JP5156528B2 - Beverage in airtight container with high foam retention - Google Patents

Beverage in airtight container with high foam retention Download PDF

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JP5156528B2
JP5156528B2 JP2008198613A JP2008198613A JP5156528B2 JP 5156528 B2 JP5156528 B2 JP 5156528B2 JP 2008198613 A JP2008198613 A JP 2008198613A JP 2008198613 A JP2008198613 A JP 2008198613A JP 5156528 B2 JP5156528 B2 JP 5156528B2
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JP2009050259A (en
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成一郎 池田
祐子 山本
孝司 井上
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株式会社ポッカコーポレーション
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Description

本発明は、密閉容器入り飲料で容器を振ることで泡が立ち、振った後容器を開缶しても5分以上泡沫が保持することができ、視覚的にカプチーノ風の起泡した飲料、すなわち泡沫の保持性が高い飲料及びその製造方法に関する。 The present invention, foam is generated by shaking the container with a beverage in a sealed container, foam can be retained for 5 minutes or more even if the container is opened after shaking, a cappuccino-like foam that is visually foamed, That is, the present invention relates to a beverage having high foam retention and a method for producing the same.

従来より、カプチーノ等のコーヒー、ミルクセーキ、シェイクドリンク、抹茶は泡が形成された飲料で、視覚的かつ口当たりが滑らかとなるテクスチャーを楽しむことができることとして知られている。   Conventionally, coffee such as cappuccino, milk shakes, shake drinks, and matcha tea are known as foamed beverages that can be enjoyed with a visually smooth texture.

これらの特徴をもつ密閉容器入り飲料を製造する方法が検討され、報告されている。すなわち、製造工程中の起泡を抑制し、かつ加熱殺菌後密閉容器に充填された飲料において、容器を振ることで安定的な泡を形成することができる、起泡性飲料の製造方法及びその飲料が開示されている(特許文献1〜8)。
しかし、これらの先行技術は、起泡性に主眼がおかれ、泡沫の保持性について満足するものがないのが現状であった。
A method for producing a hermetically sealed beverage having these characteristics has been studied and reported. That is, in a beverage that suppresses foaming during the manufacturing process and is filled in a sealed container after heat sterilization, a stable foam can be formed by shaking the container, and a method for producing the foamable beverage and its Beverages are disclosed (Patent Documents 1 to 8).
However, these prior arts have been focused on the foaming property, and there is nothing that satisfies the foam retention.

また、これらの先行技術には、泡沫の長時間維持について格別の検討がなされていないだけでなく、温度に対する検討もなされていない。すなわち、アイスでもホットでも、すぐれた起泡性と泡沫の長時間保持性を併有した飲料については、何も記載されていない。 In addition, these prior arts have not been specially studied for maintaining the foam for a long time, and have not been studied for temperature. That is, nothing is described about a beverage having both excellent foaming properties and long-term foam retention properties, whether iced or hot.

更にまた、下記するように、リキャップ機能を有する容器と有機的に組み合わせて、密閉容器入り飲料を数回に分けたりあるいは時間をかけたりして飲む場合においても、その都度、容器を振ることにより、すぐれた起泡性と泡沫の長時間保持性を併有する飲料については、これらの先行技術は何も開示するところがない。 In addition, as described below, in the case of organically combining with a container having a recapping function and drinking a beverage in a sealed container divided into several times or taking time, drink the container each time. As for beverages having both excellent foaming properties and long-term foam retention, these prior arts disclose nothing.

一方、密閉容器入り飲料において、リキャップ機能を有した容器が登場しており、一気に飲み終えるのではなく、数分の時間をかけて飲むことも多くなっている。特にリキャップ機能を有した容器に関しては、キャップの直径が38mm以上の大口径のものも登場し、内容液自体を飲み口からそのまま見ることが可能となっている。このリキャップ機能を有した容器と起泡性飲料とを組み合わせ、視覚的かつ口当たりが滑らかとなるテクスチャーを楽しむことができるような飲料を体感することにより、今まで以上に嗜好性をより高められ、また満足できるものと考えられる。
特開昭59−224673号公報 特開昭60−87775号公報 特開平04−30746号公報 特開平10−295339号公報 特開平11−56244号公報 特開2000−14319号公報 特開2000−60507号公報 特開2000−157232号公報
On the other hand, in a sealed container beverage, a container having a recapping function has appeared, and it is often consumed over several minutes rather than finishing drinking all at once. In particular, with regard to a container having a recapping function, a large-diameter cap having a diameter of 38 mm or more has appeared, and the content liquid itself can be seen as it is from the drinking mouth. By combining the container with this recapping function and a foamable beverage, and experiencing a beverage that can enjoy a texture that is visually smooth and mouthfeel, the palatability can be enhanced more than ever before, It is also considered satisfactory.
JP 59-224673 A JP-A-60-87775 Japanese Patent Laid-Open No. 04-30746 JP-A-10-295339 Japanese Patent Laid-Open No. 11-56244 JP 2000-14319 A JP 2000-60507 A JP 2000-157232 A

本発明は、密閉容器入り飲料の飲用温度帯である4〜60℃の温度範囲で、起泡性に優れ、その泡沫が短時間に消えず保持され、視覚的且つテクスチャーとしても泡沫を楽しむことができる品質が安定な泡沫の保持性の高い密閉容器入り飲料を提供することを目的とする。 The present invention is excellent in foaming property in a temperature range of 4 to 60 ° C., which is a drinking temperature range for beverages in a sealed container, and the foam is maintained without disappearing in a short time, and enjoys the foam visually and as a texture. An object of the present invention is to provide a hermetically sealed beverage with a high foam-retaining property and a stable quality.

本発明者らは、上記目的達成のために、各方面から検討の結果、原料の選択とこれらの新規配合により、泡沫が保持されることをはじめて見出し、しかもこの泡沫保持性が長時間維持され、そのうえ、この性質がホットの場合でもアイスの場合でも、つまり、広い温度帯において発揮されることもはじめて見出した。更に、起泡性についても従来技術と何ら遜色がないことも確認した。 As a result of investigations from various directions, the present inventors have found for the first time that foam is retained by selection of raw materials and these new formulations, and this foam retention is maintained for a long time. In addition, it has been found for the first time that this property is exhibited in a wide temperature range, whether it is hot or iced. Furthermore, it was also confirmed that the foaming property was not inferior to the prior art.

すなわち本発明は、これらの有用新知見に基づき、更に研究の結果遂に完成されたものであって;
請求項1に記載の発明は、泡沫の保持性が高い飲料が、乳由来のタンパク質を0.6重量%以上、動物性由来の脂肪及び/又は植物性由来の脂肪を0.2重量%以上含有し、トータルHLBが14以上である乳化剤を含有することを特徴とする。
請求項2に記載の発明は、請求項1記載の泡沫の保持性が高い飲料において、前記乳化剤を0.2重量%以上含有し、前記乳由来のタンパク質含量(重量%)と乳化剤含量(重量%)との積が、0.12〜0.49となることを特徴とする。
請求項3に記載の発明は、請求項1〜2のいずれか1項に記載の泡沫の保持性が高い飲料において、前記乳由来のタンパク質が、脱脂粉乳が主成分であり、その割合が飲料全量中の2.8重量%以上含有することを特徴とする。
請求項4に記載の発明は、請求項1〜3のいずれか1項に記載の泡沫の保持性が高い飲料において、容器を振ることで泡沫が5分以上消滅しないことを特徴とする。
請求項5に記載の発明は、請求項4記載の泡沫の保持性が高い飲料において、4℃〜60℃の温度範囲の飲料でも前記泡沫が5分以上消滅しないことを特徴とする。
That is, the present invention was finally completed as a result of further research based on these useful new findings;
In the invention according to claim 1, the beverage having high foam retention is 0.6% by weight or more of milk-derived protein, 0.2% by weight or more of animal-derived fat and / or vegetable-derived fat. And an emulsifier having a total HLB of 14 or more.
The invention according to claim 2 is the beverage having high foam retention according to claim 1, wherein the emulsifier is contained in an amount of 0.2% by weight or more, and the protein content (% by weight) and the emulsifier content (weight) of the milk. %) Is 0.12 to 0.49.
Invention of Claim 3 is a drink with high foam retention property of any one of Claims 1-2, The protein derived from the milk is skim milk powder as a main component, The ratio is a drink. It is characterized by containing 2.8% by weight or more in the total amount.
The invention according to claim 4 is characterized in that in the beverage having high foam retention according to any one of claims 1 to 3, the foam does not disappear for more than 5 minutes by shaking the container.
The invention according to claim 5 is characterized in that in the beverage with high foam retention according to claim 4, the foam does not disappear for 5 minutes or more even in a beverage in a temperature range of 4 ° C to 60 ° C.

請求項6に記載の発明は、請求項1〜5のいずれか1項に記載の泡沫の保持性が高い飲料において、密閉容器がリキャップ機能を有していることを特徴とする。
請求項7に記載の発明は、請求項6記載の泡沫の保持性が高い飲料において、前記リキャップ機能を有した密閉容器のキャップの直径が38mm以上の口径であることを特徴とする。
The invention described in claim 6 is characterized in that, in the beverage having high foam retention according to any one of claims 1 to 5, the sealed container has a recapping function.
The invention described in claim 7 is characterized in that, in the beverage having a high foam retention property according to claim 6, the diameter of the cap of the sealed container having the recapping function is a caliber of 38 mm or more.

請求項8に記載の発明は、起泡性を有する密閉容器入り飲料の製造において、乳由来のタンパク質を0.6重量%以上、動物性由来の脂肪及び/又は植物性由来の脂肪を0.2重量%以上含有し、トータルHLBが14以上である乳化剤を含有せしめること、を特徴とする泡沫の保持性が高い飲料を製造する方法に関するものである。   In the invention according to claim 8, in the production of a sealed container-containing beverage having foaming properties, 0.6% by weight or more of milk-derived protein, 0.0% of animal-derived fat and / or vegetable-derived fat is provided. The present invention relates to a method for producing a beverage having high foam retention, characterized by containing an emulsifier containing 2% by weight or more and having a total HLB of 14 or more.

本発明によれば、密閉容器入り飲料の飲用温度帯である4〜60℃の温度範囲で、起泡性に優れ、その泡沫が短時間に消えず保持し、視覚的且つテクスチャーとしても泡沫を楽しむことができる品質が安定な泡沫の保持性の高い密閉容器入り飲料を提供することができる。また、リキャップできる容器を使用することにより、何度も起泡させ、泡沫を維持しつづけることも可能である。したがって、リキャップ機能を有する容器との新規組み合わせによって、従来にない新規にして卓越した効果も奏される。   According to the present invention, in a temperature range of 4 to 60 ° C., which is a drinking temperature zone for beverages in a hermetically sealed container, the foam is excellent in foaming property, and the foam does not disappear in a short time, and the foam is visually and textured. It is possible to provide a hermetically sealed beverage with a highly stable foam holding property that can be enjoyed. Further, by using a container that can be recapped, it is possible to cause foaming many times and continue to maintain the foam. Therefore, a novel combination with a container having a recapping function also brings about a new and outstanding effect that has never been achieved before.

以下、本発明に係る泡沫の保持性の高い密閉容器入り飲料を具体化した一実施形態について、詳述する。   Hereinafter, an embodiment embodying a sealed container-containing beverage with high foam retention according to the present invention will be described in detail.

本発明にいう泡沫の保持性の高い密閉容器入り飲料は、コーヒー乳飲料、ミルク紅茶、ミルクココア、ミルク抹茶、ミルクセーキ、イチゴミルク、バナナミルクのような各種フルーツ味のミルク等の乳飲料が挙げられる。本発明の飲料は容器を振ることにより飲料液の表面上に泡沫を生じる飲料であり、例えばカプチーノのように上層部に泡を形成し、下層部が液状であるものが該当する。   Examples of the beverage in a sealed container with high foam retention according to the present invention include milk beverages such as coffee milk beverages, milk tea, milk cocoa, milk matcha, milk shakes, strawberry milk, and banana milk. It is done. The beverage of the present invention is a beverage in which bubbles are formed on the surface of the beverage liquid by shaking the container. For example, a cappuccino foam is formed in the upper layer portion and the lower layer portion is liquid.

本発明で用いられる乳由来のタンパク質とは、乳成分に存在するタンパク質全体を示すが、乳成分として、脱脂粉乳単独か、脱脂粉乳を主原料として牛乳または全粉乳のいずれかまたは両方を組合わせて用いることができる。その他、適宜、練乳、脱脂乳、濃縮乳、脱脂濃縮乳、部分脱脂乳、生クリーム、バター等を配合しても良い。また、これら乳成分において特に脱脂粉乳が好ましく、その割合が飲料全量中の2.8重量%以上含有することが好ましい。前記の乳成分は、飲料全量中の乳由来のタンパク質が0.6重量%以上、好ましくは0.65重量%以上1.3重量%以下となるような量を配合する。乳由来のタンパク質が0.6重量%未満の場合、泡沫が持続しにくい。また、乳由来のタンパク質が多過ぎても泡沫が持続しにくくなる。   Milk-derived protein used in the present invention refers to the entire protein present in the milk component, but as the milk component, skim milk powder alone or skim milk powder or whole milk powder or a combination of both is used. Can be used. In addition, condensed milk, skim milk, concentrated milk, skim concentrated milk, partially skimmed milk, fresh cream, butter and the like may be blended as appropriate. Of these milk components, nonfat dry milk is particularly preferable, and the proportion thereof is preferably 2.8% by weight or more based on the total amount of beverage. The milk component is blended in such an amount that the milk-derived protein in the total amount of the beverage is 0.6% by weight or more, preferably 0.65% by weight or more and 1.3% by weight or less. When the protein derived from milk is less than 0.6% by weight, the foam is difficult to persist. Moreover, even if there is too much protein derived from milk, it becomes difficult to maintain foam.

本発明で用いられる動・植物性由来の脂肪としては、動物性由来の脂肪及び/又は植物性由来の脂肪が使用される。例えば、動物性由来の脂肪として牛乳や全粉乳などの乳由来の脂肪が挙げられ、植物性由来の脂肪としてパーム油、パーム核油、やし油、ナタネ油、大豆油、コーン油、ゴマ油、米油、オリーブ油、綿実油、アマニ油、桐油、及び椿油等が挙げられる。また、水素添加、分別、エステル交換等の加工がこれらに施された加工油脂を用いてもよい。また、これら動・植物性由来の脂肪を0.2重量%以上、好ましくは0.2重量%よりも多く0.8重量%以下となるような量を配合する。動・植物性由来の脂肪が0.2重量%より少ない場合は、期待する風香味に欠け、また0.8重量%より多い場合は、起泡性及び泡沫の保持性が悪くなる。 As animal- and plant-derived fats used in the present invention, animal-derived fats and / or plant-derived fats are used. For example, fats derived from milk such as cow milk and whole powdered milk can be cited as fats derived from animals, and palm oil, palm kernel oil, palm oil, rapeseed oil, soybean oil, corn oil, sesame oil, Examples include rice oil, olive oil, cottonseed oil, linseed oil, tung oil, and cocoon oil. Moreover, you may use the processing fats and oils which processed these, such as hydrogenation, fractionation, and transesterification. Further, the amount of these animal / plant derived fats is added in an amount of 0.2% by weight or more, preferably more than 0.2% by weight and 0.8% by weight or less. When the fat derived from animals or plants is less than 0.2% by weight, the expected flavor is lacking, and when it is more than 0.8% by weight, foamability and foam retention are deteriorated.

本発明で用いられる乳化剤としては、食品用として通常用いられるものであれば特に限定されず、具体例として、例えばグリセリン脂肪酸エステル、ショ糖脂肪酸エステル、ソルビタン脂肪酸エステル、プロピレングリコール脂肪酸エステル、及びレシチンが挙げられる。グリセリン脂肪酸エステルの具体例としては、ポリグリセリンエステル、モノグリセライド、及びジグリセリンモノ脂肪酸エステルが挙げられる。これらは、単独で含有されてもよいし、2種以上が組み合わされて含有されてもよい。   The emulsifier used in the present invention is not particularly limited as long as it is usually used for food. Specific examples include glycerin fatty acid ester, sucrose fatty acid ester, sorbitan fatty acid ester, propylene glycol fatty acid ester, and lecithin. Can be mentioned. Specific examples of the glycerin fatty acid ester include polyglycerin ester, monoglyceride, and diglycerin monofatty acid ester. These may be contained alone or in combination of two or more.

更にこれらの単独または混合乳化剤のHLB値が14以上を有するものを用いる。HLB値とは、乳化剤分子が持つ油になじみやすい性質と水になじみやすい性質のバランスを表したもので、親水基を持たない物質をHLB=0とし、親油基を持たず親水基のみを持つ物質をHLB=20として等分した値を示す。親油性に対し親水性が大きいほどHLB値も大きく、水に溶けやすい性質の乳化剤であり、逆の場合は水に溶けにくい性質となる。2種以上混合された乳化剤のHLB値は、各乳化剤のHLB値の加重平均となる。前記乳化剤は、飲料全量中の0.2〜0.4重量%、好ましくは0.29〜0.34重量%になるよう添加する。乳化剤の添加量が0.2重量%より低い場合は、製品に所望な起泡性が十分に得ることができず、0.4重量%より多い場合は、風味に影響を及ぼすことから好ましくない。また、使用する乳化剤の脂肪酸組成としてパルミチン酸が80%以上含有することが好ましい。   Furthermore, those having an HLB value of 14 or more of these single or mixed emulsifiers are used. The HLB value represents the balance between the properties of the emulsifier molecules that are easy to adjust to oil and the properties that are easy to adjust to water. A substance that does not have a hydrophilic group is HLB = 0, and it does not have a lipophilic group and has only a hydrophilic group. A value obtained by equally dividing a substance having HLB = 20 is shown. The higher the hydrophilicity compared to the lipophilicity, the larger the HLB value, and the easier it is to dissolve in water. In the opposite case, the emulsifier becomes less soluble in water. The HLB value of the emulsifier mixed in two or more types is a weighted average of the HLB values of each emulsifier. The emulsifier is added in an amount of 0.2 to 0.4% by weight, preferably 0.29 to 0.34% by weight, based on the total amount of beverage. When the added amount of the emulsifier is lower than 0.2% by weight, the desired foaming property cannot be sufficiently obtained in the product, and when it exceeds 0.4% by weight, the flavor is affected, which is not preferable. . Moreover, it is preferable that palmitic acid contains 80% or more as a fatty acid composition of the emulsifier to be used.

乳由来のタンパク質及び乳化剤において、乳由来のタンパク質含量(重量%)と乳化剤含量(重量%)の積が、0.12〜0.49、好ましくは0.19〜0.44となる場合、泡沫の保持性が高くなる。この値から外れた場合は、泡沫の保持性が十分ではなく、短時間で泡沫が消滅するおそれがあり、商品として適さない傾向にある。   When milk-derived protein and emulsifier have a product of milk-derived protein content (% by weight) and emulsifier content (% by weight) of 0.12 to 0.49, preferably 0.19 to 0.44, foam The retention of is increased. When it deviates from this value, the foam retainability is not sufficient, the foam may disappear in a short time, and tends to be unsuitable as a product.

なお、乳由来のタンパク質及び乳化剤においては、これらを混合する工程を有し、混合した後、均質化する。均質化する方法としては、通常の常圧ホモゲナイザーのほか、15MPa以上、好ましくは15〜50MPaの高圧で均質化する高圧ホモゲナイザーや高いせん断力を有しているホモゲナイザーなどを使用することができる。本発明における泡沫の保持性の高い密閉容器入り飲料には、飲料の種類に応じ、コーヒー、紅茶、ココア、抹茶、果汁等の原料液を単独または混合し、乳成分を配合して乳入り飲料とすることのできるものであれば特に限定はされない。原料液としては、それぞれの原料の抽出液、乾燥粉体の溶解液、搾汁液などが挙げられる。 In addition, in milk-derived protein and an emulsifier, it has the process of mixing these, and after mixing, it homogenizes. As a homogenizing method, a normal atmospheric homogenizer, a high pressure homogenizer homogenizing at a high pressure of 15 MPa or more, preferably 15 to 50 MPa, a homogenizer having a high shearing force, or the like can be used. The beverage in a sealed container with high foam retention in the present invention, depending on the type of beverage, a raw liquid such as coffee, tea, cocoa, matcha tea, fruit juice or the like is mixed alone, and a milk component is blended to contain the milk beverage. There is no particular limitation as long as it can be. Examples of the raw material liquid include an extract of each raw material, a solution of dried powder, and a squeezed liquid.

更に、飲料の風香味を損なわない範囲内において、副原料としてショ糖、グルコース、フルクトース、キシロース、果糖ブドウ糖液糖、糖アルコール、人工甘味料等の甘味料や、加熱殺菌による乳タンパク質の沈殿生成を防止できるものであれば特に限定はされないが、例えば重曹が好適に用いられる。pH調整剤、安定剤、酸味料、酸化防止剤、香料などを配合しても良い。 Furthermore, as long as the flavor of the beverage is not impaired, sweeteners such as sucrose, glucose, fructose, xylose, fructose dextrose liquid sugar, sugar alcohol, artificial sweeteners, and milk protein precipitates are produced by heat sterilization. Although it will not specifically limit if it can prevent, For example, baking soda is used suitably. You may mix | blend a pH adjuster, a stabilizer, a sour agent, antioxidant, a fragrance | flavor, etc.

前記安定剤としては、乳化の安定化、増粘等の機能により品質の安定化が望めるものであれば特に限定されないが、例えばでんぷん、セルロース、カラギーナン、アラビアガム、グアガム、キサンタンガム、ローカストビーンガム、ジェランガム、ペクチン、プルラン等の植物起源の多糖類及びその誘導体が好適に用いられる。 The stabilizer is not particularly limited as long as the quality can be stabilized by functions such as stabilization of emulsification and thickening, for example, starch, cellulose, carrageenan, gum arabic, guar gum, xanthan gum, locust bean gum, Polysaccharides of plant origin such as gellan gum, pectin, pullulan and their derivatives are preferably used.

内容液は、密閉容器に充填されるため、殺菌を施すのが好ましく、殺菌方法としては、内容液自体を殺菌する超高温殺菌(UHT殺菌)や高温短時間殺菌(HTST殺菌)と容器に充填した後に殺菌するレトルト殺菌等を用いることができる。 Since the content liquid is filled in an airtight container, it is preferable to sterilize. As sterilization methods, ultra high temperature sterilization (UHT sterilization) or high temperature short time sterilization (HTST sterilization) to sterilize the content liquid itself and filling the container The retort sterilization etc. which are sterilized after carrying out can be used.

また、内容液の品質保持として、脱気した水や不活性ガス雰囲気下での調合、充填を行うことで内容液の酸化劣化の防止をすることができる。 In addition, as the quality of the content liquid is maintained, the content liquid can be prevented from oxidative deterioration by blending and filling in a degassed water or inert gas atmosphere.

本発明における密閉容器としては、缶(アルミニウム、スチール)、ビン(ガラス)、ペットボトル、フルオープンの容器が使用できるが、リキャップ機能を有した容器が望ましく、更には内容液を視認しやすい容器でキャップの直径が38mm以上の大口径のものが好ましい。リキャップ機能を有することで、起泡が少ない場合やより起泡させたい場合、クリーミーな泡を体感したい場合は、適宜満足のいくまで容器を振とうすることが可能になる。泡の調整も適宜可能である。 As the sealed container in the present invention, cans (aluminum, steel), bottles (glass), PET bottles, and full-open containers can be used. However, a container having a recapping function is desirable, and the contents liquid can be easily visually confirmed. A cap having a large diameter of 38 mm or more is preferable. By having a recapping function, it is possible to shake the container to an appropriate degree of satisfaction when foaming is less or when foaming is desired, or when creamy foam is desired. The foam can be adjusted as appropriate.

本発明における泡沫の保持性の高い密閉容器入り飲料は、飲用する際に、適時、例えば10秒〜1分間、手にて容器を振ることにより、気泡性に優れた、飲料の表面に緻密性及び形状保持性に優れた泡沫を有する飲料となり、視覚的且つテクスチャーとして楽しむことができる。更に、該飲料は、アイスでもホットでも飲用することができる。 The beverage in an airtight container with high foam retention in the present invention, when drunk, is shaken by hand for a time, for example, for 10 seconds to 1 minute, so that the surface of the beverage is dense with excellent foamability. And it becomes the drink which has the foam excellent in shape retainability, and can enjoy it visually and as a texture. Furthermore, the beverage can be drunk either iced or hot.

本発明に係る泡沫保持飲料を製造するには、飲料全量中の乳由来のタンパク質が0.6重量%以上、動・植物性由来の脂肪が0.2重量%以上となる量の乳成分及び動・植物性脂肪、トータルHLBが14以上である乳化剤、及び所望するのであれば、安定剤を順次(又は同時に)溶解し、得られた溶解液を通常のホモゲナイザーあるいは15MPa以上の条件で高圧ホモゲナイザーにより均質化する。 To produce a foam-retaining beverage according to the present invention, milk components in an amount such that the protein derived from milk in the total amount of the beverage is 0.6% by weight or more, and the fat derived from animals and plants is 0.2% by weight or more, and Animal / vegetable fat, emulsifier with total HLB of 14 or more, and if desired, stabilizers are dissolved sequentially (or simultaneously), and the resulting solution is a normal homogenizer or a high pressure homogenizer under conditions of 15 MPa or more. To homogenize.

得られた均質化液を原料液に添加して最後に定量になるようゲージアップして、調合液とする。さらに調合液を前記ホモゲナイザーで均質化しても良い。また、前記溶解液の段階では均質化せず、調合液の段階で均質化することもできる。原料液としては、各原料の抽出液、乾燥粉体の溶解液、これらにショ糖、その他の副原料を添加したものが挙げられる。 The obtained homogenized liquid is added to the raw material liquid, and finally gauged up so as to be a fixed amount to obtain a preparation liquid. Further, the preparation liquid may be homogenized with the homogenizer. Further, it is possible to homogenize at the stage of the preparation liquid without being homogenized at the stage of the solution. Examples of the raw material liquid include an extract of each raw material, a solution of dry powder, and those obtained by adding sucrose and other auxiliary materials to these.

例えばコーヒーの場合、コーヒー抽出液にショ糖を添加して溶解した後、重曹を加えてpHを調整し、これを原料液として使用することができる。 For example, in the case of coffee, after adding sucrose to a coffee extract and dissolving it, sodium bicarbonate is added to adjust the pH, and this can be used as a raw material liquid.

得られた調合液を80〜95℃に昇温した後、リキャップ機能を有する容器に充填し、常法にしたがって殺菌して泡沫の保持性の高い密閉容器入りコーヒー飲料を得る。 After heating up the obtained preparation liquid to 80-95 degreeC, it fills with the container which has a recapping function, and it sterilizes in accordance with a conventional method, and obtains the coffee drink with an airtight container with high foam retention property.

本発明に係る飲料は、比較例に比して起泡性が高いだけでなく、泡沫の保持性が高く、起泡して5分間室温放置後において、泡沫部分の容積の減少率がわずか1〜5%程度、アイスの場合でも5〜10%程度、ホットの場合でも10〜18%程度であって、泡沫の保持性が高いという著効が奏される。 The beverage according to the present invention not only has a high foaming property as compared with the comparative example, but also has a high foam retention property, and after foaming and standing at room temperature for 5 minutes, the rate of decrease in the volume of the foamed part is only 1 About 5%, about 5 to 10% even in the case of ice, and about 10 to 18% even in the case of hot, and has a remarkable effect that the foam retention is high.

また、10分間という長時間室温放置後においても、泡沫部分の容積の減少率がわずか1〜5%程度にすぎず、アイスの場合でも5〜18%程度、ホットの場合でも5〜18%程度であって泡沫の保持性が高いという著効が奏される。10分間放置後においてもこのように泡沫の高い保持性が得られることは従来未知であってきわめて顕著な効果である。 Moreover, even after standing at room temperature for a long time of 10 minutes, the decrease rate of the volume of the foam portion is only about 1 to 5%, about 5 to 18% even in the case of ice, and about 5 to 18% even in the case of hot. And the remarkable effect that foam retainability is high is produced. Such a high retention of foam even after being left for 10 minutes is an unprecedented and extremely remarkable effect.

したがって本発明は、起泡性を有する密閉容器入り飲料において、泡沫を長時間維持する方法ないし泡沫部分の容積の減少を抑制ないし防止する方法も提供するものである。 Therefore, the present invention also provides a method for maintaining foam for a long time or a method for suppressing or preventing a decrease in the volume of the foam portion in a sealed container-containing beverage having foaming properties.

次に、各実施例を挙げて前記実施態様を更に具体的に説明するが、本発明はこれらに限定されるものではない。 Next, although the said embodiment is demonstrated more concretely, giving each Example, This invention is not limited to these.

(実施例1)
焙煎したコーヒー豆を粉砕後、95℃の熱水でコーヒー豆量に対し約9倍量の湯にて40分間抽出を行った。抽出された液は、金属メッシュ(80メッシュ)を通過後、冷却プレートに供され、20℃以下で保持した。得られた液(以下、コーヒー抽出液)の可溶性固形分はBx3.00であり、抽出率は28%であった。このコーヒー抽出液を最終1000mlあたりでの焙煎豆の使用量が54gになるように秤量した。この抽出液に、ショ糖50g添加し完全に溶解した後、調合液のpHが6.5になるよう重曹を1.25g添加した。
Example 1
After the roasted coffee beans were pulverized, extraction was performed with hot water at 95 ° C. for about 40 minutes with about 9 times the amount of coffee beans. The extracted liquid was passed through a metal mesh (80 mesh) and then supplied to a cooling plate and kept at 20 ° C. or lower. The obtained liquid (hereinafter referred to as coffee extract) had a soluble solid content of Bx3.00 and an extraction rate of 28%. This coffee extract was weighed so that the amount of roasted beans used per 1000 ml was 54 g. To this extract, 50 g of sucrose was added and completely dissolved, and then 1.25 g of sodium bicarbonate was added so that the pH of the prepared solution was 6.5.

次いで、飲料全量中に対して、乳成分として乳由来のタンパク質含量が0.98重量%になる量を60℃の水300gで溶解した脱脂粉乳23gおよび全粉乳9.5gに、植物性油脂として0.2重量%となる量のナタネ由来の乳化植物油脂4.3gと、乳化剤として0.34重量%となる量のショ糖脂肪酸エステル(HLB16)3.5gと、安定剤として増粘多糖類0.6gを順次溶解した。この溶解液を前記コーヒー抽出液に添加して最後に1000mlになるようゲージアップしたものを調合液とした。 Next, with respect to the total amount of beverage, 23 g of skimmed milk powder and 9.5 g of whole milk powder in which the milk-derived protein content of 0.98% by weight is dissolved in 300 g of water at 60 ° C. Emulsified vegetable oil and fat derived from rapeseed in an amount of 0.2% by weight, 3.5 g of sucrose fatty acid ester (HLB16) in an amount of 0.34% by weight as an emulsifier, and thickening polysaccharide as a stabilizer 0.6 g was dissolved sequentially. The solution was added to the coffee extract and gauged up to a final volume of 1000 ml.

この調合液を15MPaの条件で高圧ホモゲナイザーにより均質化した後、90℃に昇温後、キャップの直径が38mmのリキャップ機能を有する170ml容量の缶に充填し、レトルト殺菌(123.5℃、26分間、F=45)を行い、目的とする泡沫の保持性の高い密閉容器入りコーヒー飲料を得た。
なお、前記コーヒー飲料は、乳由来のタンパク質含量が0.98重量%、動・植物性由来の脂肪が0.47重量%、乳化剤含量が0.34重量%、乳由来のタンパク質含量(重量%)と乳化剤含量(重量%)との積が0.33となっている。
The mixture was homogenized with a high-pressure homogenizer under the condition of 15 MPa, heated to 90 ° C., filled into a 170 ml capacity can with a recap function with a cap diameter of 38 mm, and retort sterilized (123.5 ° C., 26 F 0 = 45) for a minute, and the desired coffee beverage in a sealed container with high foam retention was obtained.
The coffee beverage has a milk-derived protein content of 0.98% by weight, animal and vegetable fats of 0.47% by weight, an emulsifier content of 0.34% by weight, and a milk-derived protein content (% by weight). ) And the emulsifier content (% by weight) is 0.33.

(比較例1)
実施例1記載の秤量したコーヒー抽出液に、ショ糖50g添加し完全に溶解した後、調合液のpHが6.5になるよう重曹を1.25g添加した。飲料全量中に対して、乳成分として乳由来のタンパク質含量が1.31重量%になる量を60℃の水300gで溶解した脱脂粉乳40gに、乳化剤として0.03重量%になる量のショ糖脂肪酸エステル(HLB16)0.3gと、起泡剤として卵白ペプタイド0.8gと、安定剤として増粘多糖類0.6gを順次溶解した。この溶解液を前記コーヒー抽出液に添加して最後に1000mlになるようゲージアップしたものを調合液とした。
(Comparative Example 1)
50 g of sucrose was added to the weighed coffee extract described in Example 1 and completely dissolved, and then 1.25 g of sodium bicarbonate was added so that the pH of the prepared solution was 6.5. An amount of 0.03% by weight as emulsifier is added to 40 g of skim milk powder in which the amount of protein derived from milk as a milk component is 1.31% by weight dissolved in 300 g of water at 60 ° C. A sugar fatty acid ester (HLB16) 0.3 g, an egg white peptide 0.8 g as a foaming agent, and a thickening polysaccharide 0.6 g as a stabilizer were sequentially dissolved. The solution was added to the coffee extract and gauged up to a final volume of 1000 ml.

この調合液を15MPaの条件で高圧ホモゲナイザーにより均質化した後、90℃に昇温後、リキャップ機能を有する170ml容量の缶に充填し、レトルト殺菌(123.5℃、26分間、F=45)を行い、卵白ペプチドを気泡剤として添加された密閉容器入り起泡性コーヒー飲料を得た。
なお、前記コーヒー飲料は、乳由来のタンパク質含量が1.31重量%、動・植物性由来の脂肪が0.04重量%、乳化剤含量が0.03重量%、乳由来のタンパク質含量(重量%)と乳化剤含量(重量%)との積が0.04となっている。
This mixed solution was homogenized with a high-pressure homogenizer under the condition of 15 MPa, heated to 90 ° C., filled into a 170 ml capacity can with a recap function, and retort sterilized (123.5 ° C., 26 minutes, F 0 = 45 ) To obtain a foamable coffee beverage in a sealed container to which egg white peptide was added as a foaming agent.
The coffee beverage has a milk-derived protein content of 1.31% by weight, an animal / plant-derived fat content of 0.04% by weight, an emulsifier content of 0.03% by weight, and a milk-derived protein content (% by weight). ) And the emulsifier content (% by weight) is 0.04.

(比較例2)
実施例1記載の秤量したコーヒー抽出液に、ショ糖50g添加し完全に溶解した後、調合液のpHが6.5になるよう重曹を1.25g添加した。飲料全量中に対して、乳成分として乳由来のタンパク質含量が0.98重量%になる量を60℃の水300gで溶解した脱脂粉乳30gに、乳脂肪として0.23重量%となる量の乳脂肪(クリーム)5.14gと、植物性油脂として0.08重量%となる量のナタネ由来の乳化植物油脂1.71gと、乳化剤として0.34重量%になる量のショ糖脂肪酸エステル(HLB11)3.5gと、安定剤として増粘多糖類0.6gを順次溶解した。この溶解液を前記コーヒー抽出液に添加して最後に1000mlになるようゲージアップしたものを調合液とした。
(Comparative Example 2)
50 g of sucrose was added to the weighed coffee extract described in Example 1 and completely dissolved, and then 1.25 g of sodium bicarbonate was added so that the pH of the prepared solution was 6.5. An amount of 0.23% by weight as milk fat is added to 30 g of skim milk powder in which the amount of protein derived from milk as a milk component is 0.98% by weight dissolved in 300 g of water at 60 ° C. 5.14 g of milk fat (cream), 1.71 g of emulsified vegetable oil derived from rapeseed in an amount of 0.08% by weight as vegetable oil, and sucrose fatty acid ester in an amount of 0.34% by weight as an emulsifier ( 3.5 g of HLB11) and 0.6 g of thickening polysaccharide as a stabilizer were sequentially dissolved. The solution was added to the coffee extract and gauged up to a final volume of 1000 ml.

この調合液を15MPaの条件で高圧ホモゲナイザーにより均質化した後、90℃に昇温後、リキャップ機能を有する170ml容量の缶に充填し、レトルト殺菌(123.5℃、26分間、F=45)を行い、乳化剤のHLB値が低い乳化剤を使用した密閉容器入り起泡性コーヒー飲料を得た。
なお、前記コーヒー飲料は、乳由来のタンパク質含量が0.98重量%、動・植物性由来の脂肪が0.34重量%、乳化剤含量が0.34重量%、乳由来のタンパク質含量(重量%)と乳化剤含量(重量%)との積が0.33となっている。
This mixed solution was homogenized with a high-pressure homogenizer under the condition of 15 MPa, heated to 90 ° C., filled into a 170 ml capacity can with a recap function, and retort sterilized (123.5 ° C., 26 minutes, F 0 = 45 ) To obtain a foamable coffee beverage in an airtight container using an emulsifier having a low HLB value of the emulsifier.
The coffee beverage has a milk-derived protein content of 0.98% by weight, animal and vegetable fats of 0.34% by weight, an emulsifier content of 0.34% by weight, and a milk-derived protein content (% by weight). ) And the emulsifier content (% by weight) is 0.33.

(試験例1)
実施例1で作製した泡沫の保持性の高い密閉容器入りコーヒー飲料(実施例1)及び比較例1で作製した密閉容器入り起泡性コーヒー飲料(比較例1)を用いて、以下の方法にて測定した。
(Test Example 1)
Using the foam-contained coffee beverage (Example 1) with high foam retention property produced in Example 1 and the foamed coffee beverage (Comparative Example 1) produced in Comparative Example 1, the following method was used. Measured.

測定方法:使用するコーヒー飲料(以下、サンプル)は予め4〜10℃にし、試験は室温(20〜28℃)で実施した。サンプルを100ml容量のガラス製メスシリンダーに起泡しないように注意しながら50ml注ぎ、口部に市販のラップを装着し、液が漏れないように手によって6秒間に上下10回(30cm幅)になるよう振とうした後直ちに静置し、静置直後、5分後、10分後の泡沫部分の容積を測定した。
結果を表1及び図1に示す。
Measurement method: The coffee beverage to be used (hereinafter referred to as sample) was previously set to 4 to 10 ° C., and the test was performed at room temperature (20 to 28 ° C.). Pour 50 ml of the sample into a 100 ml glass graduated cylinder, taking care not to foam, attach a commercially available wrap to the mouth, and by hand 10 times up and down (30 cm width) for 6 seconds so that the liquid does not leak. The mixture was allowed to stand immediately after shaking, and the volume of the foamed portion was measured immediately after standing, 5 minutes later, and 10 minutes later.
The results are shown in Table 1 and FIG.

Figure 0005156528
Figure 0005156528

表1のとおり静置直後は、実施例1の泡沫部分の容積は26mlで、比較例1の泡沫部分の容積は14mlとなり、実施例1の方が比較例1に比べ泡沫部分の容積が大きく、起泡性において優れていることが明らかとなった。また、図1のとおり静置5分後においては、実施例1の泡沫部分の減少容積は1mlとなっており、ほとんど減少していなかった。一方、比較例1の泡沫部分の減少容積は4mlとなり泡沫容積の減少が見られた。更に、静置10分後においても、実施例1の泡沫部分の減少容積は2mlとなっており、ほとんど減少していなかったが、比較例1の泡沫部分の減少容積は9mlとなりかなりの泡沫の減少が見られた。すなわち、実施例1は静置10分後においても静置直後と泡沫部分の容積はほとんど変化が無く、泡沫を保持していることが確認され、比較例1と比べ泡沫の保持性に優れていることが明らかとなった。 Immediately after standing as shown in Table 1, the volume of the foam part of Example 1 is 26 ml, the volume of the foam part of Comparative Example 1 is 14 ml, and the volume of the foam part of Example 1 is larger than that of Comparative Example 1. It was revealed that the foaming property was excellent. Further, as shown in FIG. 1, after 5 minutes of standing, the reduced volume of the foam portion of Example 1 was 1 ml, and was hardly reduced. On the other hand, the reduction volume of the foam part of Comparative Example 1 was 4 ml, and the reduction of the foam volume was observed. Furthermore, even after 10 minutes of standing, the reduced volume of the foam part of Example 1 was 2 ml and was hardly reduced, but the reduced volume of the foam part of Comparative Example 1 was 9 ml, which was quite foamy. A decrease was seen. That is, in Example 1, even after 10 minutes of standing, the volume of the foam part is almost the same as that immediately after standing, and it is confirmed that the foam is retained. It became clear that

以上のことから、実施例1は比較例1と比べ起泡性及び泡沫の保持性に優れていることが確認された。 From the above, it was confirmed that Example 1 was superior in foaming property and foam retention property as compared with Comparative Example 1.

(試験例2)
実施例1で作製した泡沫の保持性の高い密閉容器入りコーヒー飲料(実施例1)及び比較例2で作製した密閉容器入り起泡性コーヒー飲料(比較例2)を用いて、以下の方法にて測定した。
(Test Example 2)
Using the foamed coffee beverage (Example 1) having a high foam retention property produced in Example 1 and the foaming coffee beverage (Comparative Example 2) in the sealed container produced in Comparative Example 2, the following method was used. Measured.

測定方法:使用するコーヒー飲料(以下、サンプル)は予め、4〜10℃(アイス)または55〜60℃(ホット)にし、試験は室温(20〜28℃)で実施した。サンプルを100ml容量のガラス製メスシリンダーに起泡しないように注意しながら50ml注ぎ、口部に市販のラップを装着し、液が漏れないように手によって6秒間に上下10回(30cm幅)になるよう振とうした後直ちに静置し、静置直後、5分後、10分後の泡沫部分の容積を測定した。 Measurement method: The coffee beverage to be used (hereinafter referred to as sample) was previously set to 4 to 10 ° C. (ice) or 55 to 60 ° C. (hot), and the test was performed at room temperature (20 to 28 ° C.). Pour 50 ml of the sample into a 100 ml glass graduated cylinder, taking care not to foam, attach a commercially available wrap to the mouth, and by hand 10 times up and down (30 cm width) for 6 seconds so that the liquid does not leak. The mixture was allowed to stand immediately after shaking, and the volume of the foamed portion was measured immediately after standing, 5 minutes later, and 10 minutes later.

結果を表2(アイス)、表3(ホット)及び図2(アイス)、図3(ホット)に示す。 The results are shown in Table 2 (Ice), Table 3 (Hot), FIG. 2 (Ice), and FIG. 3 (Hot).

Figure 0005156528
Figure 0005156528

Figure 0005156528
Figure 0005156528

表2のとおりサンプルを予め4〜10℃にした場合、静置直後は、実施例1の泡沫部分の容積は18mlで、比較例2の泡沫部分の容積は18mlとなり、全く差は認められなかった。しかし、図2のとおり静置5分後においては、実施例1の泡沫部分の減少容積は5mlであったが、比較例2の泡沫部分の減少容積は15mlとかなり泡沫容積の減少が見られた。更に、静置10分後においても、実施例1の泡沫部分の減少容積は、比較例2と比べ少なく、実施例1の方が泡沫の保持性に優れていることが明らかとなった。 When the sample was previously set to 4 to 10 ° C. as shown in Table 2, immediately after standing, the volume of the foam part of Example 1 was 18 ml, and the volume of the foam part of Comparative Example 2 was 18 ml, and no difference was observed. It was. However, as shown in FIG. 2, after 5 minutes of standing, the reduced volume of the foam part of Example 1 was 5 ml, but the reduced volume of the foam part of Comparative Example 2 was 15 ml, and the foam volume was considerably reduced. It was. Furthermore, even after 10 minutes of standing, the reduced volume of the foam portion of Example 1 was smaller than that of Comparative Example 2, and it was revealed that Example 1 was superior in foam retention.

一方、表3のとおりサンプルを予め55〜60℃にした場合、静置直後は、実施例1の泡沫部分の容積は42mlで、比較例2の泡沫部分の容積は40mlとなり、ほとんど差は認められなかった。しかし、図3のとおり静置5分後においては、実施例1の泡沫部分の減少容積は4mlであったが、比較例2の泡沫部分の減少容積は10mlとかなり泡沫容積の減少が見られた。更に、静置10分後においても、実施例1の泡沫部分の減少容積は4mlで静置5分後と変化が無かった。一方、比較例2の泡沫部分の減少容積は16mlとなり更に泡沫部分の容積が減少していることが確認された。すなわち、実施例1は比較例2と比べ、泡沫の保持性に優れていることが明らかとなった。 On the other hand, when the sample was previously set to 55 to 60 ° C. as shown in Table 3, immediately after standing, the volume of the foam part of Example 1 was 42 ml, and the volume of the foam part of Comparative Example 2 was 40 ml. I couldn't. However, as shown in FIG. 3, after 5 minutes of standing, the reduced volume of the foam part of Example 1 was 4 ml, but the reduced volume of the foam part of Comparative Example 2 was 10 ml, and the foam volume was considerably reduced. It was. Further, even after 10 minutes of standing, the reduced volume of the foam part of Example 1 was 4 ml, which was unchanged from that after 5 minutes of standing. On the other hand, the reduced volume of the foam part of Comparative Example 2 was 16 ml, and it was confirmed that the volume of the foam part was further reduced. That is, it was revealed that Example 1 was superior in foam retention compared to Comparative Example 2.

密閉容器入り飲料は、一般的にアイスまたはホットで販売される。アイスの飲用温度は4〜10℃の温度範囲であり、ホットの飲用温度は55〜60℃の温度範囲とされている。当然のことながら、アイスの温度範囲あるいはホットの温度範囲において起泡性及び泡沫の保持性が優れていなければならない。上記の試験において、アイス及びホットの温度範囲において、実施例1は優れた起泡性及び泡沫の保持性を有していることが確認された。 Sealed beverages are typically sold on ice or hot. Ice drinking temperature is in the temperature range of 4-10 ° C, and hot drinking temperature is in the temperature range of 55-60 ° C. As a matter of course, the foamability and foam retention must be excellent in the ice temperature range or the hot temperature range. In the above test, it was confirmed that Example 1 had excellent foamability and foam retention in the ice and hot temperature ranges.

(実施例2)
実施例1記載の秤量したコーヒー抽出液に、ショ糖50g添加し完全に溶解した後、調合液のpHが6.5になるよう重曹を1.25g添加した。飲料全量中に対して、乳成分として乳由来のタンパク質含量が1.01重量%になる量を60℃の水300gで溶解した脱脂粉乳23gおよび全粉乳9.5gに、植物性油脂として0.29重量%となる量のナタネ由来の乳化植物油脂6.0gと、乳化剤として0.34重量%となる量のショ糖脂肪酸エステル(HLB16)3.5gと、安定剤として増粘多糖類0.3gを順次溶解した。この溶解液を前記コーヒー抽出液に添加して最後に1000mlになるようゲージアップしたものを調合液とした。
(Example 2)
50 g of sucrose was added to the weighed coffee extract described in Example 1 and completely dissolved, and then 1.25 g of sodium bicarbonate was added so that the pH of the prepared solution was 6.5. The amount of the protein content derived from milk as a milk component is 1.01% by weight with respect to the total amount of beverage in 23 g of skim milk powder and 9.5 g of whole milk powder dissolved in 300 g of water at 60 ° C. Emulsified vegetable oil and fat derived from rapeseed in an amount of 29% by weight, 3.5 g of sucrose fatty acid ester (HLB16) in an amount of 0.34% by weight as an emulsifier, and 0.1% of thickening polysaccharide as a stabilizer. 3 g was dissolved sequentially. The solution was added to the coffee extract and gauged up to a final volume of 1000 ml.

この調合液を20MPaの条件で高圧ホモゲナイザーにより均質化した後、90℃に昇温後、リキャップ機能を有する170ml容量の缶に充填し、レトルト殺菌(123.5℃、26分間、F=45)を行い、目的とする泡沫の保持性の高い密閉容器入りコーヒー飲料を得た。
なお、前記コーヒー飲料は、乳由来のタンパク質含量が1.01重量%、動・植物性由来の脂肪が0.55重量%、乳化剤含量が0.34重量%、乳由来のタンパク質含量(重量%)と乳化剤含量(重量%)との積が0.34となっている。
This mixed solution was homogenized with a high-pressure homogenizer under the condition of 20 MPa, heated to 90 ° C., filled into a 170 ml can having a recap function, and retort sterilized (123.5 ° C., 26 minutes, F 0 = 45 ) To obtain a coffee beverage in a hermetically sealed container with high foam retention.
The coffee beverage has a milk-derived protein content of 1.01% by weight, animal and vegetable fats of 0.55% by weight, an emulsifier content of 0.34% by weight, and a milk-derived protein content (% by weight). ) And the emulsifier content (% by weight) is 0.34.

(実施例3)
飲料全量中に対して、乳成分として乳由来のタンパク質含量が1.01重量%になる量を60℃の水300gで溶解した脱脂粉乳23gおよび全粉乳9.5gに、植物性油脂として0.29重量%となる量のナタネ由来の乳化植物油脂6.0gと、乳化剤として0.34重量%となる量のショ糖脂肪酸エステル(HLB16)3.5gと、安定剤として増粘多糖類0.6g及び7.1重量%となる量のショ糖74gを順次溶解し、更に0.43重量%の抹茶4.5gを添加した。この溶解液を高速攪拌ミキサーにて分散後、調合液のpHが7.0になるよう重曹を0.4g添加して、最後に1000mlになるようゲージアップしたものを調合液とした。
(Example 3)
The amount of the protein content derived from milk as a milk component is 1.01% by weight with respect to the total amount of beverage in 23 g of skim milk powder and 9.5 g of whole milk powder dissolved in 300 g of water at 60 ° C. Emulsified vegetable oil and fat derived from rapeseed in an amount of 29% by weight, 3.5 g of sucrose fatty acid ester (HLB16) in an amount of 0.34% by weight as an emulsifier, and 0.1% of thickening polysaccharide as a stabilizer. 6 g and 74 g of sucrose in an amount of 7.1% by weight were sequentially dissolved, and further 0.43% by weight of 4.5 g of matcha tea was added. After this dissolved solution was dispersed with a high-speed stirring mixer, 0.4 g of sodium bicarbonate was added so that the pH of the prepared solution was 7.0, and finally the gauge was increased to 1000 ml to obtain a prepared solution.

この調合液を、20MPaの条件で高圧ホモゲナイザーにより均質化し、90℃に昇温後、キャップの直径が46mmのリキャップ機能を有する170ml容量の缶に充填し、レトルト殺菌(123.5℃、26分間、F=45)を行い、目的とする泡沫の保持性の高い密閉容器入り抹茶ミルク飲料を得た。
なお、前記抹茶ミルク飲料は、乳由来のタンパク質含量が1.01重量%、動・植物性由来の脂肪が0.55重量%、乳化剤含量が0.34重量%、乳由来のタンパク質含量(重量%)と乳化剤含量(重量%)との積が0.34となっている。
This mixed solution was homogenized with a high-pressure homogenizer under the condition of 20 MPa, heated to 90 ° C., filled into a 170 ml capacity can with a cap cap diameter of 46 mm, and retort sterilized (123.5 ° C., 26 minutes) , F 0 = 45) to obtain a green tea milk drink in a hermetically sealed container with high foam retention.
The matcha milk beverage has a milk-derived protein content of 1.01% by weight, an animal / plant-derived fat content of 0.55% by weight, an emulsifier content of 0.34% by weight, and a milk-derived protein content (weight). %) And the emulsifier content (% by weight) is 0.34.

(実施例4)
飲料全量中に対して乳成分として乳由来のタンパク質含量が1.01重量%になる量を60℃の水300gで溶解した脱脂粉乳23gおよび全粉乳9.5gに、植物性油脂として0.29重量%となる量のナタネ由来の乳化植物油脂6.0gと、乳化剤として0.34重量%となる量のショ糖脂肪酸エステル(HLB16)3.5gと、安定剤として増粘多糖類0.6g及び5.9重量%となる量のショ糖61.3gを順次溶解した。この溶解液に調合液のpHが7.0になるよう重曹を0.4g添加した後、0.1重量%となるようにバナナフレーバー1.0gを添加し、最後に1000mlになるようゲージアップしたものを調合液とした。
Example 4
The amount of protein content derived from milk as 1.01% by weight as a milk component in the total amount of beverage is dissolved in 23 g of skim milk powder and 9.5 g of whole milk powder dissolved in 300 g of water at 60 ° C., and 0.29 as vegetable oil. Emulsified vegetable oil and fat derived from rapeseed in an amount of% by weight, 3.5 g of sucrose fatty acid ester (HLB16) in an amount of 0.34% by weight as an emulsifier, and 0.6 g of thickening polysaccharide as a stabilizer. And 61.3 g of sucrose in an amount of 5.9% by weight were dissolved in order. Add 0.4g of baking soda to the solution so that the pH of the preparation is 7.0, add 1.0g of banana flavor to 0.1% by weight, and finally increase the gauge to 1000ml. The prepared solution was used as a preparation liquid.

この調合液を20MPaの条件で高圧ホモゲナイザーにより均質化し、90℃に昇温後、リキャップ機能を有する170ml容量の缶に充填し、レトルト殺菌(123.5℃、26分間、F=45)を行い、目的とする泡沫の保持性の高い密閉容器入りフレーバー入り乳飲料(バナナ風味ミルク飲料)を得た。
なお、前記フレーバー入り乳飲料は、乳由来のタンパク質含量が1.01重量%、動・植物性由来の脂肪が0.55重量%、乳化剤含量が0.34重量%、乳由来のタンパク質含量(重量%)と乳化剤含量(重量%)との積が0.34となっている。
This mixed solution was homogenized with a high-pressure homogenizer under the condition of 20 MPa, heated to 90 ° C., filled into a 170 ml capacity can with a recap function, and retort sterilized (123.5 ° C., 26 minutes, F 0 = 45). A flavored milk beverage (banana flavored milk beverage) in a sealed container with high foam retention was obtained.
The flavored milk beverage has a milk-derived protein content of 1.01% by weight, an animal / plant-derived fat content of 0.55% by weight, an emulsifier content of 0.34% by weight, and a milk-derived protein content ( % By weight) and the emulsifier content (% by weight) are 0.34.

(比較例3)
飲料全量中に対して乳成分として乳由来のタンパク質含量が1.01重量%になる量を60℃の水300gで溶解した脱脂粉乳および全粉乳に、植物性油脂として0.29重量%となる量のナタネ由来の乳化植物油脂と、乳化剤として0.1重量%となる量のショ糖脂肪酸エステル(HLB16)と、安定剤として増粘多糖類0.6g及び5.9重量%となる量のショ糖61.3gを順次溶解した。この溶解液に調合液のpHが7.0になるよう重曹を0.4g添加した後、0.1重量%となるようにバナナフレーバー1.0gを添加し、最後に1000mlになるようゲージアップしたものを調合液とした。
(Comparative Example 3)
In skim milk powder and whole milk powder in which the amount of protein derived from milk as a milk component is 1.01% by weight with 300 g of water at 60 ° C. is 0.29% by weight as vegetable oil. An amount of emulsified vegetable oil derived from rapeseed, an amount of sucrose fatty acid ester (HLB16) of 0.1% by weight as an emulsifier, and 0.6 g and 5.9% by weight of thickening polysaccharide as a stabilizer. 61.3 g of sucrose was dissolved in order. Add 0.4g of baking soda to the solution so that the pH of the preparation is 7.0, add 1.0g of banana flavor to 0.1% by weight, and finally increase the gauge to 1000ml. The prepared solution was used as a preparation liquid.

この調合液を20MPaの条件で高圧ホモゲナイザーにより均質化し、90℃に昇温後、リキャップ機能を有する170ml容量の缶に充填し、レトルト殺菌(123.5℃、26分間、F=45)を行い、乳化剤含量が0.2重量%より少ない密閉容器入りフレーバー入り乳飲料(バナナ風味ミルク飲料)を得た。
なお、前記フレーバー入り乳飲料は、乳由来のタンパク質含量が1.01重量%、動・植物性由来の脂肪が0.55重量%、乳化剤含量が0.1重量%、乳由来のタンパク質含量(重量%)と乳化剤含量(重量%)との積が0.1となっている。
This mixed solution was homogenized with a high-pressure homogenizer under the condition of 20 MPa, heated to 90 ° C., filled into a 170 ml capacity can with a recap function, and retort sterilized (123.5 ° C., 26 minutes, F 0 = 45). And a flavored milk beverage (banana flavored milk beverage) in a sealed container having an emulsifier content of less than 0.2% by weight was obtained.
The flavored milk beverage has a milk-derived protein content of 1.01% by weight, an animal / plant-derived fat of 0.55% by weight, an emulsifier content of 0.1% by weight, and a milk-derived protein content ( Weight%) and the emulsifier content (wt%) are 0.1.

(試験例3)
実施例2で作製した泡沫の保持性の高い密閉容器入りコーヒー飲料(実施例2)及び実施例3で作製した泡沫の保持性の高い密閉容器入り抹茶ミルク飲料(実施例3)を用いて、以下の方法にて測定した。
測定方法は試験例1と同様に行った。
結果を表4及び図4に示す。
(Test Example 3)
Using the coffee beverage (Example 2) in a sealed container with high foam retention property produced in Example 2 and the matcha milk drink (Example 3) in a sealed container with high foam retention property produced in Example 3, It measured by the following method.
The measurement method was the same as in Test Example 1.
The results are shown in Table 4 and FIG.

Figure 0005156528
Figure 0005156528

表4のとおり静置直後は、実施例2の泡沫部分の容積は20mlで、実施例3の泡沫部分の容積は18mlとなり、実施例2のコーヒー飲料と同様実施例3の抹茶ミルク飲料も起泡性において優れていることが明らかとなった。また、図4のとおり実施例2及び3とも静置5分後では、泡沫部分の減少容積が6ml程度で静置直後よりも約3割程度減少したが、静置10分後では、著しい減少は無く、泡沫を保持していることが確認され、実施例1の場合と同様、実施例2及び3のいずれも泡沫の保持性に優れていることが明らかとなった。   Immediately after standing as shown in Table 4, the volume of the foam part of Example 2 was 20 ml, the volume of the foam part of Example 3 was 18 ml, and the matcha milk drink of Example 3 was also started like the coffee drink of Example 2. It became clear that it was excellent in foamability. In addition, as shown in FIG. 4, in both Examples 2 and 3, after 5 minutes of standing, the reduced volume of the foam portion was about 6 ml, which was about 30% less than that immediately after standing, but after 10 minutes of standing, it decreased significantly. It was confirmed that the foam was retained, and as in Example 1, both Examples 2 and 3 were excellent in foam retention.

(試験例4)
実施例4で作製した泡沫の保持性の高い密閉容器入りフレーバー入り乳飲料(バナナ風味ミルク飲料)(実施例4)及び比較例3で作製した密閉容器入りフレーバー入り乳飲料(バナナ風味ミルク飲料)(比較例3)を用いて、以下の方法にて測定した。
測定方法は試験例1と同様に行った。
結果を表5及び図5に示す。
(Test Example 4)
Flavored milk beverage in a sealed container (banana flavored milk beverage) (Example 4) and a flavored milk beverage in a sealed container (banana flavored milk beverage) produced in Comparative Example 3 with high foam retention in Example 4 Using (Comparative Example 3), the measurement was carried out by the following method.
The measurement method was the same as in Test Example 1.
The results are shown in Table 5 and FIG.

Figure 0005156528
Figure 0005156528

表5のとおり静置直後は、実施例4の泡沫部分の容積は15mlで、比較例3の泡沫部分の容積は13mlとなり、実施例4と比較例3の泡沫部分の容積に大差は認められなかった。しかし、図5のとおり静置10分後においては、実施例4の泡沫部分の減少容積は5mlであったが、比較例3の泡沫部分の減少容積は10mlとなり、実施例4と比べ比較例3は著しい容積の減少が認められた。すなわち、実施例4は、泡沫を保持していることが確認され、比較例3と比べ泡沫の保持性に優れていることが明らかとなった。   Immediately after standing as shown in Table 5, the volume of the foam part of Example 4 was 15 ml, the volume of the foam part of Comparative Example 3 was 13 ml, and there was a large difference in the volume of the foam part of Example 4 and Comparative Example 3 There wasn't. However, after 10 minutes of standing as shown in FIG. 5, the reduced volume of the foam part of Example 4 was 5 ml, but the reduced volume of the foam part of Comparative Example 3 was 10 ml, which was a comparative example compared to Example 4. No. 3 was markedly reduced in volume. That is, Example 4 was confirmed to hold foam, and was found to be superior in foam retention compared to Comparative Example 3.

次に、上記実施形態及び別例から把握できる技術的思想について、それらの効果とともに以下に追記する。 Next, technical ideas that can be grasped from the above-described embodiment and other examples will be described below together with their effects.

(1)起泡性を有する密閉容器入り飲料において、乳由来のタンパク質を0.6重量%以上、動物性及び/又は植物性由来の脂肪を0.2重量%よりも多く好ましくは0.25重量%以上含有せしめるとともに、トータルHLBが14以上である乳化剤を含有せしめること、を特徴とする泡沫の保持性が高い飲料の製造方法、あるいは、泡沫の保持方法。 (1) In a sealed container-containing beverage having foaming properties, the protein derived from milk is 0.6% by weight or more and the fat derived from animals and / or plants is more than 0.2% by weight, preferably 0.25. A method for producing a beverage with high foam retention, or a method for retaining foam, characterized by comprising an emulsifier having a total HLB of 14 or more while containing at least wt%.

(2)起泡性を有する密閉容器入り飲料の製造工程において、乳由来のタンパク質を0.6重量%以上、動物性及び/又は植物性由来の脂肪を0.2重量%よりも多くなる量の乳成分及び脂肪を、トータルHLBが14以上である乳化剤とともに、原料液に添加すること、を特徴とする泡沫の保持性が高い飲料の製造方法、あるいは、泡沫の保持方法。   (2) In the production process of a beverage in a hermetically sealed container having foaming properties, the amount of protein derived from milk is 0.6% by weight or more, and the fat derived from animals and / or plants is more than 0.2% by weight A method for producing a beverage with high foam retention, or a method for retaining foam, characterized in that the milk component and fat are added to a raw material liquid together with an emulsifier having a total HLB of 14 or more.

試験例1での振とう静置後の泡沫部分の容積の減少量を示す。The reduction | decrease amount of the volume of the foam part after shaking standing in Test Example 1 is shown. 試験例2でのアイス温度範囲のサンプルを用いた振とう静置後の泡沫部分の容積の減少量を示す。The amount of reduction | decrease of the volume of the foam part after stationary shaking using the sample of the ice temperature range in Experiment 2 is shown. 試験例2でのホット温度範囲のサンプルを用いた振とう静置後の泡沫部分の容積の減少量を示す。The amount of reduction of the volume of the foam part after shaking standing using the sample of the hot temperature range in Test Example 2 is shown. 試験例3での振とう静置後の泡沫部分の容積の減少量を示す。The reduction | decrease amount of the volume of the foam part after shaking standing in Test Example 3 is shown. 試験例4での振とう静置後の泡沫部分の容積の減少量を示す。The amount of reduction | decrease of the volume of the foam part after shaking stationary in Test Example 4 is shown.

Claims (8)

起泡性を有する密閉容器入り飲料において、乳由来のタンパク質を0.6重量%以上、動物性及び/又は植物性由来の脂肪を0.2重量%以上0.8重量%以下含有し、トータルHLBが14以上である乳化剤を0.2〜0.4重量%含有することを特徴とする泡沫の保持性が高い飲料。 In a sealed container-containing beverage having foaming properties, milk-derived protein is contained in an amount of 0.6% by weight or more, and animal and / or plant-derived fat is contained in an amount of 0.2% by weight or more and 0.8% by weight or less. A beverage having high foam retention, comprising 0.2 to 0.4% by weight of an emulsifier having an HLB of 14 or more. 前記乳由来のタンパク質含量(重量%)と前記乳化剤含量(重量%)との積が、0.12〜0.49となることを特徴とする請求項1に記載の泡沫の保持性が高い飲料。   The beverage with high foam retention according to claim 1, wherein the product of the milk-derived protein content (wt%) and the emulsifier content (wt%) is 0.12 to 0.49. . 前記乳由来のタンパク質が、脱脂粉乳が主成分であり、その割合が飲料全量中の2.8重量%以上含有することを特徴とする請求項1又は2に記載の泡沫の保持性が高い飲料。   The milk-derived protein contains skim milk powder as a main component, and the proportion thereof is 2.8% by weight or more based on the total amount of the beverage. The beverage with high foam retention according to claim 1 or 2, . 容器を振とう後泡沫が5分以上消滅しないことを特徴とする請求項1〜3のいずれか1項に記載の泡沫の保持性が高い飲料。   The beverage having high foam retention according to any one of claims 1 to 3, wherein the foam does not disappear for more than 5 minutes after shaking the container. 4℃〜60℃の温度範囲の飲料でも前記泡沫が5分以上消滅しないことを特徴とする請求項4に記載の泡沫の保持性が高い飲料。   The beverage having a high foam retention property according to claim 4, wherein the foam does not disappear for 5 minutes or more even in a beverage in a temperature range of 4 ° C to 60 ° C. 密閉容器がリキャップ機能を有していることを特徴とする請求項1〜5のいずれか1項に記載の泡沫の保持性が高い飲料。   The closed container has a recapping function, and the beverage having high foam retention according to any one of claims 1 to 5. 前記リキャップ機能を有した密閉容器のキャップの直径が38mm以上の口径であることを特徴とする請求項6に記載の泡沫の保持性が高い飲料。   The beverage with high foam retention according to claim 6, wherein the diameter of the cap of the sealed container having the recapping function is 38 mm or more. 起泡性を有する密閉容器入り飲料において、乳由来のタンパク質を0.6重量%以上、動物性及び/又は植物性由来の脂肪を0.2重量%以上0.8重量%以下含有せしめるとともに、トータルHLBが14以上である乳化剤を0.2〜0.4重量%含有せしめることを特徴とする泡沫の保持性が高い飲料の製造方法。 In a beverage in a closed container having foaming properties, 0.6% by weight or more of milk-derived protein, 0.2% by weight or more and 0.8% by weight or less of animal and / or vegetable-derived fat are contained, A method for producing a beverage with high foam retention, characterized by containing 0.2 to 0.4% by weight of an emulsifier having a total HLB of 14 or more.
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