JP5320831B2 - Vertical furnace operation method and furnace powdering prevention equipment - Google Patents

Description

  TECHNICAL FIELD The present invention relates to a vertical furnace operating method for preventing in-furnace powdering of vertical furnace charging coke used in a blast furnace or the like.

  In the blast furnace for producing hot metal, iron ore such as sintered ore and lump ore, and massive coke as a heat source and reducing material source are alternately charged from the top of the furnace, and the upper part of the furnace (shaft) Part) are deposited in layers. And the high-temperature air blown into the furnace from the tuyeres at the bottom of the furnace burns the coke accumulated in the furnace to generate high-temperature gas, and the high-temperature gas is between the iron ores and coke particles. The gap flows toward the top of the furnace, and the iron ore and coke are heated, and at the same time, the iron ore is reduced and melted. Therefore, if the gap between the particles is not properly secured, the distribution of the gas flow in the furnace becomes inappropriate for operation, the situation in the furnace becomes worse, and stable and smooth operation cannot be performed. Or, the productivity of the blast furnace decreases. That is, it is very important to ensure the air permeability of the raw material layer for blast furnace operation. When powder is mixed into the raw material charged from the top of the furnace, air permeability is hindered. Therefore, it is necessary to prevent the powder from being mixed as much as possible.

  In addition to the powder mixed into the raw material and charged into the furnace, there is also a problem of powder generated in the furnace. Coke exists in a lump until it is combusted by oxygen supplied from the tuyere at the bottom of the furnace after being charged from the top of the furnace, but lacks fragile parts due to physical contact with other raw materials. As a result, coke powder is generated. This powder becomes clogged between the raw material particles and causes deterioration of the stability and controllability of the gas flow in the furnace. For this reason, it is important to suppress pulverization while coke descends in the furnace.

In order to prevent the occurrence of chipping of the fragile portion, many attempts have been made to keep the coke strength high. For example, even if a large amount of non-caking coal that causes coke strength to be reduced is added to the raw coal, the coke strength will not be reduced. A method of preventing strength reduction of the obtained coke by adding to caking coal and then charging and coking into a coke oven is known (see, for example, Patent Document 1). There is also a method for producing coke having a high porosity and a certain level of strength by adding a pore-forming agent and a binder during blending of raw coal and then charging and coking into a coke oven. It is known (for example, refer to Patent Document 2).
JP 2000-8047 A Japanese Patent Laid-Open No. 11-236573

  The methods described in Patent Document 1 and Patent Document 2 are techniques for improving coke strength by adding an additive to raw coal to improve the average substrate strength of the coke produced.

  However, even when the average substrate strength of coke is improved by blending such an additive, local blending variation (segregation) occurs in the raw material charged into the coke oven. Therefore, in part, coke with a weak substrate is manufactured, and when coke is charged into a blast furnace, the weak coke is pulverized in the furnace.

  Although it is conceivable to use only coal that can produce high-strength coke as the raw material for coke, such coal is expensive, and it is not practical to produce coke using only such varieties of coal. . Even if the strength of the produced coke is low, it is desirable to prevent the coke from being pulverized.

  Therefore, the object of the present invention is to solve such problems of the prior art, and can be applied to any kind of coke, and sufficiently suppresses the pulverization of vertical furnace charging coke such as a blast furnace. An object of the present invention is to provide a vertical furnace operating method that enables smooth and stable furnace operation.

The features of the present invention for solving such problems are as follows.
(1) Using a hopper having a height of 20 m or more, after charging the coke from the upper part of the hopper and discharging it from the lower part, the coke is separated into a lump part and a powdery part, and the separated lump form A method of operating a vertical furnace characterized by using a part in a vertical furnace.
(2) By applying a frictional force and / or compressive force to the surface of the coke in the hopper, the coke is separated into a lump portion and a powdery portion, and the separated lump portion is charged into a vertical furnace. A vertical furnace operating method characterized by being used as
(3) The method for operating a vertical furnace as described in (1) or (2), wherein a sieve is formed by sieving to form a lump on a sieve having a particle size of 6 mm or more.
(4) The method for operating a vertical furnace according to any one of (1) to (3), wherein the coke subjected to the drying treatment is separated into a lump part and a powdery part.
(5) The method for operating a vertical furnace according to (4), wherein the coke is dried in a hopper.
(6) In the operation method of the vertical furnace according to any one of (1) to (5), by adjusting the height of the coke charging surface in the hopper, the coke charged into the vertical furnace is adjusted. A method of operating a vertical furnace characterized by controlling strength.
(7) Used when charging coke into the vertical furnace, a hopper having a height of 20 m or more, a supply conveyor for supplying coke to the hopper, and a discharge for conveying the coke discharged from the hopper Conveyor, sieving device for sieving coke discharged from the discharge conveyor, and conveyor for vertical furnace that conveys the top of the sieve screened by the sieving device for charging from the top of the vertical furnace An in-furnace powdering prevention facility characterized by comprising:
(8) The in-furnace powdering prevention device according to (7), wherein the hopper has a chute capable of moving up and down for supplying coke to the hopper.

  According to the present invention, it is possible to suppress pulverization of coke charged in a vertical furnace such as a blast furnace, and within a certain range of the strength of coke used, it is possible to sufficiently suppress regardless of strength. it can. This enables smooth and stable furnace operation, and improves the productivity of the furnace.

  Conventional handling of coke for vertical furnace charging has been made in order to minimize the impact on the coke and prevent coke pulverization. In other words, the handling that prevents the coke from being damaged due to the force applied to the coke during the process of conveying the coke to the vertical furnace has been considered good. However, when the coke has a fragile portion, pulverization occurs in the furnace no matter how small the impact applied to the coke before charging the vertical furnace. Therefore, the present inventors conversely increase the impact applied to the coke before charging the vertical furnace, thereby preliminarily pulverizing the fragile part of the surface of the coke, and removing the powdery part into the vertical furnace. It is thought that the coke pulverization in the furnace can be suppressed by charging, and the coke is rubbed together using a hopper, and the coke is lumped and powdered by applying frictional force to the surface of the coke. The present invention was completed by finding that it was possible to prevent in-furnace pulverization by using the separated lump portion in a vertical furnace. In addition to frictional force, coke lamination inside the hopper adds compressive force to the coke at the bottom of the hopper, facilitating the destruction of the coke not only due to the fragile part of the coke surface but also due to cracks existing inside the coke. More powdery parts can be generated and separated. When the frictional force and the compressive force are added together, a better effect can be exhibited.

  Separation of the massive part and the powdery part is preferably performed using a sieve. The mass portion charged in the furnace preferably has a particle size of about 6 mm or more, and preferably has a screen size of 6 mm or more.

  If the water content of the coke is high, the sieving efficiency is reduced, and there is a case where the lumpy part and the powdery part are not sufficiently separated, so the coke that has been dried is separated into the lumpy part and the powdery part. It is preferable to do. It is efficient to dry the coke together with application of frictional force and compression impact in a hopper described later.

  In order to impart frictional force or compressive force to the coke, it is only necessary to rub the coke together, and even if it is dropped to a normal hopper etc., a certain effect can be obtained, but in order to promote powdering of the fragile part It is preferable to increase the hopper height and increase the compressive force due to the load received by the coke at the bottom of the hopper. For this purpose, the height of the hopper is preferably 20 m or more. If it is 25 m or more, it is more effective. Here, the height of the hopper is a distance from the lower discharge port of the hopper to the top plate.

  Further, it is effective to provide an uneven portion on the inner wall of the hopper in order to improve the frictional force.

  For such a hopper, it is possible to modify and use a hopper that is usually installed in a raw material charging line for a vertical furnace, but in addition to the existing hopper, a friction force and a compression force are applied. Newly installing a dedicated hopper is more effective because it increases the chance of applying friction to coke.

  In addition, it can be considered that the coke yield decreases and the coke cost increases by separating and removing the powdery part, but powdered coke is used in various applications as a high value-added product in steelworks and others. Therefore, the coke as a whole can be used effectively, and the cost increase does not become a problem.

  The vertical furnace used in the present invention is a blast furnace, a shaft furnace, a gasification melting furnace, a coke bed type melting furnace, or the like, and uses massive coke.

  Hereinafter, an embodiment when the present invention is used in a blast furnace will be described based on the circumstances leading to the present invention.

  The red hot coke pushed out from the coke oven is lowered to a discharge place on a belt conveyor called a wharf after sprinkling fire. Then, after cutting out from the wharf, the mass is crushed with a coke cutter (a type of roll crusher) and then only the desired size is used in the blast furnace through a sieve under the hopper (storage tank) of the blast furnace. . In recent years, in view of energy saving and environmental measures, there is a case where reddish coke is cooled with gas and called “dry fire extinguishing” and then sent to the blast furnace through the same route.

  First, the present inventors consider that in such conventional coke treatment, the fragile portion of coke is not completely removed, but is charged into a blast furnace, and after applying sufficient frictional force between cokes, sieving is performed. I thought that the weak part could be removed by doing. As shown in FIG. 1, a hopper type sizing means 1 (hereinafter simply referred to as a hopper) is further provided in a route for sending from the coke factory or from the coke product yard to the storage tank. The fragile portion was separated and powdered, passed through a sieve 2 and adjusted to a predetermined particle size (for example, 30 to 75 mm), and then sent to a blast furnace storage tank. At that time, a coke sample is collected between the hopper 1 and the sieve 2, the strength test of the coke sample is performed, and the strength data is fed back to the hopper 1 to feed the hopper into the hopper charging level (the amount of coke into the hopper 1). By adjusting the time during which the frictional force is applied to the coke and the compression force in the hopper and adjusting the compression force (the height position of the coke charging surface 15 that varies depending on the charging amount), the charging standard for strength and particle size ( For example, the strength of the coke charged into the blast furnace was controlled by charging the blast furnace with coke that satisfies in-house standards.

  Here, as an example, the hopper 1 may be configured as shown in FIG. That is, the hopper 1 has a sufficient height, and the coke is supplied from above by the charging chute 5 and cut out from the coke discharge port 3 at the lower part of the hopper 1, so that the coke 16 passes the inside of the hopper from the upper part. When moving to the lower part, a frictional force is applied between the cokes and between the coke and the inner wall of the hopper (preferably having irregularities). The coke discharged from the lower part of the hopper 1 is sent to a sieve 2 in a subsequent process. It is preferable that the charging chute 5 has a structure that can move up and down, and that the distance to the charging surface in the hopper can be changed to adjust the drop impact received by the charged coke. As the charging chute 5, it is preferable to use a method in which coke slides down a spiral passage.

  The dimensions of the hopper 1 may be appropriately determined according to the amount of coke to be processed. However, as described above, the compression force applied to the coke can be controlled by adjusting the hopper charging height. It is necessary to take enough.

  Moreover, in this embodiment, as above-mentioned, the coke discharged | emitted from the hopper 1 is sent to the sieve 2, and is arrange | equalized with the particle size used by a blast furnace, Before sampling to the sieve 2, a part of coke is sampled. The strength test is performed, and this strength test method may be a test method appropriately determined for each blast furnace. As an example, there is a drum strength defined in JIS K 2151 (Chapter 9, “Coke Test Methods”, 9.2: Drum Method). Of course, a tumbler method described in the same standard or the like, which is generally used as a test method for coke strength, may be used.

  When the result of the strength test is higher than the upper limit of the control value of the target strength in the blast furnace supplying the coke, the charging level of the hopper 1 is lowered (the coke charging surface in the hopper is set low). . As a result, the time during which frictional force is applied to the coke is shortened, and the compression force applied is also reduced. In addition, when it is lower than the lower limit of the management value of the target strength, the charging level of the hopper 1 is increased (the coke charging surface in the hopper is set high). As a result, the time during which the frictional force is applied to the coke is lengthened, and the compression force applied is also increased. In this case, if a charging chute that freely drops from the upper part of the hopper 1 is used, the drop impact when charging the coke into the hopper is larger when the level is lowered and smaller when the level is raised. Therefore, the direction of charging into the hopper is in the opposite direction to the strength of the frictional force and compressive force to be applied to the coke. It is preferable to drop.

  By adjusting the charging level of the hopper 1 in this way and adjusting the extent to which the fragile part of the coke is destroyed, the coke strength is not less than a certain value without changing the blending of raw coal during the production of coke. Therefore, smooth and stable blast furnace operation can be performed. If the coke strength is higher than the upper limit of the target strength even if the charging level of the hopper 1 is lowered, the coal to be supplied to the coke oven is manufactured at a lower cost and with lower strength. It may be changed to a formulation using In addition, when the charging level is positively increased and a strength higher than the target is obtained, the composition can be made inexpensive so that the strength decreases to the target strength.

  As mentioned above, the case where a hopper type facility is used as a means for forcibly removing the fragile portion of coke was taken as an example, but it is a tank structure like a hopper, and a coke surface is applied by applying a frictional force to the coke surface. Any structure may be used as long as it has a function to remove the weak part of the material in advance and can change the frictional force, compressive force, and application time thereof. In addition, if a weak part is previously removed from coke as in the present invention, the amount of powder coke below the sieve 2 that cannot be used in a blast furnace increases. Generally, in steel mills, powder coke is used as a fuel for sintering raw materials, etc. Because it can be used effectively, it is not wasted.

  Next, separation of the coke that has been subjected to the drying process into a lump part and a powdery part will be described.

  When the frictional force is applied to the surface of the coke and when the compressive force is applied to the coke, the coke powder part is generated when the coke used contains a large amount of water. When using a sieve for separation, the powdery part cannot be sufficiently separated and removed by this sieve, or the sieve itself is clogged and the coke powdery part cannot be removed. . The powdery part that adheres to the coke lump and cannot be separated and removed by sieving is transported to the top of the vertical furnace while being attached to the coke lump, and is dried by the heat in the furnace. Since the coke lump is separated from the surface of the coke lump, a large amount of powdery coke is charged into the furnace, and the powdery part flows through the gap between the raw materials in the furnace and clogs the gap between the raw materials. When the present invention is used for coke having a high water content, such as the phenomenon of hindering the stable gas flow, there is a concern that the effect of the present invention cannot be sufficiently exhibited.

  It is known that a phenomenon in which a powdery part adheres to a coke-like part and separation thereof becomes difficult increases in proportion to the water content of the coke. Therefore, it is preferable to sieve the coke in a dry state, and it is preferable that the amount of water contained in the coke is as small as possible. For that purpose, when applying frictional force or drop impact to the surface of coke, it is arranged at the downstream side to reduce the coke-containing water content by applying constant heat to coke in advance, at the same time or after application. Therefore, it is preferable to dry the coke before sieving.

  The heating method for drying the coke is preferably performed by introducing a heating gas into a container containing coke, and various heating gases generated in a factory are preferably used. In order to remove moisture contained in coke, it is desirable to use hot-blast furnace combustion exhaust gas and heating furnace exhaust gas with low oxygen concentration. However, a heating gas as a dedicated hot-air generation source by installing a combustion furnace, electric furnace, etc. Can also be generated. In addition, as long as nitrogen for controlling the oxygen concentration is introduced, a heated gas such as a cooler exhaust heat of a sintering machine can be used.

  The temperature of the heated gas is sufficient if the coke can be dried, and 60 ° C. or higher is sufficient for drying the coke, and it is desirable to set it to 200 ° C. or lower. This is because moisture contained in coke, which is a carbonaceous material, is dried, so that it is difficult to prevent fire and explosion if the temperature of the heated gas is too high.

  An embodiment in the case of drying coke in a hopper will be described with reference to FIG. In FIG. 1, coke supplied into the hopper 1 via the supply conveyor 4 and the charging chute 5 is dried by the heated gas blown into the hopper 1 from the heated gas blowing nozzle 8 at the lower portion of the hopper 1. It moves and the fragile part is powdered by friction and compressive force. 6 is a heating gas supply duct, and 7 is a heating gas supply fan. The coke discharged from the coke outlet 3 is conveyed to the sieve 2 by the discharge conveyor 13 and separated into a lump part and a powdery part by sieving. The lump portion on the sieve is conveyed by the vertical furnace conveyor 12 and is charged from the top of the vertical furnace by the charging device. The powdery part under the sieve is conveyed by the powder extraction conveyor 14 and used separately. 9 is a dust collecting bag filter, 10 is a dust collecting fan, and 11 is an exhaust gas chimney.

The same equipment as shown in FIG. 1 was used, and a test was conducted in which a coke treatment of 25 t / H was performed and conveyed to a blast furnace. As the hopper 1, a hopper having an inner wall interval of 7 m and a height of 25 m (a maximum height of the coke charging surface of 23 m) was used. In addition, a chute that can move up and down and has a spiral drop passage is provided to reduce the change in the drop impact force even if the level charged in the hopper 1 changes, and the coke is dropped near the charging surface. I let you. Sampling was performed on the upstream side of the sieve 2 at regular time intervals, and coke strength was measured. As a comparative example, the strength of coke not charged into the hopper 1 was also measured. Strength of the coke was measured at prescribed in JIS K 2151 "drum strength", the particle size of the coke sample when strength measurement 15 mm, as 150rpm rotational speed of the test drum, the so-called "drum intensity (symbol DI ^0.99 ₁₅ ) ”. The sieve mesh of the sieve 2 was 6 mm.

  In the case of the comparative example in which the treatment by the hopper 1 is not performed, the coke strength sampled on the upstream side of the sieve 2 is 84.3 on average, but the coke is fed by the hopper 1 to the charging level at the top of the hopper. When charged and discharged, the drum strength of the coke increased to 84.9. That is, the weak part of the coke is removed by the frictional force between the coke inside the hopper and the inner wall of the hopper, and further by the compressive force, thereby increasing the strength of the coke charged into the blast furnace by 0.6 points. did it.

  In the case of the operation test of the present invention in which the sieve top of the sieve 2 is charged into the blast furnace after the treatment with the hopper, compared with the normal operation in which the sieve top of the sieve 2 is charged into the blast furnace without performing the treatment with the hopper. In addition, coke pulverization in the blast furnace was suppressed, so the air permeability of the blast furnace was improved, the gas flow distribution in the furnace was maintained properly, the furnace condition was stabilized, and smooth operation was possible. The amount of molten iron increased by 5% under the same operating conditions.

  When applying frictional force and compressive force to the surface of coke with a hopper using the same equipment as shown in FIG. 1, the coke is kept constant with combustion exhaust gas of 200 ° C. or lower and air of 60 ° C. or lower. In the case where drying was performed with the heat of the above reduced to reduce the water content of coke, and in the case where drying was not performed, the respective treatments were performed and sieved. When the water content of the coke discharged from the coke discharge port 3 of the hopper 1 is 2 mass% or less and the coke with a high water content (3 to 5 mass%) without applying heat, the mass after sieving The separation of the coke and the powdery coke was compared. The results are shown in FIG. The vertical axis in FIG. 2 is the ratio of the powdery part having a particle size of 6 mm or less, which is the fraction under the sieve, mixed on the sieve when sieving with a 6 mm sieve mesh. When the black circle is dried, This is the case when it did not dry.

  In FIG. 2, for example, when the coke with a moisture content of more than 4 mass% when not dried is reduced to a moisture content of 0 mass% by drying, the separation situation differs greatly, and when a sieve with a mesh size of 6 mm is used, The mixing rate of coke (-6 mm) having a particle size of 6 mm or less is reduced from the 3 mass% range to about 0.5 mass%. The reduction in the water content of coke greatly affected the separation of the powdery portion of coke, and it was found that the drying treatment is very effective in preventing in-furnace powdering for coke having a high water content.

It is the schematic which shows one Embodiment of this invention. The graph which shows the effect of drying of coke.

Explanation of symbols

DESCRIPTION OF SYMBOLS 1 Hopper 2 Sieve 3 Coke discharge port 4 Supply conveyor 5 Charge chute 6 Heated gas supply duct 7 Heated gas supply fan 8 Heated gas blowing nozzle 9 Dust collection bag filter 10 Dust collection fan 11 Exhaust gas stack 12 Conveyor for vertical furnace 13 Discharge conveyor 14 Powder extraction conveyor 15 Coke charging surface 16 Coke

Claims (5)

Height Ri der than 20 m, a hopper coke is charged, the sieve comprises a
The hopper has a chute that can move up and down so that the distance to the coke charging surface in the hopper can be changed , using an in-furnace powdering prevention facility ,
Was charged with the coke to the hopper, by adjusting the height of the coke instrumentation Irimen controls the compression force of the coke added in the hopper, and by vertically moving the chute, the Bring the chute close to the coke charging surface, drop the coke, and reduce the change in drop impact force that the coke receives,
After discharging the coke from the lower part of the hopper , the coke is separated into a lump part and a powdery part on a sieve having a particle size of 6 mm or more by the sieve ,
A method for operating a vertical furnace, comprising using the separated lump portion in a vertical furnace. Conduct a strength test of the coke sample collected between the hopper and the sieve,
When the strength data is higher than the upper limit of the control value of the target strength in the vertical furnace, the height position of the coke charging surface is reduced, and when lower than the lower limit of the control value of the target strength, 2. The vertical furnace operating method according to claim 1, wherein the height position of the coke charging surface is raised . The method for operating a vertical furnace according to claim 1 or 2, wherein the coke subjected to the drying treatment is separated into a lump part and a powdery part. The method for operating a vertical furnace according to claim 3 , wherein coke is dried in a hopper. Used when charging coke into a vertical furnace,
A hopper having a height of 20 m or more;
A supply conveyor for supplying coke to the hopper;
A discharge conveyor for conveying coke discharged from the hopper;
A sieving device for sieving the coke discharged from the discharge conveyor;
A shaft furnace for the conveyor for conveying the upper sieve that sieved to the instrumentation needful from the top of the shaft furnace by sieve have divided device, a furnace powdering prevention facility Ru provided with,
The hopper, the furnace powdering prevention equipment, characterized in Rukoto to have a vertically movable chute to allow changing the distance to the coke instrumentation Irimen within the hopper.

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