とを造粒することにより、水に加えた際に、沈降溶解性がよく、速やかに沈降溶解する、コラーゲンを含む造粒物を得ることが記載されている。また、特許文献4,5には、コラーゲンペプチドを含有する溶液を真空乾燥により乾燥し、粉体化して、水への溶解適性等の品質に優れ、飲食品や化粧品への配合に有利な、コラーゲンペプチド粉体組成物を得ることが記載されている。   On the other hand, Patent Document 3 discloses that the non-porous and flaky collagen peptide powder obtained by the drum drying method and the binder are granulated, so that when added to water, the sedimentation solubility is good. It is described that a granulated product containing collagen that rapidly settles and dissolves is obtained. In Patent Documents 4 and 5, a solution containing a collagen peptide is dried by vacuum drying, powdered, excellent in quality such as solubility in water, and advantageous for blending into foods and drinks, Obtaining a collagen peptide powder composition is described.

ドラム乾燥や真空乾燥を施した粉体を電子顕微鏡で観察すると、密なブロック構造をとっており、中空構造をとらずに空気を含まないため、水に加えた際には沈むという特徴があり、これらの技術はその性質を活かした方法である。   When the powder that has been subjected to drum drying or vacuum drying is observed with an electron microscope, it has a dense block structure and does not have a hollow structure and does not contain air. These techniques are methods that take advantage of their properties.

しかしながら、水へ溶解して用いるタイプの混合調味料や粉末食品等であって、特に親水性の高いタンパク質や糖質を多く含むものについては、ドラム乾燥や真空乾燥に処すると、水に溶かす際の沈降性は改善するが、かえって分散性や湿潤性が悪くなり、結果として溶解適性の改良には繋がらなかった。   However, mixed seasonings and powdered foods of the type that are used by dissolving in water, especially those that contain a lot of highly hydrophilic proteins and sugars, can be dissolved in water when subjected to drum drying or vacuum drying. However, the dispersibility and wettability deteriorated. As a result, the solubility was not improved.

特開2004−121061号公報JP 2004-121061 A 特開2008−104435号公報JP 2008-104435 A 特開2009−171903号公報JP 2009-171903 A 特開2011−178666号公報JP 2011-178666 A 特開2012−196156号公報JP 2012-196156 A

本発明の目的は、上記従来技術にかんがみ、水への沈降性、分散性等の溶解適性に優れ、糖質、タンパク質、食物繊維、油脂、ミネラルなどの各成分が多様に含まれる、混合調味料や粉末食品等の加工食品であっても、それを迅速に溶かすことができるようにした、造粒顆粒及びその製造方法を提供することにある。   The object of the present invention is, in view of the above-mentioned prior art, excellent in solubility such as sedimentation in water, dispersibility, etc., and contains various ingredients such as carbohydrates, proteins, dietary fiber, fats and oils, mixed seasoning An object of the present invention is to provide a granulated granule and a method for producing the granulated granule so that it can be rapidly dissolved even in processed foods such as foods and powdered foods.

上記目的を達成するため、本発明の造粒顆粒は、油脂と乳化剤とを含有する真空乾燥粉末を、20質量%〜100質量%の割合で配合して流動造粒してなることを特徴とする。   In order to achieve the above object, the granulated granule of the present invention is characterized by being formed by fluid granulation by blending a vacuum dry powder containing fats and oils and an emulsifier in a proportion of 20% by mass to 100% by mass. To do.

本発明の造粒顆粒によれば、油脂と乳化剤とを含有する真空乾燥粉末を、造粒加工の粉体原料の一部または全部として、配合して顆粒化したので、真空乾燥加工による効果と造粒加工による効果とが相乗的に活かされ、水への沈降性、分散性等の溶解適性に優れた造粒顆粒となすことができる。   According to the granulated granule of the present invention, the vacuum dried powder containing fats and oils and the emulsifier is blended and granulated as part or all of the powder raw material for granulation processing. The effect of the granulation process is synergistically utilized, and a granulated granule having excellent solubility suitability such as water settling and dispersibility can be obtained.

本発明の造粒顆粒においては、前記真空乾燥粉末が、油脂を5質量%〜25質量%含有することが好ましい。   In the granulated granule of this invention, it is preferable that the said vacuum-dried powder contains 5 mass%-25 mass% of fats and oils.

また、前記真空乾燥粉末が、その全体の70質量%以上が12メッシュ(目開き1.42mm)をパスし、かつ、80メッシュ(目開き182μm)にオンするものであることが好ましい。   In addition, it is preferable that 70% by mass or more of the vacuum-dried powder passes 12 mesh (aperture 1.42 mm) and turns on to 80 mesh (aperture 182 μm).

一方、本発明の造粒顆粒の製造方法は、油脂と乳化剤と水とを含有する真空乾燥材料を均質化処理した後に真空乾燥して真空乾燥粉末を調製し、前記真空乾燥粉末を20質量%〜100質量%の割合で配合して流動造粒することを特徴とする。   On the other hand, in the method for producing granulated granules of the present invention, a vacuum-dried powder containing fats and oils, an emulsifier and water is homogenized and then vacuum-dried to prepare a vacuum-dried powder. It mix | blends in the ratio of -100 mass%, and is characterized by carrying out fluid granulation.

本発明の造粒顆粒の製造方法によれば、油脂と乳化剤と水とを含有する真空乾燥材料を均質化処理した後に真空乾燥して真空乾燥粉末を調製し、その真空乾燥粉末を、造粒加工の粉体原料の一部または全部として、配合して顆粒化したので、真空乾燥加工による効果と造粒加工による効果とが相乗的に活かされ、水への沈降性、分散性等の溶解適性に優れた造粒顆粒を得ることができる。   According to the method for producing a granulated granule of the present invention, a vacuum-dried material containing fats and oils, an emulsifier and water is homogenized and then vacuum-dried to prepare a vacuum-dried powder, and the vacuum-dried powder is granulated. As part or all of the powder raw material for processing, it is blended and granulated, so the effect of vacuum drying and the effect of granulation are used synergistically, dissolving in sedimentation, dispersibility, etc. in water A granulated granule excellent in suitability can be obtained.

本発明の造粒顆粒の製造方法においては、前記真空乾燥粉末が、油脂を5質量%〜25質量%含有することが好ましい。   In the manufacturing method of the granulated granule of this invention, it is preferable that the said vacuum dry powder contains 5 mass%-25 mass% of fats and oils.

また、前記真空乾燥後に得られた乾燥物を解砕し、整粒して、前記真空乾燥粉末として、その全体の70質量%以上が12メッシュ(目開き1.42mm)をパスし、かつ、80メッシュ(目開き182μm)にオンするものを調製することが好ましい。   In addition, the dried product obtained after the vacuum drying is crushed, sized, and 70% by mass or more of the vacuum-dried powder passes 12 mesh (aperture 1.42 mm), and It is preferable to prepare a material that turns on to 80 mesh (aperture 182 μm).

本発明によれば、油脂と乳化剤とを含有する真空乾燥粉末を、造粒加工の粉体原料の一部または全部として、配合して顆粒化することにより、真空乾燥加工による効果と造粒加工による効果とを相乗的に活かして、水への沈降性、分散性等の溶解適性に優れた造粒顆粒を得ることができる。これにより、糖質、タンパク質、食物繊維、油脂、ミネラルなどの各成分が多様に含まれる、混合調味料や粉末食品等の加工食品であっても、それを迅速に溶かすことができるようにした、造粒顆粒を提供することができる。   According to the present invention, the vacuum-dried powder containing fats and oils and the emulsifier is blended and granulated as part or all of the powder raw material for granulation, and the effect and granulation processing by the vacuum-drying process are performed. Taking advantage of the effects of the above, it is possible to obtain granulated granules having excellent solubility suitability such as sedimentation in water and dispersibility. As a result, even processed foods such as mixed seasonings and powdered foods that contain various ingredients such as carbohydrates, proteins, dietary fiber, fats and minerals can be quickly dissolved. Granules can be provided.

まず、本発明の造粒顆粒を得るために用いられる食品原料について説明する。   First, the food raw material used in order to obtain the granulated granule of this invention is demonstrated.

[食品原料]
本発明で用いられる油脂としては、食品に利用可能な油脂であればよく、特に制限されるものではない。例えば、大豆、トウモロコシ、菜種、えごま、シソ、オリーブ、米、ココナッツ等を由来とする植物性油脂、家畜の乳、卵及び魚由来の動物性油脂、中鎖脂肪酸などが挙げられるが、特に大豆、トウモロコシ、菜種等の植物性油脂が好ましい。これらの油脂は、単独で用いてもよく、2種以上を併用してもよい。
[Food ingredients]
The fats and oils used in the present invention are not particularly limited as long as they are usable for foods. Examples include vegetable oils derived from soybeans, corn, rapeseed, sesame seeds, perilla, olives, rice, coconuts, animal oils derived from domestic milk, eggs and fish, medium chain fatty acids, etc. Vegetable oils such as corn and rapeseed are preferred. These fats and oils may be used independently and may use 2 or more types together.

本発明で用いられる乳化剤としては、食品に利用可能な乳化剤であればよく、特に制限されるものではないが、好ましくはHLB値7〜16、より好ましくはHLB値8〜11の各種乳化剤が用いられ、例えばショ糖脂肪酸エステル、酵素分解レシチン、有機酸モノグリセリド、ポリグリセリン脂肪酸エステルなどが挙げられる。これらの乳化剤は、単独で用いてもよく、2種以上を併用してもよい。   The emulsifier used in the present invention is not particularly limited as long as it is an emulsifier that can be used in foods, but various emulsifiers having an HLB value of 7 to 16, more preferably an HLB value of 8 to 11 are used. Examples thereof include sucrose fatty acid ester, enzymatically decomposed lecithin, organic acid monoglyceride, polyglycerin fatty acid ester and the like. These emulsifiers may be used independently and may use 2 or more types together.

本発明においては、上記の油脂及び乳化剤以外にも、その造粒顆粒に各種の食品原料を配合することに、特に制限はない。   In the present invention, in addition to the oils and fats and emulsifiers described above, there are no particular limitations on blending various food materials into the granulated granules.

例えば、糖質として、デキストリン、デンプン、加工デンプン、オリゴ糖、二糖類、単糖類、糖アルコール、増粘多糖類、機能性多糖類などが挙げられる。   Examples of the saccharide include dextrin, starch, modified starch, oligosaccharide, disaccharide, monosaccharide, sugar alcohol, thickening polysaccharide, and functional polysaccharide.

また、タンパク質として、乳たんぱく質、ホエイたんぱく質、カゼイン、大豆たんぱく質及びそのペプチド類、コラーゲンペプチド、卵白ペプチドなどが挙げられる。   Examples of the protein include milk protein, whey protein, casein, soybean protein and peptides thereof, collagen peptide, egg white peptide and the like.

また、ミネラル分として、ナトリウム、カリウム、カルシウム、マグネシウム、鉄分、その他微量元素などが挙げられる。   Examples of the mineral content include sodium, potassium, calcium, magnesium, iron, and other trace elements.

また、ペプチド・アミノ酸類、ビタミン類、ポリフェノール類、食物繊維、甘味料、呈味料、香料等の栄養成分及び食品添加物を、適宜配合することができる。   In addition, nutritional components such as peptides and amino acids, vitamins, polyphenols, dietary fiber, sweeteners, flavoring agents, and flavors, and food additives can be appropriately blended.

これらの食品原料は、後述するように、真空乾燥粉末の原料としても、また、それに追加される造粒材料の原料としても用いることができる。   As will be described later, these food raw materials can be used as a raw material for a vacuum-dried powder or as a raw material for a granulating material added thereto.

本発明の造粒顆粒は、油脂と乳化剤とを含有する真空乾燥粉末を、20質量%〜100質量%の割合で配合して流動造粒してなるものである。   The granulated granule of the present invention is obtained by blending a vacuum-dried powder containing fats and oils and an emulsifier at a ratio of 20% by mass to 100% by mass and subjecting it to fluid granulation.

以下には真空乾燥粉末について説明する。   The vacuum dried powder will be described below.

[真空乾燥粉末]
真空乾燥粉末を調製するために、上述したような油脂及び乳化剤を含有し、さらに上述したようなその他の食品原料を適宜含有する真空乾燥材料を準備する。
[Vacuum dry powder]
In order to prepare a vacuum-dried powder, a vacuum-dried material containing the above-described fats and emulsifiers and further containing other food materials as described above is prepared.

上記真空乾燥材料は、得られる真空乾燥粉末中での含有量に換算して、油脂を5質量%〜25質量%含有することが好ましく、10質量%〜15質量%含有することがより好ましい。油脂は、食品素材の各成分の混合、分散、乳化などを助けるので、これにより溶解適性の向上に寄与できる真空乾燥粉末を得ることができる。なお、油脂の含有量が多すぎると、他の栄養成分等の配合量が相対的に確保できないので、好ましくない。   The vacuum dry material preferably contains 5% by mass to 25% by mass of oil and fat, more preferably 10% by mass to 15% by mass in terms of the content in the obtained vacuum dry powder. Oils and fats help to mix, disperse, emulsify, and the like of each component of the food material, so that a vacuum-dried powder that can contribute to improving dissolution suitability can be obtained. In addition, when there is too much content of fats and oils, since compounding quantities, such as another nutrient component, cannot be ensured relatively, it is unpreferable.

上記真空乾燥材料は、得られる真空乾燥粉末中での含有量に換算して、乳化剤を0.5質量%〜2.75質量%含有することが好ましく、1.0質量%〜1.5質量%含有することがより好ましい。乳化剤は、上記油脂とともに、食品素材の各成分の混合、分散、乳化などを助けるので、これにより溶解適性の向上に寄与できる真空乾燥粉末を得ることができる。なお、乳化剤の含有量が多すぎると、風味、呈味に影響があるので、好ましくない。   The vacuum-dried material preferably contains 0.5% by mass to 2.75% by mass of an emulsifier in terms of the content in the obtained vacuum-dried powder, and 1.0% by mass to 1.5% by mass. % Content is more preferable. The emulsifier helps the mixing, dispersion, emulsification, and the like of the ingredients of the food material together with the above fats and oils, thereby obtaining a vacuum-dried powder that can contribute to improvement in solubility. In addition, when there is too much content of an emulsifier, since it has influence on flavor and taste, it is not preferable.

上記真空乾燥材料は、得られる真空乾燥粉末中での含有量に換算して、デキストリン、オリゴ糖、ショ糖等の糖質を45質量%〜75質量%含有することが好ましく、50質量%〜70質量%含有することがより好ましい。これによれば、これらの糖質が真空乾燥の基材として機能するので、更により溶解適性の向上に寄与できる真空乾燥粉末を得ることができる。なお、このような基材の含有量が多すぎると、他の栄養成分等の配合量が相対的に確保できないので、好ましくない。   The vacuum-dried material preferably contains 45% to 75% by weight of carbohydrates such as dextrin, oligosaccharide, and sucrose in terms of the content in the obtained vacuum-dried powder, and 50% to It is more preferable to contain 70 mass%. According to this, since these saccharides function as a substrate for vacuum drying, it is possible to obtain a vacuum-dried powder that can further contribute to the improvement of dissolution suitability. In addition, when there is too much content of such a base material, since the compounding quantity of another nutrient component etc. cannot be ensured relatively, it is unpreferable.

上記真空乾燥材料の水分含量は、適宜所定の水分含量の食品原料を用いたり、加水したりして、真空乾燥に適した水分含量に調整される。その際、温水を加水してもよく、水分調整後に殺菌またはそれに準ずる方法で処理してもよい。また、真空乾燥時の起泡を低減するため、シリコーン、アルコール等の消泡剤を添加してもよい。真空乾燥材料中の水分含量は、5質量%以下であることが好ましく、3質量%以下であることがより好ましい。   The moisture content of the vacuum-dried material is adjusted to a moisture content suitable for vacuum drying by appropriately using or adding water to a food material having a predetermined moisture content. At that time, warm water may be added, and after moisture adjustment, it may be sterilized or treated by a method equivalent thereto. In order to reduce foaming during vacuum drying, an antifoaming agent such as silicone or alcohol may be added. The moisture content in the vacuum-dried material is preferably 5% by mass or less, and more preferably 3% by mass or less.

本発明においては、上記真空乾燥材料に均質化処理を施すことが好ましい。これにより、上記油脂及び乳化剤による、食品素材の各成分の混合、分散、乳化などを助ける効果をより高めることができ、更により溶解適性の向上に寄与できる真空乾燥粉末を得ることができる。均質化処理は、当業者に周知の方法並びに装置によって、例えばホモジナイザーなどを用いて行なうことができるが、油脂を多く含む場合には、乳化をより完全にするため10MPa〜50MPaの高圧処理を伴うホモジナイザーで行なうことが好ましく、15MPa〜30MPaの高圧処理で行なうことがより好ましい。   In the present invention, it is preferable to homogenize the vacuum-dried material. Thereby, the effect which helps the mixing, dispersion | distribution, emulsification, etc. of each component of a foodstuff by the said fats and oils and an emulsifier can be heightened more, and the vacuum-dried powder which can contribute to the improvement of solubility property more can be obtained. The homogenization treatment can be performed by a method and apparatus well known to those skilled in the art, for example, using a homogenizer or the like. It is preferable to carry out with a homogenizer, and it is more preferred to carry out with a high pressure treatment of 15 MPa to 30 MPa.

真空乾燥は、当業者に周知の方法並びに装置によって行うことができる。例えば、連続式ベルト乾燥装置(CVD)、真空ドラム式乾燥装置(VDD)、凍結乾燥(FD)などが好ましく採用される。   Vacuum drying can be performed by methods and apparatus well known to those skilled in the art. For example, a continuous belt dryer (CVD), a vacuum drum dryer (VDD), freeze drying (FD), etc. are preferably employed.

真空乾燥によれば、パフ状、燐片状の乾燥物が得られるので、それを適宜解砕することで、粉末状にして、真空乾燥粉末とすることができる。   According to vacuum drying, a puff-like or flake-like dried product is obtained. By crushing it appropriately, it can be made into a powder and made into a vacuum-dried powder.

本発明においては、真空乾燥後に得られた乾燥物を解砕し、整粒して、その全体の70質量%以上が、JIS規格による標準篩を用いて12メッシュ(目開き1.42mm)をパスし、かつ、80メッシュ(目開き182μm)にオンするものを調製することが好ましく、その全体の80質量%以上が12メッシュ(目開き1.42mm)をパスし、かつ、80メッシュ(目開き182μm)にオンするものを調製することがより好ましく、その全体の90質量%以上が12メッシュ(目開き1.42mm)をパスし、かつ、80メッシュ(目開き182μm)にオンするものを調製することが最も好ましい。これによれば、より溶解適性の向上に寄与できる真空乾燥粉末となすことができる。   In the present invention, the dried product obtained after vacuum drying is crushed and sized, and 70% by mass or more of the total is 12 mesh (aperture 1.42 mm) using a standard sieve according to JIS standards. It is preferable to prepare a material that passes and turns on 80 mesh (mesh opening 182 μm), and 80% by mass or more of the whole passes 12 mesh (mesh opening 1.42 mm) and 80 mesh (mesh opening). It is more preferable to prepare a material that turns on at an opening of 182 μm), and 90% by mass or more of the whole passes through 12 mesh (aperture 1.42 mm) and turns on at 80 mesh (aperture 182 μm). Most preferably it is prepared. According to this, it can be set as the vacuum-dried powder which can contribute to the improvement of solubility property more.

解砕及び整粒の方法に特に制限はなく、当業者に周知の方法並びに装置によって行うことができる。   There is no restriction | limiting in particular in the method of crushing and sizing, It can carry out by the method and apparatus well-known to those skilled in the art.

以下には造粒加工について説明する。   The granulation process will be described below.

[造粒加工]
造粒加工のため、上記のようにして得られた真空乾燥粉末を20質量%〜100質量%、より好ましくは25質量%〜100質量%、更により好ましくは30質量%〜100質量%の割合で有し、さらに適宜その他の食品原料を含有する造粒材料を準備する。造粒材料中の真空乾燥粉末が20質量%未満であると、溶解適性の向上に寄与する効果に乏しいので、好ましくない。一方で、溶解適性に寄与する真空乾燥粉末の割合は、造粒顆粒全体の少なくとも20質量%あればよいので、真空乾燥工程の製造コストを抑えたり、真空乾燥に適さない食品素材を造粒時に追加したりしたい場合には、真空乾燥粉末の割合を、例えば80質量%以下、より典型的には50質量%以下としてもよい。
[Granulation processing]
For granulation, the vacuum-dried powder obtained as described above is 20% by mass to 100% by mass, more preferably 25% by mass to 100% by mass, and still more preferably 30% by mass to 100% by mass. And a granulating material containing other food ingredients as appropriate is prepared. When the vacuum-dried powder in the granulated material is less than 20% by mass, the effect of contributing to improvement in dissolution suitability is poor, which is not preferable. On the other hand, the proportion of the vacuum-dried powder that contributes to dissolution suitability should be at least 20% by mass of the entire granulated granule. Therefore, the manufacturing cost of the vacuum drying process can be reduced, or a food material that is not suitable for vacuum drying is granulated. For example, the ratio of the vacuum-dried powder may be 80% by mass or less, more typically 50% by mass or less.

真空乾燥粉末に追加して、造粒材料とする食品素材としては、上述した各種の食品原料を用いることができる。この場合、真空乾燥粉末の調製に用いた食品素材以外のものを用いてもよく、同じものを用いてもよい。すなわち、得られる造粒顆粒の一部又は全部が上記真空乾燥粉末で構成され、造粒時に追加した食品素材でその残部が構成されるようにすればよい。   In addition to the vacuum-dried powder, the above-described various food materials can be used as a food material that is used as a granulating material. In this case, a material other than the food material used for the preparation of the vacuum-dried powder may be used, or the same material may be used. That is, a part or all of the granulated granules to be obtained may be composed of the vacuum dried powder, and the rest may be composed of the food material added during granulation.

造粒加工の際には、得られる造粒顆粒中での含有量に換算して、デキストリン、オリゴ糖、ショ糖等の糖質を10質量%〜45質量%を使用することが好ましく、15質量%〜40質量%を使用することがより好ましい。これによれば、これらの糖質が造粒顆粒の基材として機能するので、更により溶解適性の向上した造粒顆粒を得ることができる。なお、この基材の含有量は、真空乾燥粉末に含まれるものと、真空乾燥粉末に追加して造粒材料とする食品素材に含まれるものとを合算した含有量である。このような基材の含有量が多すぎると、他の栄養成分等の配合量が相対的に確保できないので、好ましくない。   In the granulation process, it is preferable to use 10% by mass to 45% by mass of saccharides such as dextrin, oligosaccharide, and sucrose in terms of the content in the obtained granulated granule, It is more preferable to use mass% to 40 mass%. According to this, since these saccharides function as a base material for the granulated granule, it is possible to obtain a granulated granule further improved in solubility. In addition, content of this base material is content which added what is contained in the vacuum-dried powder, and what is contained in the foodstuff raw material used as a granulation material in addition to vacuum-dried powder. When there is too much content of such a base material, since the compounding quantities, such as another nutrient component, cannot be ensured relatively, it is unpreferable.

また、真空乾燥粉末にはタンパク質を含有する食品原料を配合せずに、この造粒加工の際に、得られる造粒顆粒中での含有量に換算して、タンパク質を5質量%〜30質量%使用することが好ましく、10質量%〜25質量%使用することがより好ましい。これによれば、タンパク質の種類によっては、それを真空乾燥に処すると分散性、湿潤性に乏しくなるので、これを回避して、更により溶解適性の向上した造粒顆粒を得ることができる。   In addition, the vacuum-dried powder does not contain a protein-containing food material, and is converted into the content in the granulated granules obtained during the granulation process, so that the protein content is 5 mass% to 30 mass%. % Is preferably used, and more preferably 10% by mass to 25% by mass. According to this, depending on the type of protein, when it is subjected to vacuum drying, the dispersibility and wettability become poor, and this can be avoided, and granulated granules with further improved solubility can be obtained.

造粒手段としては、空気で流動化させた粉体層に水やバインダー液をスプレーして凝集造粒する、流動造粒の方式が採用される。これによれば、上記真空乾燥粉末を、その粉末状のまま造粒に供することができる。そのバインダー液としては、グァーガム、キサンタンガム等の増粘多糖類、デキストリン、デンプン、単糖類、ゼラチン、乳化剤を含む油脂等の溶液が挙げられる。なお、このバインダー液の使用量は少量であり、得られる造粒顆粒100質量部に対して、固形分換算にして0.01〜0.10質量部程度であり、本発明による造粒顆粒の成分構成にほとんど影響を与えない。   As the granulating means, a fluidized granulation method is adopted, in which water or a binder liquid is sprayed on the powder layer fluidized with air to perform aggregation granulation. According to this, the said vacuum dry powder can be used for granulation with the powder form. Examples of the binder liquid include solutions of thickening polysaccharides such as guar gum and xanthan gum, dextrins, starches, monosaccharides, gelatin, and fats and oils containing emulsifiers. In addition, the usage-amount of this binder liquid is a small amount, and is about 0.01-0.10 mass part in conversion of solid content with respect to 100 mass parts of the granulated granules to be obtained. Almost no influence on the composition of ingredients.

本発明の造粒顆粒は、例えば、ダイエット粉末飲料、プロテイン高配合の粉末飲料、栄養ドリンク用粉末などの用途に好適に用いられる。これによれば、従来、比較的大量(例えば8倍量)の水に対し、シェイクにより分散させていた方式を、少量(例えば2倍量)の水に加えてスプーンで撹拌するだけで簡単に溶かす方式にできるので、摂取する者の負担を軽減することが可能となる。また、溶解適性に寄与する真空乾燥粉末の割合は、造粒顆粒全体の少なくとも20質量%あればよいので、製造コストを抑えることが可能となる。   The granulated granule of the present invention is suitably used for applications such as diet powder drinks, powder drinks with high protein content, and powders for energy drinks. According to this, a method that has been dispersed by shaking for a relatively large amount (for example, 8 times the amount of water) in the past is simply added to a small amount (for example, a double amount) of water and stirred with a spoon. Since it can be melted, it is possible to reduce the burden on those who take it. Moreover, since the ratio of the vacuum-dried powder that contributes to dissolution suitability should be at least 20% by mass of the entire granulated granule, the production cost can be suppressed.

また、従来、実用性の面から液体の形態で提供されていた医療用濃厚流動食についても、溶解適性が改善されたことにより、顆粒の形態で提供することが可能となる。これにより、賞味期限の延長、重量の軽量化による輸送コストの軽減、水中で不安定な機能性食品成分の配合などが可能となる。   Further, a concentrated liquid food for medical use that has been conventionally provided in liquid form from the viewpoint of practicality can also be provided in the form of granules due to improved dissolution suitability. This makes it possible to extend the shelf life, reduce transportation costs by reducing the weight, and blend functional food ingredients that are unstable in water.

このような用途に適用する場合、その造粒顆粒中にタンパク質を5〜30質量%含有することが好ましく、10〜25質量%含有することがより好ましい。また、造粒顆粒中に糖質を10質量%〜45質量%含有することが好ましく、15質量%〜40質量%含有することがより好ましい。   When applying to such a use, it is preferable to contain 5-30 mass% of protein in the granulated granule, and it is more preferable to contain 10-25 mass%. Moreover, it is preferable to contain 10 mass%-45 mass% of carbohydrates in a granulated granule, and it is more preferable to contain 15 mass%-40 mass%.

以下に実施例を挙げて本発明について更に具体的に説明する。なお、これらの実施例は本発明の範囲を限定するものではない。   Hereinafter, the present invention will be described in more detail with reference to examples. In addition, these Examples do not limit the scope of the present invention.

<試験例1>
下記表1に示す配合で造粒顆粒を調製した。
<Test Example 1>
Granulated granules were prepared with the formulation shown in Table 1 below.

具体的には、表1中のA欄に示す配合の原材料100質量部をおよそ40〜50質量部の水に加え、60℃にて20分間攪拌し、ホモジナイザー(「APVホモジナイザー」、日本APV株式会社)にて均質化処理を施した。これを真空乾燥装置(「真空ベルト乾燥機」株式会社日阪製作所)に供し、得られた乾燥物を家庭用ミキサーで解砕し、ステンレス製の篩により、全体の70質量%が12メッシュ(目開き1.42mm)をパスし、かつ、80メッシュ(目開き182μm)にオンするように整粒して、真空乾燥粉末を得た。   Specifically, 100 parts by mass of the raw material blended in the column A in Table 1 is added to approximately 40 to 50 parts by mass of water, and stirred at 60 ° C. for 20 minutes, followed by homogenizer (“APV homogenizer”, Japan APV stock). Company). This was subjected to a vacuum drying apparatus (“Vacuum Belt Dryer”, Nisaka Manufacturing Co., Ltd.), and the resulting dried product was pulverized with a home-use mixer. The particle size was adjusted so as to pass through a mesh (1.42 mm) and turn on to 80 mesh (mesh 182 μm) to obtain a vacuum-dried powder.

次いで、表1中のB欄に示す配合で、この真空乾燥粉末を各割合で用いた原材料を、流動層造粒装置(「FLOW COATER MULTI」、株式会社大川原製作所)に供して造粒した。その際、バインダー液として0.5質量%キサンタンガム溶液を、流動層造粒装置に供する粉体100質量部に対して16質量部(固形分換算にして0.08質量部)用いた。   Next, the raw materials using the vacuum-dried powders in the proportions shown in the column B in Table 1 were granulated by using a fluidized bed granulator (“FLOW COATER MULTI”, Okawara Seisakusho Co., Ltd.). In that case, 0.5 mass% xanthan gum solution as a binder liquid was used 16 mass parts (0.08 mass part in conversion of solid content) with respect to 100 mass parts of powder used for a fluid bed granulator.

以下には、調製した試料1〜試料6の特徴をまとめた。   The characteristics of the prepared samples 1 to 6 are summarized below.

[試料1]
油脂を5質量%、乳化剤を0.5質量%含有する真空乾燥粉末を、流動層造粒装置に供する粉体に100質量%の割合で配合した。
[Sample 1]
A vacuum-dried powder containing 5% by mass of fats and oils and 0.5% by mass of an emulsifier was blended in a proportion of 100% by mass with the powder used for the fluidized bed granulator.

[試料2]
油脂を10質量%、乳化剤を1質量%含有する真空乾燥粉末を、流動層造粒装置に供する粉体に50質量%の割合で配合した。
[Sample 2]
A vacuum-dried powder containing 10% by mass of fat and oil and 1% by mass of an emulsifier was blended in a proportion of 50% by mass with the powder to be used in the fluidized bed granulator.

[試料3]
油脂を15質量%、乳化剤を1.5質量%含有する真空乾燥粉末を、流動層造粒装置に供する粉体に30質量%の割合で配合した。
[Sample 3]
A vacuum-dried powder containing 15% by mass of fat and oil and 1.5% by mass of an emulsifier was blended in a proportion of 30% by mass with the powder used for the fluidized bed granulator.

[試料4]
油脂を25質量%、乳化剤を2.5質量%含有する真空乾燥粉末を、流動層造粒装置に供する粉体に20質量%の割合で配合した。
[Sample 4]
A vacuum-dried powder containing 25% by mass of fats and oils and 2.5% by mass of an emulsifier was blended in a proportion of 20% by mass with the powder used for the fluidized bed granulator.

[試料5]
油脂を27.5質量%、乳化剤を2.75質量%含有する真空乾燥粉末を、流動層造粒装置に供する粉体に10質量%の割合で配合した。
[Sample 5]
A vacuum-dried powder containing 27.5% by mass of fat and oil and 2.75% by mass of an emulsifier was blended at a rate of 10% by mass with the powder to be used in the fluidized bed granulator.

[試料6]
真空乾燥粉末とせずにすべての原材料を流動層造粒装置にそのまま供した。その際、油脂としては粉末油脂(油脂55%質量含有)を9質量%の割合で配合した。
[Sample 6]
All raw materials were used as they were in a fluidized bed granulator without vacuum drying powder. At that time, powdered fats and oils (containing 55% by weight of fats and oils) were blended at a ratio of 9% by weight as the fats and oils.

試料1〜試料6について、水への沈降性と分散性を評価した。具体的には、25℃の水に5質量%となるように顆粒を添加し、30秒間観察して、自重で沈み、白濁するまでの時間を測定し、その後スパーテルで撹拌しながら(2回転/秒)、白濁が消えて水に溶け込むまでの時間を測定した。   Samples 1 to 6 were evaluated for water sedimentation and dispersibility. Specifically, granules are added to water at 25 ° C. so as to be 5% by mass, observed for 30 seconds, measured for the time until it sinks under its own weight and becomes cloudy, and then stirred with a spatula (two rotations) / Second), the time until the white turbidity disappeared and dissolved in water was measured.

評価は、下記表2に示す基準に基づいて沈降性と分散性とを評価したうえ、その総合評価をスコア化した。結果を下記表3に示す。   Evaluation evaluated the sedimentation property and dispersibility based on the reference | standard shown in following Table 2, and scored the comprehensive evaluation. The results are shown in Table 3 below.

表3に示すように、油脂と乳化剤とを含有する真空乾燥粉末を、造粒時に100質量%の割合で配合した試料1、その割合が50質量%である試料2、その割合が30質量%である試料3、その割合が20質量%である試料4は、それぞれ良好な水への沈降性、分散性を示した。特に試料1〜試料3の結果が顕著に優れていた。一方、油脂と乳化剤とを含有する真空乾燥粉末を、造粒時に10質量%の割合で配合した試料5や、真空乾燥粉末を配合しないで造粒した試料6では、水への沈降性や分散性が悪かった。よって、造粒する原材料中に、油脂と乳化剤とを含有する真空乾燥粉末の割合が多いほど、水への沈降性、分散性に優れていることが明らかとなった。また、その真空乾燥粉末を20〜30質量%程度の比較的低い割合で配合した場合でも、水への沈降性と分散性の改善効果が得られることが明らかとなった。   As shown in Table 3, the sample 1 which mix | blended the vacuum-drying powder containing fats and oils and an emulsifier in the ratio of 100 mass% at the time of granulation, the sample 2 whose ratio is 50 mass%, and the ratio is 30 mass% Sample 3 and Sample 4 having a ratio of 20% by mass showed good sedimentation properties and dispersibility in water, respectively. In particular, the results of Samples 1 to 3 were remarkably excellent. On the other hand, in sample 5 in which a vacuum-dried powder containing fats and oils and an emulsifier is blended at a ratio of 10% by mass at the time of granulation, and in sample 6 granulated without blending in a vacuum-dried powder, water sedimentation and dispersion The nature was bad. Therefore, it was clarified that the higher the ratio of the vacuum-dried powder containing fats and oils and emulsifiers in the raw material to be granulated, the better the water settling and dispersibility. Moreover, even when the vacuum-dried powder was blended at a relatively low ratio of about 20 to 30% by mass, it became clear that the effect of improving the sedimentation property and dispersibility in water was obtained.

<試験例2>
試験例1と同様にして、下記表4に示す配合で、造粒顆粒を調製した。なお、造粒のバインダー液としては、0.5質量%グァーガム溶液を用いた。
<Test Example 2>
In the same manner as in Test Example 1, granulated granules were prepared with the composition shown in Table 4 below. In addition, 0.5 mass% guar gum solution was used as the binder liquid for granulation.

以下には、調製した試料7〜試料10の特徴をまとめた。   The characteristics of the prepared samples 7 to 10 are summarized below.

[試料7]
油脂を5質量%、乳化剤を0.5質量%含有する真空乾燥粉末を、流動層造粒装置に供する粉体に20質量%の割合で配合した。
[Sample 7]
A vacuum-dried powder containing 5% by mass of fat and oil and 0.5% by mass of an emulsifier was blended in a proportion of 20% by mass with the powder used for the fluidized bed granulator.

[試料8]
油脂を25質量%、乳化剤を2.5質量%含有する真空乾燥粉末を、流動層造粒装置に供する粉体に100質量%の割合で配合した。
[Sample 8]
A vacuum-dried powder containing 25% by mass of fat and oil and 2.5% by mass of an emulsifier was blended in a ratio of 100% by mass with the powder to be used in the fluidized bed granulator.

[試料9]
油脂を30質量%、乳化剤を3質量%含有する真空乾燥粉末を、流動層造粒装置に供する粉体に30質量%の割合で配合した。
[Sample 9]
A vacuum-dried powder containing 30% by mass of fat and oil and 3% by mass of an emulsifier was blended in a proportion of 30% by mass with the powder to be used in the fluidized bed granulator.

[試料10]
油脂及び乳化剤を含有しない真空乾燥粉末を、流動層造粒装置に供する粉体に30質量%の割合で配合した。
[Sample 10]
A vacuum-dried powder that does not contain fats and oils and an emulsifier was blended in a proportion of 30% by mass with the powder to be used in the fluidized bed granulator.

試料7〜試料10について、試験例1と同様にして、水への沈降性と分散性を評価した。結果を下記表5に示す。   Samples 7 to 10 were evaluated for water sedimentation and dispersibility in the same manner as in Test Example 1. The results are shown in Table 5 below.

表5に示すように、油脂と乳化剤とを含有しその油脂の含有量が5質量%である真空乾燥粉末を、造粒時に20質量%の割合で配合した試料7と、油脂と乳化剤とを含有しその油脂の含有量が25質量%である真空乾燥粉末を、造粒時に100質量%の割合で配合した試料8は、それぞれ良好な水への沈降性、分散性を示した。一方、油脂と乳化剤とを含有しその油脂の含有量が30質量%である真空乾燥粉末を、造粒時に30質量%の割合で配合した試料9では、総合的には良好な溶解適性が得られたものの、試料7,8に比べて、水への沈降性がやや悪く、総合スコアでやや劣る結果となった。この理由は、真空乾燥粉末中に油脂の含有量が多すぎたためと考えられた。また、デキストリンとショ糖と塩類(ミネラル分)を含有し、油脂と乳化剤とを配合せずに調製した真空乾燥粉末を、造粒時に30質量%の割合で配合した試料10では沈降性は良いものの分散性が悪かった。よって、真空乾燥粉末により、水への沈降性と分散性の改善効果を充分に付与するためには、その真空乾燥粉末中に油脂と乳化剤とを含有する必要があることが明らかとなった。   As shown in Table 5, a sample 7 containing a fat and oil and an emulsifier and containing 5% by mass of the fat and oil in a proportion of 20% by mass at the time of granulation, and the oil and fat and the emulsifier Sample 8 containing a vacuum-dried powder containing 25% by mass of fat and oil in a proportion of 100% by mass during granulation showed good sedimentation and dispersibility in water. On the other hand, sample 9 containing a fat and oil and an emulsifier and containing 30% by mass of the fat and oil in a proportion of 30% by mass at the time of granulation has an overall good dissolution suitability. However, compared with the samples 7 and 8, the sedimentation property in water was slightly poor, and the overall score was slightly inferior. The reason for this was considered that the content of fats and oils was too much in the vacuum-dried powder. In addition, sample 10 containing dextrin, sucrose and salts (mineral content) and prepared without blending oil and fat and emulsifier in a proportion of 30% by mass at the time of granulation has good sedimentation. The dispersibility of things was bad. Therefore, it has been clarified that the vacuum dried powder needs to contain fats and oils and an emulsifier in order to sufficiently impart the effect of improving the sedimentation property and dispersibility in water.

<試験例3>
試験例1と同様にして、下記表6に示す配合で、造粒顆粒を調製した。その際、真空乾燥粉末の整粒の程度を、下記表6に示すように替えた。
<Test Example 3>
In the same manner as in Test Example 1, granulated granules were prepared with the formulation shown in Table 6 below. At that time, the degree of sizing of the vacuum-dried powder was changed as shown in Table 6 below.

以下には、調製した試料11〜試料13の特徴をまとめた。   The characteristics of the prepared samples 11 to 13 are summarized below.

[試料11]
油脂を15質量%、乳化剤を1.5質量%含有し、その全体の70質量%が12メッシュ(目開き1.42mm)をパスし、かつ、80メッシュ(目開き182μm)にオンするように整粒した、真空乾燥粉末を調製した。これを、流動層造粒装置に供する粉体に30質量%の割合で配合した。
[Sample 11]
It contains 15% by mass of fat and oil and 1.5% by mass of emulsifier, and 70% by mass of the total passes 12 mesh (aperture 1.42 mm) and is turned on to 80 mesh (aperture 182 μm). A sized vacuum-dried powder was prepared. This was mix | blended in the ratio of 30 mass% to the powder with which it uses for a fluid bed granulator.

[試料12]
油脂を15質量%、乳化剤を1.5質量%含有し、その全体の90質量%が12メッシュ(目開き1.42mm)をパスし、かつ、80メッシュ(目開き182μm)にオンするように整粒した、真空乾燥粉末を調製した。これを、流動層造粒装置に供する粉体に30質量%の割合で配合した。
[Sample 12]
It contains 15% by mass of fat and oil and 1.5% by mass of emulsifier, and 90% by mass of the total passes 12 mesh (aperture 1.42 mm) and turns on to 80 mesh (aperture 182 μm). A sized vacuum-dried powder was prepared. This was mix | blended in the ratio of 30 mass% to the powder with which it uses for a fluid bed granulator.

[試料13]
油脂を15質量%、乳化剤を1.5質量%含有し、その全体の40質量%が12メッシュ(目開き1.42mm)をパスし、かつ、80メッシュ(目開き182μm)にオンし、なお且つその全体の60質量%が80メッシュ(目開き182μm)をパスするように整粒した、真空乾燥粉末を調製した。これを、流動層造粒装置に供する粉体に30質量%の割合で配合した。
[Sample 13]
Contains 15% by mass of fat and oil and 1.5% by mass of emulsifier, and 40% by mass of the oil passes 12 mesh (aperture 1.42 mm) and turns on to 80 mesh (aperture 182 μm). A vacuum-dried powder was prepared so that 60% by mass of the total particle size passed 80 mesh (mesh opening 182 μm). This was mix | blended in the ratio of 30 mass% to the powder with which it uses for a fluid bed granulator.

試料11〜試料13について、試験例1と同様にして、水への沈降性と分散性を評価した。結果を下記表7に示す。   Samples 11 to 13 were evaluated for water sedimentation and dispersibility in the same manner as in Test Example 1. The results are shown in Table 7 below.

表7に示すように、油脂と乳化剤とを含有する真空乾燥粉末であって、その全体の70質量%が12メッシュ(目開き1.42mm)をパスし、かつ、80メッシュ(目開き182μm)にオンするように整粒した該真空乾燥粉末を、造粒時に30質量%の割合で配合した試料11と、油脂と乳化剤とを含有する真空乾燥粉末であって、その全体の90質量%が12メッシュ(目開き1.42mm)をパスし、かつ、80メッシュ(目開き182μm)にオンするように整粒した該真空乾燥粉末を、造粒時に30質量%の割合で配合した試料12は、それぞれ良好な水への沈降性、分散性を示した。特に試料12の結果が顕著に優れていた。一方、油脂と乳化剤とを含有する真空乾燥粉末であって、その全体の40質量%が12メッシュ(目開き1.42mm)をパスし、かつ、80メッシュ(目開き182μm)にオンし、なお且つその全体の60質量%が80メッシュ(目開き182μm)にパスするように整粒した該真空乾燥粉末を、造粒時に30質量%の割合で配合した試料13では、総合的には良好な溶解適性が得られたものの、試料11,12に比べて、水への沈降性がやや悪く、総合スコアでやや劣る結果となった。よって、真空乾燥粉末の粒度が所定の範囲に揃えられていると、水への沈降性と分散性の改善効果がより高くなることが明らかとなった。   As shown in Table 7, it is a vacuum-dried powder containing fats and oils and an emulsifier, and 70% by mass of the whole passes 12 mesh (aperture 1.42 mm) and 80 mesh (aperture 182 μm) The vacuum-dried powder containing the sample 11 blended at a ratio of 30% by mass at the time of granulation, the oil and fat, and the emulsifier, and 90% by mass of the total is Sample 12 was prepared by blending the vacuum-dried powder that passed through 12 mesh (aperture 1.42 mm) and sized so as to be turned on to 80 mesh (aperture 182 μm) at the rate of 30% by mass during granulation. Each showed good sedimentation and dispersibility in water. In particular, the result of Sample 12 was remarkably excellent. On the other hand, it is a vacuum-dried powder containing fats and oils and an emulsifier, and 40% by mass of the powder passes 12 mesh (aperture 1.42 mm) and is turned on to 80 mesh (aperture 182 μm). In addition, Sample 13 in which 60% by mass of the whole was sized so that it passed 80 mesh (mesh opening 182 μm) was blended at a rate of 30% by mass at the time of granulation was good overall. Although dissolution suitability was obtained, compared with Samples 11 and 12, the sedimentation property in water was slightly poor, and the overall score was slightly inferior. Therefore, it has been clarified that when the particle size of the vacuum-dried powder is set within a predetermined range, the effect of improving the sedimentation property and dispersibility in water becomes higher.

<製造例>
下記表8に示す配合でダイエットドリンク粉末を調製した。
<Production example>
Diet drink powder was prepared according to the formulation shown in Table 8 below.

具体的には、表8中のA欄に示す配合の原材料100質量部をおよそ40〜50質量部の水に加え、60℃にて20分間攪拌し、ホモジナイザー(「APVホモジナイザー」、日本APV株式会社)にて均質化処理を施した。これを真空乾燥装置(「真空ベルト乾燥機」、株式会社日阪製作所)に供し、得られた乾燥物を家庭用ミキサーで解砕し、ステンレス製の篩により、全体の70質量%が12メッシュ(目開き1.42mm)をパスし、かつ、80メッシュ(目開き182μm)にオンするように整粒して、真空乾燥粉末を得た。   Specifically, 100 parts by mass of the raw material having the composition shown in the column A in Table 8 is added to approximately 40 to 50 parts by mass of water and stirred at 60 ° C. for 20 minutes, and then homogenizer (“APV homogenizer”, Japan APV Co., Ltd.) Company). This was subjected to a vacuum drying apparatus (“Vacuum Belt Dryer”, Nisaka Manufacturing Co., Ltd.), and the resulting dried product was pulverized with a household mixer, and a total of 70% by mass was 12 mesh by a stainless steel sieve. The particles were sized so as to pass (mesh 1.42 mm) and turn on to 80 mesh (mesh 182 μm) to obtain a vacuum-dried powder.

次いで、この真空乾燥粉末を、表1中のB欄に示す配合で用いた原材料を、流動層造粒装置(「FLOW COATER MULTI」、株式会社大川原製作所)に供して造粒した。その際、バインダー液として0.5質量%キサンタンガム溶液を、流動層造粒装置に供する粉体100質量部に対して1.6質量部(固形分換算にして0.08質量部)用いた。   Next, the raw materials used in the composition shown in column B of Table 1 were granulated by using the vacuum-dried powder in a fluidized bed granulator (“FLOW COATER MULTI”, Okawara Seisakusho Co., Ltd.). In that case, 0.5 mass% xanthan gum solution as a binder liquid was used 1.6 mass parts (0.08 mass part in conversion of solid content) with respect to 100 mass parts of the powder used for a fluid bed granulator.

得られたダイエットドリンク粉末の20gを、コップに入れた200mLの水に添加したところ、その粉末はすぐに沈降して、スプーンで10回ほどかき混ぜて30秒程度で完全に溶解させることができた。このダイエットドリンクは、風味よく、すっきり感ある飲みやすいドリンクであった。   When 20 g of the obtained diet drink powder was added to 200 mL of water in a cup, the powder immediately settled, and was stirred about 10 times with a spoon and completely dissolved in about 30 seconds. . This diet drink was tasty, refreshing and easy to drink.

Claims (2)

油脂と乳化剤とを含有し、その全体の70質量%以上が12メッシュ(目開き1.42mm)をパスし、かつ、80メッシュ(目開き182μm)にオンするものである真空乾燥粉末であって、前記油脂を5質量%〜25質量%含有する該真空乾燥粉末を、20質量%〜100質量%の割合で配合して流動造粒してなることを特徴とする造粒顆粒。 Contains a fat and an emulsifier, more than 70% by weight of the whole is passed 12 mesh (mesh opening 1.42 mm), and a vacuum-dried powder is intended to be turned on 80 mesh (mesh opening 182Myuemu) A granulated granule obtained by blending the vacuum-dried powder containing 5% by mass to 25% by mass of the oil and fat in a proportion of 20% by mass to 100% by mass and subjecting it to fluid granulation. 油脂と乳化剤と水とを含有し、前記油脂を5質量%〜25質量%含有する真空乾燥材料を均質化処理した後に真空乾燥し、得られた乾燥物を解砕し、整粒して、前記真空乾燥粉末として、その全体の70質量%以上が12メッシュ(目開き1.42mm)をパスし、かつ、80メッシュ(目開き182μm)にオンする真空乾燥粉末を調製し、前記真空乾燥粉末を20質量%〜100質量%の割合で配合して流動造粒することを特徴とする造粒顆粒の製造方法。


It contains fats and oils, an emulsifier and water, vacuum dried after homogenizing the vacuum-dried material containing 5% to 25% by weight of the fats and oils , pulverized the resulting dried product, sized, As the vacuum dried powder, 70% by mass or more of the whole passes through 12 mesh (aperture 1.42 mm) and is turned on to 80 mesh (aperture 182 μm), and the vacuum dried powder is prepared. A method for producing a granulated granule, characterized by blending 20% by mass to 100% by mass in a flow granulation.


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