JP4440549B2 - Valve with isolation membrane body and method for detecting breakage of isolation membrane body - Google Patents

Valve with isolation membrane body and method for detecting breakage of isolation membrane body Download PDF

Info

Publication number
JP4440549B2
JP4440549B2 JP2003011199A JP2003011199A JP4440549B2 JP 4440549 B2 JP4440549 B2 JP 4440549B2 JP 2003011199 A JP2003011199 A JP 2003011199A JP 2003011199 A JP2003011199 A JP 2003011199A JP 4440549 B2 JP4440549 B2 JP 4440549B2
Authority
JP
Japan
Prior art keywords
fluid passage
temperature
plug
valve
isolation film
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2003011199A
Other languages
Japanese (ja)
Other versions
JP2004225735A (en
Inventor
茂樹 松浦
稔浩 浅野
哲也 高富
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Daiwa Can Co Ltd
Original Assignee
Daiwa Can Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Daiwa Can Co Ltd filed Critical Daiwa Can Co Ltd
Priority to JP2003011199A priority Critical patent/JP4440549B2/en
Publication of JP2004225735A publication Critical patent/JP2004225735A/en
Application granted granted Critical
Publication of JP4440549B2 publication Critical patent/JP4440549B2/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Landscapes

  • Basic Packing Technique (AREA)
  • Details Of Valves (AREA)
  • Filling Of Jars Or Cans And Processes For Cleaning And Sealing Jars (AREA)

Description

【0001】
【発明の属する技術分野】
本発明は隔離膜体付きバルブ、特にその隔離膜体の破損検出機構及び破損検出方法に関するものである。
【0002】
【従来の技術】
容器に内容物を充填するノズルの開口部を開閉する充填バルブや、食品タンクの食品供給口または排液口の開口部を開閉する栓バルブ等では、開口部から雑菌や異物の侵入を防止するため、また逆にバルブの作動部側へ内容物が侵入してしまうことを防止するためにバルブの開口部側とバルブの作動部側とをダイヤフラムやベローズ等の変形可能な材質で形成された隔離膜体で隔離することが行われている(例えば特許文献1〜4を参照)。
【0003】
【特許文献1】
特公昭63−44601号公報
【特許文献2】
実公平1−18482号公報
【特許文献3】
特許第3214113号公報
【特許文献4】
特開2001−219996号公報
【0004】
【発明が解決しようとする課題】
上記の充填バルブや栓バルブに使用される隔離膜体は、洗浄や殺菌のため開口部側に所望温度に加熱された洗浄液または過酸化水素水や水蒸気等の殺菌液さらに乾燥用の加熱無菌空気等が流されることで急速に劣化し、度重なる開閉による繰り返し変形で破損し小孔が開くことがある。
隔離膜体に小孔が開いた場合、その小孔から容器やタンクに雑菌や異物が混入してしまうおそれがある。特に無菌充填法では容器に内容物を充填して容器を密封した後に施す殺菌工程を省略するため、最悪の場合内容液が腐敗してしまうことが考えられる。さらに、バルブに使用される隔離膜体はその構成上、外部からみえない配置になっている場合がほとんどであり、隔離膜体の破損を確認するためには定期的な分解点検が必要であった。そのため隔離膜体の破損を容易に検出することができるバルブ及びその破損検出方法が求められていた。
【0005】
本発明は上記課題に鑑みなされたものであり、その目的は極めて簡単な構成で隔離膜体の破損を検出することが可能なバルブ及び破損検出方法を提供することにある。
【0006】
【課題を解決するための手段】
上記目的を達成するために、本発明の隔離膜体付きバルブは、流体の通路となる流体通路部を内部に設け、前記流体通路部の流出口又は/及び流入口を開閉するための栓体手段と、該栓体手段の進退移動を行う移動手段と、前記栓体手段及び前記流体通路部の壁と固着し且つ前記栓体手段の動きに伴い変形する隔離膜体と、を備え、前記栓体手段の進出時に前記流出口又は/及び流入口を閉栓し、前記栓体手段の後退時に前記流出口又は/及び流入口を開放して前記流出口又は/及び流入口の開閉を行い、且つ前記隔離膜体により前記流体通路部側と前記移動手段側とを隔離する隔離膜体付きバルブにおいて、前記流体通路部の壁より連続して該栓体手段の後退方向へと、前記栓体手段、前記移動手段及び前記隔離膜体とともに一体の空間を形成するように、断面凹字形の有底筒状に形成され、その筒状の外周表面が外部に露出しており、その底部において該移動手段を貫通させて該栓体手段と該移動手段とを連結させており、且つ該空間と外部とを直接連通する空気抜き穴が設けられたハウジング部と、該ハウジング部内に該空気抜き穴を介して設置され、該ハウジング部内の空間の温度を検知する温度検知手段と、を備え、前記温度検知手段により測定された前記ハウジング部内の温度情報により前記隔離膜体の破損を検出することを特徴とする。
【0007】
本発明の隔離膜体の破損検出方法は、流体の通路となる流体通路部を内部に設け、前記流体通路部の流出口又は/及び流入口を開閉するための栓体手段と、該栓体手段の進退移動を行う移動手段と、前記栓体手段及び前記流体通路部の壁と固着し且つ前記栓体手段の動きに伴い変形する隔離膜体と、を備え、前記栓体手段の進出時に前記流出口又は/及び流入口を閉栓し、前記栓体手段の後退時に前記流出口又は/及び流入口を開放して前記流出口又は/及び流入口の開閉を行い、且つ前記隔離膜体により前記流体通路部側と前記移動手段側とを隔離する隔離膜体付きバルブにおいて、前記栓体手段、前記移動手段及び前記隔離膜体とともに一体の空間を形成するように、断面凹字形の有底筒状に形成され、その筒状の外周表面が外部に露出しており、その底部において該移動手段を貫通させて該栓体手段と該移動手段とを連結させており、且つ該空間と外部とを直接連通する空気抜き穴が設けられたハウジング部と、該ハウジング部内に該空気抜き穴を介して設置され、該ハウジング部内の空間の温度を検知する温度検知手段とを備えた隔離膜体付きバルブにおける隔離膜体の破損検出方法であって、前記流体通路内を外気温よりも高い温度の流体が通過しているときに、前記ハウジング部内の空間の温度情報を測定し、測定した温度情報と予め測定しておいた正常時の基準温度情報とを比較することにより、前記隔離膜体の破損を検出することを特徴とする。
【0008】
また、上記の隔離膜体の破損検出方法において、前記測定した温度情報が、前記流体通路内を外気温よりも高い温度の流体が通過し始めてから所定時間経過した後の温度情報であり、前記基準温度情報が、前記流体通路内を外気温よりも高い温度の流体が通過し始めてから所定時間経過した後の基準温度情報であり、該測定した温度情報が、該基準温度情報よりも高温であったときに隔離膜体に破損が存在すると判断することが好適である。
【0009】
【発明の実施の形態】
以下に本発明の隔離膜体付きバルブについて図面を参考にして詳述する。図1は本発明の隔離膜体付きバルブの断面図である。本発明の隔離膜体付きバルブ10は、液体の状態や気体の状態での流体の通路となる流体通路部12と、流体通路部12の流入口16を開閉するための栓体手段(栓体24)と、該栓体24の移動を行う移動手段(ロッド28、エアシリンダー26)と、前記栓体24の動きに伴い変形する隔離膜体14と、を備えている。この隔離膜体14により前記流体通路部12側と前記移動手段側とが隔離されている。さらに移動手段側に隔離膜体14を囲むようにハウジング部20が設置され、該ハウジング部20内に温度検知手段(温度センサ22)が備えられている。
【0010】
この実施形態ではバルブの開閉を行うための栓体手段として、流入口16に嵌入して流入口16を閉じる栓体24を備えている。また、栓体24を移動させる移動手段として、栓体24に連結されたロッド28と、該ロッド28に接続されたエアシリンダー26とを備えている。このエアシリンダー26により栓体24の移動をおこない、バルブの開閉を行う。図1は栓体24が開いた状態であり、流体通路部12を流体が流れている場合を示している。つまり、タンク等の排出口46に接続されたバルブの流入口16から、流体通路部12を通り、バルブの流出口18につながった排液管30から流体が排出される。
【0011】
隔離膜体14は、その栓体24側を押さえ板32によって栓体24に固着され、またその外縁側をハウジング部20に固着している。このように隔離膜体14によって流体通路部12と、エアシリンダー26等が設置されたバルブの移動手段側とが遮断される。つまり、隔離膜体14によって、流体通路部12をなす空間の境界の一部が形成される。また、ハウジング部20は移動手段側で隔離膜体14とロッド28を囲むように設置されている。このハウジング部20には栓体24の動きをスムーズにするための空気抜き穴34が設けられ、その空気抜き穴34のところに温度センサ22が設置されている。
【0012】
以上が本発明の概略構成である。次に各構成要素の詳細な説明を行う。図1と図2が本発明の隔離膜体付きバルブであり、図1はバルブが開いた状態、図2はバルブが閉じた状態を示している。図1と図2では対応する部分に同一符号を付けた。
バルブ10の流体通路部12の流入口16は、タンク等の排出口46に固着され使用される。栓体24はその先端部がリング状のパッキング48で囲まれており、バルブを閉じた状態では図2のように、栓体24の先端部が流入口16に嵌入しており流体の流れが止められている。栓体24はロッド28を介してエアシリンダー26に接続され、このエアシリンダー26により、栓体24の開閉が行われる。隔離膜体14は栓体24の移動に伴った変形が可能な構成となっている。この隔離膜体14には、アラミド繊維で補強されたエチレンプロピレンゴム製のベローズ、ダイヤフラム等の従来公知な構成を用いればよい。
【0013】
また、隔離膜体14とロッド28を囲むようにハウジング部20が備えられており、隔離膜体14は栓体24側を押さえ板32で押さえられ栓体24に気密に固着しており、また外縁側をハウジング部20に気密に固着されている。このように、隔離膜体14は流体通路部12を外界と気密に遮断するようになっている。 また、ロッド28と栓体24の間には円筒形の案内筒36があり、この案内筒36を包むように隔離膜体14が変形する(図1、2参照)。
また、ハウジング部20には空気抜き穴34が設けられており、このため栓体24の開閉に伴う隔離膜体14の変形が容易になる。
【0014】
エアシリンダー26が収縮すると、図1に示すように栓体24がバルブの流入口16との嵌合を解き、バルブの流出口18につながった排液管30と、バルブに接続されたタンクの排出口46が連通しタンク内の残液や洗浄液等が排出される。このとき隔離膜体14はハウジング部20の内側及び案内筒36の外側に沿って変形し、ハウジング部20内の空気は空気抜き穴34から排出され、ハウジング部20内の空気が隔離膜体の変形を阻害しない構成となっている。また、図2に示すように、逆にバルブの流入口16を閉じるためエアシリンダー26を伸ばすと、空気抜き穴34から空気が流入して隔離膜体14が案内筒36を包むように変形し栓体24がバルブの流入口16に嵌入してタンクの排出口46を密封する。
【0015】
さて、本発明の特徴部分は、隔離膜体によって隔てられた流体通路部の外部である移動手段側に温度検知手段を備えたところにある。以下に隔離膜体の破損検出方法の説明を行う。
まず、あらかじめ隔離膜体が正常な状態でハウジング内の温度の時間変化を測定する。つまり、図1に示したように、流体通路部12を高温の流体(通常の状態に加温された洗浄液や殺菌液等)が流れた状態でのハウジング部20内の温度の時間変化を測定する。図3は隔離膜体の部分を拡大した図である。図3(a)が正常時、図3(b)が破損時の状態を模式的に示している。
【0016】
基準温度情報の設定は、図3(a)で示したような正常時のハウジング部内の温度を測定することで行われる。ハウジング部内の温度は、隔離膜体やバルブの壁を通した熱伝導によって決まるものであり、そのバルブに固有の温度、温度変化を示す。このように測定された所定時間範囲の温度上昇グラフやある時点での温度等を基準温度情報として設定手段40により設定され、コンピュータ38に含まれるメモリなどの記憶手段42に記憶される。この基準温度情報の設定は、温度測定データを温度センサ22からコンピュータ38の設定手段40へと送り自動的に行うようにしてもよい。
【0017】
隔離膜体の破損検出は、上記のようにして求められた基準温度情報との比較によって行われる。図1のように流体通路部12内を高温の流体が流れた状態でハウジング部20内の温度センサ22により、ハウジング部20内部の温度の時間変化を測定する。この測定温度情報は、コンピュータ38内の記憶手段42へと送られ記憶される。そこで、予め記憶されている基準温度情報と測定温度情報とをコンピュータ38内の比較手段44により比較し、破損の有無を検出する。
【0018】
破損の有無は所定の時点での温度等の温度情報の特性を比較することで確認される。図3(b)では隔離膜体が破損した状態を模式的に示している。隔離膜体に破損部があれば所定時間範囲に測定された温度変化は正常状態での温度変化よりも急激な変化を示し、ハウジング部内の温度が正常状態よりも常に高い温度を生ずることになる。なぜなら、前記のようなバルブに固有な温度変化に加え、図3(b)に示すように破損部からの流体の漏れによる熱の移動が加わるためである。このように、破損部から漏れた流体が直接温度センサ22に接触することによる温度変化、もしくは流体の漏れによるハウジング部内の間接的な温度変化を温度センサ22が検知することで破損検出が可能となる。
【0019】
正常状態での温度変化と破損のある場合の温度変化は、ある時間経過した範囲内で顕著で安定した差異が生じるため、温度変化の測定をその時間範囲内で行うようにするのが好ましい。
このように本発明の隔離膜体付きバルブでは、隔離膜体の外部側に温度検知手段を備えたため、簡単な構成で隔離膜体の破損を検出できる。また、本発明の隔離膜体の破損検出方法では、定期的なバルブの分解点検によってしか発見できなかった隔離膜体の破損を、バルブを分解することなく検出することが可能となる。
また、エアシリンダーをコンピュータに接続し、破損が検知されたときにバルブを自動的に閉じるような構成、または警告信号を発するような構成にすることも可能である。
【0020】
【実施例】
本発明の隔離膜体付きバルブは、栓バルブ、充填バルブ等に使用することができる。図4は、本発明の隔離膜体付きバルブを栓バルブとして無菌充填装置のタンクの排液口に装着した例である。無菌充填装置は、例えばプラスチックカップや罐等の容器内に食品内容液を充填するために使用される。本発明のバルブ10はタンク50の排出口46に装着されている。
タンク50の上方の側壁には、タンク50内へ窒素ガスなどの不活性ガスを充填して内容液を酸化から守るためのガス導入口52があり、タンク50の下方側壁にはタンク50内へ内容液を供給する内容液供給口54が設けられている。
【0021】
タンク50の底には充填バルブ56を設置しており、該充填バルブ56は、リング状のアウターピストン58と中央の円柱状のインナーピストン60によって定量充填を可能にしている。
また、タンク50内には穴の開いた断面円弧形の攪拌板62が吊り下げられており、該攪拌板62は、エアシリンダー(図示せず)によって上下に動かされ、容器に内容液を充填しているときに、タンク50内の内容液に沈殿が起きないようにしている。また、攪拌板62を支えるロッド64のすべり軸受け66にはノズル68からの過熱水蒸気が通され、該すべり軸受け66からタンク50内へ雑菌や異物が侵入しないようになっている。
【0022】
概略以上のような構成で、本発明の破損検出方法の試験を行った。ただし、タンクの容量は100リットルで、充填バルブを7本備え、直径約50mmの栓バルブを5本備えた構成とした。この栓バルブのうちの一本を本発明のバルブとして、ハウジング部内の温度変化を測定した。図5は正常時の状態と、隔離膜体が破損した状態での温度変化を示したグラフである。横軸を時間(秒)、縦軸を温度(℃)とした。
図5のグラフAが正常な状態の温度変化を示したものであり、グラフBが隔離膜体に10mmのスリットを入れ、破損した隔離膜体を想定した場合の温度変化を示したものである。
【0023】
まずバルブを閉じた状態で、タンク内を殺菌するために130℃の過熱水蒸気を0.2MPaの圧力で500kg/hourの量をタンクの天井付近に設置した配管69からタンク内に供給した(図4参照)。タンク内に過熱水蒸気を供給してから180秒後にバルブを開き、その後2540秒後に過熱水蒸気の供給を中止した。
【0024】
タンクに過熱水蒸気を供給し始めた0秒では、グラフA及びグラフB共に、約20℃程度の室温を呈している。そして、約180秒後にバルブの栓体を開くと、グラフA(正常な状態)ではその約60秒後から昇温を開始した。また、正常な隔離膜体をもつバルブでは、ハウジング内の温度変化は隔離膜体やバルブの壁面を通しての熱伝導によるため、バルブ表面からの放熱の効果と合わさって、緩やかな温度変化を示す。つまりグラフAから分かるように、熱伝導で伝わって来る熱と表面からの放熱のために5℃程度の範囲の昇降を示しながら、緩やかに100℃程度まで上昇している。過熱水蒸気の供給を停止した後は、放熱により温度は下降していく。また過熱水蒸気は水となってバルブの排液管から排出される。
【0025】
一方グラフB(隔離膜体にスリットを入れ、破損を想定した場合)には、スリットから過熱水蒸気が直接漏れる等の原因で、バルブの開放後グラフAよりも短時間に急速に温度上昇し、ハウジング内の温度は120℃程度に跳ね上がった。さらに、グラフBの場合は最終的に過熱水蒸気の温度である約130℃まで上昇しそこで平衡に達した。過熱水蒸気の供給停止後は、グラフAの場合と同様に温度が下降していく。
【0026】
本実施例の装置の場合、隔離膜体の破損が小さなものであっても、過熱水蒸気の供給開始後500秒〜1000秒(バルブの開放後320秒〜820秒)の間で、正常な隔離膜体を持ったもの(グラフA)と破損した隔離膜体を持ったもの(グラフB)とのハウジング内の温度差が安定して顕著になる。そこで、この間の温度情報を基準温度情報(グラフA)として設定し、この基準温度情報とこの間に測定した測定温度情報(グラフB)とを比較し破損の有無を検出するのが好ましい。つまり、過熱水蒸気の供給後500秒〜1000秒の間の所定時間範囲での温度情報を比較し、測定温度情報が基準温度情報よりも高温に成った状態を検出して破損の有無を検出する。本実施例の装置の場合、過熱水蒸気の供給後500秒〜1000秒の間の基準温度情報(グラフA)は、50℃〜85℃であり、測定温度情報(グラフB)は120℃〜130℃であるので、45℃以上の差が有るため、確実に破損が検出される。
なお、本実施例では、本発明の隔離膜体付きバルブを栓バルブとして用いたが、充填バルブに適用してもよいことは明らかである。
【0027】
【発明の効果】
本発明の隔離膜体付きバルブによれば、移動手段側に温度検知手段を備えたことで、簡単な構成かつ容易に隔離膜体の破損を検出することができる。また、本発明の隔離膜体の破損検出方法によれば、ハウジング部内の温度情報を検知することで、バルブを分解点検の必要なく、隔離膜体の破損を検出することが可能となる。
【図面の簡単な説明】
【図1】本発明の隔離膜体付きバルブの概略構成図。
【図2】本発明の隔離膜体付きバルブの断面図。
【図3】バルブの隔離膜体部分の拡大模式図。
【図4】本発明の隔離膜体付きバルブを取りつけたタンクの概略構成図。
【図5】ハウジング内部の温度変化を示すグラフ。
【符号の説明】
10…隔離膜体付きバルブ
12…流体通路部
14…隔離膜体
16…流入口
18…流出口
20…ハウジング部
22…温度センサ
24…栓体
26…エアシリンダー
28…ロッド
[0001]
BACKGROUND OF THE INVENTION
The present invention relates to a valve with an isolation film body, and more particularly to a damage detection mechanism and a damage detection method for the isolation film body.
[0002]
[Prior art]
The filling valve that opens and closes the opening of the nozzle that fills the contents of the container and the plug valve that opens and closes the opening of the food supply port or drainage port of the food tank prevent invasion of germs and foreign substances from the opening. Therefore, on the contrary, the valve opening side and the valve operating side are formed of a deformable material such as a diaphragm or a bellows in order to prevent contents from entering the valve operating side. Isolation with an isolation film body is performed (see, for example, Patent Documents 1 to 4).
[0003]
[Patent Document 1]
Japanese Patent Publication No. 63-44601 [Patent Document 2]
Japanese Utility Model Publication 1-18482 [Patent Document 3]
Japanese Patent No. 3214113 [Patent Document 4]
JP-A-2001-219996 [0004]
[Problems to be solved by the invention]
The isolation membrane used in the above filling valve and plug valve is a cleaning liquid heated to a desired temperature on the opening side for cleaning or sterilization or a sterilizing liquid such as hydrogen peroxide or steam, and heated aseptic air for drying. May be rapidly deteriorated by flowing, and the like, and may be damaged by repeated deformation due to repeated opening and closing, and a small hole may be opened.
When a small hole is opened in the isolation film body, there is a possibility that germs and foreign substances may be mixed into the container or tank from the small hole. In particular, in the aseptic filling method, since the sterilization step to be performed after filling the container with the contents and sealing the container is omitted, it is conceivable that in the worst case, the contents liquid will rot. In addition, the isolation membrane used for the valve is often arranged so that it cannot be seen from the outside due to its configuration, and periodic disassembly and inspection is necessary to confirm damage to the isolation membrane. It was. Therefore, there has been a demand for a valve that can easily detect breakage of the isolation film body and a breakage detection method thereof.
[0005]
The present invention has been made in view of the above problems, and an object of the present invention is to provide a valve and a breakage detection method capable of detecting breakage of an isolation film body with a very simple configuration.
[0006]
[Means for Solving the Problems]
In order to achieve the above object, a valve with an isolation film body according to the present invention is provided with a fluid passage portion serving as a fluid passage inside, and a plug body for opening and closing the outlet or / and the inlet of the fluid passage portion. Means, a moving means for moving the plug body means forward and backward, and an isolation film body fixed to the wall of the plug body means and the fluid passage portion and deformed in accordance with the movement of the plug body means, The outlet or / and inlet is closed when the plug means advance, and the outlet or / and inlet is opened and the outlet or / and inlet is opened and closed when the plug means is retracted. In addition, in the valve with a separation membrane body that separates the fluid passage portion side and the moving means side from each other by the separation membrane body, the stopper body continuously extends from the wall of the fluid passage portion in the backward direction of the plug body means. hand stage, a space integral with the moving unit及 beauty said separator member As formed, is formed into a bottomed cylindrical cross-section concave shape, the outer peripheral surface of the tubular is exposed to the outside, and said closure body means and said moving means by penetrating the moving means at its bottom And a housing part provided with an air vent hole that directly communicates the space and the outside, and a temperature that is installed in the housing part via the air vent hole and detects the temperature of the space in the housing part Detecting means, and detecting breakage of the isolation film body based on temperature information in the housing portion measured by the temperature detecting means.
[0007]
The method for detecting breakage of a separation membrane body according to the present invention includes a fluid passage portion serving as a fluid passage inside, plug means for opening and closing the outlet or / and the inlet of the fluid passage portion, and the stopper A moving means for moving the means forward and backward, and an isolation film body fixed to the wall of the plug means and the fluid passage portion and deformed in accordance with the movement of the plug means, and when the plug means is advanced The outlet or / and inlet is closed, and the outlet or / and inlet is opened and closed when the plug means is retracted, and the outlet or / and inlet is opened and closed. in separator body with valve for isolating said moving means side to the fluid passage portion side, the plug body hand stage, so as to form a space integral with said moving means及 beauty the separator body, the cross-sectional concave shape It is formed in a bottomed cylindrical shape, and its cylindrical outer peripheral surface is exposed to the outside And the housing portion and by connecting the said closure body means and said moving means by penetrating the moving means, the vent holes and direct communication between the space and the outside is provided at the bottom thereof, the housing A method for detecting breakage of an isolation membrane body in a valve with an isolation membrane body provided with a temperature detection means for detecting the temperature of a space in the housing portion installed through the air vent hole in the portion, When a fluid having a temperature higher than the outside air temperature is passing, the temperature information of the space in the housing part is measured, and the measured temperature information is compared with the normal reference temperature information measured in advance. By this, the breakage of the isolation film body is detected.
[0008]
Further, in the above-described method for detecting breakage of the separator film, the measured temperature information is temperature information after a predetermined time has elapsed since a fluid having a temperature higher than the outside air temperature starts to pass through the fluid passage, The reference temperature information is reference temperature information after a predetermined time has elapsed since a fluid having a temperature higher than the outside air temperature starts to pass through the fluid passage, and the measured temperature information is higher than the reference temperature information. It is preferable to determine that there is damage to the isolation film body.
[0009]
DETAILED DESCRIPTION OF THE INVENTION
The valve with a separator according to the present invention will be described in detail below with reference to the drawings. FIG. 1 is a sectional view of a valve with a separator according to the present invention. The valve 10 with a separator according to the present invention includes a fluid passage portion 12 serving as a fluid passage in a liquid state or a gas state, and a plug means (plug body) for opening and closing the inlet 16 of the fluid passage portion 12. 24), moving means (rod 28, air cylinder 26) for moving the plug body 24, and the isolation film body 14 deformed in accordance with the movement of the plug body 24. The isolation film body 14 isolates the fluid passage portion 12 side from the moving means side. Further, a housing part 20 is installed on the moving means side so as to surround the isolation film body 14, and a temperature detection means (temperature sensor 22) is provided in the housing part 20.
[0010]
In this embodiment, as a plug body means for opening and closing the valve, a plug body 24 that is fitted into the inlet 16 and closes the inlet 16 is provided. Further, as moving means for moving the plug 24, a rod 28 connected to the plug 24 and an air cylinder 26 connected to the rod 28 are provided. The plug 24 is moved by the air cylinder 26 to open and close the valve. FIG. 1 shows a state in which the plug 24 is open, and fluid flows through the fluid passage portion 12. In other words, the fluid is discharged from the inlet 16 of the valve connected to the outlet 46 of the tank or the like, through the fluid passage portion 12 and from the drain pipe 30 connected to the outlet 18 of the valve.
[0011]
The isolation film body 14 is fixed to the plug body 24 on the plug body 24 side by a pressing plate 32, and the outer edge side is fixed to the housing portion 20. In this manner, the isolation membrane body 14 blocks the fluid passage portion 12 from the moving means side of the valve on which the air cylinder 26 and the like are installed. That is, a part of the boundary of the space forming the fluid passage portion 12 is formed by the isolation film body 14. Moreover, the housing part 20 is installed so that the isolation membrane body 14 and the rod 28 may be enclosed by the moving means side. The housing portion 20 is provided with an air vent hole 34 for smooth movement of the plug body 24, and the temperature sensor 22 is installed at the air vent hole 34.
[0012]
The above is the schematic configuration of the present invention. Next, each component will be described in detail. 1 and 2 show a valve with an isolation membrane according to the present invention. FIG. 1 shows a state in which the valve is opened, and FIG. 2 shows a state in which the valve is closed. In FIG. 1 and FIG. 2, the same reference numerals are assigned to corresponding parts.
The inlet 16 of the fluid passage portion 12 of the valve 10 is used by being fixed to an outlet 46 such as a tank. The distal end of the plug 24 is surrounded by a ring-shaped packing 48. When the valve is closed, the distal end of the plug 24 is fitted into the inlet 16 as shown in FIG. Stopped. The plug 24 is connected to an air cylinder 26 via a rod 28, and the plug 24 is opened and closed by the air cylinder 26. The isolation film body 14 is configured to be deformable with the movement of the plug body 24. The separator 14 may have a conventionally known configuration such as an ethylene propylene rubber bellows or diaphragm reinforced with aramid fibers.
[0013]
In addition, a housing part 20 is provided so as to surround the isolation film body 14 and the rod 28, and the isolation film body 14 is pressed against the plug body 24 by a pressing plate 32 and is airtightly fixed to the plug body 24. The outer edge side is airtightly fixed to the housing part 20. In this way, the isolation film body 14 is configured to block the fluid passage portion 12 from the outside in an airtight manner. A cylindrical guide tube 36 is provided between the rod 28 and the plug 24, and the isolation film member 14 is deformed so as to wrap the guide tube 36 (see FIGS. 1 and 2).
Further, the housing part 20 is provided with an air vent hole 34, and therefore, the deformation of the isolation film body 14 accompanying opening and closing of the plug body 24 is facilitated.
[0014]
When the air cylinder 26 contracts, as shown in FIG. 1, the plug 24 is disengaged from the inlet 16 of the valve, and the drain pipe 30 connected to the outlet 18 of the valve and the tank connected to the valve A discharge port 46 communicates with the remaining liquid, cleaning liquid, etc. in the tank. At this time, the isolation film body 14 is deformed along the inside of the housing part 20 and the outside of the guide tube 36, the air in the housing part 20 is discharged from the air vent hole 34, and the air in the housing part 20 is deformed of the isolation film body. It is the composition which does not inhibit. In contrast, when the air cylinder 26 is extended to close the inlet 16 of the valve, as shown in FIG. 2, air flows in from the air vent hole 34 so that the isolation membrane body 14 wraps around the guide cylinder 36 and is plugged. 24 fits into the inlet 16 of the valve and seals the outlet 46 of the tank.
[0015]
The characteristic part of the present invention resides in that a temperature detecting means is provided on the moving means side outside the fluid passage portion separated by the isolation film body. A method for detecting breakage of the separator film will be described below.
First, the time change of the temperature in the housing is measured in advance with the isolation film body in a normal state. That is, as shown in FIG. 1, the time change of the temperature in the housing part 20 is measured when a high-temperature fluid (cleaning liquid or sterilizing liquid heated to a normal state) flows through the fluid passage part 12. To do. FIG. 3 is an enlarged view of a portion of the isolation film body. FIG. 3 (a) schematically shows a normal state, and FIG. 3 (b) schematically shows a damaged state.
[0016]
The setting of the reference temperature information is performed by measuring the temperature in the housing part at the normal time as shown in FIG. The temperature in the housing portion is determined by heat conduction through the wall of the isolation membrane body or the valve, and shows a temperature and a temperature change specific to the valve. The temperature rise graph in the predetermined time range measured in this way, the temperature at a certain time point, etc. are set as reference temperature information by the setting means 40 and stored in the storage means 42 such as a memory included in the computer 38. The reference temperature information may be set automatically by sending temperature measurement data from the temperature sensor 22 to the setting means 40 of the computer 38.
[0017]
Detection of the breakage of the isolation film body is performed by comparison with the reference temperature information obtained as described above. As shown in FIG. 1, a time change in the temperature inside the housing portion 20 is measured by the temperature sensor 22 in the housing portion 20 in a state where a high-temperature fluid flows in the fluid passage portion 12. This measured temperature information is sent to and stored in the storage means 42 in the computer 38. Therefore, the reference temperature information stored in advance and the measured temperature information are compared by the comparison means 44 in the computer 38 to detect the presence or absence of damage.
[0018]
The presence or absence of breakage is confirmed by comparing the characteristics of temperature information such as temperature at a predetermined time. FIG. 3B schematically shows a state where the separator film body is damaged. If there is a damaged part in the isolation film body, the temperature change measured in the predetermined time range shows a more rapid change than the temperature change in the normal state, and the temperature in the housing part is always higher than the normal state. . This is because, in addition to the temperature change inherent to the valve as described above, heat transfer due to fluid leakage from the damaged portion is added as shown in FIG. As described above, the temperature sensor 22 detects the temperature change caused by the fluid leaking from the damaged part directly contacting the temperature sensor 22 or the indirect temperature change in the housing part caused by the fluid leak, thereby enabling the damage detection. Become.
[0019]
Since the temperature change in the normal state and the temperature change in the case of breakage have a remarkable and stable difference within a certain time range, it is preferable to measure the temperature change within the time range.
As described above, in the valve with the isolation film body according to the present invention, since the temperature detection means is provided on the outside of the isolation film body, the damage of the isolation film body can be detected with a simple configuration. In addition, according to the method for detecting breakage of the isolation film body of the present invention, it is possible to detect the breakage of the isolation film body, which can be found only by periodic disassembly and inspection of the valve, without disassembling the valve.
It is also possible to connect the air cylinder to a computer and automatically close the valve when a breakage is detected, or to generate a warning signal.
[0020]
【Example】
The valve with a separator according to the present invention can be used for a plug valve, a filling valve and the like. FIG. 4 shows an example in which the valve with a separator according to the present invention is attached to a drain port of a tank of an aseptic filling apparatus as a plug valve. The aseptic filling device is used for filling a food content liquid in a container such as a plastic cup or a basket. The valve 10 of the present invention is attached to the discharge port 46 of the tank 50.
The upper side wall of the tank 50 has a gas inlet 52 for filling the tank 50 with an inert gas such as nitrogen gas to protect the content liquid from oxidation, and the lower side wall of the tank 50 enters the tank 50. A content liquid supply port 54 for supplying the content liquid is provided.
[0021]
A filling valve 56 is provided at the bottom of the tank 50, and the filling valve 56 is capable of quantitative filling by a ring-shaped outer piston 58 and a central cylindrical inner piston 60.
Further, a stirring plate 62 having an arc-shaped cross section with a hole is suspended in the tank 50, and the stirring plate 62 is moved up and down by an air cylinder (not shown) to transfer the content liquid into the container. When filling, the content liquid in the tank 50 is prevented from being precipitated. Further, superheated steam from the nozzle 68 is passed through the slide bearing 66 of the rod 64 that supports the stirring plate 62 so that germs and foreign substances do not enter the tank 50 from the slide bearing 66.
[0022]
The test of the damage detection method of the present invention was performed with the above-described configuration. However, the tank had a capacity of 100 liters, was equipped with 7 filling valves and 5 plug valves with a diameter of about 50 mm. One of the plug valves was used as a valve of the present invention, and the temperature change in the housing portion was measured. FIG. 5 is a graph showing temperature changes in a normal state and in a state in which the isolation film body is damaged. The horizontal axis is time (seconds), and the vertical axis is temperature (° C.).
A graph A in FIG. 5 shows a change in temperature in a normal state, and a graph B shows a change in temperature when a 10 mm slit is formed in the separator and a damaged separator is assumed. .
[0023]
First, with the valve closed, in order to sterilize the tank, superheated steam at 130 ° C. was supplied into the tank at a pressure of 0.2 MPa and an amount of 500 kg / hour from a pipe 69 installed near the ceiling of the tank (FIG. 4). The valve was opened 180 seconds after the superheated steam was supplied into the tank, and the supply of superheated steam was stopped after 2540 seconds.
[0024]
In 0 seconds when superheated steam is started to be supplied to the tank, both the graph A and the graph B exhibit a room temperature of about 20 ° C. Then, when the valve plug was opened after about 180 seconds, in graph A (normal state), the temperature started to increase after about 60 seconds. Further, in a valve having a normal isolation film body, the temperature change in the housing is due to heat conduction through the isolation film body and the wall surface of the valve, and therefore, a moderate temperature change is shown together with the effect of heat radiation from the valve surface. That is, as can be seen from the graph A, the temperature gradually rises to about 100 ° C. while showing a rise and fall in a range of about 5 ° C. due to heat transferred by heat conduction and heat radiation from the surface. After the supply of superheated steam is stopped, the temperature decreases due to heat dissipation. The superheated steam becomes water and is discharged from the drain pipe of the valve.
[0025]
On the other hand, in graph B (when a slit is inserted in the separator film and damage is assumed), the temperature rises more rapidly in a shorter time than graph A after the valve is opened due to, for example, direct leakage of superheated steam from the slit, The temperature in the housing jumped to about 120 ° C. Further, in the case of graph B, the temperature finally increased to about 130 ° C., which is the temperature of superheated steam, and reached equilibrium there. After the supply of superheated steam is stopped, the temperature decreases as in the case of graph A.
[0026]
In the case of the apparatus of the present embodiment, even if the separator film body is smallly damaged, normal isolation is performed between 500 seconds and 1000 seconds after starting the supply of superheated steam (320 seconds to 820 seconds after opening the valve). The temperature difference in the housing between the one with the membrane body (graph A) and the one with the damaged separator membrane body (graph B) becomes stable and remarkable. Therefore, it is preferable to set the temperature information during this period as reference temperature information (graph A) and compare the reference temperature information with measured temperature information measured during this time (graph B) to detect the presence or absence of breakage. That is, the temperature information in a predetermined time range between 500 seconds and 1000 seconds after the supply of superheated steam is compared, and the presence or absence of breakage is detected by detecting the state where the measured temperature information is higher than the reference temperature information. . In the case of the apparatus of the present embodiment, the reference temperature information (graph A) for 500 seconds to 1000 seconds after the supply of superheated steam is 50 ° C. to 85 ° C., and the measured temperature information (graph B) is 120 ° C. to 130 ° C. Since it is ° C., there is a difference of 45 ° C. or more, so damage is reliably detected.
In the present embodiment, the valve with a separator according to the present invention is used as a plug valve, but it is obvious that the valve may be applied to a filling valve.
[0027]
【The invention's effect】
According to the valve with an isolation film body of the present invention, it is possible to easily detect the breakage of the isolation film body by providing the temperature detection means on the moving means side. In addition, according to the method for detecting breakage of the isolation film body of the present invention, it is possible to detect breakage of the isolation film body without detecting the valve by disassembling and checking the temperature information in the housing portion.
[Brief description of the drawings]
FIG. 1 is a schematic configuration diagram of a valve with a separator according to the present invention.
FIG. 2 is a cross-sectional view of a valve with a separator according to the present invention.
FIG. 3 is an enlarged schematic view of a separation membrane body portion of the valve.
FIG. 4 is a schematic configuration diagram of a tank equipped with a valve with a separator film according to the present invention.
FIG. 5 is a graph showing a temperature change inside the housing.
[Explanation of symbols]
DESCRIPTION OF SYMBOLS 10 ... Valve with isolation membrane body 12 ... Fluid passage part 14 ... Isolation film body 16 ... Inlet 18 ... Outlet 20 ... Housing part 22 ... Temperature sensor 24 ... Plug body 26 ... Air cylinder 28 ... Rod

Claims (3)

流体の通路となる流体通路部を内部に設け、前記流体通路部の流出口又は/及び流入口を開閉するための栓体手段と、該栓体手段の進退移動を行う移動手段と、前記栓体手段及び前記流体通路部の壁と固着し且つ前記栓体手段の動きに伴い変形する隔離膜体と、を備え、前記栓体手段の進出時に前記流出口又は/及び流入口を閉栓し、前記栓体手段の後退時に前記流出口又は/及び流入口を開放して前記流出口又は/及び流入口の開閉を行い、且つ前記隔離膜体により前記流体通路部側と前記移動手段側とを隔離する隔離膜体付きバルブにおいて、
前記流体通路部の壁より連続して該栓体手段の後退方向へと、前記栓体手段、前記移動手段及び前記隔離膜体とともに一体の空間を形成するように、断面凹字形の有底筒状に形成され、その筒状の外周表面が外部に露出しており、その底部において該移動手段を貫通させて該栓体手段と該移動手段とを連結させており、且つ該空間と外部とを直接連通する空気抜き穴が設けられたハウジング部と、
該ハウジング部内に該空気抜き穴を介して設置され、該ハウジング部内の空間の温度を検知する温度検知手段と、を備え、
前記温度検知手段により測定された前記ハウジング部内の温度情報により前記隔離膜体の破損を検出することを特徴とする隔離膜体付きバルブ。
A fluid passage portion serving as a fluid passage; plug means for opening and closing the outlet or / and inlet of the fluid passage portion; moving means for moving the stopper means forward and backward; and the stopper An isolation membrane that is fixed to the body means and the wall of the fluid passage portion and deforms as the plug means moves, and closes the outlet or / and the inlet when the plug means advances. When the plug means is retracted, the outlet or / and the inlet is opened to open / close the outlet or / and the inlet, and the fluid passage section side and the moving means side are separated by the isolation film body. In a valve with an isolating membrane to isolate,
To backward direction of said closure member means continuously from the wall of the fluid passage portion, the plug body hand stage, so as to form a space integral with said moving means及 beauty the separator body, closed cross-sectional concave shape It is formed in a bottom cylindrical shape, the outer peripheral surface of the cylindrical shape is exposed to the outside, and the stopper means and the moving means are connected by penetrating the moving means at the bottom, and the space A housing part provided with an air vent hole that directly communicates with the outside;
A temperature detecting means that is installed in the housing part through the air vent hole and detects the temperature of the space in the housing part;
The isolation membrane body-equipped valve is characterized in that breakage of the isolation membrane body is detected from temperature information in the housing portion measured by the temperature detection means.
流体の通路となる流体通路部を内部に設け、前記流体通路部の流出口又は/及び流入口を開閉するための栓体手段と、該栓体手段の進退移動を行う移動手段と、前記栓体手段及び前記流体通路部の壁と固着し且つ前記栓体手段の動きに伴い変形する隔離膜体と、を備え、前記栓体手段の進出時に前記流出口又は/及び流入口を閉栓し、前記栓体手段の後退時に前記流出口又は/及び流入口を開放して前記流出口又は/及び流入口の開閉を行い、且つ前記隔離膜体により前記流体通路部側と前記移動手段側とを隔離する隔離膜体付きバルブにおいて、前記流体通路部の壁より連続して該栓体手段の後退方向へと、前記栓体手段、前記移動手段及び前記隔離膜体とともに一体の空間を形成するように、断面凹字形の有底筒状に形成され、その筒状の外周表面が外部に露出しており、その底部において該移動手段を貫通させて該栓体手段と該移動手段とを連結させており、且つ該空間と外部とを直接連通する空気抜き穴が設けられたハウジング部と、該ハウジング部内に該空気抜き穴を介して設置され、該ハウジング部内の空間の温度を検知する温度検知手段とを備えた隔離膜体付きバルブにおける隔離膜体の破損検出方法であって、
前記流体通路内を外気温よりも高い温度の流体が通過しているときに、前記ハウジング部内の空間の温度情報を測定し、
測定した温度情報と予め測定しておいた正常時の基準温度情報とを比較することにより、前記隔離膜体の破損を検出することを特徴とする隔離膜体の破損検出方法。
A fluid passage portion serving as a fluid passage; plug means for opening and closing the outlet or / and inlet of the fluid passage portion; moving means for moving the stopper means forward and backward; and the stopper An isolation membrane that is fixed to the body means and the wall of the fluid passage portion and deforms as the plug means moves, and closes the outlet or / and the inlet when the plug means advances. When the plug means is retracted, the outlet or / and the inlet is opened to open / close the outlet or / and the inlet, and the fluid passage section side and the moving means side are separated by the isolation film body. formed in the separator body valved to isolate, and to the retracted direction of said closure member means continuously from the wall of the fluid passage portion, the plug body hand stage, a space integral with said moving means及 beauty said separator member So that it is formed into a bottomed cylindrical shape with a concave cross section, and its cylindrical shape The outer peripheral surface is exposed to the outside, and by coupling the said closure body means and said moving means by penetrating the moving means, the vent holes and direct communication between the space and the outside is provided at the bottom thereof A method for detecting breakage of an isolation film body in a valve with an isolation film body comprising a housing portion and a temperature detection means that is installed in the housing portion through the air vent hole and detects the temperature of the space in the housing portion. And
When a fluid having a temperature higher than the outside air temperature passes through the fluid passage, the temperature information of the space in the housing part is measured,
A method for detecting breakage of an isolation film body, wherein the breakage of the isolation film body is detected by comparing measured temperature information with reference temperature information measured in advance under normal conditions.
請求項2記載の隔離膜体の破損検出方法において、
前記測定した温度情報が、前記流体通路内を外気温よりも高い温度の流体が通過し始めてから所定時間経過した後の温度情報であり、
前記基準温度情報が、前記流体通路内を外気温よりも高い温度の流体が通過し始めてから所定時間経過した後の基準温度情報であり、
該測定した温度情報が、該基準温度情報よりも高温であったときに隔離膜体に破損が存在すると判断することを特徴とする隔離膜体の破損検出方法。
In the method for detecting breakage of the separator film according to claim 2,
The measured temperature information is temperature information after a predetermined time has elapsed since a fluid having a temperature higher than the outside air temperature starts to pass through the fluid passage.
The reference temperature information is reference temperature information after a predetermined time has elapsed since the fluid having a temperature higher than the outside air temperature starts to pass through the fluid passage.
A method for detecting breakage of an isolation film body, characterized in that when the measured temperature information is higher than the reference temperature information, the isolation film body is judged to be damaged.
JP2003011199A 2003-01-20 2003-01-20 Valve with isolation membrane body and method for detecting breakage of isolation membrane body Expired - Fee Related JP4440549B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2003011199A JP4440549B2 (en) 2003-01-20 2003-01-20 Valve with isolation membrane body and method for detecting breakage of isolation membrane body

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2003011199A JP4440549B2 (en) 2003-01-20 2003-01-20 Valve with isolation membrane body and method for detecting breakage of isolation membrane body

Publications (2)

Publication Number Publication Date
JP2004225735A JP2004225735A (en) 2004-08-12
JP4440549B2 true JP4440549B2 (en) 2010-03-24

Family

ID=32900172

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2003011199A Expired - Fee Related JP4440549B2 (en) 2003-01-20 2003-01-20 Valve with isolation membrane body and method for detecting breakage of isolation membrane body

Country Status (1)

Country Link
JP (1) JP4440549B2 (en)

Also Published As

Publication number Publication date
JP2004225735A (en) 2004-08-12

Similar Documents

Publication Publication Date Title
CN101588985B (en) Filling system
US6601618B2 (en) Filling apparatus and filling method therefor
US7082848B2 (en) Method of transferring a representative fluid sample from a pressurized source into a sample bottle
US8544315B2 (en) At rest vacuum state for vacuum decay leak testing method and system
JP7300187B2 (en) Diaphragm valve and its monitoring method
CN107076636A (en) Membrane well with the measurement volume for thick leak-testing
CN109724667A (en) The detection method and system of liquid volume percent and the distributor with the system in container
JP4567454B2 (en) A test leak device for a sniffing leak probe.
US6595040B1 (en) Test leak unit
CN102245227A (en) Apparatus for treating a medical liquid, and method for checking the leaktightness of the apparatus
JP4440549B2 (en) Valve with isolation membrane body and method for detecting breakage of isolation membrane body
EP2740684A1 (en) Retaining valve and liquid vessel
CN104797916B (en) The method for testing leak detection system
US11898938B2 (en) Method and system, using a colorimetric indicator, for detecting a possible loss of integrity of a flexible bag for biopharmaceutical product
CN204882162U (en) Self -disposable formula oil well associated gas hydrogen sulfide sampling test device of row of exempting from
ITGE20130010A1 (en) DEVICE FOR PROTECTING A LIQUID FROM OXIDATION
US5810040A (en) Container for storing liquids
US20170176283A1 (en) Endoscope reprocessor, and leak test method of endoscope reprocessor
EP1920231A1 (en) Cell for testing fluids at elevated pressures
CN106092457A (en) A kind of detecting device for sealing property of ball valves
CN106568674B (en) Fluid test device and the dissolution of test pressurized fluid and/or gas-entrained method
KR200488821Y1 (en) Packing inspection equipment for leaks in a cover pouch
JP7427020B2 (en) Adapter part for connecting a medical hollow body to a tension/compression measuring device, test assembly, method for testing the tightness of a medical hollow body, and use of the tensile/compression measuring device
CN211696854U (en) Leakage detection device
JP2006053068A (en) Leak test method for inlet sealed section of bag container

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20051208

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20080911

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20080916

A521 Written amendment

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20081117

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20090407

A521 Written amendment

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20090608

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20090915

A521 Written amendment

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20091111

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20091215

A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20100107

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20130115

Year of fee payment: 3

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20140115

Year of fee payment: 4

LAPS Cancellation because of no payment of annual fees