JP3809648B2 - Moving filter filter - Google Patents

Moving filter filter Download PDF

Info

Publication number
JP3809648B2
JP3809648B2 JP2002022620A JP2002022620A JP3809648B2 JP 3809648 B2 JP3809648 B2 JP 3809648B2 JP 2002022620 A JP2002022620 A JP 2002022620A JP 2002022620 A JP2002022620 A JP 2002022620A JP 3809648 B2 JP3809648 B2 JP 3809648B2
Authority
JP
Japan
Prior art keywords
filter medium
filtration
filter
tank
pipe
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP2002022620A
Other languages
Japanese (ja)
Other versions
JP2003220305A (en
Inventor
栄一 石垣
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ishigaki Co Ltd
Original Assignee
Ishigaki Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ishigaki Co Ltd filed Critical Ishigaki Co Ltd
Priority to JP2002022620A priority Critical patent/JP3809648B2/en
Publication of JP2003220305A publication Critical patent/JP2003220305A/en
Application granted granted Critical
Publication of JP3809648B2 publication Critical patent/JP3809648B2/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D24/00Filters comprising loose filtering material, i.e. filtering material without any binder between the individual particles or fibres thereof
    • B01D24/46Regenerating the filtering material in the filter
    • B01D24/4668Regenerating the filtering material in the filter by moving the filtering element
    • B01D24/4689Displacement of the filtering material to a compartment of the filtering device for regeneration

Description

【0001】
【発明の属する技術分野】
本発明は、上水、下水、産業廃水等の懸濁液のろ過装置の改良に関し、特に本発明は珪藻土をろ材として使用し、汚染したろ材を循環させて洗浄再生する移動ろ床式ろ過装置の改良に係るもので、連続して清澄ろ過が行なえるろ過装置に関するものである。
【0002】
【従来の技術】
従来、ろ床を構成するろ材が移動し、このろ材を移動させて洗浄再生し、ろ床の上部に返送する上向流移動ろ床式ろ過装置は公知であり、よく知られている。そして、ろ材として比重が1.0以上の粒状の砂等を用い、汚染した砂を輸送するのに圧縮空気で作動するエアリフト管を使用し、ろ過槽上部の洗浄装置で洗浄再生してろ材層の上部へ返送し、洗浄排水は外部に排出するろ過装置もよく知られている。
【0003】
また、特開平6−47208号公報には、ろ床を構成するろ材として砂粒状の珪藻土を使用したろ過装置において、密閉式のろ過槽の上部に設けた原水供給管から原水を供給し、下降流でろ材層を通過させる間に懸濁物を珪藻土ろ材で除去し、処理水をろ過槽の底部に設けている取出管から取出すようにしたものである。そして、懸濁物によって汚染したろ材を洗浄再生する場合には、前記取出管から洗浄水を供給し、上向流でろ材層を通過させて、ろ材に付着している懸濁物をろ材から剥離させ、汚れた洗浄排水は前記原水供給管より外部へ排出するようにしている。
【0004】
【発明が解決しようとする課題】
図3は従来公知の上向流移動ろ床式ろ過装置を概念的に示した縦断面図であり、原水はろ過槽30下部に設けられた供給口31に供給され、供給口31に接続されているループ状のヘッダー管32と、このヘッダー管32に立設された複数本の流入管33からループ状の分配傘34を介してろ材層35下部に均等に供給される。このようにして供給された原水は、粒状の砂で形成されたろ材層35中を上昇する間に、ろ材層35で夾雑物が捕捉され、その処理水はろ過槽30上部に設けられた処理水取出口36から槽外に排出される。そして、ろ材層35下部の汚染した砂はろ過槽30中心部に立設されたエアリフト管37の下部に圧縮空気を供給することにより、エアリフト管37を上昇し、ろ過槽30上部に配設している洗浄塔38内で、処理水によって洗浄再生される。洗浄されたろ材35aは洗浄塔38内とエアリフト管37外周部に配設しているシュート37a、38aにより、分配されながらろ材層35の上面に返送される。洗浄塔38内で洗浄され、ろ材35aから分離した夾雑物は洗浄塔38上部に設けられている洗浄排水口39から槽外に排出される。上述のろ材35aとして粒状の砂を用いた移動ろ床式ろ過装置ではろ材粒子の表面は平坦で、吸着孔が無く、粒子間隙も大きいので微細なコロイド状の懸濁物は捕捉できずろ材層35を通過するため、処理水の水質が悪化するという課題があった。
【0005】
また、特開平6−47208号公報に記載の発明においては、ろ材に珪藻土を使用しているので、多孔質な特性を有する珪藻土によって、前記のような問題のある微細なコロイド状の懸濁物でも、この珪藻土特有の多孔質によって捕捉されるので、清澄ろ過が行なえ、処理水の水質も良好となるものである。しかしながら、特開平6−47208号公報に記載の発明におけるろ材の洗浄方法では、洗浄中はろ過運転を停止する必要があり、連続運転が行なえずろ過装置が大型になり、設置面積が広くなる。また、洗浄水を逆洗するだけの洗浄方法のため、珪藻土の多孔質部で捕捉された懸濁物は剥離出来ないという問題があり、さらに、洗浄圧力を高くすれば、ろ材が流失するという課題もある。
【0006】
【課題を解決するための手段】
前述した課題を解決するため、本発明は密閉型のろ過槽内部に水より重い粒状のろ材を積層してろ材層を形成し、前記ろ材層の下層部とろ過槽の上部で開口し、前記ろ材を圧縮空気によってろ材層の底部から引抜いて、上方へ移送するとともに該ろ材を洗浄再生してろ材層の上部へと循環させるようにしたエアリフト管を立設し、前記ろ過槽に装填するろ材には珪藻土を使用し、前記ろ材層上方のろ過室に設けた原水の供給口から原水を圧入供給してろ材層中を下降させ、その処理水を前記ろ過槽の下部から取出すようにしたものである。
【0007】
また、ろ過槽に立設したエアリフト管の上端開口部の外周部に分離槽を配設し、前記ろ過槽のろ過室内から該ろ過槽の天板より上方に突出し、前記分離槽を囲撓する洗浄塔を立設し、該洗浄塔の頂部からろ材の洗浄装置を垂設し、該洗浄装置の下端は前記分離槽内まで延設し、前記洗浄塔の上方側部にはろ材の洗浄排出口を設け、前記ろ過槽、洗浄塔、エアリフト管、洗浄装置は略同心状に配設し、前記ろ材の洗浄装置として、超音波洗浄機を用い、前記洗浄塔の上部にはエア排気用のレベル計と、エア排気口を設け、該エア排気口には前記レベル計と連動して開閉する調節弁を設けたものである。
【0008】
また、前記ろ過槽の下部に設けた処理水の取出口は、処理水の取出管に接続されているループ状のヘッダー管と、該ヘッダー管に立設された複数本の流出管と、該流出管の上方に設けられ該流出管へ流入する処理水を均等に分配するループ状の分配傘とで構成し、この分配傘の下面部と、前記洗浄塔と洗浄排出口との開口部にはろ材流失防止用のフィルターを張設した。
【0009】
【発明の実施の形態】
本発明に係る装置は上述のように構成してあるので、上記ろ材層の上部に圧入供給された原水はろ材層中を下降する間に夾雑物(懸濁物)がろ材(珪藻土)に捕捉され、そのろ液(処理水)はろ過槽の下部から槽外へ排出される。これと同時に、エアリフト管に圧縮空気を供給することによって、ろ材層の底部のろ材が引抜かれ、積層したろ材が上方から下方へ徐々に移動する。そして、引抜かれたろ材は、ろ過槽下部の処理水と共にエアリフト管内を撹拌されながら上方の分離槽まで移送される。
【0010】
エアリフト管内において、ろ材の表面に付着した夾雑物は移送中に撹拌されることにより、ろ材表面から剥離する。そして、分離槽まで移送されたろ材は分離槽内に垂下している超音波洗浄機により超音波振動が加えられ、ろ材の多孔質部で捕捉している微細な懸濁物を剥離する。分離槽からオーバーフローしたろ材は洗浄塔内を沈降し、洗浄塔内部とエアリフト管外周部に配設されたシュートにより、分配されながらろ材層上面に供給される。そして、剥離した軽い夾雑物は分離槽からオーバーフローした後、洗浄排出口から槽外へ排出される。この際、ろ材の一部が洗浄排水中に混入していても、洗浄塔と洗浄排出口との開口部にろ材流失防止用のフィルターを張設しているので、ろ材が流失する恐れはない。
【0011】
また、エアリフト管内に供給された圧縮空気は、ろ材と共に上昇し、洗浄塔の上部に蓄積するので、洗浄塔内の液面が圧縮空気に押され徐々に低下する。この液面が洗浄排水口より低くなると、洗浄排水を槽外に排出することが出来なくなる為、洗浄塔上部に設けたレベル計により、前記液面を検出し、設定値以下になると洗浄塔上部のエア排気口に設けている調節弁を開き、洗浄塔上部に蓄積している圧縮空気を大気へ放出する。再び、洗浄塔内の液面が上昇して前記レベル計の設定値以上になると、前記調節弁を閉じる。
【0012】
一方、ろ材を通過して夾雑物を捕捉され、清澄になったろ液(処理水)はろ材層下方に配設されたループ状の分配傘の下面から、均等に分配傘内に流入する。前記分配傘の下面にはろ材流失防止用のフィルターが張設されているので、ろ液だけが流入し、このろ液は分配傘内に立設している複数本の流出管を通じて、前記流出管の下部に接続している処理水取出管から、ろ過槽の外周部に設けられたループ状のヘッダー管に集合し、前記ヘッダー管の一ヵ所に設けている処理水取出口より槽外に排出される。以下、図面に基づいて本発明の移動ろ床式ろ過装置を具体的に説明する。
【0013】
【実施例】
図1は本発明に係るろ過装置1を模式的に表した縦断面図である。図1において、ろ過槽2は下部が略円錐形をした中空円筒状の密閉容器であり、ろ過槽2の内部下方にはろ材層4を形成する粒状のろ材3が積層されている。本発明では前記ろ材3に市販の珪藻土3aを使用する。珪藻土3aは多孔質で大きな空隙率を有し、粒子自体の強度が大きいという特性がある。そして、ろ過槽2の内部上方にはろ過室6を構成し、ろ過室6の上部には、原水を圧入供給する供給口7が設けられている。ろ過槽2の下方には処理水取出部14fが設けられている。前記供給口7から夾雑物や懸濁物を含む原水がポンプ等でろ過室6内に圧入供給され、ろ材層4中を下降し、珪藻土3aが夾雑物や懸濁物を捕捉することによってろ過され、処理水として処理水取出部14fから槽外へ排出される。
【0014】
処理水取出部14fは処理水取出管14aの一端に処理水取出口14を設け、他端をループ状のヘッダー管14bに接続し、該ヘッダー管14bに立設した複数本の流出管14cと、ループ状の分配傘14dで構成している。ヘッダー管14bはろ過槽2の下方外部に設けられ、該ヘッダー管14bに立設した複数本の流出管14cはろ過槽2の円錐部を貫通して、上端をろ材層4内で開口している。分配傘14dは流出管14cの上端開口の上方を覆うように配設されている。分配傘14dの下面には、ろ材3の最小粒径よりも細かい目のフィルター14eを張設しているので、ろ材3が処理水と共に排出されることはない。
【0015】
エアリフト管5はろ過槽2と同心状に立設されており、エアリフト管5の下端は、ろ過槽2底部近辺のろ材層4内で開口している。エアリフト管5の下部には圧縮空気の供給口(図示せず)が設けられており、圧縮空気をエアリフト管5の下部に供給することにより、ろ材層4底部のろ材3がろ過槽2底部の処理水と共にエアリフト管5内を上昇し、積層しているろ材3は徐々に上方から下方に移動する。そして、エアリフト管5内を上昇するろ材3はろ材3…同志の衝突と、処理水によって撹拌、洗浄されながら上方に移送される。
【0016】
エアリフト管5の上端は、ろ過槽2の上部で開口しており、この開口部の外周部は円筒形状の分離槽8の底面と同心状に連接され、分離槽8の上面は密閉状態のろ過槽内で開放されている。この分離槽8の外周部を囲撓する形で円筒形状の洗浄塔9が同心状に立設され、該洗浄塔9の下端はろ過室6内で開口し、上端はろ過槽2の天板を貫通して上方に突出して、上端には天板を設けている。洗浄塔9の上部側面でろ過槽2の外部の位置には洗浄排出口11が設けられ、この洗浄排出口11と洗浄塔9との開口部にはろ材3の最小粒径より細かい目のフィルター11aが張設されている。そして、洗浄塔9の天板の中央には洗浄装置10が垂設されており、その先端部は分離槽8内まで延設している。該洗浄装置10はろ材3に珪藻土3aを使用する場合には、超音波によって珪藻土3a粒子を振動させる超音波洗浄機10aを使用するのが最も効果的であり、使用する超音波の周波数帯としては、20KHz〜40KHzの範囲が効果的である。
【0017】
洗浄再生されたろ材3は分離槽8をオーバーフローして、洗浄塔9内を沈降する。この時、ろ材3はエアリフト管5外周面及び洗浄塔9内周面に多段に配設されているシュート5a、9aに接触しながら分配され、ろ材層4の上面に供給される。そして、ろ材3と共に分離槽8をオーバーフローした軽い夾雑物を含む洗浄排水は、前記洗浄排出口11から夾雑物と共に槽外に排出される。一部のろ材3が洗浄排水に混入した場合でも、前記のフィルター11aによって、ろ材3が洗浄排水と共に排出することは無いものである。尚、図中の符号11bは洗浄排水の排水量を調節するための調節弁である。
【0018】
又、ろ材3と共にエアリフト管内を上昇する圧縮空気は、洗浄塔9上部に蓄積し、洗浄塔9内の液面は圧縮空気に押され徐々に低下してくる。この圧縮空気を排気する為に、洗浄塔9上部に設けたレベル計12により低下している液面を検出し、液面がレベル計12の設定値以下に達すると「開」信号を発し、洗浄塔9上部のエア排気口13に設けている調節弁13aを開き、洗浄塔9上部に蓄積されている圧縮空気をエア排気口13から大気へ排気する。そして、液面が再び上昇してレベル計12の設定値以上に達すると「閉」信号を発し、前記調節弁13aを閉じるようにしている。尚、符号15はろ材3等を取出す際に使用するドレーン口である。
【0019】
このように構成されたろ過装置1を用いることにより、夾雑物(懸濁物)を含む原水は、供給口7からろ過室6内に供給され、ろ材層4を下降する。懸濁物はこの間に珪藻土3aに捕捉され、ろ液(処理水)はろ過槽2下部に設けた処理水取出部14fを通り、処理水取出口14から槽外に排出される。一方、ろ材層4底部の汚染した珪藻土3aはエアリフト管5に圧縮空気を供給することにより、ろ過槽2下部の処理水と共にエアリフト管5を撹拌されながら上方の分離槽8まで移送される。この間に珪藻土3a粒子の表面に付着している夾雑物は剥離する。珪藻土3a粒子の多孔質部に捕捉された懸濁物は分離槽8内に設けた超音波洗浄機10aの超音波振動によって剥離する。剥離した軽い夾雑物(懸濁物)は一緒に上昇してきた処理水と共に洗浄排水として、洗浄排出口11より槽外に排出され、洗浄再生された珪藻土3aは洗浄塔9内を沈降しながら、シュート5a、9aによって分配され、ろ材層4の上面に供給される。
【0020】
上述した珪藻土3aの粒径は0.1〜2.0mm程度のものを使用するが、砂を用いた従来の上向流移動床式ろ過装置のろ材粒子径(0.6〜1.2mm)よりも小さな粒子径(0.5mm程度以下)の珪藻土3aだけを使用すれば、更に、精密な清澄ろ過が行なえる。又、小さな粒子径だけの珪藻土3aを使用することにより、安息角が小さくなり、ろ過槽2下部の円錐状部の傾斜を緩くでき、ろ過槽2の高さが低くなり、ろ過装置1の全高も低くなる。
【0021】
図2は本発明に係るろ過装置1の他の実施例を模式的に表した縦断面図である。図2におけるろ過槽2及び洗浄塔9は開放型にしているので、原水を圧入供給せず、水柱L(ろ材層4上面から供給口7までの高さ)をろ過力とするため、ろ過装置1の全高が図1の密閉式のものと比較して高くなる。しかしながら、エアリフト管5上部から排出される圧縮空気の排気装置が不要となり、イニシャルコストの低減が図れる。ろ過方法については、図1の密閉式のものと同様のため、その説明は省略する。
【0022】
【発明の効果】
本発明に係る移動ろ床式ろ過装置は、従来から用いられている砂粒子をろ材とした上向流移動ろ床式ろ過装置に比べ、ろ材に多孔質を持つ珪藻土粒子を使用しているので、従来の移動ろ床式ろ過装置では捕捉することが出来なかった微細なコロイド状の懸濁物質も、珪藻土の多孔質で捕捉でき、より清澄な精密ろ過が行なえるようになった。又、ろ材の洗浄においては、汚染したろ材をエアリフト管で移送する間に行なう撹拌、洗浄と分離槽内で行なう超音波による振動の2段階洗浄により、珪藻土の多孔質内に捕集されている微細な懸濁物質まで剥離することが出来、完全に洗浄再生をした珪藻土をろ材層の上面に返送するので、連続で安定した清澄ろ過がおこなえる。
【0023】
ろ過槽を密閉式にしておけば、原水を圧入供給できるため、ろ過装置の全高を低くでき、建屋等のイニシャルコストの低減が図れる。そして、小さい粒径だけの珪藻土を使用することにより、プレコートろ過や精密ろ過膜に相当する清澄な精密ろ過をすることが出来る。また、安息角が小さくなり、ろ過槽下部の円錐状部の傾斜が緩くできるので、更に、ろ過装置の全高が低くなる。
【図面の簡単な説明】
【図1】本発明に係る移動ろ床式ろ過装置を模式的に表した縦断面図である。
【図2】本発明に係る移動ろ床式ろ過装置の他の実施例を模式的に表した縦断面図である。
【図3】従来の上向流移動ろ床式ろ過装置を模式的に表した縦断面図である。
【符号の説明】
1 ろ過装置
2 ろ過槽
3 ろ材
3a 珪藻土
4 ろ材層
5 エアリフト管
6 ろ過室
7 供給口
8 分離槽
9 洗浄塔
10 洗浄装置
10a 超音波洗浄機
11 洗浄排出口
11a、14e フィルター
12 レベル計
13 エア排気口
13a 調節弁
14 処理水取出口
14a 処理水取出管
14b ヘッダー管
14c 流出管
14d 分配傘
[0001]
BACKGROUND OF THE INVENTION
The present invention relates to an improvement of a filtration device for suspensions of clean water, sewage, industrial wastewater, etc. In particular, the present invention uses a diatomaceous earth as a filter material, and circulates the contaminated filter material to wash and regenerate it. The present invention relates to a filtration device that can continuously perform clarification filtration.
[0002]
[Prior art]
2. Description of the Related Art Conventionally, an up-flow moving filter bed type filtration device in which a filter medium constituting a filter bed moves, this filter medium is moved, washed and regenerated, and returned to the upper part of the filter bed is known and well known. Then, granular sand having a specific gravity of 1.0 or more is used as a filter medium, an air lift pipe that operates with compressed air is used to transport the contaminated sand, and the filter medium layer is washed and regenerated with a cleaning device at the top of the filter tank. There is also a well-known filtration device that returns to the top of the water and discharges the washing waste water to the outside.
[0003]
In addition, in JP-A-6-47208, in a filtration apparatus using sand granular diatomaceous earth as a filter medium constituting a filter bed, raw water is supplied from a raw water supply pipe provided at the upper part of a sealed filtration tank, and then descended. The suspended matter is removed with a diatomaceous earth filter medium while passing through the filter medium layer in a flow, and the treated water is taken out from an extraction pipe provided at the bottom of the filtration tank. When the filter medium contaminated by the suspension is washed and regenerated, wash water is supplied from the take-out pipe, and the filter medium is passed through the filter medium in an upward flow so that the suspension adhering to the filter medium is removed from the filter medium. Peeled and dirty cleaning wastewater is discharged from the raw water supply pipe to the outside.
[0004]
[Problems to be solved by the invention]
FIG. 3 is a longitudinal sectional view conceptually showing a conventionally known upward flow moving filter type filtration device. Raw water is supplied to a supply port 31 provided at a lower portion of the filtration tank 30 and connected to the supply port 31. A loop-shaped header pipe 32 and a plurality of inflow pipes 33 erected on the header pipe 32 are equally supplied to the lower part of the filter medium layer 35 via the loop-shaped distribution umbrella 34. While the raw water supplied in this manner rises in the filter medium layer 35 formed of granular sand, impurities are captured by the filter medium layer 35, and the treated water is treated at the upper part of the filter tank 30. It is discharged out of the tank through the water outlet 36. The contaminated sand at the lower part of the filter medium layer 35 is supplied to the lower part of the air lift pipe 37 erected at the center of the filter tank 30 to raise the air lift pipe 37 and disposed at the upper part of the filter tank 30. The cleaning tower 38 is cleaned and regenerated with treated water. The cleaned filter medium 35 a is returned to the upper surface of the filter medium layer 35 while being distributed by the chutes 37 a and 38 a disposed in the cleaning tower 38 and the outer periphery of the air lift pipe 37. The contaminants cleaned in the cleaning tower 38 and separated from the filter medium 35a are discharged out of the tank from a cleaning drain 39 provided in the upper part of the cleaning tower 38. In the moving filter bed type filtration device using granular sand as the filter medium 35a described above, the surface of the filter medium particles is flat, there are no adsorption holes, and the particle gap is large, so that a fine colloidal suspension cannot be captured and the filter medium layer. Therefore, there is a problem that the quality of the treated water deteriorates.
[0005]
Further, in the invention described in JP-A-6-47208, diatomaceous earth is used as a filter medium, so that the above-mentioned problematic colloidal suspension is caused by diatomaceous earth having porous characteristics. However, since it is captured by the porous material unique to the diatomaceous earth, clarification filtration can be performed and the quality of the treated water is improved. However, in the method for cleaning a filter medium according to the invention described in JP-A-6-47208, it is necessary to stop the filtration operation during the cleaning, the continuous operation cannot be performed, the filtration device becomes large, and the installation area becomes large. In addition, because the washing method is simply backwashing the washing water, there is a problem that the suspension trapped in the porous part of the diatomaceous earth cannot be separated, and further, if the washing pressure is increased, the filter medium will be washed away. There are also challenges.
[0006]
[Means for Solving the Problems]
In order to solve the above-mentioned problem, the present invention forms a filter medium layer by laminating a granular filter medium heavier than water inside a sealed filter tank, and opens at a lower layer part of the filter medium layer and an upper part of the filter tank, The filter medium is pulled out from the bottom of the filter medium layer with compressed air and transferred upward, and an air lift pipe is installed so that the filter medium is washed and regenerated and circulated to the upper part of the filter medium layer. Diatomaceous earth was used, and raw water was press-fitted from the raw water supply port provided in the filtration chamber above the filter medium layer to lower the filter medium layer, and the treated water was taken out from the lower part of the filter tank. It is.
[0007]
In addition, a separation tank is disposed on the outer peripheral portion of the upper end opening of the air lift pipe installed in the filtration tank, and projects upward from the top plate of the filtration tank from the filtration chamber of the filtration tank to surround the separation tank. A cleaning tower is erected, a filter medium cleaning device is suspended from the top of the cleaning tower, the lower end of the cleaning device extends to the inside of the separation tank, and the filter medium cleaning discharge is disposed on the upper side of the cleaning tower. An outlet is provided, and the filtration tank, the cleaning tower, the air lift pipe, and the cleaning device are disposed substantially concentrically. An ultrasonic cleaner is used as the filter medium cleaning device, and the upper portion of the cleaning tower is used for air exhaust. A level meter and an air exhaust port are provided, and the air exhaust port is provided with a control valve that opens and closes in conjunction with the level meter.
[0008]
The treated water outlet provided in the lower part of the filtration tank includes a loop-shaped header pipe connected to the treated water outlet pipe, a plurality of outflow pipes erected on the header pipe, It is composed of a loop-shaped distribution umbrella that is provided above the outflow pipe and distributes the treated water flowing into the outflow pipe evenly, and is provided at the lower surface of the distribution umbrella and at the openings of the washing tower and the washing outlet. A filter was installed to prevent the loss of filter media.
[0009]
DETAILED DESCRIPTION OF THE INVENTION
Since the apparatus according to the present invention is configured as described above, the raw water press-fitted to the upper part of the filter medium layer is trapped by the filter medium (diatomaceous earth) while the contaminants (suspension) are descending the filter medium layer. The filtrate (treated water) is discharged from the lower part of the filtration tank to the outside of the tank. At the same time, by supplying compressed air to the air lift pipe, the filter medium at the bottom of the filter medium layer is pulled out, and the stacked filter medium gradually moves downward from above. The extracted filter medium is transferred to the upper separation tank while being stirred in the air lift pipe together with the treated water at the lower part of the filtration tank.
[0010]
In the air lift pipe, the foreign substances adhering to the surface of the filter medium are separated from the surface of the filter medium by being stirred during the transfer. Then, the filter medium transferred to the separation tank is subjected to ultrasonic vibration by an ultrasonic cleaner hanging in the separation tank, and the fine suspension trapped in the porous portion of the filter medium is peeled off. The filter medium overflowed from the separation tank settles in the washing tower, and is supplied to the upper surface of the filter medium layer while being distributed by the chute disposed inside the washing tower and the outer periphery of the air lift pipe. Then, the peeled light impurities overflow from the separation tank, and are then discharged out of the tank through the cleaning discharge port. At this time, even if a part of the filter medium is mixed in the cleaning wastewater, a filter for preventing the loss of the filter medium is stretched at the opening of the cleaning tower and the cleaning discharge port, so there is no risk of the filter medium flowing out. .
[0011]
The compressed air supplied into the air lift pipe rises together with the filter medium and accumulates in the upper part of the washing tower, so that the liquid level in the washing tower is pushed by the compressed air and gradually decreases. If this liquid level becomes lower than the washing drain port, it becomes impossible to discharge the washing wastewater outside the tank. Therefore, the liquid level is detected by a level meter provided at the upper part of the washing tower. The control valve provided at the air exhaust port is opened, and the compressed air accumulated in the upper part of the washing tower is released to the atmosphere. When the liquid level in the washing tower rises again and exceeds the set value of the level meter, the control valve is closed.
[0012]
On the other hand, the filtrate (treated water) that has passed through the filter medium and trapped impurities and has been clarified flows equally into the distribution umbrella from the lower surface of the loop-shaped distribution umbrella disposed below the filter medium layer. Since a filter for preventing the loss of filter media is stretched on the lower surface of the distribution umbrella, only the filtrate flows in, and this filtrate flows through the plurality of outflow pipes standing in the distribution umbrella. Collected from the treated water outlet pipe connected to the lower part of the pipe into a loop-shaped header pipe provided in the outer periphery of the filtration tank, and out of the tank from the treated water outlet provided in one place of the header pipe Discharged. Hereinafter, the moving filter bed type filtration apparatus of the present invention will be specifically described with reference to the drawings.
[0013]
【Example】
FIG. 1 is a longitudinal sectional view schematically showing a filtration device 1 according to the present invention. In FIG. 1, the filtration tank 2 is a hollow cylindrical hermetic container having a substantially conical lower portion, and a granular filter medium 3 forming a filter medium layer 4 is laminated below the filter tank 2. In the present invention, commercially available diatomaceous earth 3 a is used for the filter medium 3. Diatomaceous earth 3a is porous and has a large porosity, and has the characteristics that the strength of the particles themselves is high. And the filtration chamber 6 is comprised above the inside of the filtration tank 2, and the supply port 7 which press-fits and supplies raw | natural water is provided in the upper part of the filtration chamber 6. As shown in FIG. A treated water extraction part 14 f is provided below the filtration tank 2. The raw water containing impurities and suspensions is press-fitted and supplied into the filtration chamber 6 by a pump or the like from the supply port 7, descends through the filter medium layer 4, and the diatomaceous earth 3 a captures the impurities and suspensions. Then, it is discharged out of the tank from the treated water outlet 14f as treated water.
[0014]
The treated water outlet 14f has a treated water outlet 14 provided at one end of the treated water outlet pipe 14a, the other end connected to a loop-shaped header pipe 14b, and a plurality of outflow pipes 14c erected on the header pipe 14b. The loop-shaped distribution umbrella 14d is used. The header pipe 14b is provided outside the lower part of the filtration tank 2, and a plurality of outflow pipes 14c provided upright on the header pipe 14b pass through the conical portion of the filtration tank 2 and have an upper end opened in the filter medium layer 4. Yes. The distribution umbrella 14d is disposed so as to cover the upper end opening of the outflow pipe 14c. Since the filter 14e having an eye smaller than the minimum particle diameter of the filter medium 3 is stretched on the lower surface of the distribution umbrella 14d, the filter medium 3 is not discharged together with the treated water.
[0015]
The air lift pipe 5 is erected concentrically with the filtration tank 2, and the lower end of the air lift pipe 5 opens in the filter medium layer 4 near the bottom of the filtration tank 2. A compressed air supply port (not shown) is provided at the lower part of the air lift pipe 5, and by supplying the compressed air to the lower part of the air lift pipe 5, the filter medium 3 at the bottom of the filter medium layer 4 is attached to the bottom of the filtration tank 2. The inside of the air lift pipe 5 rises together with the treated water, and the stacked filter media 3 gradually move downward from above. Then, the filter medium 3 rising in the air lift pipe 5 is transferred upward while being stirred and washed with the filter medium 3.
[0016]
The upper end of the air lift pipe 5 is opened at the upper part of the filtration tank 2, the outer periphery of the opening is connected concentrically with the bottom surface of the cylindrical separation tank 8, and the upper surface of the separation tank 8 is hermetically sealed. It is open in the tank. A cylindrical washing tower 9 is concentrically arranged so as to surround the outer periphery of the separation tank 8, the lower end of the washing tower 9 is opened in the filtration chamber 6, and the upper end is the top plate of the filtration tank 2. The top plate is provided at the upper end. A washing discharge port 11 is provided on the upper side of the washing tower 9 at a position outside the filtration tank 2, and an opening of the washing discharge port 11 and the washing tower 9 has a finer filter than the minimum particle size of the filter medium 3. 11a is stretched. A cleaning device 10 is suspended in the center of the top plate of the cleaning tower 9, and its tip extends to the inside of the separation tank 8. When the diatomaceous earth 3a is used for the filter medium 3, it is most effective to use the ultrasonic cleaning machine 10a that vibrates the diatomaceous earth 3a particles by ultrasonic waves. Is effective in the range of 20 KHz to 40 KHz.
[0017]
The filter medium 3 regenerated by washing overflows the separation tank 8 and settles in the washing tower 9. At this time, the filter medium 3 is distributed in contact with the chutes 5 a and 9 a arranged in multiple stages on the outer peripheral surface of the air lift pipe 5 and the inner peripheral surface of the cleaning tower 9, and is supplied to the upper surface of the filter medium layer 4. Then, the cleaning wastewater containing the light contaminants overflowing the separation tank 8 together with the filter medium 3 is discharged out of the tank together with the impurities from the cleaning discharge port 11. Even when a part of the filter medium 3 is mixed into the cleaning wastewater, the filter 11a is not discharged together with the cleaning wastewater by the filter 11a. In addition, the code | symbol 11b in a figure is an adjustment valve for adjusting the waste_water | drain amount of washing waste_water | drain.
[0018]
Further, the compressed air that rises in the air lift pipe together with the filter medium 3 accumulates in the upper part of the washing tower 9, and the liquid level in the washing tower 9 is pushed by the compressed air and gradually decreases. In order to exhaust the compressed air, the liquid level that is lowered is detected by a level meter 12 provided at the upper part of the cleaning tower 9, and when the liquid level reaches a set value or less of the level meter 12, an “open” signal is generated, The control valve 13a provided at the air exhaust port 13 at the top of the cleaning tower 9 is opened, and the compressed air accumulated at the top of the cleaning tower 9 is exhausted from the air exhaust port 13 to the atmosphere. When the liquid level rises again and reaches the set value of the level meter 12 or more, a “closed” signal is issued to close the control valve 13a. Reference numeral 15 denotes a drain port used when removing the filter medium 3 and the like.
[0019]
By using the thus configured filtration device 1, raw water containing impurities (suspension) is supplied from the supply port 7 into the filtration chamber 6 and descends the filter medium layer 4. During this time, the suspended matter is captured by the diatomaceous earth 3a, and the filtrate (treated water) passes through the treated water outlet 14f provided at the lower part of the filtration tank 2 and is discharged from the treated water outlet 14 to the outside. On the other hand, the contaminated diatomaceous earth 3a at the bottom of the filter medium layer 4 is transferred to the upper separation tank 8 while supplying the compressed air to the air lift pipe 5 and stirring the air lift pipe 5 together with the treated water below the filtration tank 2. During this time, impurities adhering to the surface of the diatomaceous earth 3a particles are peeled off. The suspension trapped in the porous portion of the diatomaceous earth 3a particles is peeled off by ultrasonic vibration of an ultrasonic cleaner 10a provided in the separation tank 8. The peeled light impurities (suspension) are discharged together with the treated water that has risen together as cleaning wastewater, and discharged from the cleaning outlet 11 to the outside of the tank. The washed and regenerated diatomaceous earth 3a settles in the cleaning tower 9, It is distributed by the chutes 5 a and 9 a and supplied to the upper surface of the filter medium layer 4.
[0020]
Although the particle diameter of the diatomaceous earth 3a described above is about 0.1 to 2.0 mm, the particle diameter of the filter medium (0.6 to 1.2 mm) of the conventional upward flow moving bed type filter using sand is used. If only diatomaceous earth 3a having a smaller particle size (about 0.5 mm or less) is used, further precise clarification filtration can be performed. Moreover, by using the diatomaceous earth 3a having only a small particle diameter, the angle of repose is reduced, the inclination of the conical portion at the bottom of the filtration tank 2 can be loosened, the height of the filtration tank 2 is lowered, and the total height of the filtration device 1 Also lower.
[0021]
FIG. 2 is a longitudinal sectional view schematically showing another embodiment of the filtration device 1 according to the present invention. Since the filtration tank 2 and the washing tower 9 in FIG. 2 are open type, the raw water is not press-fitted and the water column L (height from the upper surface of the filter medium layer 4 to the supply port 7) is used as a filtration force. The total height of 1 is higher than that of the closed type shown in FIG. However, an exhaust device for compressed air discharged from the upper portion of the air lift pipe 5 is not required, and the initial cost can be reduced. The filtration method is the same as that of the hermetic type of FIG.
[0022]
【The invention's effect】
Since the moving filter bed filtration device according to the present invention uses diatomaceous earth particles having a porous filter medium, compared to the upward flow filter bed filtration device using sand particles as a filter material conventionally used. Fine colloidal suspended solids that could not be captured by the conventional moving filter type filtration device can also be captured by the porous diatomaceous earth, and more precise microfiltration can be performed. In the cleaning of the filter medium, the contaminated filter medium is trapped in the porous diatomaceous earth by two-stage cleaning of stirring, cleaning and ultrasonic vibration performed in the separation tank while being transferred by the air lift pipe. Even fine suspended solids can be peeled off, and diatomaceous earth that has been completely washed and regenerated is returned to the upper surface of the filter medium layer, so that continuous and stable clarification filtration can be performed.
[0023]
If the filtration tank is hermetically sealed, the raw water can be press-fitted and supplied, so the overall height of the filtration device can be lowered, and the initial cost of buildings and the like can be reduced. And by using diatomaceous earth with only a small particle diameter, it is possible to perform fine microfiltration corresponding to precoat filtration or microfiltration membrane. Moreover, since the angle of repose becomes small and the inclination of the conical part at the lower part of the filtration tank can be loosened, the overall height of the filtration device is further lowered.
[Brief description of the drawings]
FIG. 1 is a longitudinal sectional view schematically showing a moving filter bed type filtration apparatus according to the present invention.
FIG. 2 is a longitudinal sectional view schematically showing another embodiment of the moving filter bed type filtration apparatus according to the present invention.
FIG. 3 is a longitudinal sectional view schematically showing a conventional upward flow moving filter type filtration apparatus.
[Explanation of symbols]
DESCRIPTION OF SYMBOLS 1 Filtration apparatus 2 Filtration tank 3 Filter medium 3a Diatomaceous earth 4 Filter medium layer 5 Air lift pipe 6 Filtration chamber 7 Supply port 8 Separation tank 9 Washing tower 10 Washing apparatus 10a Ultrasonic cleaner 11 Washing discharge port 11a, 14e Filter 12 Level meter 13 Air exhaust Port 13a Control valve 14 Treated water outlet 14a Treated water outlet pipe 14b Header pipe 14c Outlet pipe 14d Distributing umbrella

Claims (6)

ろ過槽(2)内部に水より重い粒状のろ材(3)を積層してろ材層(4)を形成し、前記ろ材層(4)の下層部とろ過槽(2)の上部で開口し、前記ろ材(3)を圧縮空気によってろ材層(4)の底部から引抜いて上方へ移送するとともに、該ろ材(3)を洗浄再生してろ材層(4)の上部へと循環させるようにしたエアリフト管(5)を立設したろ過装置(1)において、前記ろ過槽(2)を密閉型に形成し、前記ろ過槽(2)に装填するろ材(3)には珪藻土(3a)を使用し、前記ろ材層(4)上方のろ過室(6)に設けた原水の供給口(7)から原水を圧入供給してろ材層(4)中を下降させ、その処理水を前記ろ過槽(2)の下部から取出すようにしたことを特徴とする移動ろ床式ろ過装置。  A filter medium (4) is formed by laminating a granular filter medium (3) heavier than water inside the filter tank (2), and is opened at the lower part of the filter medium layer (4) and the upper part of the filter tank (2). The filter medium (3) is pulled out from the bottom of the filter medium layer (4) by compressed air and transferred upward, and the filter medium (3) is washed and regenerated to circulate to the upper part of the filter medium layer (4). In the filtration device (1) erected with the pipe (5), the filtration tank (2) is formed in a closed type, and diatomaceous earth (3a) is used as the filter medium (3) to be loaded in the filtration tank (2). The raw water is press-fitted from the raw water supply port (7) provided in the filtration chamber (6) above the filter medium layer (4) to lower the filter medium layer (4), and the treated water is supplied to the filter tank (2). ) A moving filter bed type filtering device characterized in that it is taken out from the lower part. 上記ろ過槽(2)に立設したエアリフト管(5)の上端開口部の外周部に分離槽(8)を配設し、前記ろ過槽(2)のろ過室(6)内から該ろ過槽(2)の天板より上方に突出し、前記分離槽(8)を囲撓する洗浄塔(9)を立設し、該洗浄塔(9)の頂部からろ材(3)の洗浄装置(10)を垂設し、該洗浄装置(10)の下端は前記分離槽(8)内まで延設し、前記洗浄塔(9)の上方側部にはろ材(3)の洗浄排出口(11)を設け、前記ろ過槽(2)、洗浄塔(9)、エアリフト管(5)、洗浄装置(10)は略同心状に配設したことを特徴とする請求項1に記載の移動ろ床式ろ過装置。  A separation tank (8) is disposed on the outer periphery of the upper end opening of the air lift pipe (5) erected in the filtration tank (2), and the filtration tank is inserted from the filtration chamber (6) of the filtration tank (2). A washing tower (9) protruding above the top plate of (2) and surrounding the separation tank (8) is erected, and a washing device (10) for the filter medium (3) from the top of the washing tower (9) The lower end of the cleaning device (10) extends into the separation tank (8), and the cleaning outlet (11) of the filter medium (3) is provided on the upper side of the cleaning tower (9). The moving filter bed filtration according to claim 1, wherein the filtration tank (2), the washing tower (9), the air lift pipe (5), and the washing device (10) are arranged substantially concentrically. apparatus. 上記ろ材(3)の洗浄装置(10)として超音波洗浄機(10a)を用いたことを特徴とする請求項2に記載の移動ろ床式ろ過装置。  The moving filter bed type filtration device according to claim 2, wherein an ultrasonic cleaner (10a) is used as the cleaning device (10) for the filter medium (3). 上記洗浄塔(9)の上部にエア排気用のレベル計(12)と、エア排気口(13)を設け、該エア排気口(13)には前記レベル計(12)と連動して開閉する調節弁(13a)を設けたことを特徴とする請求項1又は請求項2に記載の移動ろ床式ろ過装置。An air exhaust level meter (12) and an air exhaust port (13) are provided in the upper part of the washing tower (9), and the air exhaust port (13) is opened and closed in conjunction with the level meter (12). The moving filter bed type filtration device according to claim 1 or 2, further comprising a control valve (13a). 上記ろ過槽(2)の下部に設けた処理水取出口(14)は、処理水取出管(14a)に接続されているループ状のヘッダー管(14b)と、該ヘッダー管(14b)に立設された複数本の流出管(14c)と、該流出管(14c)の上方に設けられ該流出管(14c)へ流入する処理水を均等に分配するループ状の分配傘(14d)とで構成していることを特徴とする請求項1又は請求項2に記載の移動ろ床式ろ過装置。The treated water outlet (14) provided at the lower part of the filtration tank (2) is provided with a loop-shaped header pipe (14b) connected to the treated water outlet pipe (14a) and the header pipe (14b). A plurality of outflow pipes (14c) provided, and a loop-shaped distribution umbrella (14d) provided above the outflow pipe (14c) and equally distributing treated water flowing into the outflow pipe (14c) The moving filter bed type filtration apparatus according to claim 1 or 2 , wherein the apparatus is configured. 上記分配傘(14d)の下面部と、上記洗浄塔(9)と洗浄排出口(11)との開口部にろ材流失防止用のフィルター(11a、14e)を張設したことを特徴とする請求項5に記載の移動ろ床式ろ過装置。 Claims, characterized in that the stretched and the lower surface portion, the washing tower (9) and the cleaning outlet (11) filter for filtration media erosion prevention to the opening of the (11a, 14e) of the distribution bevel (14d) Item 6. The moving filter type filtration device according to Item 5 .
JP2002022620A 2002-01-31 2002-01-31 Moving filter filter Expired - Lifetime JP3809648B2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2002022620A JP3809648B2 (en) 2002-01-31 2002-01-31 Moving filter filter

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2002022620A JP3809648B2 (en) 2002-01-31 2002-01-31 Moving filter filter

Publications (2)

Publication Number Publication Date
JP2003220305A JP2003220305A (en) 2003-08-05
JP3809648B2 true JP3809648B2 (en) 2006-08-16

Family

ID=27745568

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2002022620A Expired - Lifetime JP3809648B2 (en) 2002-01-31 2002-01-31 Moving filter filter

Country Status (1)

Country Link
JP (1) JP3809648B2 (en)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5271229B2 (en) * 2009-10-05 2013-08-21 大道産業株式会社 Filtration system
AU2010340292B2 (en) * 2010-01-08 2015-05-14 Parkson Corporation Method and computer program product for treating liquid containing impurities
KR101041411B1 (en) * 2010-11-01 2011-06-14 유승열 Filtration apparatus
JP5763503B2 (en) * 2011-11-07 2015-08-12 三機工業株式会社 Moving bed type upflow continuous sand filtration device and operation method thereof
CN103845930B (en) * 2014-02-17 2015-11-25 中持水务股份有限公司 A kind of filtrate retains high strength backwash rhone
JP7259538B2 (en) * 2019-05-17 2023-04-18 住友金属鉱山株式会社 liquid filter

Also Published As

Publication number Publication date
JP2003220305A (en) 2003-08-05

Similar Documents

Publication Publication Date Title
US7704382B2 (en) Gravity type fiber filter
US6319413B1 (en) Method of filtering liquid using a vertical filter
JPH0318483B2 (en)
CA1242979A (en) Pressure filter (hpc clarifil)
CN2936380Y (en) Unpowered waste water filtering and sterilizing treating device
JP3809648B2 (en) Moving filter filter
MXPA05013350A (en) Solid liquid filtration apparatus and method.
JPH0217908A (en) Method for washing solid-liquid separation apparatus
JP2599538B2 (en) Inclined plate type sedimentation tank and method for preventing clogging thereof
JPH1071305A (en) Moving filter bed type filter
JPH06277407A (en) Device filtering suspension liquid
JP2706080B2 (en) Filtration device and its cleaning method
KR100606602B1 (en) The filter system can be cleaning to use ultrasonic vibrations and how to clean it
JP2002035511A (en) Filter apparatus
JP4277589B2 (en) Upflow filter
JP2003265905A (en) Flocculating and settling apparatus
KR102050980B1 (en) Water purifier system having water purifier process and backwash process
KR200355755Y1 (en) The filter system can be cleaning to use ultrasonic vibrations
JP3815616B2 (en) Upflow filter
KR200149548Y1 (en) Device for removing suspended solid particles i
JP4699981B2 (en) Filtration apparatus and filtration method
WO2004045742A1 (en) Water filter and a method of water purification, backwashing and rinsing
JPS5920334Y2 (en) Continuous "filtration" device
JPH0717365Y2 (en) Continuous sand filter
JPS5946649B2 (en) Horizontal flow deep filtration device

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20040119

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20060223

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20060228

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20060411

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20060501

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20060514

R150 Certificate of patent or registration of utility model

Free format text: JAPANESE INTERMEDIATE CODE: R150

Ref document number: 3809648

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20090602

Year of fee payment: 3

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20100602

Year of fee payment: 4

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20100602

Year of fee payment: 4

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20110602

Year of fee payment: 5

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20120602

Year of fee payment: 6

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20130602

Year of fee payment: 7

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

S531 Written request for registration of change of domicile

Free format text: JAPANESE INTERMEDIATE CODE: R313531

R350 Written notification of registration of transfer

Free format text: JAPANESE INTERMEDIATE CODE: R350

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

EXPY Cancellation because of completion of term