JP5018568B2 - Disc type polymer filter, disc type polymer filter assembly and polymer film - Google Patents

Description

  The present invention relates to a disk-type polymer filter, a disk-type polymer filter assembly, and a polymer film in which foreign substances such as polymer staying degradation products are difficult to be mixed into a product.

  Conventionally, films manufactured using polyester, polypropylene, polyamide, polycarbonate, polyolefin, and acrylic resin are generally manufactured by a process as shown in FIG.

  FIG. 8 is a schematic diagram illustrating an example of a film manufacturing apparatus.

  In FIG. 8, the film production apparatus 80 is provided with an extruder 1, a gear pump 2, a filter 3, a base 4, a cooling roll 5, a stretching device 6, and a winder 7 in this order from the upstream side in the polymer flow direction. A thickness meter 8 is installed between the stretching device 6 and the winder 7, and a thickness controller 9 is electrically connected to the thickness meter 8 and the base 4.

  In the above apparatus, the raw material polymer is supplied to the extruder 1, melted, and then extruded to the gear pump 2. The gear pump 2 has a function of making the discharge amount (delivery amount) constant. The molten resin discharged by a constant amount is removed from the foreign matter and the like through the filter 3 and then supplied to the base 4. The base 4 is provided with a slit having a predetermined gap, and the molten resin is extruded from the slit into a sheet shape, cooled and solidified on the rotating cooling roll 5, and then a solidified sheet 10 is obtained. The solidified sheet 10 is subsequently stretched by the stretching device 6 and wound up as a film by the winder 7. At that time, the thickness gauge 8 measures the film thickness at each position in the width direction of the film (direction orthogonal to the paper surface), and the thickness controller 9 determines the slit gap of the base 4 based on the obtained thickness data. An adjusted product film having a thickness within a certain range (small variation in thickness) is obtained.

  The filter 3 used in the above apparatus includes a leaf disk type, a cylindrical filter, a screen type, and the like, and is appropriately used according to the quality of the film to be manufactured and the manufacturing conditions. In many cases, a plurality of leaf discs are laminated and used in a tree shape, and a metal fiber type or a porous type is used as a filter medium. Hereinafter, this disk type filter will be described with reference to FIGS.

  FIG. 2 is a schematic cross-sectional view showing a conventional disk type filter.

  In FIG. 2, a disk-type filter 30 includes a filter element 11 having a filtration function, and a punching member (polymer introduction member) that supports the filter element 11 and guides the polymer into the disk from a plurality of polymer inlets 90 ′. 12, a retainer mesh (filter support member) 13 that supports the punching member, and a hub member 14 that collects these members and receives a load when the disks are stacked. The filter element 11 and the hub member 14 include: At the welded portion 16, the punching member 12 and the hub member 14 are connected at the welded portion 17.

  FIG. 3 shows, with arrows (solid lines), how the polymer flows through the conventional disk-type filter 30 shown in FIG. The polymer flows between a casing (not shown) and a tree in which disk filters are stacked, enters through the gaps between the stacked disk filters, passes through the filter element 11 and the punching member 12, passes through the retainer mesh 13, and is a hub. It is led to a conduction hole provided in the member 14 and finally enters a center post (not shown) and flows downstream.

  At this time, in the conventional disk-type filter 30, the polymer flows in the filter element 11 in the portion supported by the punching member 12, but the polymer flows in the hub member in the filter element in the portion supported by the hub member 14. Since there is no flow path, the polymer may not stay flowing in the portion of the filter element corresponding to the portion sandwiched between the welded portion 16 and the welded portion 17 (the polymer flow indicated by the broken line arrow does not occur). . If the polymer stays, depending on the type and composition, transformation, thermal degradation, and aging degradation may occur, and the degraded polymer flows out to the filter element portion supported by the punching member due to the influence of fluctuation in filtration pressure and the like, and the solidified sheet 10 It often occurred as a foreign object defect.

As for this problem, for example, as shown in Patent Document 1, it is disclosed as a solution means to provide a polymer inlet similar to the punching member in a portion of the hub member that supports the filter element. However, simply providing a hole in the hub member cannot completely remove the staying portion, and the polymer flow rate varies in each part of the filter element supported by the hub member and the punching member, resulting in a deteriorated polymer. Foreign matter often occurred on the solidified sheet 10.
Japanese Utility Model Publication No. 6-29612

  An object of the present invention is to provide a disk-type polymer filter, a disk-type polymer filter assembly, and a polymer film in which foreign matters such as polymer deteriorating degradation products are hardly mixed into a product.

  To achieve the above object, the present invention has the following features.

(1) A polymer element and a polymer introduction member are connected to the hub member, and the filter element and the polymer introduction member are stacked in order from the upstream side in the polymer flow direction, and the hub member attaches the filter element to the hub member. It has a filter element support part for supporting, and the pressure loss A of the filter element corresponding to this filter element support part and the pressure loss B of the filter element in other parts satisfy the relationship of A ≦ B. A disk-type polymer filter in which at least a part of the filter element support part is made of a sintered metal porous body .

( 2 ) The disk-type polymer filter according to (1 ), wherein a through hole for allowing the polymer to flow through the filter element support portion is provided.

( 3 ) A disk-type polymer filter assembly in which the disk-type polymer filter and the spacer member according to (1) or (2) are alternately laminated, wherein at least a part of the spacer member is a metal sintered porous Disc type polymer filter assembly composed of a body.

( 4 ) The disk-type polymer filter assembly according to ( 3 ) above, wherein a through hole for allowing a polymer to flow through the spacer member is provided.

( 5 ) Manufactured using the disk-type polymer filter described in any one of (1) to ( 2 ) above or the polymer passed through the disk-type polymer filter assembly described in ( 3 ) or ( 4 ) above. Polymer film.

  According to the present invention, a disk-type polymer filter and a disk-type polymer that can eliminate a stay portion that has been generated by using a conventional hub member and are less likely to be contaminated with foreign substances (such as polymer stay-deteriorated products). A filter assembly can be provided, and by forming a film using the polymer that has passed through the filter, a polymer film with few defects can be provided.

  Hereinafter, embodiments of the present invention will be described with reference to the drawings. Of course, the present invention is not limited to these.

  FIG. 1 is a schematic cross-sectional view showing a disk-type polymer filter according to an embodiment of the present invention, and FIG. 4 is a schematic cross-sectional view showing the flow of a polymer in the disk-type polymer filter. In FIG. 1, a disk-type polymer filter 20 includes a filter element 11 having a filtration function, and a punching member (polymer introduction member) that supports the filter element 11 and guides the polymer into the disk from a plurality of polymer inlets 90. ) 12, a retainer mesh (filter support member) 13 that supports the punching member 12, and a hub member 14 that collects these members and receives a load at the time of stacking the disks. The filter element 11 and the hub member 14 is a welded portion 16, and the punching member 12 and the hub member 14 are connected by a welded portion 17, and other parts are joined by welding as necessary. Further, the hub member 14 is provided with a filter element support portion 21 (portion for supporting the filter element 11). The portion is made of a sintered metal porous body and is connected to the hub member 14 by a welded portion 22. Yes.

  The disc-type polymer filter of the present invention configured as described above has sufficient retention of the polymer in the filter element portion corresponding to the filter element support portion as shown by the solid line arrow A in FIG. It can be remarkably reduced, foreign matters such as polymer degradation products are hardly generated, and an excellent polymer filter can be produced.

  FIG. 5 is a schematic longitudinal sectional view showing a disk-type polymer filter according to another embodiment of the present invention. The basic configuration is the same as that of the disk-type polymer filter shown in FIG. A plurality of polymer flow holes 23 are provided in the filter element support portion of the hub member 14 formed of a porous body.

  In the present invention, for example, by configuring the filter element support portion of the hub member 14 to circulate as described above, the pressure loss A of the filter element corresponding to this filter element support portion, and other The pressure loss B of the partial filter element is configured to satisfy the relationship of A ≦ B.

  By comprising in this way, after the polymer which flows between disk filters reaches | attains the part corresponded to a filter element support part, it will flow so that it may pass through a filter element and a support part, without staying in the part.

Further, as a configuration satisfying the relationship of A ≦ B, as described above, the filter element support portion of the hub member is formed of a metal sintered porous body, and further in the example shown in FIG. Realized by providing multiple polymer flow holes 23 in the filter element support part of the body, and increasing the density of the polymer flow holes, that is, the number of holes in the filter element support part compared to other parts Is possible.

As described above, whether or not the pressure loss of each part of the filter element satisfies the relationship of A ≦ B by the filter element support provided on the hub member, as will be described below, the apparatus shown in FIG. This is determined by the method using

FIG. 6 is a schematic cross-sectional view of an apparatus for measuring the pressure loss value of a filter element.
In FIG. 6A, the filter pressure loss measuring device 50 is configured so that the filter element 11 and the members (the punching member 12 and the retainer mesh 24) that support the filter element 11 can be inserted into the casing 25 in an overlapping manner. It has a structure in which a pressure gauge 26 and a pressure gauge 27 are provided at the upper and lower parts of the piping. By this device, it is possible to measure the pressure loss of the filter element having a predetermined configuration by subtracting the value P2 of the pressure gauge 27 from the value P1 of the pressure gauge 26 when the polymer is flowed from the filter element side. It becomes. In the case of FIG. 6A, the pressure loss value of the filter element in the portion other than the filter element corresponding to the filter element support provided on the hub member is measured. Similarly, FIG. 6B shows a case where the configuration of the measurement object is measured in such a manner that the filter element 11, the sintered metal porous body 21, and the retainer mesh 24 are stacked in order from the upstream direction in the polymer flow direction. The pressure loss value of the filter element corresponding to the filter element support provided on the hub member can be measured.

  In the measurement, it is preferable to use a polymer that is actually used as the polymer to be circulated. For example, as a pseudo polymer, a uniluve of NOF Corporation or an edible chickenpox can be used.

  In the present invention, the metal sintered porous body is preferably a metal powder type sintered body, and may be reinforced with metal fibers or the like. Moreover, it is preferable to provide the polymer circulation holes 23 shown in FIG. 5 with the same density and size as the punching member. The hole diameter is preferably about 1 to 2 mm, but is not limited to these ranges.

  In addition, as shown in FIG. 7, the disk-type polymer filter of the present invention is preferably used as an assembly in which spacer members are alternately laminated. In this case, at least a part of the spacer members is a sintered metal porous body. It is preferable that it is comprised. It is also preferable that a through hole for allowing the polymer to flow through the spacer member is provided. Of course, you may use both together.

  For example, FIG. 7A shows a configuration in which a spacer member 28 made of a sintered metal porous body is installed between the filters on the disk-type polymer filter having the configuration shown in FIG. 1, and FIG. 7B shows a spacer member. Shows a configuration in which holes through which a polymer flows are provided in the vertical direction and the horizontal direction. By adopting such a configuration, it is possible to eliminate a slight retention portion generated between the spacer member and the filter element 11.

  A configuration in which several spacer members are provided radially in the radial direction of the disk is preferable, and the thickness and width are preferably optimized depending on the polymer used. Specifically, for example, the thickness is preferably in the range of 0.5 to 10 mm, and the width is preferably in the range of 1 to 20 mm.

  The size of the disk type filter of the present invention is preferably about 100 mm to 450 mm in outer diameter. Various materials can be used for the disk-type filter of the present invention. Any material can be used for the filter element 11 as long as the material has a so-called filtration function, such as a stainless steel metal fiber, a sintered porous body, and a mesh. Although the filtration accuracy depends on the quality requirements of the product, ultra-high precision filter media such as 1 to 3 μm cut may be used, filter media such as 10 to 20 μm cut may be used, and filter media of 30 μm cut or more may be used. Also good.

  Examples of materials that can be used for the filter element, polymer introduction member, retainer mesh (filter support member), hub member, and spacer member include stainless steel SUS304, SUS316, SUS630, SUS420, etc., but carbon steel is also used. May be.

  In the above description, the metal-based material is mainly described. However, depending on the type of polymer, the filter can be formed of a resin-based material or a ceramic-based material.

  In general, a plurality of filters are used by laminating them, but the same effect can be obtained even if they are used in units of one sheet.

  The polymer applicable in the present invention is not particularly limited, such as polyester, polypropylene, polyamide, polycarbonate, polyolefin, acrylic resin, and may be a thermoplastic resin or a thermosetting resin.

  In addition, the polymer film produced by using the polymer passed through the disk-type polymer filter or the disk-type polymer filter assembly of the present invention described above is used for packaging such as a package or a laminate, for a magnetic recording medium such as a digital video camera, It can be used in various industries and applications such as optical applications such as displays and semiconductor applications such as flexible substrates. The polymer film to be produced may have a single layer configuration in the thickness direction or may have a multilayer configuration of two or more layers.

[Example 1]
A polymer film was manufactured using a disk-type polymer filter having the configuration shown in FIG. 1 and a film manufacturing apparatus as shown in FIG. The polymer was polyester, the extrusion temperature was 280 ° C., the discharge rate was 700 kg / hr, the filter element was a metal fiber with a filtration accuracy of 15 μm, and 50 filters with a 300 mm outer size were used. A sintered metal porous body was used for the filter element support of the hub member. As the sintered metal porous body, SUS316 was used, and the size was about 10 mm in the disk radial direction. In order to make the pressure loss equal to that of the other portions, a sintered metal porous body having the same pressure loss as that of the polymer passing through the punching member was selected. In order to confirm the design, the pressure loss of the material having the same configuration was measured using the measuring apparatus shown in FIG. 6, and as a result, the sintered metal porous body had a lower pressure loss of about 0.2 kg / cm ^2. Because there was, it was adopted as it was. The die was manufactured for one week using a T-die with a slit gap of 1.4 mm. As a result, no foreign material defect due to the deteriorated polymer occurred during sheet production, and a film of good quality was obtained.

  In order to confirm the presence / absence of the staying portion and clarify the effect of the present invention, the filter was cooled and decomposed with the polymer attached after the film was manufactured, and the presence / absence of discoloration of the polymer near the hub member of the disk was confirmed. As a result, the location where the polymer stayed and discolored was not found, and the effect of the present invention could be confirmed.

[Example 2]
A polymer film was produced using a disk-type polymer filter having the configuration shown in FIG. 5 and a film production apparatus as shown in FIG. The polymer used was polyolefin, the extrusion temperature was 260 ° C., the discharge rate was 100 kg / hr, the filter element was a porous sintered metal filter element with a filtration accuracy of 20 μm, and 30 filters with an outer diameter of 150 mm were used. A polymer circulation hole was provided in the filter element support portion of the hub member using a sintered metal porous body. As the sintered metal porous body, SUS316 was used, and the size was about 10 mm in the disk radial direction. In order to design the pressure loss equal to that of the other portions, a sintered metal porous body having the same pressure loss as that of the polymer passing through the punching member when the polymer flow hole is provided was selected. The polymer circulation holes were provided with a diameter of 1.0 mm at three locations in the radial direction and 30 locations in the circumferential direction. In order to confirm the design, the pressure loss of the material having the same configuration was measured using the measuring apparatus shown in FIG. 6. As a result, it was about 0.1 kg / cm ² when the polymer flow hole was provided in the sintered metal porous body. Since the pressure loss was low, it was adopted as it was.

  The die was manufactured using a T-die with a slit gap of 1.2 mm for 1 week. As a result, no foreign material defect due to the deteriorated polymer occurred during sheet production, and a film of good quality was obtained.

  In order to confirm the presence / absence of the staying portion and clarify the effect of the present invention, the filter was cooled and decomposed with the polymer attached after the film was manufactured, and the presence / absence of discoloration of the polymer near the hub member of the disk was confirmed. As a result, the location where the polymer stayed and discolored was not found, and the effect of the present invention could be confirmed.

[Example 3]
Using a disk-type polymer filter having the configuration shown in FIG. 7A, a polymer film was manufactured using a film manufacturing apparatus as shown in FIG. The polymer was polypropylene, the extrusion temperature was 250 ° C., the discharge rate was 300 kg / hr, the filter element was a metal fiber with a filtration accuracy of 20 μm, and 50 filters with a 300 mm outer size were used.

A sintered metal porous body was used for the filter element support of the hub member. As the sintered metal porous body, SUS316 was used, and the size was about 15 mm in the disk radial direction. In order to make the pressure loss equal to that of the other portions, a sintered metal porous body having the same pressure loss as that of the polymer passing through the punching member was selected. In order to confirm the design, the pressure loss of the material having the same configuration was measured using the measuring apparatus shown in FIG. 6. As a result, the sintered metal porous body had a lower pressure loss of about 0.15 kg / cm ^2. Because there was, it was adopted as it was. A metal sintered porous body similar to that of the hub member was also used for the spacer member. The die was manufactured for one week using a T-die having a slit gap of 2.1 mm. As a result, no foreign material defect due to the deteriorated polymer occurred during sheet production, and a film of good quality was obtained.

  In order to confirm the presence / absence of the staying portion and clarify the effect of the present invention, the filter was cooled and decomposed with the polymer attached after the film was manufactured, and the presence / absence of discoloration of the polymer near the hub member of the disk was confirmed. As a result, the location where the polymer stayed and discolored was not found, and the effect of the present invention could be confirmed.

[Comparative Example 1]
A polymer film was manufactured using a disk-type polymer filter having the configuration shown in FIG. 2 and a film manufacturing apparatus as shown in FIG. The polymer used was an acrylic resin, the extrusion temperature was 260 ° C., the discharge rate was 120 kg / hr, the filter element was a metal fiber with a filtration accuracy of 20 μm, and 70 filters with an outer diameter of 300 mm were used. The die was manufactured for one week using a T-die set with a slit gap of 1.3 mm. As a result, a foreign material defect caused by a deteriorated polymer occurred during sheet manufacture at a fixed position in the width direction of the sheet, and a sheet with good quality could not be obtained.

  Similarly, in order to confirm the presence or absence of the staying portion, the filter was cooled and decomposed in a state where the polymer was adhered after the sheet was manufactured, and the presence or absence of discoloration of the polymer near the hub member of the disk was confirmed.

It is a schematic sectional drawing of the disk type polymer filter which concerns on one embodiment of this invention. It is a schematic sectional drawing which shows the conventional disc type polymer filter. It is a schematic sectional drawing which shows the polymer flow of the conventional disc type polymer filter. It is a schematic sectional drawing which shows the polymer flow of the disk type polymer filter of FIG. It is a schematic sectional drawing of the disk type polymer filter which concerns on another one Embodiment of this invention. It is a schematic sectional drawing of the apparatus which measures the pressure loss of a filter element. It is a schematic sectional drawing which shows the disk type polymer filter assembly which concerns on one embodiment of this invention. It is the schematic of a general film manufacturing apparatus.

Explanation of symbols

DESCRIPTION OF SYMBOLS 1 Extruder 2 Gear pump 3 Filter 4 Cap 5 Cooling roll 6 Stretching device 7 Winder 8 Thickness meter 9 Thickness controller 10 Solidified sheet 11 Filter element 12 Punching member (polymer introduction member)
13 Retainer mesh (filter support member)
14 Hub member 15 Spacer member 16 Welded portion 17 Welded portion 20 Disc type polymer filter 21 Metal sintered porous body (filter element support portion)
22 welded portion 23 polymer flow hole provided in hub member 24 support body (retainer mesh, filter support member)
25 Pressure loss measurement casing 26 Primary pressure gauge 27 Secondary pressure gauge 28 Metal sintered porous body (spacer member)
29 Spacer member with polymer flow hole 30 Disc type polymer filter 40 Disc type polymer filter 50 Filter pressure loss measuring device 60 Disc type polymer filter assembly (part)
70 Disc type polymer filter assembly (part)
80 Film production apparatus 90 Polymer inflow hole 100

Claims (5)

The filter element and the polymer introduction member are connected to the hub member, and the filter element and the polymer introduction member are stacked in order from the upstream side in the polymer distribution direction, and the hub member supports the filter element. and having a filter element support part, and the pressure loss a filter element corresponding to the filter element support part, and the pressure loss B of the filter element of the other portion is the filter so as to satisfy the a ≦ B the relationship A disk-type polymer filter in which at least a part of an element support is made of a sintered metal porous body . The disk-type polymer filter according to claim 1, wherein a through-hole for allowing a polymer to flow through the filter element support portion is provided. 3. A disk-type polymer filter assembly in which the disk-type polymer filter and spacer members according to claim 1 or 2 are alternately stacked, wherein at least a part of the spacer member is made of a sintered metal porous body. Disc type polymer filter assembly. The disc-type polymer filter assembly according to claim 3 , wherein a through hole for allowing a polymer to flow through the spacer member is provided. Disk-type polymer filter according to any one of claims 1-2 or a polymer film produced using a polymer passed through a disc-type polymer filter assembly according to claim 3 or 4,.

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