JP5465543B2 - Graphitization furnace - Google Patents

Graphitization furnace Download PDF

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JP5465543B2
JP5465543B2 JP2010009103A JP2010009103A JP5465543B2 JP 5465543 B2 JP5465543 B2 JP 5465543B2 JP 2010009103 A JP2010009103 A JP 2010009103A JP 2010009103 A JP2010009103 A JP 2010009103A JP 5465543 B2 JP5465543 B2 JP 5465543B2
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JP2011148642A (en
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昌宏 北
博 岡田
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住友電設株式会社
株式会社高橋電器製作所
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この発明は、電気製鋼用黒鉛電極などの製造工程において、焼成済みの炭素質成形体(被処理材)を黒鉛化するのに用いる黒鉛化炉、特に、直接黒鉛化法(LWG法)で大型の黒鉛電極材などを製造するのに適した黒鉛化炉に関する。   The present invention relates to a graphitization furnace used for graphitizing a calcined carbonaceous molded body (material to be treated) in a manufacturing process of an electric steelmaking graphite electrode, and particularly, a large-scale direct graphitization method (LWG method). The present invention relates to a graphitization furnace suitable for manufacturing graphite electrode materials and the like.

電気製鋼用黒鉛電極は、通常、コークス粉粒とピッチバインダーの混合原料を円柱状に成形し、これを1500℃以下の温度で焼成し、次いで、得られた材料又はこれにピッチを含浸させたものを1000℃以下の温度で再焼成し、その後さらに、以上の工程を経て得られた炭素質成形体を抵抗加熱法で2500〜3000℃の高温に加熱して黒鉛化する方法で製造されている。   A graphite electrode for electric steelmaking is usually formed by mixing a mixed raw material of coke powder particles and pitch binder into a cylindrical shape, firing it at a temperature of 1500 ° C. or lower, and then impregnating the obtained material or this with pitch. It is manufactured by recalcining the material at a temperature of 1000 ° C. or lower, and then heating the carbonaceous molded body obtained through the above steps to a high temperature of 2500 to 3000 ° C. by a resistance heating method and graphitizing. Yes.

その黒鉛化が首記の直接黒鉛化法で行なわれる。再焼成済みの炭素質成形体を長尺の黒鉛化炉の内部に直列に配列して挿入し、周辺を保温と酸化防止のためのコークス詰粉で被包充填する。そして、この状態で末端の炭素質成形体に当接したターミナル電極を介して通電し、炭素質成形体を電気抵抗によって発熱させ、3000℃程度まで昇温させて黒鉛化処理する。   The graphitization is performed by the direct graphitization method mentioned above. The refired carbonaceous compacts are inserted in series inside a long graphitization furnace, and the periphery is encapsulated with coke filling for heat retention and oxidation prevention. And in this state, it supplies with electricity through the terminal electrode which contact | abutted the carbonaceous molded object of the terminal, heat-generates a carbonaceous molded object by electrical resistance, raises to about 3000 degreeC, and graphitizes.

この直接黒鉛化法では、個々の炭素質成形体の突き合わせ面間に生じる接触抵抗によって、製品の破損、亀裂の原因になる局部的な異常発熱が起こる虞があり、その対策として、直列に配列した炭素質成形体をプッシャーで軸方向に押圧し、炭素質成形体相互の突き合わせ面における接触抵抗の低減と安定化を図ることが行なわれている(下記特許文献1参照)。   In this direct graphitization method, the contact resistance generated between the butting surfaces of the individual carbonaceous molded bodies may cause local abnormal heat generation that causes product damage and cracks. The pressed carbonaceous compact is pressed in the axial direction with a pusher to reduce and stabilize the contact resistance between the butted surfaces of the carbonaceous compacts (see Patent Document 1 below).

また、プッシャーによる押圧と個々の炭素質成形体の接着を併用する方法や個々の炭素質成形体の突き合わせ面間や末端の炭素質成形体とそれに当接させる水冷ターミナル電極との間に炭素質成形体よりも電気比抵抗値の高い炭素質導電材を介在させる方法なども開発されている(下記特許文献2,3参照)。   In addition, there is a method in which pressing by a pusher and adhesion of individual carbonaceous molded bodies are used together, or between the butting surfaces of individual carbonaceous molded bodies and between the carbonaceous molded body at the end and the water-cooled terminal electrode that is in contact with the carbonaceous molded body. A method of interposing a carbonaceous conductive material having a higher electrical specific resistance value than the molded body has also been developed (see Patent Documents 2 and 3 below).

さらに、直列配置の炭素質成形体を一群として横2列に配置されたチャンバにその炭素質成形体群をそれぞれ挿入し、2組の炭素質成形体群の他端を互いに電気的に接続し、各組の炭素質成形体群の一端に陰陽のターミナル電極をそれぞれ当接させて通電する、生産性や設備のスペース効率などに優れた黒鉛化炉も開発されている。   Further, the carbonaceous compacts are inserted into chambers arranged in two horizontal rows as a group of serially arranged carbonaceous compacts, and the other ends of the two sets of carbonaceous compacts are electrically connected to each other. A graphitization furnace excellent in productivity, equipment space efficiency, and the like has also been developed in which a Yin and Yang terminal electrode is brought into contact with one end of each group of carbonaceous molded body groups.

炭素質成形体群を並列配置にして一括処理するその黒鉛化炉では、各組の炭素質成形体群を電気的に直列につなぐ方法として、炉の奥端にカーボンブロックを配置し、そのカーボンブロックに2組の炭素質成形体群の他端を押し付けて電気導通の中継をカーボンブロックによって行なう方法が通常採られている。   In the graphitization furnace in which the carbonaceous compact groups are arranged in parallel and processed together, a carbon block is arranged at the back end of the furnace as a method of electrically connecting each group of carbonaceous compact groups in series. A method is generally employed in which the other ends of the two sets of carbonaceous compacts are pressed against the block, and electrical conduction is relayed by the carbon block.

このほか、黒鉛化炉などに電力を供給する給電装置が下記特許文献4に開示され、さらに、黒鉛化炉の炉体に関する発明が下記特許文献5などに開示されている。   In addition, a power supply device for supplying power to a graphitization furnace or the like is disclosed in the following Patent Document 4, and further, an invention related to the furnace body of the graphitization furnace is disclosed in the following Patent Document 5 or the like.

特公昭63−66766号公報Japanese Examined Patent Publication No. 63-66766 特開平5−78111号公報JP-A-5-78111 特開平9−227232号公報JP-A-9-227232 特開2006−12457号公報JP 2006-12457 A 米国特許第5299225号明細書US Pat. No. 5,299,225

並列配置の炭素質成形体群には、黒鉛化処理時の熱膨張差や予備焼成で個々の炭素質成形体の寸法誤差などにより、全体の軸方向寸法(長さ)にずれが生じる。   In the group of carbonaceous molded bodies arranged in parallel, the overall axial dimension (length) is shifted due to a difference in thermal expansion during graphitization treatment or a dimensional error of individual carbonaceous molded bodies due to preliminary firing.

各炭素質成形体群のセット時の長さは、炭素質成形体相互の突合せ面などに介在する導電材の軸方向寸法を変えることによって等しくなるように調整することができる。しかしながら、黒鉛化処理時の熱膨張量などが不均一になるため、炭素質成形体群の軸方向寸法のずれは不可避の問題として発生する。   The set lengths of the respective carbonaceous molded body groups can be adjusted to be equal by changing the axial dimension of the conductive material interposed between the butted surfaces of the carbonaceous molded bodies. However, since the amount of thermal expansion at the time of graphitization is not uniform, a deviation in the axial dimension of the carbonaceous molded body group occurs as an inevitable problem.

プッシャーによる片側からの押圧では、軸方向寸法の吸収能力が制限され、力の伝達ロスも生じやすい。それが原因で2つのチャンバの炭素質成形体群の軸方向寸法にずれが生じたときに軸方向押圧力がばらつくため、炭素質成形体の相互突き合わせ面の面圧が不均一になる。また、長尺炉では特に、力の伝達ロスが大きくなって押圧力が不足しがちとなり、そのために加熱条件が不安定、不均一になって得られる製品の破損、亀裂、変質、粉化などが起こる。   In the pressing from one side by the pusher, the absorption capacity of the axial dimension is limited, and transmission loss of force is likely to occur. As a result, the axial pressing force varies when the axial dimensions of the carbonaceous molded body groups of the two chambers deviate from each other, resulting in nonuniform surface pressures on the mutual butted surfaces of the carbonaceous molded bodies. Also, especially in long furnaces, the transmission loss of force increases and the pressing force tends to be insufficient, resulting in unstable, uneven heating conditions, product damage, cracks, alteration, pulverization, etc. Happens.

この発明は、かかる不具合を回避するために、焼成済み炭素質成形体が直列に配列された炭素質成形体群を並列配置のチャンバに挿入し、それを電気的に直列につないで加熱処理する方式の黒鉛化炉を、炭素質成形体群の熱膨張量の違いなどによる長さ変動の吸収が規制なくなされ、各列の炭素質成形体群の通電条件や軸方向押圧が安定して炭素質成形体が均一に加熱されるようにすることを課題としている。   In order to avoid such inconveniences, the present invention inserts a group of carbonaceous molded bodies in which baked carbonaceous molded bodies are arranged in series into a chamber arranged in parallel, and heats them by electrically connecting them in series. The graphitization furnace of the system is made to absorb the fluctuation of length due to the difference in the amount of thermal expansion of the carbonaceous compact group, and the current-carrying conditions and axial pressure of the carbonaceous compact group in each row are stable. An object of the present invention is to uniformly heat the molded product.

上記の課題を解決するため、この発明においては、以下の要素を備える黒鉛化炉にした。
1)互いに区画された並列配置の2つのチャンバを有する軸方向に長い炉体。
2)前記炉体の一端側において炉外から前記2つのチャンバに個別に臨ませる軸方向スライド可能な2個の第1ターミナル電極。
3)各炉体の他端側において炉外から前記2箇所のチャンバに個別に臨ませる軸方向スライド可能な2個の各々が上下面を有する第2ターミナル電極。
4)第1、第2ターミナル電極を個々に軸方向に押圧するプッシャー。
5)前記第1、第2ターミナル電極に働く反力を個々に受ける反力柱。
6)前記2個の第2ターミナル電極を炉外で電気的に導通させる接続器。
ここで言う軸方向とは、炉体の長手方向を指す。
In order to solve the above problems, in the present invention, a graphitization furnace having the following elements is provided.
1) An axially long furnace body having two chambers arranged in parallel and separated from each other.
2) Two axially slidable first terminal electrodes individually facing the two chambers from outside the furnace at one end side of the furnace body.
3) Second terminal electrodes each having two upper and lower surfaces that can be slid in the axial direction individually facing the two chambers from outside the furnace at the other end of each furnace body.
4) A pusher that individually presses the first and second terminal electrodes in the axial direction.
5) A reaction force column that individually receives reaction forces acting on the first and second terminal electrodes.
6) A connector for electrically connecting the two second terminal electrodes outside the furnace.
The axial direction here refers to the longitudinal direction of the furnace body.

また、各チャンバに直列に配列される複数の焼成済み炭素質成形体の相互突き合せ面に前記プッシャーで面圧を加え、この状況で、2個の第1ターミナル電極間に通電して炭素質成形体を電気抵抗で所定温度に加熱するものにした。   Further, a surface pressure is applied to the mutual butted surfaces of a plurality of calcined carbonaceous molded bodies arranged in series in each chamber by the pusher, and in this situation, the carbonaceous material is energized between the two first terminal electrodes. The molded body was heated to a predetermined temperature with electric resistance.

そしてさらに、前記接続器を、以下の要素を備えるものにした。
i)前記2個の第2ターミナル電極の上面又は下面にそれぞれ連結して自由端側を対向させる水平配置の一対の導体板。
ii)一端が一方の前記導体板に、他端が他方の前記導体板にそれぞれ炉体長手直角方向に長い長孔に通される垂直なピボット軸で回動可能に連結される可動フレーム。
iii)前記可動フレームに支持される対向配置の上部可撓導体及び下部可撓導体。
iv)上部可撓導体の両端の下面及び下部可撓導体の両端の上面にそれぞれ設ける炉体軸方向に長い上部接点及び下部接点。
v)上部可撓導体と下部可撓導体を対向方向に付勢して前記上部接点と下部接点を前記導体板の上下面に押しつける接点押圧ばね。
Furthermore, the connector has the following elements.
i) A pair of horizontally arranged conductor plates that are respectively connected to the upper or lower surfaces of the two second terminal electrodes and face the free ends.
ii) A movable frame that is pivotally connected to one of the conductor plates and the other end to the other conductor plate by a vertical pivot shaft that is passed through a long hole extending in a direction perpendicular to the length of the furnace body.
iii) Opposed upper flexible conductor and lower flexible conductor supported by the movable frame.
iv) Upper and lower contacts that are long in the axial direction of the furnace body, provided on the lower surfaces of both ends of the upper flexible conductor and on the upper surfaces of both ends of the lower flexible conductor, respectively.
v) A contact pressing spring that urges the upper flexible conductor and the lower flexible conductor in opposite directions to press the upper contact and the lower contact against the upper and lower surfaces of the conductor plate.

この黒鉛化炉の好ましい構成を以下に列挙する。
(a)前記接続器と同一構成の接続器を前記第2ターミナル電極の上部と下部の双方に有し、前記2個の第2ターミナル電極相互の電気接続が第2ターミナル電極の上部と下部の2箇所でなされるもの。
(b)前記上部可撓導体と下部可撓導体との間に、上下の可撓導体を相反する方向に押し動かして前記上部接点と下部接点を前記導体板から引き離す押圧解除機構を備えたもの。
(c)前記第2ターミナル電極の上面と下面を平坦な面にしてその上面と下面に、前記導体板を面接触させて取付けたもの。
(d)前記上部接点及び下部接点のコンタクト面をR面にしたもの。
(e)前記上部可撓導体、下部可撓導体、上部接点、下部接点をそれぞれ前記炉体の軸方向に複数に分割したもの。
Preferred configurations of this graphitization furnace are listed below.
(A) A connector having the same configuration as that of the connector is provided on both the upper and lower portions of the second terminal electrode, and electrical connection between the two second terminal electrodes is provided between the upper and lower portions of the second terminal electrode. What is done in two places.
(B) A pressing release mechanism is provided between the upper flexible conductor and the lower flexible conductor to push and move the upper and lower flexible conductors in opposite directions to separate the upper and lower contacts from the conductor plate. .
(C) The upper surface and the lower surface of the second terminal electrode are made flat and the conductor plate is attached to the upper and lower surfaces in surface contact.
(D) A contact surface of the upper contact and the lower contact is an R surface.
(E) The upper flexible conductor, the lower flexible conductor, the upper contact, and the lower contact are each divided into a plurality in the axial direction of the furnace body.

この発明の黒鉛化炉は、2個の第2ターミナル電極の電気接続を炉外で行なって炭素質成形体群を両側からプッシャーで押圧する。また、2個の第2ターミナル電極を導通させる接続器を上記の構成にすることで、2個の第2ターミナル電極に炉体軸方向への移動の自由度を付与する。   In the graphitization furnace according to the present invention, the two second terminal electrodes are electrically connected outside the furnace, and the carbonaceous compact group is pressed from both sides with a pusher. Moreover, the freedom degree of the movement to a furnace body axial direction is provided to two 2nd terminal electrodes by making the connector which conducts two 2nd terminal electrodes into said structure.

横2列に並べた炭素質成形体群の電気接続を、炉内のカーボンブロックによって行なう炉の場合、炭素質成形体群の軸方向押圧を炉の片側からしか行なえず、2箇所のチャンバに挿入された炭素質成形体群に熱膨張差が生じたときに両チャンバ内炭素質成形体の突き合わせ部の面圧がばらつく。   In the case of a furnace in which the carbonaceous compact groups arranged in two horizontal rows are electrically connected by the carbon block in the furnace, the axial pressing of the carbonaceous compact groups can be performed only from one side of the furnace, and the two chambers are connected to each other. When a difference in thermal expansion occurs in the inserted carbonaceous molded body group, the surface pressure of the butted portions of the carbonaceous molded bodies in both chambers varies.

その問題に対し、炭素質成形体群の電気接続を炉外で行なう構造にして炭素質成形体群を両側からプッシャーで押圧することで、その不具合を解消して面圧のばらつきを減少させることができる。   In response to this problem, the carbonaceous molded body group is electrically connected to the outside of the furnace, and the carbonaceous molded body group is pressed with a pusher from both sides, thereby eliminating the problem and reducing variations in surface pressure. Can do.

また、2個の第2ターミナル電極を炉外で電気的に接続する方法として、一般的なフレキシブル導体を用いる図12〜図14の接続構造を検討した。この接続構造は、第2ターミナル電極4の上面と下面にL型導体板21をボルト止めして取付け、2個の第2ターミナル電極のL型導体板21,21間をフレキシブル導体22でつなぐものである。フレキシブル導体22は、ボルトで軸方向に締め付けてL型導体板21に端部を連結する。   Moreover, the connection structure of FIGS. 12-14 using a general flexible conductor was examined as a method of electrically connecting the two second terminal electrodes outside the furnace. In this connection structure, an L-shaped conductor plate 21 is bolted to the upper and lower surfaces of the second terminal electrode 4 and the flexible conductor 22 connects between the L-shaped conductor plates 21 and 21 of the two second terminal electrodes. It is. The flexible conductor 22 is tightened in the axial direction with a bolt to connect the end to the L-shaped conductor plate 21.

この図12〜図14の接続構造では、2つのチャンバに挿入された炭素質成形体群の軸方向寸法がずれるとフレキシブル導体22が撓み、それによって第2ターミナル電極4,4の軸方向への相対変位が許容される。   In the connection structure of FIGS. 12 to 14, the flexible conductor 22 bends when the axial dimension of the carbonaceous molded body group inserted in the two chambers is shifted, thereby causing the second terminal electrodes 4 and 4 to move in the axial direction. Relative displacement is allowed.

ところが、この接続構造は、第2ターミナル電極間に設けるフレキシブル導体22が炉外に設置される設備点検用の歩廊23と干渉し、図示のような導体配置ができないという問題が生じた。   However, in this connection structure, the flexible conductor 22 provided between the second terminal electrodes interferes with the facility inspection corridor 23 installed outside the furnace, and there is a problem that the conductor arrangement as illustrated cannot be performed.

また、この接続構造は、2箇所のチャンバに挿入された炭素質成形体群の熱膨張差が大きくなると、フレキシブル導体22に対して引っ張り力が働き、そのためにL型導体板21との間の接触抵抗が変動して電気導通の安定が損なわれる可能性がある。さらに、炉内の温度は3000℃にも達するため、接続部の輻射熱による温度上昇が著しい状況下で引っ張り力を受けることになり、従って、耐久性確保の面でも好ましくない。   Further, in this connection structure, when the difference in thermal expansion between the carbonaceous molded body groups inserted into the two chambers becomes large, a tensile force acts on the flexible conductor 22, and therefore, the connection between the L-shaped conductor plate 21 and the flexible conductor 22. The contact resistance may fluctuate and the stability of electrical conduction may be impaired. Furthermore, since the temperature in the furnace reaches 3000 ° C., it is subjected to a tensile force under a situation where the temperature rise due to the radiant heat of the connecting portion is significant, and therefore, it is not preferable in terms of ensuring durability.

これに加え、2個の第2ターミナル電極間にフレキシブル導体22の変位吸収能を超える相対移動が生じた場合、フレキシブル導体22の外れや断線が起こる虞もある。   In addition, when relative movement exceeding the displacement absorption capacity of the flexible conductor 22 occurs between the two second terminal electrodes, the flexible conductor 22 may be disconnected or disconnected.

この発明の黒鉛化炉に採用した接続器は、これらの問題にも対応したものである。この接続器の導体板は、炉内の炭素質成形体が熱膨張したとき、或いは冷却されて収縮したときに、それぞれの導体板に連結されている第2ターミナル電極と一体になって軸方向に動く。   The connector employed in the graphitization furnace of the present invention also addresses these problems. When the carbonaceous molded body in the furnace is thermally expanded or cooled and contracts, the conductor plate of this connector is integrated with the second terminal electrode connected to each conductor plate in the axial direction. It moves to.

そのときの対の導体板の軸方向移動量が、各列の炭素質成形体群の熱伸縮量の不可避のずれなどによって異なると、接続器の可動フレームがピボット軸を支点にして回動する。   If the amount of axial movement of the pair of conductor plates at that time differs due to the unavoidable deviation of the amount of thermal expansion / contraction of the carbonaceous molded body groups in each row, the movable frame of the connector rotates about the pivot shaft. .

上部接点と下部接点は各導体板を挟みつけているが、接点押圧ばねの力で挟持圧を加えているので接続器の可動フレームの回動は支障なくなされ、その回動が進行している間も上部接点と下部接点が安定した力で導体板に押しつけられるため、2個の第2ターミナル電極間の電気導通が安定して維持される。   The upper contact and the lower contact sandwich each conductor plate, but because the clamping pressure is applied by the force of the contact pressing spring, the movable frame of the connector is turned without any trouble, and the turning is progressing. Since the upper contact and the lower contact are pressed against the conductor plate with a stable force, the electrical conduction between the two second terminal electrodes is stably maintained.

また、2個の第2ターミナル電極の電気接続を上記接続器で行うことで、図12の接続部に比べて上下方向の接続器設置スペースを縮小して歩廊との干渉の問題をなくすことができる。さらに、その接続器を使用することでプッシャーによるターミナル電極の軸方向押圧を第2ターミナル電極が配置される炉体の他端側でも支障なく行うことができる。   Also, by performing the electrical connection of the two second terminal electrodes with the above-mentioned connector, the space for installing the connector in the vertical direction can be reduced as compared with the connection part of FIG. 12, and the problem of interference with the corridor can be eliminated. it can. Furthermore, by using the connector, the axial push of the terminal electrode by the pusher can be performed without any trouble on the other end side of the furnace body in which the second terminal electrode is disposed.

このように、2個の第2ターミナル電極の電気接続を上記接続器で行うことで、炭素質成形体群の熱膨張差による長さ変動の吸収が安定してなされ、各列の炭素質成形体群の炉の両側からのプッシャーによる軸方向押圧が安定して炭素質成形体が均一に加熱されるようになる。
なお、好ましいとした構成の作用・効果は後に説明する。
As described above, the electrical connection of the two second terminal electrodes is performed by the connector, so that the length variation due to the difference in thermal expansion of the carbonaceous molded body group is stably absorbed, and the carbonaceous molding of each row is performed. The axial pressing by the pushers from both sides of the furnace of the body group is stabilized and the carbonaceous molded body is heated uniformly.
The operation and effect of the preferred configuration will be described later.

この発明の黒鉛化炉の概要を示す平面図The top view which shows the outline | summary of the graphitization furnace of this invention 図1の黒鉛化炉の概要を示す側面図Side view showing the outline of the graphitization furnace in FIG. 第2ターミナル電極の相互電気接続部の平面図Plan view of the mutual electrical connection of the second terminal electrode 図3のX−X線に沿った断面図Sectional drawing along the XX line of FIG. 図3のY−Y線に沿った図The figure along the YY line of FIG. 第2ターミナル電極に接続器の導体板を取り付けた状態の平面図Top view of the state where the conductor plate of the connector is attached to the second terminal electrode 第2ターミナル電極の軸方向変位量が、右側で大となったときの接続器の動作を示す平面図The top view which shows operation | movement of a connector when the axial direction displacement amount of a 2nd terminal electrode becomes large on the right side 第2ターミナル電極の軸方向変位量が、左側で大となったときの接続器の動作を示す平面図The top view which shows operation | movement of a connector when the axial direction displacement amount of a 2nd terminal electrode becomes large on the left side 接続器の他の例を示す平面図Plan view showing another example of connector 図9の接続器の端面図End view of the connector of FIG. 図9の接続器の側面図Side view of the connector of FIG. 第2ターミナル電極の接続構造の参考例を示す平面図The top view which shows the reference example of the connection structure of the 2nd terminal electrode 図12の接続構造の側面図Side view of the connection structure of FIG. 図12の接続構造の斜視図12 is a perspective view of the connection structure of FIG.

以下、添付図面の図1〜図11に基づいて、この発明の黒鉛化炉の実施の形態を説明する。
図1に示すように、例示の黒鉛化炉1は、軸方向に長く形成された炉体2と、対向配置の第1ターミナル電極3及び第2ターミナル電極4と、それらのターミナル電極を個々に押圧するプッシャー5を有する。そして、さらに、第1、第2ターミナル電極3,4に働く反力を個々に受ける反力柱6と、対をなす2個の第2ターミナル電極4,4を炉外で電気的に導通させる接続器7を組み合わせて構成されている。
Hereinafter, an embodiment of a graphitization furnace according to the present invention will be described with reference to FIGS.
As shown in FIG. 1, an exemplary graphitization furnace 1 includes a furnace body 2 that is formed long in the axial direction, first terminal electrodes 3 and second terminal electrodes 4 that are opposed to each other, and these terminal electrodes individually. It has a pusher 5 to press. Further, the reaction force column 6 that individually receives the reaction force acting on the first and second terminal electrodes 3 and 4 and the two second terminal electrodes 4 and 4 that make a pair are electrically connected outside the furnace. The connector 7 is combined.

炉体2は、互いに区画された並列配置の2つのチャンバ2aを有する(図1参照)。その炉体2の一端側に、炉外から炉壁を貫通して2つのチャンバ2a、2aに個別に臨ませる2個の第1ターミナル電極3が設けられている。   The furnace body 2 has two chambers 2a arranged in parallel and separated from each other (see FIG. 1). Two first terminal electrodes 3 are provided on one end side of the furnace body 2 so as to penetrate the furnace wall from the outside of the furnace and individually face the two chambers 2a and 2a.

各第1ターミナル電極3は、軸方向スライド可能に配置されており、炉外において給電装置8経由で電源(図のそれはブスバー母線11)に接続される。   Each first terminal electrode 3 is arranged so as to be slidable in the axial direction, and is connected to a power source (that is, busbar bus 11 in the figure) via a power feeding device 8 outside the furnace.

また、炉体2の他端側に、炉外から炉壁を貫通して2つのチャンバ2a、2aに個別に臨ませる2個の第2ターミナル電極4が設けられている。その第2ターミナル電極4も軸方向スライド可能になっている。この第2ターミナル電極4は共に平坦な上面4aと下面4bを有する。   Further, two second terminal electrodes 4 are provided on the other end side of the furnace body 2 so as to penetrate the furnace wall from the outside of the furnace and individually face the two chambers 2a and 2a. The second terminal electrode 4 is also slidable in the axial direction. The second terminal electrode 4 has a flat upper surface 4a and lower surface 4b.

炉体2は周知の構造のものでよい。上記特許文献5などに詳しい構造が開示されている。従って、ここでの詳細説明は省く。   The furnace body 2 may have a known structure. A detailed structure is disclosed in Patent Document 5 and the like. Therefore, the detailed description here is omitted.

プッシャー5は、油圧シリンダなどで構成される。このプッシャー5が建屋内に設置された反力柱6に支持されて第1、第2ターミナル電極3、4を、軸方向、かつ両者が互いに近づく方向に押圧する。   The pusher 5 is composed of a hydraulic cylinder or the like. The pusher 5 is supported by the reaction force column 6 installed in the building and presses the first and second terminal electrodes 3 and 4 in the axial direction and in the direction in which both approach each other.

反力柱6は、図2に示すように炉外に設置され、その反力柱6で、ターミナル電極を軸方向に押圧して炭素質成形体の突き合せ部に面圧を加えたときにプッシャー5に加わる反力を受け止めるようにしている。   The reaction force column 6 is installed outside the furnace as shown in FIG. 2, and when the reaction force column 6 presses the terminal electrode in the axial direction and applies a surface pressure to the butted portion of the carbonaceous molded body, The reaction force applied to the pusher 5 is received.

接続器7は、第2ターミナル電極4の上部と下部に設けられ(図4参照)、2個の第2ターミナル電極4,4の相互電気接続が2組の接続器7でなされる。   The connector 7 is provided at the upper part and the lower part of the second terminal electrode 4 (see FIG. 4), and the two second terminal electrodes 4 and 4 are connected to each other by the two sets of connectors 7.

それぞれの接続器7は、図3〜図6に示した水平配置の一対の導体板7a、7aR、Lは、説明の便宜上付した)と、両導体板間に配置される可動フレーム7bを有する。また、可動フレーム7bの一端を一方の導体板7aに、他端を他方の導体板7aにそれぞれ連結するピボット軸7cと、対向配置の上部可撓導体7d及び下部可撓導体7dと、炉体軸方向に長い上部接点7e及び下部接点7eを有し、さらに、上部接点7eと下部接点7eを互いに接近する方向に付勢する接点押圧ばね7fを有する。 Each connector 7 includes a pair of horizontally disposed conductor plates 7a R and 7a L ( R and L are given for convenience of explanation) shown in FIGS. 3 to 6 and a movable plate disposed between the two conductor plates. It has a frame 7b. The movable frame 7b one end of the one conductor plate 7a R, and a pivot shaft 7c which respectively connect the other end to the other conductor plate 7a L, upper flexible conductor 7d U and lower flexible conductor 7d B of opposed And an upper contact 7e U and a lower contact 7e B that are long in the furnace body axis direction, and further, a contact pressing spring 7f that urges the upper contact 7e U and the lower contact 7e B toward each other.

導体板7a,7aは、各第2ターミナル電極4,4の上面と下面にそれぞれ連結して自由端側を対向させている。この導体板7a,7aの第2ターミナル電極4に対する連結は、ボルト9によってなされている。その導体板7a,7aは、第2ターミナル電極4,4の平坦な上面と下面に面接触させており、電気導通の安定性に優れる。 The conductor plates 7a R and 7a L are connected to the upper and lower surfaces of the second terminal electrodes 4 and 4, respectively, and are opposed to the free ends. The conductor plates 7a R and 7a L are connected to the second terminal electrode 4 by bolts 9. The conductor plates 7a R and 7a L are in surface contact with the flat upper and lower surfaces of the second terminal electrodes 4 and 4, and are excellent in electrical conduction stability.

可動フレーム7bは、対向配置の上枠fと下枠f、及びその2者を連結する連結枠fからなる。この可動フレーム7bの導体板7a,7aに対する連結が前記ピボット軸7cによってなされる。 Movable frame 7b is top frame f 1 and the lower frame f 2 of oppositely disposed, and a connecting frame f 3 which connects the two parties. The movable frame 7b is connected to the conductor plates 7a R and 7a L by the pivot shaft 7c.

導体板7a,7aには、平面視で炉体の長手方向に対して直角方向に長い長孔7gを設けてあり、その長孔7gにピボット軸7cが通される。可動フレーム7bは、そのピボット軸7cを支点にして回動することができる。 The conductor plates 7a R and 7a L are provided with a long hole 7g which is long in a direction perpendicular to the longitudinal direction of the furnace body in plan view, and a pivot shaft 7c is passed through the long hole 7g. The movable frame 7b can rotate with its pivot shaft 7c as a fulcrum.

上部可撓導体7dと下部可撓導体7dは、可動フレーム7bで支持している。可動フレーム7bは、上下の可撓導体の両端を個々に上下動可能に差し込む横向き開口の差し込み部Sを両端に備えている。その差し込み部Sは上下二段に配置され、上部、下部の各差し込み部S間に平行配置の2つの支持壁Wが設置される。 Upper flexible conductor 7d U and the lower flexible conductor 7d B is supported by the movable frame 7b. The movable frame 7b is provided with insertion portions S with lateral openings at both ends into which both ends of the upper and lower flexible conductors are individually inserted so as to be movable up and down. The insertion portions S are arranged in two upper and lower stages, and two support walls W arranged in parallel are installed between the upper and lower insertion portions S.

上部可撓導体7dと下部可撓導体7dは、可動フレーム7bの熱伸縮による上部接点7eと下部接点7eの相対変位を吸収し得るものであればよく、さほど大きな変位吸収能は要求されない。 The upper flexible conductor 7d U and the lower flexible conductor 7d B only need to be able to absorb the relative displacement of the upper contact 7e U and the lower contact 7e B due to the thermal expansion and contraction of the movable frame 7b. Not required.

上部接点7eと下部接点7eは、コンタクト面をR面にした接点であり、上部可撓導体7dの両端の下面及び下部可撓導体7dの両端の上面にそれぞれ一体的に設けられる。前記支持壁Wには、それ等の接点に対応させた貫通孔を設けており、その貫通孔に上部接点7eと下部接点7eがそれぞれ出没自在に差し込まれる。 The upper contact 7e U and the lower contact 7e B are contacts with the R contact surface, and are integrally provided on the lower surfaces of both ends of the upper flexible conductor 7d U and the upper surfaces of both ends of the lower flexible conductor 7d B , respectively. . The support wall W is provided with through holes corresponding to the contact points, and the upper contact point 7e U and the lower contact point 7e B are respectively inserted into the through holes so as to be able to appear and retract.

この上部接点7eと下部接点7e及びそれを個別に保持する上部、下部の可撓導体7d,7dは、図示のように、軸方向に分割したものが動きの自由度が高くて好ましい。上部接点7eと下部接点7eは、分割後も軸方向に長い姿を有する接点となっている。 The upper contact 7e U and the lower contact 7e B and the upper and lower flexible conductors 7d U and 7d B that hold the individual contacts are divided in the axial direction as shown in the figure, and the degree of freedom of movement is high. preferable. The upper contact 7e U and the lower contact 7e B are contacts that are long in the axial direction even after being divided.

接点押圧ばね7fは、各差し込み部Sの内部に組み込まれており、上部可撓導体7dと下部可撓導体7dの両端部を互いに接近する方向に付勢する。その付勢力により支持壁Wを貫通した上部接点7eと下部接点7eが導体板7a,7aの自由端側の上下面に押し当てられる。 Contact pressure spring 7f is incorporated inside each spigot S, biases the opposite end portions of the upper flexible conductors 7d U and the lower flexible conductor 7d B toward each other. Due to the biasing force, the upper contact 7e U and the lower contact 7e B penetrating the support wall W are pressed against the upper and lower surfaces of the conductor plates 7a R and 7a L on the free end side.

なお、図示したように、上部、下部の可撓導体7d,7dが軸方向に分割されている場合には、各分割可撓導体を接点押圧ばね7fで個々に押圧して各接点の導体板に対する押圧が平均化した圧力でなされるようにしておくのがよい。 As shown in the figure, when the upper and lower flexible conductors 7d U and 7d B are divided in the axial direction, each of the divided flexible conductors is individually pressed by the contact pressing spring 7f to It is preferable that the pressure on the conductor plate is made at an averaged pressure.

例示の黒鉛化炉1には、以上のように構成された接続器7が第2ターミナル電極4の下面側にも設けられ、2個の第2ターミナル電極4,4の電気接続が、その第2ターミナル電極4,4の上部と下部の2箇所でなされている。このようにすることで、接続器7に対する負荷を軽減して接続器7の耐久性を向上させることができる。なお、下側の接続器7の導体板7a,7aは、第2ターミナル電極4の下面4bに固定される。 In the illustrated graphitization furnace 1, the connector 7 configured as described above is provided also on the lower surface side of the second terminal electrode 4, and electrical connection between the two second terminal electrodes 4, 4 is performed in the first graphitizing furnace 1. Two terminal electrodes 4 and 4 are formed at the upper and lower portions. By doing in this way, the load with respect to the connector 7 can be reduced and the durability of the connector 7 can be improved. The conductor plates 7 a R and 7 a L of the lower connector 7 are fixed to the lower surface 4 b of the second terminal electrode 4.

給電装置8は、第1ターミナル電極3に導体板を接続し、その導体板を断路器の上下の接点で挟みつけるように構成された前掲の特許文献4に開示されるものが、導体板の相対移動の自由度に優れて好ましい。   The power feeding device 8 is disclosed in the aforementioned Patent Document 4 configured to connect a conductor plate to the first terminal electrode 3 and sandwich the conductor plate between the upper and lower contacts of the disconnector. It is preferable because of its excellent freedom of relative movement.

以上のように構成された例示の黒鉛化炉1は、再焼成済みの炭素質成形体Cを各チャンバ2aの内部に直列に配列し、周辺を保温と酸化防止のためのコークス詰粉などで被包充填する。そして、この状態で末端の炭素質成形体に当接したターミナル電極を介して通電する。   In the exemplary graphitization furnace 1 configured as described above, the re-fired carbonaceous compacts C are arranged in series inside the chambers 2a, and the periphery thereof is made of coke filling powder for keeping heat and preventing oxidation. Encapsulate and fill. And in this state, it supplies with electricity through the terminal electrode which contact | abutted to the carbonaceous molded object of the terminal.

第1ターミナル電極3に給電装置8を接続し、2個の第2ターミナル電極4を接続器7
でつなぐ。
The power supply device 8 is connected to the first terminal electrode 3, and the two second terminal electrodes 4 are connected to the connector 7.
Connect.

また、プッシャー5で第1、第2ターミナル電極3,4を炉の両端から軸方向に押圧し、各炭素質成形体Cの相互突き合せ面に所要の面圧を加える。   Further, the first and second terminal electrodes 3 and 4 are pressed in the axial direction from both ends of the furnace by the pusher 5, and a required surface pressure is applied to the mutual butted surfaces of the carbonaceous molded bodies C.

そしてこの状態で直流電源から電力を供給して炭素質成形体群Cg,Cgに電気を流す。こうして各炭素質成形体Cを電気抵抗によって発熱させ、所要温度(一般には3000℃程度)まで昇温させて黒鉛化処理を行なう。 In this state, electric power is supplied from a DC power source to cause electricity to flow through the carbonaceous molded body groups C R g and C L g. In this way, each carbonaceous molded body C is heated by electric resistance and is heated to a required temperature (generally about 3000 ° C.) to perform graphitization.

この加熱により各チャンバ2aに収容された炭素質成形体群Cg,Cgが熱膨張する。そのときの炭素質成形体群Cg,Cgの熱膨張量が等しければ、接続器7の左右の導体板7a,7aと上部、下部の接点7eU,7eの相対位置が変化せずに維持され、接続器7による電気接続の状態変化が全く起こらない。 This is accommodated in each chamber 2a by heating the carbonaceous molding group C R g, C L g is thermally expanded. If the amount of thermal expansion of the carbonaceous molded body groups C R g and C L g at that time is equal, the relative positions of the left and right conductor plates 7a R and 7a L of the connector 7 and the upper and lower contacts 7e U and 7e B Is maintained unchanged, and the state of the electrical connection by the connector 7 does not change at all.

一方、炭素質成形体群Cg,Cgの熱膨張量に差が生じて両炭素質成形体群Cg,Cgの軸方向長さが変わると、接続器7の可動フレーム7bが、左右のピボット軸7cを支点にして図7、図8に示すように回動する。 On the other hand, carbonaceous molding group C R g, C L the thermal expansion difference occurs between both carbonaceous molding group g C R g, when the axial length of the C L g is changed, moving the connector 7 The frame 7b rotates as shown in FIGS. 7 and 8 with the left and right pivot shafts 7c as fulcrums.

可動フレーム7bは、炭素質成形体群Cgの熱膨張量が炭素質成形体群Cgの熱膨張量よりも大きいときには、図7に示すように、平面視で時計回りの方向に回動し、左右の炭素質成形体群Cg,Cgの熱膨張量の大小関係が上記と逆の場合は、図8に示すように、平面視で反時計回りの方向に回動する。 When the thermal expansion amount of the carbonaceous molded body group C R g is larger than the thermal expansion amount of the carbonaceous molded body group C L g, the movable frame 7b is rotated in the clockwise direction in plan view as shown in FIG. If the magnitude relationship between the thermal expansion amounts of the left and right carbonaceous molded body groups C R g and C L g is opposite to the above, as shown in FIG. 8, it rotates in the counterclockwise direction as seen in a plan view. Move.

このとき、上部接点7eと下部接点7eは、導体板7a,7aに対してバネの力で単純に押し付けられているので、それらの接点を導体板7a,7aに喰い込ませるような力が発生せず、そのために2個の第2ターミナル電極4,4の軸方向相対変位が支障なく進行する。 At this time, the upper contact 7e U and the lower contact 7e B are simply pressed against the conductor plates 7a R and 7a L by the force of the spring, so that these contacts bite into the conductor plates 7a R and 7a L. Such a force does not occur, so that the axial relative displacement of the two second terminal electrodes 4 and 4 proceeds without any trouble.

そしてその間も、接続器7の上部接点7eと下部接点7eが平均した圧力で左右の導体板7a,7aに押しつけられ、接続器7による電気接続条件の変動が起こらない。 In the meantime, the upper contact 7e U and the lower contact 7e B of the connector 7 are pressed against the left and right conductor plates 7a R and 7a L with an average pressure, so that the electrical connection conditions by the connector 7 do not vary.

また、各炭素質成形体群Cg,Cgを炉の両端からプッシャー5で押圧することで炭素質成形体相互の突合せ面の接触抵抗の変動も殆ど起こらない。 Further, when the respective carbonaceous molded body groups C R g and C L g are pressed by the pushers 5 from both ends of the furnace, the contact resistance of the butt surfaces between the carbonaceous molded bodies hardly varies.

これにより、各列の炭素質成形体群の通電条件が安定して炭素質成形体が均一に加熱され、加熱のばらつきによる品質のばらつきや品質不良の問題が解消される。   As a result, the energization conditions of the carbonaceous molded body groups in each row are stabilized and the carbonaceous molded bodies are heated uniformly, and the problems of quality variations and quality defects due to variations in heating are solved.

また、2個の第2ターミナル電極4,4の電気接続を接続器7で行ったことで、上下方向の接続器設置スペースが縮小され、必要に応じて図13の位置に設ける歩廊との干渉をなくすことができる。   Further, the electrical connection of the two second terminal electrodes 4 and 4 is performed by the connector 7, so that the space for installing the connector in the vertical direction is reduced, and interference with the corridor provided at the position of FIG. 13 as necessary. Can be eliminated.

図9〜図11に、接続器7の変形例を示す。黒鉛化炉は、同一工場内に並列配置にして複数基設けることが多い。その場合、経済的な方法として、同一接続器を着脱可能にし、ひとつの接続器を複数の炉で共用することが考えられる。その方法を採る場合、上部接点7eと下部接点7eの導体板に対する押圧を解除可能となすことが必要となる。 9 to 11 show modifications of the connector 7. In many cases, a plurality of graphitization furnaces are arranged in parallel in the same factory. In that case, as an economical method, it is conceivable to make the same connector detachable and share one connector among a plurality of furnaces. When this method is adopted, it is necessary to be able to release the pressing of the upper contact 7e U and the lower contact 7e B against the conductor plate.

図9〜図11の接続器7は、その機能を付与したものであって、上部可撓導体7dと下部可撓導体7d間に押圧解除機構10を追設している。その他の部分は図3の接続器と同一構成である。従って、ここでの説明は、押圧解除機構10のみについて行なう。 Connector 7 of 9 to 11, there is imparted with the function, and additionally provided a pressure release mechanism 10 between the upper flexible conductor 7d U and the lower flexible conductor 7d B. Other parts are the same as those of the connector of FIG. Therefore, the description here will be made only for the press release mechanism 10.

図示の押圧解除機構10は、周知のスライダクランク機構を応用したものであって、駆動軸10aと、その駆動軸10aの両端付近に各々固定するクランク10bと、各クランクの両端に一端がピンで回動可能に連結された対をなす2本のリンク10cと、その2本のリンク10cの他端にそれぞれ取り付けるスライドピン10dとで構成されている。   The illustrated pressure release mechanism 10 is an application of a known slider crank mechanism, and includes a drive shaft 10a, a crank 10b fixed near both ends of the drive shaft 10a, and one end at each end of each crank. The two links 10c are paired so as to be rotatable, and the slide pins 10d are respectively attached to the other ends of the two links 10c.

駆動軸10aは、ハンドル(図示せず)を取り付ける入力部ipを一端に有している。この駆動軸10aが連結枠fの対向側壁間に回転可能に横架され、入力部ipに取り付けたハンドルの操作によって回転駆動される。 The drive shaft 10a has an input part ip to which a handle (not shown) is attached at one end. The drive shaft 10a is rotatably laterally placed between the opposite side walls of the connecting frame f 3, it is rotated by operation of the handle attached to the input unit ip.

クランク10bに連結されたリンク10cは、駆動軸10aの両端付近に対応した姿勢にして配置され、その駆動軸10aの両端付近の対応した姿勢のリンク10cにスライドピン10dの両端が固定されている。そのスライドピン10dは、可動フレームの連結枠fに設けられたガイド部(図示せず。縦長の溝や孔で構成される)に案内されて上下に動くことができる。 The link 10c connected to the crank 10b is disposed in a posture corresponding to the vicinity of both ends of the drive shaft 10a, and both ends of the slide pin 10d are fixed to the link 10c in a corresponding posture near both ends of the drive shaft 10a. . As the slide pin 10d can guide portion provided on the connecting frame f 3 of the movable frame (not shown. Constituted by elongated grooves or holes) is guided by the moving up and down.

スライドピン10dは、対をなすリンクの一方に取り付けられたものが上部可撓導体7dの湾曲した部分に、他方に取り付けられたものが下部可撓導体7dの湾曲部にそれぞれ接するようにしている。 Slide pin 10d is the portion that is attached to one of the links in a pair curved upper flexible conductor 7d U, which is attached to the other as in contact with the curved portion of the lower flexible conductor 7d B ing.

この接続器7は、駆動軸10aを、それに取り付けたハンドルを操作して回転させる。その操作でクランク10bに対するリンク10cの連結点が変位し、そのために、2本のスライドピン10dが駆動軸10aから遠ざかる方向に押し動かされる。これにより、上部可撓導体7dと下部可撓導体7dが相反する方向に押し動かされ、その動きに上部接点7eと下部接点7eが追従してそれらの接点の導体板7a,7aに対する押圧が解除される。 The connector 7 rotates the drive shaft 10a by operating a handle attached thereto. As a result, the connecting point of the link 10c with respect to the crank 10b is displaced, so that the two slide pins 10d are pushed away from the drive shaft 10a. As a result, the upper flexible conductor 7d U and the lower flexible conductor 7d B are pushed and moved in opposite directions, and the upper contact 7e U and the lower contact 7e B follow the movement, and the conductor plates 7a R , 7a L is released.

その押圧の解除とピボット軸7cによる導体板との連結の解除を行なうことで接続器7は取り外し可能となり、これにより、同一接続器を共通仕様の他の黒鉛化炉に共用することが可能になる。   By releasing the pressing and releasing the connection with the conductor plate by the pivot shaft 7c, the connector 7 can be removed, and thus the same connector can be shared with other graphitization furnaces of common specifications. Become.

なお、この構造では、押圧解除機構10による押圧の解除がなされたときに、上部可撓導体7dと下部可撓導体7dの両端部が接点押圧ばね7fの力に抗して離反方向に動く必要があるので、上部可撓導体7dと下部可撓導体7dは、ある程度剛性のあるものを使用する。 In this structure, when the release of the pressing by the pressing release mechanism 10 is made, in the separating direction both end portions of the upper flexible conductors 7d U and the lower flexible conductor 7d B is against the force of the contact pressure spring 7f Since it is necessary to move, the upper flexible conductor 7d U and the lower flexible conductor 7d B are used to be somewhat rigid.

なお、実施形態の接続器7は、定格電圧DC300V、定格電流90kAの仕様であり、使用時の温度上昇が懸念される。そのために、いずれも、導体板7a,7aと、上部、下部の可撓導体7d,7dと、可動フレーム7bの内部にそれぞれ水の循環通路(図示省略)を形成し、その循環通路に冷却水を流してこれらを強制冷却する構造にしてあるが、
強制冷却は必要に応じて行えばよい。
Note that the connector 7 of the embodiment has a specification with a rated voltage of DC 300 V and a rated current of 90 kA, and there is a concern about a temperature rise during use. Therefore, in each case, water circulation passages (not shown) are formed in the conductor plates 7a R and 7a L , the upper and lower flexible conductors 7d U and 7d B, and the movable frame 7b, respectively. It is structured to forcibly cool these by flowing cooling water through the passage,
The forced cooling may be performed as necessary.

1 黒鉛化炉
2 炉体
2a チャンバ
3 第1ターミナル電極
4 第2ターミナル電極
4a 上面
4b 下面
5 プッシャー
6 反力柱
7 接続器
7a,7a 導体板
7b 可動フレーム
7c ピボット軸
7d 上部可撓導体
7d 下部可撓導体
7e 上部接点
7e 下部接点
7f 接点押圧ばね
7g 長孔
W 支持壁
S 差し込み部
上枠
下枠
連結枠
8 給電装置
9 ボルト
10 押圧解除機構
10a 駆動軸
10b クランク
10c リンク
10d スライドピン
11 ブスバー母線
ip 入力部
C 炭素質成形体
g,Cg 炭素質成形体群
21 L型導体板
22 フレキシブル導体
23 歩廊
DESCRIPTION OF SYMBOLS 1 Graphitization furnace 2 Furnace body 2a Chamber 3 1st terminal electrode 4 2nd terminal electrode 4a Upper surface 4b Lower surface 5 Pusher 6 Reaction force column 7 Connector 7a R , 7a L conductor plate 7b Movable frame 7c Pivot shaft 7d U upper flexible Conductor 7d B Lower flexible conductor 7e U Upper contact 7e B Lower contact 7f Contact pressing spring 7g Long hole W Support wall S Insertion part f 1 Upper frame f 2 Lower frame f 3 Connecting frame 8 Power supply device 9 Bolt 10 Press release mechanism 10a Drive shaft 10b Crank 10c Link 10d Slide pin 11 Bus bar bus line ip Input part C Carbonaceous molded body C R g, C L g Carbonaceous molded body group 21 L-shaped conductor plate 22 Flexible conductor 23 Walkway

Claims (7)

互いに区画された並列配置の2つのチャンバ(2a)を有する軸方向に長い炉体(2)と、その炉体の一端側において炉外から前記2つのチャンバ(2a)に個別に臨ませる軸方向スライド可能な2個の第1ターミナル電極(3)と、各炉体(2)の他端側において炉外から前記2つのチャンバ(2a)に個別に臨ませる軸方向スライド可能な2個の各々が上下面を有する第2ターミナル電極(4)と、前記第1、第2ターミナル電極(3,4)を個々に軸方向に押圧するプッシャー(5)と、前記第1、第2ターミナル電極(3,4)に働く反力を個々に受ける反力柱(6)と、前記2個の第2ターミナル電極(4)を炉外で電気的に導通させる接続器(7)を有し、
各チャンバ(2a)に直列に配列される複数の焼成済み炭素質成形体(C)の相互突き合せ面に前記プッシャー(5)で面圧を加え、この状況で、2個の第1ターミナル電極(3,3)間に通電して炭素質成形体(C)を電気抵抗で所定温度に加熱する黒鉛化炉であって、
前記接続器(7)が、前記2個の第2ターミナル電極(4,4)の上面(4a)又は下面(4b)にそれぞれ連結して自由端側を対向させる水平配置の一対の導体板(7a,7a)と、一端が一方の前記導体板(7a)に、他端が他方の前記導体板(7a)にそれぞれ炉体長手直角方向に長い長孔(7g)に通される垂直なピボット軸(7c)を支点にして回動可能に連結される可動フレーム(7b)と、対向配置にして前記可動フレーム(7b)に支持される上部可撓導体(7d)及び下部可撓導体(7d)と、上部可撓導体(7d)の両端の下面及び下部可撓導体(7d)の両端の上面にそれぞれ設ける炉体軸方向に長い上部接点(7e)及び下部接点(7e)と、前記上部可撓導体(7d)と下部可撓導体(7d)を対向方向に付勢して前記上部接点(7e)と下部接点(7e)を前記導体板(7a,7a)の上下面に押し当てる接点押圧ばね(7f)を備えて構成される黒鉛化炉。
An axially long furnace body (2) having two chambers (2a) arranged in parallel and separated from each other, and an axial direction individually facing the two chambers (2a) from outside the furnace body at one end side of the furnace body Two slidable first terminal electrodes (3) and two slidable in the axial direction individually facing the two chambers (2a) from outside the furnace at the other end of each furnace body (2) Has a second terminal electrode (4) having upper and lower surfaces, a pusher (5) for individually pressing the first and second terminal electrodes (3, 4) in the axial direction, and the first and second terminal electrodes ( 3 and 4) having a reaction force column (6) that individually receives a reaction force acting on 3), and a connector (7) that electrically connects the two second terminal electrodes (4) outside the furnace,
A surface pressure is applied by the pusher (5) to the mutually butted surfaces of a plurality of calcined carbonaceous molded bodies (C) arranged in series in each chamber (2a), and in this situation, two first terminal electrodes (3, 3) is a graphitization furnace in which a carbonaceous molded body (C) is heated to a predetermined temperature with electric resistance by energizing between
The connector (7) is connected to the upper surface (4a) or the lower surface (4b) of the two second terminal electrodes (4, 4), respectively, and a pair of horizontally arranged conductor plates facing the free end side ( 7a R , 7a L ), one end is passed through one conductor plate (7a R ) and the other end is passed through the other conductor plate (7a L ) through a long hole (7g) elongated in the furnace body longitudinal direction. A movable frame (7b) that is pivotally connected with a vertical pivot shaft (7c) as a fulcrum, and an upper flexible conductor (7d U ) and a lower portion that are opposed to each other and supported by the movable frame (7b). A flexible conductor (7d B ), an upper contact (7e U ) long in the furnace body axial direction provided on the lower surface of both ends of the upper flexible conductor (7d U ) and the upper surface of both ends of the lower flexible conductor (7d B ), Lower contact (7e B ), upper flexible conductor (7d U ) and lower Contact pressing spring that biases the upper flexible conductor (7d B ) in the opposite direction and presses the upper contact (7e U ) and the lower contact (7e B ) against the upper and lower surfaces of the conductive plate (7a R , 7a L ) A graphitization furnace comprising (7f).
前記接続器(7)と同一構成の接続器(7)を前記第2ターミナル電極(4)の上部と下部の双方に有し、前記2個の第2ターミナル電極(4,4)相互の電気接続が第2ターミナル電極(4,4)の上部と下部の2箇所でなされた請求項1に記載の黒鉛化炉。   A connector (7) having the same configuration as that of the connector (7) is provided on both the upper part and the lower part of the second terminal electrode (4), and the two second terminal electrodes (4, 4) are electrically connected to each other. 2. The graphitization furnace according to claim 1, wherein the connection is made at two places, an upper part and a lower part of the second terminal electrode (4, 4). 前記上部可撓導体(7d)と下部可撓導体(7d)との間に、上下の可撓導体を相反する方向に押し動かして前記上部接点(7e)と下部接点(7e)を前記導体板(7a,7a)から引き離す押圧解除機構(10)を備えた請求項2に記載の黒鉛化炉。 Between the upper flexible conductor (7d U ) and the lower flexible conductor (7d B ), the upper and lower flexible conductors are pushed in opposite directions to move the upper contact (7e U ) and the lower contact (7e B ). graphitizing furnace according to claim 2 having the conductor plate (7a R, 7a L) pressing release mechanism away from (10) a. 前記第2ターミナル電極(4)の上面(4a)と下面(4b)を平坦な面にしてその上面(4a)と下面(4b)に、前記導体板(7a,7a)を面接触させて取付けた請求項2又は3に記載の黒鉛化炉。 The upper surface (4a) and the lower surface (4b) of the second terminal electrode (4) are made flat and the conductor plates (7a R , 7a L ) are brought into surface contact with the upper surface (4a) and the lower surface (4b). The graphitization furnace according to claim 2 or 3, wherein the graphitization furnace is attached. 前記上部接点(7e)及び下部接点(7e)のコンタクト面をR面にした請求項1〜3のいずれかに記載の黒鉛化炉。 Graphitizing furnace according to claim 1, the contact surface was to the R plane of the top contact (7e U) and bottom contacts (7e B). 前記上部接点(7e)と、下部接点(7e)をそれぞれ炉体の軸方向に複数に分割した請求項1〜5のいずれかに記載の黒鉛化炉。 It said upper contact (7e U), graphitization furnace according to claim 1 which is divided into a plurality of lower contacts (7e B) in the axial direction of the respective furnace body. 前記上部可撓導体(7d,)、下部可撓導体(7d)、上部接点(7e)、下部接点(7e)をそれぞれ炉体の軸方向に複数に分割した請求項1〜6のいずれかに記載の黒鉛化炉。 The upper flexible conductor (7d U ), the lower flexible conductor (7d B ), the upper contact (7e U ), and the lower contact (7e B ) are each divided into a plurality in the axial direction of the furnace body. A graphitization furnace according to any one of the above.
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