JP5774625B2 - Stretched film manufacturing method and film stretching equipment - Google Patents

Description

  The present invention relates to a method for producing a stretched film and a film stretching facility for stretching a film in the transport direction due to a difference in peripheral speed between a pair of rollers.

  In general, the production of a thermoplastic resin film is roughly classified into a solution casting method and a melt casting method. In the solution casting method, a dope in which a thermoplastic resin is dissolved in a solvent is cast from a die onto a support, such as a cooling drum or a drying band, and then peeled to obtain a film. In the melt film-forming method, a thermoplastic resin is melted by an extruder, then extruded from a die onto a support, for example, a cooling drum, and then peeled to form a film.

  Thermoplastic films formed by these methods, for example, cellulose acylate films, are usually stretched in the longitudinal direction (conveying direction) and transverse direction (width direction) to achieve in-plane retardation (Re) and thickness direction. The retardation (Rth) is expressed. Thereby, when using as a phase difference film of a liquid crystal display device, a viewing angle can be expanded.

  When the thermoplastic film is stretched in the longitudinal direction, the thermoplastic film is preheated by a plurality of preheating rollers and then stretched in the longitudinal direction due to a difference in peripheral speed between the pair of stretching rollers (for example, Patent Documents 1 and 2). reference). In the stretching process, the film is heated and stretched longitudinally by a preheating roller or a stretching roller. Further, after the longitudinal stretching, it is cooled by a cooling roller and sent to the next step. Thus, since heating or cooling is performed in a state where each roller is in contact with the film, wrinkles are generated in the width direction of the film, or scratches are generated due to the wrinkles.

  For example, in Patent Document 1, in order to prevent the film from coming into contact with a plurality of preheating rollers and causing scratches or wrinkles on the film surface, a plurality of preheating rollers and an upstream side are prevented. Based on the temperature change before and after film contact with each roller, the stretching roller's peripheral speed is gradually increased toward the downstream, giving appropriate tension between each preheating roller to suppress the generation of scratches and wrinkles. ing. Moreover, in patent document 2, generation | occurrence | production of an abrasion is suppressed by quenching a film after longitudinal stretching.

JP 2008-213332 A JP 2011-207168 A

  By the way, recent liquid crystal display devices are required to be lightweight, thin, and high quality, and a film to be used is required to be thin and high quality of, for example, about 25 μm to 100 μm. When such a thin film is produced by longitudinal stretching, there is a limit to the preheating method using a preheating roller as described in Patent Documents 1 and 2 and the rapid cooling method of the film, and the film surface may be scratched or wrinkled. May occur, and improvement has been demanded.

  The present invention solves such problems, and an object of the present invention is to provide a method for producing a stretched film and a film stretching facility that can cope with thinning of the film and do not cause scratches or wrinkles on the film. And

  As a result of intensive investigations on the causes of scratches and wrinkles accompanying thinning, the following findings were obtained. First, after longitudinal stretching, both side edges of the film become thick due to the neck-in that the width is reduced. A force is applied to this thick portion at the time of neck-in, and the residual stress becomes larger than other portions. When a thin film with thick parts at both ends enters the cooling roller, the effect of residual stress and the amount of shrinkage in the film transport direction due to cooling relaxation differ between the thick part and the center part at both ends. Accordingly, the length of the film in the conveying direction at both side edges is shorter than that in the central portion in the width direction. Therefore, the flatness in the full width of the film is deteriorated during cooling, resulting in unevenness. It has been found that when such a film is conveyed by being brought into contact with a cooling roller or a conveying roller, the film is rubbed strongly locally, and scratches and wrinkles are generated on the film.

Based on the above findings, the method for producing a stretched film of the present invention includes a longitudinal stretching step, a cooling step, and both side edges of the film when a stretched film is produced by stretching a film made of a strip-shaped thermoplastic resin in the transport direction. Including a removal step. In the longitudinal stretching step, the film is stretched in the transport direction due to a difference in peripheral speed between an upstream low-speed roller and a downstream high-speed roller that are arranged apart from each other in the transport direction and heat the film in contact with the film. In the longitudinal stretching step, the longitudinal stretching aspect ratio obtained by dividing the film length between the upstream low speed roller and the downstream high speed roller by the film width before stretching is 0.01 or more and 0.5 or less. In the cooling step, the film is cooled by a cooling roller disposed next to the high speed roller on the downstream side . In the film both-side edge removing step, both edges in the width direction of the film are removed by a slitter between the downstream high-speed roller and the cooling roller .

Moreover, the film extending | stretching equipment of this invention manufactures a stretched film by extending | stretching the film which consists of a strip-shaped thermoplastic resin to a conveyance direction. This film stretching equipment includes a longitudinal stretching section, a cooling section, and a side edge section removing section. The longitudinal stretching unit is disposed separately in the transport direction, and stretches the film in the transport direction due to a difference in peripheral speed between an upstream low-speed roller that contacts the film and heats the film and a downstream high-speed roller. In the longitudinal stretching portion, a longitudinal stretching aspect ratio obtained by dividing the film length between the upstream low-speed roller and the downstream high-speed roller by the film width before stretching is 0.01 or more and 0.5 or less . The cooling unit cools the film by a cooling roller disposed next to the downstream high-speed roller . The side edge portion removing portion is disposed between the downstream high speed roller and the cooling roller, and removes both side edges in the width direction of the film from the central portion by a slitter .

  In the film side edge removal step, when the width from the film thickness change start point at which the film thickness at the both side edges of the film starts to change to the both side edges of the film is defined as WFS, the film thickness change start point to the film thickness change start point. It is preferable that the widthwise side edges are removed by separating the central part and the side edges in the film width direction within WFS × 0.2 toward the side edges.

  In the longitudinal stretching step, when the glass transition temperature of the film is Tg, the film is heated to a stretching temperature Te of (Tg−20) ° C. or more and (Tg + 20) ° C. or less by the upstream low-speed roller, and then by the downstream high-speed roller. The film is preferably cooled to (Tg-100) ° C or higher and (Tg-5) ° C or lower.

It is preferable to include a preheating step of preheating the film to ( Tg- 40) ° C. or higher and (Tg-5) ° C. or lower before the longitudinal stretching step. In the preheating step, it is preferable to preheat the film by supplying heating air into the preheating chamber. Moreover, it is preferable that a preheating process spans and conveys a film on the several conveyance direction change member for changing the conveyance direction of a film and lengthening a path | pass.

  According to the present invention, since both side edges of the film that has become thick due to the neck-in due to longitudinal stretching are removed, the film unevenness caused by the film partially shrinking in the transport direction during cooling of the film Occurrence is suppressed. This eliminates the generation of scratches and wrinkles on the film.

It is a side view which shows the outline | summary of an example of the film extending | stretching equipment of this invention. It is a graph which shows an example of the thickness distribution of the film in the film width direction after longitudinal stretch cooling. It is a top view which shows the outline | summary of a slitter. It is a side view which shows the outline | summary of an example of the film extending equipment of another embodiment which has the pre-heating part by ventilation. It is a side view which shows the outline | summary of an example of the preheating part of another embodiment which has a some preheating area. It is a side view which shows the outline | summary of an example of the pre-heating part of another embodiment which controls temperature of a free roller. It is a side view which shows the outline | summary of the pre-heating part of another embodiment using a turn bar.

  As shown in FIG. 1, the film stretching facility 10 of the present invention includes a preheating unit 11, a longitudinal stretching unit 12, and a cooling unit 13. A pre-process device 9 is connected to the film stretching facility 10 on the inlet side, and a post-process device 14 is connected on the outlet side. Examples of the pre-process device 9 include a film forming facility and a film delivery device (not shown). As the film forming facility, a well-known solution film forming facility, a melt film forming facility, or the like is used. Unlike the case where the film 15 is directly sent from the film forming facility, the film delivery apparatus pulls out the film 15 from the roll film wound up in a roll shape after the film formation and supplies the film 15. Examples of the post-process device 14 include a clip tenter and a film winding device that are used in the case of lateral stretching after longitudinal stretching. When the transverse stretching is not performed continuously following the longitudinal stretching, the clip tenter is omitted, and the film 15 is wound in a roll shape by the film winding device.

  The film 15 to be stretched may be a thermoplastic resin film, and is preferably a film 15 made of cellulose acylate, norbornene resin, acrylic, polycarbonate or the like suitable for use in an optical film such as a retardation film.

  The preheating unit 11 includes a preheating roller pair 16, a first preheating roller 17, and a second preheating roller 18. The preheating roller pair 16 includes an inlet preheating roller 16a and a nip roller 16b, and nips and conveys the film 15. The film 15 is crossed over the inlet preheating roller 16a, the first preheating roller 17, and the second preheating roller 18. Thereby, the contact area of the film 15 and each preheating roller 16a, 17, 18 increases, and preheating is performed efficiently.

The preheating temperature needs to be lower than the temperature at which stretching is possible. Therefore, when the glass transition temperature of the film 15 is Tg, the film 15 is preheated to (Tg−40) ° C. or higher and (Tg−5) ° C. or lower, and the film 15 is sent to the longitudinally stretched portion 12. Specifically, the film 15 is preheated to (Tg−60) ° C. or more and (Tg−35) ° C. or less by the inlet preheating roller 16a, and the film 15 is (Tg−50) ° C. or more (Tg−) by the first preheating roller 17. 25) Preheat to below ℃ and preheat the film 15 to (Tg-40) ℃ above (Tg-5) ℃ with the second preheat roller 18 .

  The film 15 preheated to a constant temperature through the preheating unit 11 is sent to the longitudinal stretching unit 12. The longitudinal stretching unit 12 includes a low-speed roller pair 21 and a high-speed roller pair 22. The low speed roller pair 21 has a low speed roller 21a and a nip roller 21b. The high speed roller pair 22 includes a high speed roller 22a and a nip roller 22b. The low-speed roller 21a and the high-speed roller 22a are individually supplied with a temperature control medium such as water, oil, water vapor, or the like from the temperature control medium circulation unit. The rollers 21a and 22a are set to a desired surface temperature by circulating and supplying the temperature control medium. For example, the low speed roller 21a is (Tg−20) ° C. or higher and (Tg + 20) ° C. or lower, and the high speed roller 22a is (Tg−100) ° C. or higher and (Tg−5) ° C. or lower. By setting such a temperature range, uniform longitudinal stretching can be performed on the thin film 15 having a thickness of 25 μm or more and 100 μm or less.

  The film 15 stretched longitudinally by the longitudinal stretching section 12 is wound around the first cooling roller 25 and the second cooling roller 26, conveyed, and cooled. Each cooling roller 25, 26 is individually supplied with a temperature control medium from the temperature control medium circulation unit, and each roller 25, 26 is set to a desired surface temperature. For example, the first cooling roller 25 is (Tg−40) ° C. or lower, and the second cooling roller 26 is (Tg−50) ° C. or lower. The cooled film 15 is sent to the post-process device 14 by the transport rollers 27 and 28.

  Although not shown in the drawings, each of the rollers 16a, 17, 18, 21a, 22a, 25, and 26 is connected to a motor, and can rotate at a desired rotation speed. In the longitudinal stretching section 12, the film 15 is stretched in the transport direction and longitudinally stretched by the difference in peripheral speed between the low speed roller 21a and the high speed roller 22a. The peripheral speed difference between the low-speed roller 21a and the high-speed roller 22a is appropriately changed depending on the draw ratio, but is preferably set in the range of 2 m / min to 100 m / min, for example.

  When performing longitudinal stretching, the longitudinal stretching ratio is preferably in the range of 1.0 to 1.5. When the longitudinal draw ratio is in the range of more than 1.0 and 1.5 or less, the occurrence of uneven thickness can be suitably suppressed, and uneven distribution of the developed retardation is also suppressed.

  Further, the longitudinal stretch aspect ratio (Ls / W1) obtained by dividing the length Ls of the film 15 between the upstream low-speed stretching roller 21a and the downstream high-speed roller 22a by the width W1 of the film 15 before stretching is 0.01 or more. It is preferable that it is 0.5 or less. The smaller the longitudinal stretch aspect ratio, the smaller the neck-in and the greater the ratio of the uniform film thickness portion of the central portion 15a in the film thickness distribution in the film width direction. Thereby, the width | variety of the film both sides edge part 15b cut off by the slitter 31 demonstrated later can be made small, the center part 15a used as a product can be increased by that much, and a product loss can be suppressed.

By preheating the film 15 to ( Tg− 40) ° C. or more in the preheating section 11, the amount of temperature rise during heating of the film 15 by the low speed roller 21a of the longitudinal stretching section 12 does not become too large, and the speed is low. Generation of corrugated wrinkles on the roller 21a is suppressed. In addition, by preheating the film 15 to (Tg-5) ° C. or less in the preheating portion 11, the film 15 is not stretched in the preheating portion 11 and can be uniformly stretched in the longitudinal stretching portion 12. .

  A slitter 31 is disposed between the longitudinally extending portion 12 and the cooling portion 13. The slitter 31 has a pair of roll blades 31a and 31b, and cuts the film 15 in the transport direction. Thereby, the film 15 is cut | disconnected by the center part 15a and the both-sides edge part (refer FIG. 2) 15b in the width direction.

  As shown in FIG. 2, the film 15 is cut along a cutting line CL <b> 1 that is shifted from the film thickness change start point P <b> 1 toward both side edges of the film 15 by the offset amount OS <b> 1.

  FIG. 2 shows the film thickness distribution in the width direction of the film 15 when the film 15 is longitudinally stretched and cooled without being cut by the slitter 31. Both side edges 15b of the film 15 are gradually thickened by neck-in as the film thickness Ft goes to both sides.

  The film thickness change start point P1 is a point at which the film thickness Ft of the central portion 15a and both side edge portions 15b in the film width direction starts changing. The film thickness change start point P1 can be set as the cutting position. However, in this case, the width of both side edges 15b of the film separated by the slitter 31 is increased, and the film central portion 15a that can be a product is reduced accordingly, and the product loss is increased. In order to prevent this, the cutting line CL1 is shifted from the film thickness change start point P1 toward the side edge by the offset amount OS1 to a position where no scratch is generated in the next cooling step.

  The offset amount OS1 is obtained as follows, for example. When the width from the film thickness change start point P1 to both side edges of the film is WFS, the width WFS is multiplied by a coefficient 0.2 (WFS × 0.2).

  Both side edges 15b separated from the central portion 15a by the slitter 31 are sent to the rotary cutter 32 and cut into sections. The section is sent to the recycling unit 33 and recycled as the raw material of the film 15 or the like. The recycle unit 33 blows the slices by a not-shown wind sending means, passes through a crusher, a separator, and the like to make a minute slice, and stores the minute slice in a silo.

  The film 15 stretched in the longitudinal stretching section 12 is wound on a film roll by, for example, a film winder of the post-process device 14.

  In this embodiment, since the film side edges 15b that are thick due to the neck-in due to longitudinal stretching are removed, the unevenness caused by the film 15 partially shrinking in the transport direction during cooling of the film 15 is eliminated. Occurrence is suppressed. This eliminates the occurrence of scratches and wrinkles on the film 15 during cooling by the cooling rollers 25 and 26.

  Further, since both side edge portions 15b are separated from the central portion 15a by the slitter 31 before cooling, the cooling rollers 25 and 26 can be cooled without causing scratches or wrinkles. Moreover, as shown in FIG. 2, since the cutting line CL1 is shifted by the offset amount OS1 from the film thickness change start point P1 toward the side edge, the both side edges 15b are separated from the center part 15a by the slitter 31, so that the center part 15a can be left as wide as possible, and product loss can be suppressed.

  Next, instead of preheating using the preheating rollers 16a, 17, and 18 shown in FIG. 1, as shown in FIG. 4, a film stretching equipment 45 according to another embodiment having a preheating portion 44 by air blowing will be described. As shown in FIG. 1, when the preheating rollers 16a, 17, and 18 are used to preheat the film 15 by direct contact, the film 15 is thermally expanded on the preheating rollers 16a, 17, and 18 as the film 15 becomes thinner. May become corrugated. This corrugated expansion may cause wrinkles and scratches on the film 15. By replacing the heat conduction by direct contact with the film 15 by heating by blowing air, the corrugated expansion of the film 15 on the preheating rollers 16a, 17 and 18 is suppressed. In particular, generation of wrinkles and scratches due to preheating is suppressed for a thin film having a thickness of 25 μm or more and 100 μm or less before stretching of the film 15.

  A tension adjusting unit 46 is provided between the pre-process device 9 and the film stretching equipment 45. The tension adjusting unit 46 raises and lowers the tension roller 48 between the free rollers 47a and 47b by the shift mechanism 49 to maintain the tension of the film 15 in the preheating unit 44 constant. The film tension in the preheating part 44 is preferably 20 N / m or more and 200 N / m or less. If it is 20 N / m or more, the rotation failure of the free roller 55 does not occur, and the generation of scratches on the film 15 is suppressed. Further, when it is 200 N / m or less, no longitudinal stretching occurs in the preheating section 11, and proper longitudinal stretching is performed in the longitudinal stretching section 12.

  The preheating unit 11 includes a preheating chamber 50. In the preheating chamber 50, a plurality of free rollers (conveying direction changing members) 55 are arranged apart from each other in the vertical direction. By alternately winding the film 15 between the free rollers 55, the film 15 is conveyed in the vertical direction between the rollers 55, and the film path (path) in the preheating chamber 50 is set long.

  Although the film path length of the preheating chamber 50 depends on the preheating temperature and the transport speed of the film 15, it is preferably, for example, 5 m or more and 50 m or less. The free roller 55 has a diameter of, for example, 80 mm, and the contact area between the film 15 and the free roller 55 by winding the film 15 is reduced. The diameter of the free roller 55 is preferably 40 mm or greater and 150 mm or less. If it is 40 mm or more, the free roller 55 will not be bent, and the occurrence of uneven rotation and scratches due to the bending can be suppressed. Moreover, when it is 150 mm or less, the contact time with the free roller 55 falls within an appropriate range, and wrinkles are suppressed. In addition, the occurrence of scratches on the film 15 due to poor rotation of the free roller 55 is suppressed. It is preferable that the outer peripheral surface of the free roller 55 is hard chrome plated. By applying the hard chrome plating, the adhesion with the film 15 is improved, and the film 15 is difficult to slip.

  In the preheating unit 44, for example, an air supply nozzle 61 is disposed on the upper side, and an exhaust nozzle 62 is disposed on the lower side. A blower 64 and a temperature controller 65 are connected to the air supply nozzle 61 and the exhaust nozzle 62 via a duct 63. The temperature controller 65 heats a heating medium such as air to a desired temperature. The blower 64 sends the air whose temperature is adjusted by the temperature adjuster 65 to the air supply nozzle 61 through the duct 63. Heated air is sent out from the air supply nozzle 61, and the film 15 in the preheating unit 11 is preheated to a constant temperature by the heating air 66. The heating air 66 circulates from the side of the film 15 in the preheating chamber 50 and preheats the entire upper and lower surfaces of the film 15.

  The preheating temperature by the heating air 66 needs to be lower than the temperature (stretching temperature) Te at which stretching is possible. Therefore, when the glass transition temperature of the film 15 is set to Tg, the heating air 66 is supplied into the preheating unit 44 to preheat the film 15 to (Tg-40) ° C. or higher and (Tg-5) ° C. or lower. The blowing speed of the heating air from the air supply nozzle 61 is preferably 2 m / sec or more and 15 m / sec or less. When it is 2 m / sec or more, the temperature of the preheating chamber 50 can be kept uniform, and the occurrence of stretching unevenness is eliminated. Further, when it is 15 m / sec or less, the generation of scratches due to flapping of the film 15 is eliminated. In addition, except having comprised the preheating part 44 from the preheating chamber 50 by ventilation, it is the same structure as the said embodiment, and the same code | symbol is attached | subjected to the same structural member.

  In this embodiment, since the heating air 66 is sent to the preheating chamber 50 and heated by the heating air 66, the film 15 is not thermally expanded due to heat conduction due to direct contact from the preheating roller, and is not wrinkled. And scratches are suppressed.

  When one preheating chamber 50 is preheated at the same temperature, the temperature of the free roller 55 can be the same temperature as the room temperature of the preheating chamber 50. For this reason, the film 15 entering the preheating chamber 50 comes into contact with the free roller 55 on the inlet side which has been raised to the outlet temperature of the preheating chamber 50, so that the film 15 is thermally expanded and the corrugated plate repeats unevenness in the film width direction. There is concern that it will be wrinkled. In order to prevent this, the heat transfer from the free roller 55 to the film 15 is suppressed by reducing the diameter of the free roller 55 as much as possible and reducing the wrap angle in order to suppress the heating due to the heat transfer of the free roller 55. For this reason, even when the film transport speed is 40 m / min, the diameter of the free roller 55 is set to 40 mm or more and 150 mm or less, and the free roller 55 heated by the heating air 66 contacts the film 15 and is thermally expanded. Avoid deformation. Actually, the free roller 55 is at a temperature lower than the temperature in the preheating chamber 50 due to the contact with the continuously fed film 15 (which is lower than the temperature of the preheating chamber 50). Therefore, thermal deformation may not occur due to film contact with the free roller 55.

  In the above embodiment, the film 15 is heated by one preheating chamber 50. However, as shown in FIG. 5, preheating regions 68a to 68c in which the preheating chamber 68 is divided into a plurality of portions in the film conveying direction by the partition walls 69 are provided. The preheating unit 70 may be used. In addition, the same code | symbol is attached | subjected to the same structural member as the said embodiment. In this case, an air supply nozzle 61, an exhaust nozzle 62, a duct 63, a blower 64, and a temperature controller 65 are provided in each preheating region 68a to 68c, and the temperature in each preheating region 68a to 68c is measured in the film transport direction. Set to gradually increase. The temperature difference between the adjacent preheating regions 68a to 68c is, for example, 20 ° C. or more and 50 ° C. or less. If this temperature difference is less than 20 ° C., a large number of preheating zones are required to reach a desired temperature, for example, 180 ° C., and the equipment efficiency is reduced by the increase in the number of sections. Further, if the temperature difference exceeds 50 ° C., temperature non-uniformity occurs due to exchange of air between adjacent preheating regions, temperature non-uniformity occurs in the film 15 and leads to non-uniform stretching.

  The number of sections in each preheating area 68a to 68c increases or decreases according to the preheating temperature. For example, when one preheating chamber 68 is preheated at the same temperature, the film 15 entering the preheating chamber 68 contacts the free roller 55 on the inlet side raised to the outlet temperature of the preheating chamber 68, so that the film 15 is thermally expanded. However, there is a concern that wrinkled wrinkles that are repeatedly uneven in the film width direction. In order to prevent this, the preheating temperature of each of the preheating regions 68a to 68c is set to be small so that the free roller 55 heated by the heating air 66 does not expand and deform even if it contacts the film 15. And it preheats in steps to the temperature which can be longitudinally stretched by several preheating area 68a-68c.

  Further, instead of dividing the preheating chamber 68 into a plurality of pieces, as shown in FIG. 6, in one preheating chamber 79, a temperature adjustment medium is supplied to each free roller 80 by the temperature adjustment mechanisms 82a to 82c, thereby It is good also as the preheating part 83 which adjusts the surface temperature of the roller 80 for every group. In this case, the surface temperature of the free roller 80 is increased for each group in order from the entrance side. The surface temperature of each free roller 80 is set to a temperature at which the film 15 contacts and does not generate corrugated wrinkles due to thermal expansion. In addition to temperature adjustment for each group, temperature adjustment may be performed for each free roller 80. Furthermore, the temperature of the free roller 55 in the preheating chamber 68 partitioned as shown in FIG. The temperature difference between the adjacent downstream group and the upstream group free roller 80 is 50 ° C. or less, and the most upstream group free roller 80 is (Tg−40) ° C. or more (Tg−5) from the outside room temperature of the preheating chamber 79. It is the range below ℃.

  In each of the above embodiments, the free rollers 55 and 80 are used to set the film path length in the preheating chambers 50, 68, and 79 long, but instead of the free rollers 55 and 80, as shown in FIG. Alternatively, a preheating unit 86 using a turn bar (conveying direction changing member) 85 may be used. In this case, the blower 87 and the temperature controller 88 are connected to the turn bar 85 and the floating air is supplied to the turn bar 85. The floating air may be set to be the same as the preheating temperature of the preheating chamber 84 or may be set low. 6 and 7, the preheating chambers 79 and 89 include the blower 64 and the temperature controller 65 as in FIG. 4, but are not illustrated. Similarly to the embodiment of FIG. 5, the preheating chambers 79 and 89 are divided into a plurality of parts, and a fan 64 and a temperature controller 65 are provided for each of the preheating chambers 79 and 89, and the preheating temperature is set for each preheating chamber. It may be set and the preheating temperature may be gradually increased from the inlet side toward the outlet side. Further, similarly to the free roller 80 in the embodiment of FIG. 6, the temperature of the floating air from each turn bar 85 is changed individually for each turn bar 85 or for each group, and from the inlet of the preheating chamber 89 toward the outlet, The temperature may be gradually increased.

  A cellulose acylate film was used as the film 15, and preheating, longitudinal stretching, and cooling were performed. In the longitudinal stretching section 12, one-stage longitudinal stretching was performed by the upstream low-speed roller pair 21 and the downstream high-speed roller pair 22. A film delivery machine was used as the pre-process device 9 and the film 15 was pulled out from the film roll and sent to the preheating unit 11. A film winder was used as the post-process equipment 14 to wind the film 15 into a film roll. Preheating temperature is 130 ° C., stretching temperature is 150 ° C., stretching ratio is 1.5 times, stretching length is 300 mm, cooling temperature is 100 ° C., film conveyance speed is 2 m / min, film width before stretching is 600 mm, film before stretching Thickness of 100 μm, stretched film width 580 mm, stretched central uniform film thickness W2 (see FIG. 2) width 480 mm, thick part width WFS 50 mm, from film thickness change start point P1 to side edge direction The experiment was performed under different conditions such that the offset amount OS1 was 15 mm, 10 mm (WFS × 0.2), 0 mm, −10 mm, and both side edges 15b were not cut. In addition, the film thickness change start point P1 used the point which the center part uniform film thickness after extending | stretched exceeded the film thickness dispersion | variation of the film (raw film) before extending | stretching. The film thickness variation of the film before stretching is a difference (Ftmax−Ftmin) obtained by subtracting the minimum film thickness value (Ftmin) from the maximum film thickness value (Ftmax), and is 1.5 μm.

  When the offset amount OS1 was 10 mm, 0 mm, and −10 mm, no scratches or wrinkles were generated. In addition, when both side edges 15b were not cut or the offset amount OS1 was 15 mm, scratches and wrinkles occurred. The scratch was evaluated as NG (defective) when the width was 0.05 mm or more and the depth was 0.02 mm or more by microscopic observation. A wrinkle was evaluated as NG if visible by visual observation.

10, 45 Film stretching equipment 11, 44, 70, 83, 86 Preheating unit 12 Longitudinal stretching unit 13 Cooling unit 15 Films 16a, 17, 18 Preheating roller 21a Low speed roller 22a High speed roller 25, 26 Cooling roller 31 Slitter 50, 68, 79, 84, 89 Preheating chamber 55, 80 Free roller 61 Air supply nozzle 62 Exhaust nozzle 85 Turn bar

Claims (10)

In a method for producing a stretched film by stretching a film made of a strip-shaped thermoplastic resin in the transport direction,
A longitudinal stretching step in which the film is stretched in the transport direction due to a difference in peripheral speed between an upstream low-speed roller and a downstream high-speed roller that are spaced apart from each other in the transport direction and contact the film to heat the film; ,
A cooling step of cooling the film by a cooling roller disposed next to the downstream high-speed roller ;
A side edge removing step of removing both side edges in the width direction of the film by a slitter between the downstream high-speed roller and the cooling roller ,
In the longitudinal stretching step, a stretched film having a longitudinal stretching aspect ratio of 0.01 or more and 0.5 or less obtained by dividing the film length between the upstream low-speed roller and the downstream high-speed roller by the film width before stretching. Manufacturing method. In the side edge portion removing step, when the width from the film thickness change starting point at which the film thickness of the both side edge portions in the width direction starts to change to the both side edges of the film is defined as WFS, from the film thickness change starting point. wherein within both side edges WFS × 0.2 towards the method for producing a stretched film according to claim 1, wherein disconnecting the central portion and the both side edges of the film width direction to remove the both widthwise side edges. In the longitudinal stretching step, when the glass transition temperature of the film is Tg, the upstream low-speed roller heats the film to a stretching temperature Te of (Tg−20) ° C. or higher and (Tg + 20) ° C. or lower, The manufacturing method of the stretched film of Claim 1 or 2 which cools the said film to (Tg-100) degreeC or more and (Tg-5) degreeC or less with a downstream high speed roller. A preheating step of preheating the film to ( Tg- 40) ° C. or higher and (Tg-5) ° C. or lower before the longitudinal stretching step ;
In the preheating step, heating film is supplied into a preheating chamber to preheat the film , and the film is stretched over a plurality of free rollers that change the transport direction of the film, and the free roller is in contact with the film. The method for producing a stretched film according to claim 3, wherein the stretched film is set to a temperature or a diameter at which wrinkles due to thermal expansion due to heat are not generated . A preheating step of preheating the film to ( Tg- 40) ° C. or higher and (Tg-5) ° C. or lower before the longitudinal stretching step ;
The preheating step supplies the heated air to the preheating chamber heated pre said film, and said film said film into a plurality of the turn bar is over passed by are <br/> of claim 3, wherein for changing the conveying direction of the A method for producing a stretched film. In film stretching equipment for producing a stretched film by stretching a film made of a strip-shaped thermoplastic resin in the transport direction,
The film is stretched in the transport direction by the difference in peripheral speed between an upstream low-speed roller that is spaced apart in the transport direction and contacts the film to heat the film, and a downstream high-speed roller. A longitudinally stretched portion having a longitudinal stretch aspect ratio of 0.01 or more and 0.5 or less obtained by dividing the film length between the side low speed roller and the downstream high speed roller by the film width before stretching;
A cooling section that cools the film by a cooling roller disposed next to the downstream high-speed roller ;
Wherein disposed between the downstream high speed roller and the cooling roller, the film stretching equipment and a side edge portion removal unit for removing separately from Chuo portion in the width direction both side edges of the film by slitter. When the width from the film thickness change start point at which the film thickness of the both side edge portions of the width direction starts to the both side edges of the film is WFS, WFS × from the film thickness change start point toward the both side edges of the film The film stretching equipment according to claim 6, wherein within 0.2, the central part and both side edges in the film width direction are separated and the both side edges in the width direction are removed. When the glass transition temperature of the film is defined as Tg, the longitudinal stretching section heats the film to a stretching temperature Te of (Tg-20) ° C. or more and (Tg + 20) ° C. or less by the upstream low-speed roller, The film stretching equipment according to claim 6 or 7 , wherein the film is cooled to (Tg-100) ° C or higher and (Tg-5) ° C or lower by a downstream high-speed roller. Arranged in front of the longitudinally stretched part, heated air is supplied to preheat the film to ( Tg− 40) ° C. or higher and (Tg−5) ° C. or lower , and the preheated chamber is placed in contact with the film. due to the occurrence of wrinkles due to thermal expansion is set to no temperature or diameter, of a plurality of free rollers preheater and 8 any of the preceding claims 6 comprising a having to change the conveying direction of the film Film stretching equipment. A preheating chamber that is arranged in front of the longitudinally stretched portion and supplies heated air to preheat the film to ( Tg- 40) ° C. or higher and (Tg-5) ° C. or lower ; and the preheating chamber, The film stretching equipment according to any one of claims 6 to 8, further comprising a preheating unit having a plurality of turn bars for changing a conveyance direction .

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